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70-92 Boston Street - Phase 1 Initial Site investigation and Tier Classification - Appendix G - January 2006 APPENDIX G LABORATORY ANALYTICAL DATA SHEETS s CORPORATION i "Environmental Testing For The New Millennium" December 22, 2004 TRC Solutions, Inc. Foot of John Street Lowell, MA 01852 . Attn: Ms. Liz Denly RE: Client Project: Flynn-Tan, Salem, MA. Soil Samples Lab Project#: C1453 Dear Ms. Denly: Enclosed please find the data report of the required analyses for the samples associated with the above referenced project. If you have any questions regarding this report,please. call me. We appreciate your business. Si rely Edward A_ Lawler Laboratory Operations Manager 175 Metro Center Boulevard • Warwick, Rhode Island 02886-1755 (401) 732-3400 • Fax (401) 732-3499 • www.mitkem.com Analytical Data Package for TRC Solutions, Inc. Client Project: Flynn-Tan, Salem, Soil Samples Mitkem Project ID: C 1453 December 22, 2004 Revised February 8, 2005 Prepared For: TRC Solutions, Inc. Foot of John Street Lowell, MA 01852 Attn: Ms. Liz Denly Prepared By: Mitkem Corporation 175 Metro Center Boulevard. Warwick, RI 02886 (401) 732-3400 J tv DO 00 -1 z mat-; ja S o bR � LA 'G En 1 g o 4' M -e a No w o lc> 41 w Q C> CL0 1 COMPOSITE r y ILI I. GRAB to v N .iy; b v o N O WATER O v7 c Noo t tri tn. IX SOIL aO 0 1L, p V' OTHER c _ n C7 p 1 0 � rit a ro o a o vj n a z #'OF CONTAINERS o d y o d y y O n 0 u ` >3 X I?� x t H X O M > X 0 C trl S' -�-- it . it w c. V CD b a it C • - - a a o H G I � tri a� L5 x T triC.i� e D - O a t O ! F-R UA p• oa -� COMPOSITE CK3 p 0 `� y Y GRAB V N a *; � a a N4 �" " Cl -C ra t tav ` ` -r. WATER Q O; N =< o N rn O o w X SOIL O ; ro . r OTHER ro 4z t7 1 p n a `� 3 d , 0-3 — � #OF CONTAINERS o - z no x { v' z _ ci zf t7 .d "' n rS� �jt E n � 1 ppCl- PC tri �N Jj y � o ! c c c �► a a o Ilk 4.1 i eo s � a z a o 4n.. \ 6- a D u Ea' a aa X �¢ �^ `� X U O TO /f xtx w C/1 A 0 X1 xU Qi a. w `� as SHa IIV'.NOD 40# Cp K w zMo ¢ t do ' a ti ZIHH.LO O O "IIOS x x .X X x >0 00 o :x wad IMWA O oo � 7 N '-, CIO t� W l w i a 3.LISOdwoa en n .G a� e F.. d w :-v� Ms Ol 3z o a U t c� c-S c{ oCL a ¢ A A ` G w ' U z ¢ U U C�` (�. SDG Narrative Mitkem Corporation submits the enclosed data package in response to TRC Solutions' Flynn-Tan soil sample project. Under this deliverable, analysis results are presented for seventeen samples that were received on November 18 and 19, 2004 and logged in under. Mitkem Work Order Number C1453. Analyses were performed per instruction in the chain of custody form, and per additional instructions received via email on November 19, 2004, 2004 and December 7,2004-' For reference,a copy of the Mitkem Work Order form is included for cross-referencing the client sample ID.andlaboratory sample ID. The analyses were performed according.to Massachusetts DEP mand EPA SW-846 methods,.with results presented in a Level 4 format deliverable. The following observation and/or deviations are observed for the following analyses: 1. Volatile Organic Analyses: Samples were analyzed by Method 8260. .Soil sample aliquots for low level analysis were received in DI water and preserved by freezing. Surrogate standards: four surrogate standards were spiked into each analysis. Mitkem's statistical QC limits listed on the surrogate report form are wider than the MADEP 70%- 130% limits. Surrogate recoveries were within the MADEP QC limits with the exception of elevated recoveries for two surrogates each in the undiluted analysis of samples SB 1-8 and S133-6. These samples were reanalyzed using the medium level, methanol preserved aliquots with improved recoveries, however one surrogate in S133-6 remained above the upper QC limit. Please note that this sample required additional analysis at further dilution. One surrogate in the MSD of sample S135-2 was within the Mitkem limit,but below the MADEP limit. This surrogate was within the QC limits in the sample and MS analysis. - .Lab control sample/lab control sample duplicate: spike recoveries were within the Mitkem statistical QC limits with the exception of elevated recoveries for tetrahydrofuran in V2KLCS,tetrahydrofuran and 2-hexanone in V2SLCS, dichloridifluoromethane,. tetrahydrofuran in duplicate LCS V2SLCS, methyl-t-butyl ether, chloroform and tetrahydrofuran in medium level V5ALCS and methyl-t-butyl ether in duplicate LCS V5ALCS. In addition to the above compounds, the following compounds were recovered outside of the MADEP 70% - 130% limits: 2-hexanone in V2KLCS, 1,4-dioxane in duplicate LCS V2KLCS, acetone in V2SLCS. Replicate RPD were within the MADEP j 25% QC limits with the exception of trichlorofluoromethane and 1,4-dioxane in V2KLCS/D_ Please note that Mitkem's statistical QC limits document that recoveries outside of the 70%- 130%range are not uncommon for most of these compounds. Matrix spike/matrix.spike duplicate: duplicate matrix spikes were performed on sample S135-2_ Spike recoveries were within the Mitkem statistical QC limits and the MADEP. 70% - 130%QC limits with the exception of carbon disulfide, tetrahydrofuran,2- hexanone, hexachlorobutadiene and tert-amyl methyl ether in the MS and acetone,carbon disulfide,2-butanone, tetrahydrofuran,trichloroethene, tetrachloroethene, 2-hexanone, 1,1,2,2-tetrachloroethane,hexachlorobutadiene and tert amyl methyl ether in the MSD. Replicate RPDs were within the in-house 40%RPD limit, and also within the MADEP 30% RPD limit with the exception of trichlorofluoromethane,trichloroethene, tetrachloroethene and 1,1,2,2-tetrachloroethane. Most of these compounds were within the QC limits in the associated LCS. The recoveries of matrix spike, surrogate and internal standard'compounds indicate some inconsistency between the three aliquots used for sample, MS and MSD. Sample analysis: internal standard areas were below the Mitkem and MADEP QC limits in samples SB1-8, SB3-6, SB10-2 and its reanalysis, and S135-2. Samples SB1-8 and SB3-6 were reanalyzed using methanol preserved aliquots. Sample SB3-6 was reanalyzed at further dilution using the methanol preserved aliquot_ No other unusual occurrences were noted during sample analysis. 2. MADEP VPH Analysis: Samples were analyzed by VPH Method 1.1. Samples were-properly preserved.in methanol_ Please note that sample S138-2 contained greater than the recommended 5. grams +/- 25% sample amount, however the entire sample was covered by methanol. Surrogate standards: percent recoveries were within the QC limits with the exception of low recovery in SB3-6 and its dilution, and sample SB1-8 and its reanalysis. Lab control sample: spike recoveries were within the QC limits. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample S135-2. Percent recoveries were within the QC limits with the CO-C12 Aliphatics. PIease note that this analyte was present in the native unspiked sample. Sample analysis: sample SB3-6 was reanalyzed at a 2X dilution. No other unusual occurrences were noted during sample analysis. 00031- 3. Semivolatile Organic Analyses:. Samples were analyzed by Method 8270. Surrogate standards: six surrogate standards were spiked into each analysis. Mitkem's statistical QC limits listed on the surrogate report form are different than the MADEP 30%- 130%soil QC-limits. All surrogate recoveries were within the MADEP QC limits with the exception of one surrogate in sample SB1-8. One additional surrogate in-sample SB1-8 and two surrogates in sample S133-6 were outside of the Mitkem QC limit. - Lab control sample/lab control sample duplicate:spike recoveries were within the Mitkem.statistical QC limits,as well as the MADEP limits_ Mitkem LCS QC limits-are generally.within the MADEP 40-140%limits for base/neutral and 30-130% limits for acid compounds with the exception of difficult analytes_ These QC limits and the difficult compounds have been statistically determined per method requirements_ Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample SB2-2_ Several spike recoveries were outside of the Mitkem statistical QC limits. Most of these were within the MADEP limits of 40-140% for base/neutral and 30-130% for acid compounds with the exception of 2,4-dinitrophenol at 28% and 25%. All replicate RPDs were within the in-house 40% RPD limit, and also within the MADEP 30% RPD limit. Sample analysis: internal standards were outside of the QC limits in the initial and dilution analyses of samples SSl-8 and S138-2. One internal standard in sample SB 10-2 was below the MADEP 5011/o peak area limit. This sample was mistakenly not . reanalyzed,as it was evaluated as being outside of the Mitkem QC limit but within the MADEP QC limit. Please note that a minor UCM is present in the retention time range for this internal standard,which likely contributes to the low internal standard area. The continuing calibration verification standard SSTD0502C has pentachlorophenol outside of the QC acceptance criteria. Please note that this standard is only associated with dilution analyses for PAH compounds. No other unusual occurrences were noted during sample analysis. 4. MADEP EPH Analysis: Samples were analyzed by EPH Method 04/1.1. Surrogate recovery:recoveries were within the QC limits. Laboratory control sample: spike recoveries were within the QC limits in lab control j sample and duplicate LCS with the exception of nonane at 32% and 27% respectively in the LCS and duplicate LCS. NYC i Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample SB5-2. All recoveries were within the QC limits with the exception of nonane at 24% and 26%respectively in the MS and MSD. Sample analysis: samples from another Mitkem project(number C1387)analyzed after these samples caused ending continuing calibration verification standards to have selected compounds exceeding the 25% D limit. This has minimal effect on this set of samples. The response for C36 was marginally low at 26%D, while the C 19-C36 aliphatic range. was well within the limit at 5.9%D in ending CCV-F 1 D8142. This was judged.not to impact the quantitation of project samples. Several.aromatic target compounds in CCVs FID8143 and FID8159 were more than 25%D, while the%D for the aromatic range was approximately 12% in each CCV. The aromatic fractions of samples S138-2 and SB10-2 were reanalyzed. Concentrations for the effected target analytes were very similar to the initial analysis results. A contaminant in the EPH fractionation cartridges was present in the aliphatic and aromatic ranges. The identity of this contaminant has been confirmed as not related to petroleum aliphatic or aromatic hydrocarbons by GUMS, and has been subtracted from the appropriate EPH Range results. The method blank contained an additional pattern of contamination peaks in the C I 1-C22 Aromatic range exceeding the reporting limit. This pattern of peaks is due to the fractionation cartridges, and does not match a typical hydrocarbon product. No other unusual occurrences were noted during sample analysis_ 5. PCB Analysis: Samples were analyzed by Method 8082. Surrogate standards: percent recoveries were within the QC limits with the exception of one surrogate on one GC column in sample S137-2. Mitkem's statistical QC limits listed on the surrogate report form are slightly different from the MADEP 30%-150% limits. Lab control sample: spike recoveries were within the QC limits in the LCS/LCS duplicate. Mitkem's statistical QC limits listed on the LCS report form are tighter than the MADEP 40%-140% limits. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample SB2-2. All spike recoveries were within the QC limits: Mitkem's statistical QC limits listed on the LCS report form are tighter than the MADEP 401/o-140% limits. Sample analysis: no unusual occurrences were noted during sample analysis. 6_ Metals Analysis: Samples were analyzed by methods 6010B and 7471. .. Lab control sample:spike recoveries were within the QC limits. A matrix spike and matrix duplicate were analyzed instead of a duplicate LCS. Matrix spike:matrix spike analyses were performed on sample S134-14 for cyanide, SB8= 2 for metals and S133-6 for cyanide_ Spike recoveries were within the QC limits,with the exception of cyanide in sample S133-6. Post-digestion spike analysis was performed with- improved recovery. The associated cyanide sample results are qualified with the"N" flag. Matrix duplicate:matrix duplicate analyses were performed on samples S134-14 for cyanide, S138-2.for metals and SB3-6 for cyanide. Replicate RPDs were within the QC limits with the exception of vanadium, zinc and mercury in S138-2_ Sample.analysis: due to a laboratory scheduling error, cyanide analyses for samples SB4- 14 and SB10-2 were not performed within the method holding time These samples were distilled on December 9, 2004, which is the 21S`day from sample collection. Cyanide was not detected in either of these samples_ No other unusual occurrences were-noted during sample analysis. ) 7. Wet Chemistry: Selected samples were analyzed for hexavalent chromium by Method 3060/7196. Samples were received"on-hold"and analyzed per subsequent authorization from the client. Samples were analyzed in two batches, one(batch# 16056) without the insoluble hexavalent chromium spike, and the second(batch# 16250) including the insoluble hexavent chromium spike. Laboratory control sample: percent recoveries were within the QC limits. LCSD-16250 is an LCS spiked with the insoluble hexavalent-chromium spike, and is not actually an LCSD. Matrix spike: matrix spike analysis was performed on sample S139-8 in both batches. Percent recoveries were within the QC limit. Matrix spike in batch 16250 was performed with both soluble hexavelent chromium and insoluble hexavelent chromium. The insoluble hexavalent chromium spike is reported as an MSD. Percent recovery for the soluble hexavelent chromium spike was 70%_ Duplicate: duplicate analyses were performed on sample S139-8 in both batches. Replicate RPD was within the QC limits. i Sample analysis: as described above,the matrix spike using insoluble hexavelent chromium was not performed in this'batch_ The entire batch was.reanalyzed along with. an insoluble hexavelent chromium spike. The reanalyses occurred beyond the 30 day holding time for this method. No other unusual occurrences were noted during sample analysis_ All pages in this report have been numbered consecutively, starting with the title page and ending with a page saying only"Last Page of Data Report". I certify that this data package is in compliance, both_technically and for completeness,: for.other than the conditions detailed above. Release of the data contained.in'this hardcopy data package has been authorized by the laboratory manager-or his designee, as verifi the following signature. Edward A. Lawler Laboratory Operations Manager 12/28/04, Revised 2/8/05 Laboratory Name: r'�k Project Project Location: J4�e� MADEP RTN': This Form provides certifications for the following data set:[list laboratory Sample iD Number(s)) se4r 4 c iys3 Sample Matrices: O Groundwater U Soil/Sediment D Drinking Water it Other_ —8260E - 8151A( ) 8330( ) 6010B>n' 1470A11A 8270C 8081 A( ) VPH 6020( ) 9014Mt 2{ ) 8082 IN yy 80218 ( } EPH 700Q S3( ) 7196A AA i An affirmative response to questions A, B, C and D is required for`Presumptive Certainty'status A Were all samples received by the laboratory in a condition consistent with i _ that described on the Chain-of-Custody documentation for the data set? Yes O No Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed, including the requirement to note and Yes [] No' discuss in a narrative QC data that did not meet appropriate perfomiance standards or guidelines? r. Does the data included in this report meet all the analytical requirementsy2i1t`� C for"Presumptive Certainty'; as described in Section 2.0 (a), (b), (c) and No' (d) of-the-MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data'? p VPH and EPH Methods on - Was the VPH or EPH Method conducted Yes O No ' Without significant modifications(see Section 11-3 of res five Methods) A response to questions E and F below is required for"Presumptive Certainty"status E Were ail analytical QC performance standards and recommendations for O Yes ANo' the specified methods achieved? s� ywrQ � F Were results for all analyteaist compounds/elements for the specified Yes 17 No' method(s)reported? iAll Negative responses must be addressed in an attached Environmental Laboratory case narrative- 1, the undersigned, attest under the pains and penalties of perjury that,based upon my personal inquiry of those.responsible for obtaining the information, the material contained in this analytical report i , the best of my owledge and belief,accurate and complete_ Signature_ Position: Printed Name. t D f2+� ate:— CAM VII A,rev-3.2 April 2004 0008 Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: SB1-8 Date Analyzed: 11/29/04 Lab tD: C1453-OIC Aliquot Used for Analysis: 100 uL Matrix: Soil,92%Solid Sample Aliquot:.5.5g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. i Reporting Target Anabdes Result Lkad Benzene ND 27D Ethylbenzene 3,500 270 Toluene 1,300 270 o-Xylene 3,400 270 m-and p-Xylenes 410 270 MTBE ND 270 Naphthalene 310 270 QC Batch: 15868 VPH.Ranges C5-C8 Aliphatics 24,000 5,400 C9-C10 Aromatics 240,000 5,400 C9-C12 Aliphatics 240,000 5,400 Surrogate Recovery(%}: 2,5-Dibromotoluene(FID) 25` 2,5-Dibromotoluene(PID) 10* ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. =Surrogate recovery outside 709/6-130%range Page 1 of 1 C1453-61 C Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: SB1-8RE Date Analyzed: 1211104 Lab ID: C1453-01CRE Aliquot Used for Analysis: 100 uL Matrix: Soil,92%Solid Sample Aliquot: 5.5g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting - Target Analyf Results Limit Benzene ND 270 Ethylbenzene 3,f00 270 Toluene 1,100 270 o-Xylene 2,900 270. m-and p-Xylenes 350 270 MTBE ND 270 Naphthalene 460 270 QC Batch: 15906 VPH Ranges ) C5-C8 Aliphatics 22,000 5,400 C9-C10 Aromatics 220,000 5,400 C9-C12 Aliphatics 230,000 5,400 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 21* 2,5-Dibromotoluene(PID) 8.9' ND=Not Detected Except where noted in the'Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. =Surrogate recovery outside 709/030%range Page 1 of 1 C1453-01 CRE 1 i 4 I Analysis Report:Volatile Petroleum Hydrocarbons i Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1. Date Received: 11/18/04 Client ID: SB9-8 Date Analyzed: 11/26/04 Lab ID: C1453-04C Aliquot Used for Analysis: 100 uL Matrbc Soil,85%Solid Sample Aliquot: 3.99/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor 1 Reporting Target Analytes Results LL mi Benzene ND 420 Ethylbenzene ND 420 Toluene ND 420 o-Xylene ND 420 m-and p-Xylenes ND 420 MTBE ND 4.20 Naphthalene ND 420 QC Batch: 15862 VPH Ranges C5-C8 Aliphatics ND 8,400 C9-C10 Aromatics ND 8,400 C9-C12 Aliphatics ND 8,400 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 111 2,5-Dibromotoluene(PID) 110 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. '=Surrogate recovery outside 70%-130%range Page 1 of 1 C1453-04C Analysis Report:Volatile Petroleum.Hydrocarbons Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/64 Client ID: SB5-2 Date Analyzed: 11/26/04 Lab ID: C1453-06C Aliquot Used for Analysis: 100 uL Matrix: Soil, 920/6 Solid Sample Aliquot: 4.5g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting Target Analyte Results UnI t Benzene ND 320 Ethylbenzene ND 320 Toluene ND 320 o-Xylene ND 320 m-and p-Xylenes ND 320 MTBE ND 320 Naphthalene ND 320 QC Batch: 15862 VPH Ranges C5-C8 Aliphatics ND 6,500 C9-C10 Aromatics 8,200 6,500 C9-C12 Aliphatics ND 6,500 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 106 2,5-Dibromotoluene(PID) 105 ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required CA/QC procedures were achieved. No significant modifications were made to this method_ =Surrogate recovery outside 70%-1300/o range Page 1 of 1 C1453-06C Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: TRIP Date Analyzed: 12/1/04 Lab ID: C1453-08C Aliquot Used for Analysis: 100 uL Matrix: Soil, 100%Solid Sample Aliquot: 5g/5mL Concentration.in:ug/Kg,dry weight basis Dilution Factor 1 Reporting Target Analft!j Results LIm1Y Benzene NO 250 Ethylbenzene NO 250 Toluene NO 250 o-Xylene NO 250 m-and p-Xylenes NO 250 MTBE NO 250 Naphthalene NO 250 QC Batch: 15906 VPH Ranges C5-C8 Aliphatics NO 5,000 C9-C10 Aromatics NO 5,000 C9-C12 Aliphatics NO 5,000 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 119 2,5-Dibromotoluene(PID) 108 NO=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved_ f No significant modifications were made to this method. i i `=Surrogate recovery outside 70%-130%range 1 Page 1ofI C 1453-08C Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: SB-X Date Analyzed: 11/26/04 Lab ID: C1453-09C Aliquot Used for Analysis: 100 uL. Matrix: Soil,86%Solid Sample Aliquot:_ 5.7g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting -- Target AnalyL Results Una Benzene ND 300 Ethylbenzene ND 300 Toluene ND 300 o-Xylene ND 300 m-and p-Xylenes ND 300 MTBE ND 300 Naphthalene ND 300 QC Batch: 15862 VPH Ranges C5-C8 Aliphatics ND 5.900 C9-C70 Aromatics 7,800 5,900 C9-C12 Aliphatics ND 5,900 Surrogate Recovery{%): 2,5-Dibromotoluene(FID) 107 2,5-Dibromotoluene(PID) 106 ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved: No significant modifications were made to this method_ "=Surrogate recovery outside 70%-130%range Page 1 of 1 C1453-09C Analysis Report: Volatile Petroleum Hydrocarbons i Client TRC MA Date Collected: .11/17/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: SB8-2 Date Analyzed: 11/26/04 Lab ID: C1453-10C Aliquot Used for Analysis: 100 uL Matrix: Soil,87%Solid- Sample Aliquot: 7g 15mL .Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting Tared Analytes Results Limit Benzene ND 240 Ethylbenzene ND 240 Toluene ND 240 o-Xylene ND 240 m-and p-Xylenes ND 240 MTBE ND 240 Naphthalene ND 240 QC Batch: 15862 VPH Ranges C5-C8 Alfphatics ND 4,800 C9-C10 Aromatics .5,400 4,800 C9-C12 Aliphatics ND 4,800 Surrogate Recovery MY 2,5-Dibromotoluene(FID) 101 2,5-Dibromotoluene(PID) 101 ND=Not Detected Except where noted in the Project Narrative, all CWQC procedures required by the VPH method were I followed,and all performancelacceptance standards for the required QA/QC procedures were achieved. i No significant modifications were made to this method. ' =Surrogate recovery outside 70%-130%range Page 1 of 1 C1453-10C i Analysis Report Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/17/04 , Analysis: MADEP VPH 1.1 - Date Received: 11/18/04 j Client ID: SB3-6 Date Analyzed: 11/29/04 j Lab ID: C1453-12C Aliquot Used for Analysis: 100 uL II Matrix: Soil,91%Solid Sample Aliquot: 4.5g f.5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting Target Anal es Result;i Limit Benzene ND 330 Ethylbenzene 13,000 330 Toluene ND 330 o-Xylene 18,000 330 m-and p-Xylenes 1,800 330 _ MTBE ND 330 Naphthalene ND 330 QC Batch: 15868 VPH Ranges i C5-C8 Aliphatics 19,000 6,600 C9-C10 Aromatics 720,000 6,600 69-C12 Aliphatics 1,100,000 6,600 I� f Surrogate Recovery(%): I 2,5-Dibromotoluene(FID) 8.4* i 2,5-Dibromotoluene(PID) 2.6* ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures-were achieved. No significant modifications were made to this method_ *=Surrogate recovery outside 70%-130%range Page i of 1 C1453-12C i - i i Analysis Report: Volatile Petroleum Hydrocarbons Client:. TRC MA Date Collected: 1 i117/04 Analysis: MADEP VPH 1.1 Date Received: 11/18/04 Client ID: SB3-6DL Date Analyzed: 11/29/04 Lab ID: C1453-12CDL Aliquot Used for Analysis: 100 uL Matrix . . Soil,91%Solid Sample Aliquot: 4.5g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 2 Reporting Target Anabdes Result Limi Benzene- NO 660 Ethylbenzene 11,000 660 Toluene NO 660 o-Xylene 16,000 660 m-and p-Xylenes 1,000 660 MTBE NO 660 Naphthalene NO 660 QC Batch: 15868 VPH Ranges C5-C8 Allphatics 15,000 13,000 C9-C10 Aromatics 1,100,000 13,000 C9-C12 Aliphatics 1,000,000 13,000 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 2.0` 2,5-Dibromotoluene(PID) 0.76' NO=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. =Surrogate recovery outside 70%-130%range Page 1 of 1 C1453-12CDL Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 11/18/04 Analysis: MADEP VPH 1.1 Date Received: 11/19104 Client ID: SB4-14 Date Analyzed:. 11/26/04 Lab ID C1453-14C Aliquot Used for Analysis: 100 uL Matrix: Soil,97%Solid Sample Aliquot:-4.7g 15mL Concentration in:ug/Kg, dry weight.basis Dilution Factor. 1 Reporting raet An I es Results Lln Benzene ND 280 Ethylbenzene ND 280 Toluene ND 280 o-Xylene ND 280 m-and p-Xylenes ND .280 - MTBE ND 280 Naphthalene ND 280 QC Batch: 15862 VPH Ranges C5-C8 Aliphatics ND 5,600 C9-C10 Aromatics ND 5,600. C9-C12 Aliphatics ND 5,600 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 102 2,5-Dibromotoluene(PID) 99 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by.the VPH method were followed, and all performance/acceptance standards for the required CA/QC procedures were achieved. No significant modifications were made to this method. = Surrogate recovery outside 70%-130%range Page 1 of 1 C1453-14C i - Analysis Report: 61a*the Petroleum Hydrocarbons i Client: TRC MA Date Collected: 11/18/04 Analysis: MADEP VPH 1.1 Date Received: 11/19/04 i Client ID: SB2-2 Date Analyzed: 11126/04 I Lab ID: C1453-15C - Aliquot Used for Analysis: 100 uL I Matrix: Soil,96%Solid Sample Aliquot: 5.4g/5mL Concentration in:ug/Kg,dry weight basis. Dilution Factor. 1 Reporting Target Analyto Results )Limit Benzene ND 250 Ethylbenzene ND 250 Toluene ND 250 o-Xylene ND 250 m-and p-Xylenes ND 250 MTBE ND 250 Naphthalene ND 250 QC Batch: 15862 YPHf flanges C5-C8 Aliphatics NO 5,000 C9-C10 Aromatics 6,000 500 C9-C12 AliphaUcs ND 5,060 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 92 2,5-Dibromotoluene(PID) 92 I ND=Not Detected } I Except where noted in the Project Narrative,all CA/QC procedures required by the VPH method were I followed;and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. =Surrogate recovery outside 70%-130%range i l I i Page 1 of 1 C 1453-15C AnalysisReport: Volatile Petroleum Hydro carbons Client: TRC MA Date Collected: 11/18/04_ Analysis: MADEP VPH 1.1 Date Received: 11/19/04 Client ID: SB10-2 Date Analyzed: 12/1104 Lab ID: C1453-16C Aliquot Used for Analysis: 100 uL Matrix: Soil,94%Solid Sample Aliquot 5g/5mL Concentration in:ug/Kg,dry weight basis Dilution Factor. 1 Reporting - Target Ana yjes Results Benzene ND- 280 Ethylbenzene ND 280 Toluene ND 280 o-Xylene ND 280 m-and p-Xylenes ND 280 MTBE ND 280 Naphthalene ND 280 QC Batch: 159W VPH Ranges C5-C8 Aliphatics ND 5,600 C9-C10 Aromatics 6,400 5,600 C9-C12 Aliphatics ND 5,600 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 113 2,5-Dibromotoluene(PID) 105 ND=Not Detected Except where noted in the Project Narrative;all QA/QC procedures required by the VPH method were followed,and all.-performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. =Surrogate recovery outside 70%-130%range l Page 1 of 1 C1453-16C Analysis Report:Volatile Petroleum Hydrocarbons Client TRC. MA Date Collected: 11/18/04 Analysis: MADEP VPH 1.1 Date Received: 11/19/04 Client ID: TRIP Date Analyzed: 11/29/04 Lab ID. C1453-17C Aliquot Used for Analysis: 100 uL Matrix: Soil, 100%Solid Sample Aliquot 5g!5mL Concentration in:uAg,.dry weight-basis Dilution Factor. 1 Reporting Target Analydo-s Results LIMA Benzene ND 250 Ethylbenzene ND 250 Toluene ND 250 o-Xylene ND 250 m-and p-Xylenes ND 250 MT-BE ND 250 Naphthalene ND 250 QC Batch: 15868 VPH Ranges C5-C8 Aliphatics ND 5,000 C9-C10 Aromatics ND 5,000 C9-C12 Aliphatics ND 5,000 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 114 2,5-Dibromotoluene(P1D) 112 ND=Not Detected Except where noted,in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method: =Surrogate recovery outside 70%-130%range Page i of 1 C1453-17C CORPORATION Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP VPH 1.1 Client ID: VBLK4W Date Analyzed: 11/29/04 Lab ID: MB-15868 Aliquot Used for Analysis: 100 uL Matrix: Solid Sample Aliquot: 59/5mL Concentration in: ug/Kg,dry weight basis Dilution Factor. 1 Reporting Target Analvtes Results Limit Benzene ND 250 Ethylbenzene ND 250 Toluene ND 250 o-Xylene ND 250 m-and p-Xylenes ND 250 MTBE ND 250 Naphthalene ND 250 QC Batch: 15868 VPH Ranges l C5-C8 Aliphatics ND 5,000 J C9-C10 Aromatics ND 5,000 C9-C12 Aliphatics ND 5,000 Surrogate Recovery(%): 2,5-Dibrornotoluene(FID) 108 2,5-Dibromotoluene(PID) 100 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performancelacceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C1453-MB CORPORATION i Analysis Report Volatile Petroleum Hydrocarbons- Client: TRC MA Analysis: MADEP VPH 1.1 Client!D: VBLK4V Date Analyzed: 11/26/04 Lab ID: MB-15862 Aliquot Used for Analysis: 100 uL Matrix: Solid Sample Aliquot: 5g/5mL Concentration in: ug/Kg,dry weight basis Dilution Factor. 1 Reporting. Target Analvtes Results Limit Benzene ND 250 Ethylbenzene ND 250 Toluene ND 250 o-Xylene ND 250 m-and p-Xylenes ND 250 MTBE ND 250 Naphthalene ND 250 QC Batch` 15862 VPH Ranges C5-C8 Aliphatics ND 5,000 C9-C10 Aromatics ND 5,000 C9-C12 Aliphatics ND 5,000 Surrogate Recovery 2,5-Dibromotoluene(FID) 101 2,5-Dibromotoluene(PID) 96 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C 1453-MB RPO l Analysis Report: Volatile Petroleum Hydrocarbons. / Client TRC MA Analysis: MADEP VPH 1.1 Client ID: VBLK4X Date Analyzed: 1211/04 Lab ID: MB-15906 Aliquot Used for Analysis: 100 uL Matrix: Solid Sample Aliquot: 5g/5mL Concentration in: ug/Kg,dry weight basis Dilution Factor_ 1 Reporting Target Analvtes Results limit Benzene ND 250 Ethylbenzene ND 250 Toluene ND 250 o-Xylene ND 250 m-and p-Xylenes ND 250 MTBE ND 250 Naphthalene ND 250 QC Batch: 15906 VPH Ranges 1 C5-C8 Aliphatics ND 5,000 J C9-C10 Aromatics ND 5,000 C9-C12 Aliphatics ND 5,000 Surrogate Recovery(%): 2,5-Dibromotoluene tFID) 93 2,5-Dibromotoluene(PID) 84 ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed,-and all performance/acceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes_ Page 1 of 1 1 C1453-MB CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons i Lab Control Summary Client TRC_MA Matrix: Soil Lab ID: LCS-15906 Analysis Date for Blank Spike: 12/1l04 Analysis: MADEP VPH 1.1 Ana e % Recovery Benzene 103 Ethylbenzene 103 Toluene 103 o-Xylene 101 m-'and p-Xylenes 104 MTBE 93 Naphthalene 83 QC Batch: 15906 Ranee % Recovery C5-C8 Aliphatics 125 C9-C12 Alpihatics 109 C9-Cl0 Aromatics 104 Page 1 of 1 C1453-LCS O POR 1 Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client: TRC MA Matrix Soil Lab ID for Blank Spike: LCS-15868 Analysis Date for Blank Spike: 11/29/04 - Lab ID for BS Duplicate: LCSD-15868 Analysis Date for BS Duplicate: -11/29/04 Analysis: MADEP VPH IA % Recovery Analyte Blank Spike Blank Spike Duplicate RPD Benzene 101 99 2 Ethylbenzene 100 98 2 Toluene 100 99. 1 o-Xylene 98 98 0 m-and p-Xylenes 102 101 0 MTBE 90 98 8 Naphthalene 80 96 18 QC Batch: 15868 %Recovery Range Blank Spike Blank Spike Duplicate RPD % C5-C8 Aliphatics 120 115 4 C9-C12 Alpihatics 105 - 101 4 C9-C 10 Aromatics 102 102 0 Page 1 of 1 C1453-LCS CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons I Lab Control Summary Client: TRC_MA Matrix: Soil Lab ID: LCS-15862 Analysis Date for Blank Spike: 11l26/04 Analysis: MADEP VPH 1.1 Anal e % Recovery Benzene 100 Ethylbenzene 99 Toluene 99 o-Xylene 97 m-and p-Xylenes 101 MTBE 90 Naphthalene 80 QC Batch: 15862 Range % Recovery C5-C8 Aliphatics 116 C9-C12 Alpihatics 105 C9-C10 Aromatics 100 Page 1 of 1 C1453-LCS • • •O• a Analysis.Report: Volatile Petroleum Hydrocarbons Matrix Spike Summary Client: TRC MA Client ID: . SB5-2 Matrix: Soil _ Lab ID for Matrix Spike: C1453-06CMS Analysis Date for Matrix Spike: 11/26/2004 Lab ID for MS Duplicate: C1453-06GMSD Analysis'Date for MS Duplicate: 11/26/2004 Analysis:MADEP VPH 1-1 %Recovery Analyte Matrix Spike Matrix SiAe Duplicate RPD(%) Benzene 91 92 1 \ Ethylbenzene 91 91 0 J Toluene 91 92 1 o-Xylene 91 91 0 m-and p-Xylenes 93 94 1 MTBE 94 91 3 Naphthalene 98 72 30 % Recovery Range Matrix Spike Matrix Spike Duplicate RPD C5-C8 Aliphatics 97 95 2 C9-Cl2 Alpihatics 590 615 4 C9-C10 Aromatics 115 128 11 1 J Page 1 of 1 C1453-10S/10813 i i CORPORATION i i Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 0411.1 Date Collected: 11/17/04 Client ID: SB1-8 Date Received: I Ill8/04 Lab ID: C1453-01D Date Extracted: 11/27/04 Matrix:Soil, 92%Solid . Date Analyzed:1217104 F1 12/7104 F2 Concentration in:ug/kg,dry weight basis Dilution:1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics 2,700.000 11,000 C19-C36 Aliphatics 3,500,000 22,000 C11 -C22 Aromatics 1,500,000 11,000 Target Analytes Naphthalene ND 540 2-Methylnaphthatene 8,400 540 Acenaphthylene 4,100 540 Acenaphthene ND 540 Fluorene ND 540 Phenanthrene 5,000 540 Anthracene ND 540 Fluoranthene 1,100 540 Pyrene 1,100 540 Benzo(a)anthracene ND 540 Chrysene ND 540 Benzo(b)Fluoranthene ND 540 Benzo(k)Fluoranthene ND 540 Benzo(a)pyrene ND 540 Indeno(1,2,3-cd)pyrene ND 540 Dibenzo(a,h)anthracene ND 540 Benzo(ghi)perylene ND 540 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 74% o-Terphenyl 96% 2-Fluorobiphenyl 76% 2-Bromonaphthalene 53% ND=Not Detected Except where noted in'the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1453-OID 'RP,R , Analysis Report. Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected:11/17/04 Client ID: SB9-8 Date Received: 11/18/04 Lab ID: C1453-04D Date Extracted:11/27/04 Matrix:Soil,85%Solid Date Analyzed:1217/04 F1, 1217/04 F2 Concentration in:ug/kg,dry weight basis Dilution:.1 Reporting EPH Ran Results Limits C9-C18 Aliphatics ND , 12,000 C19-C36 Aliphatics 260,000 24,000 C11 -C22 Aromatics 75,000 12,000 Target Analvtes Naphthalene ND 590 2-Methylnaphthalene ND 590 Acenaphthylene ND 590 Acenaphthene ND 590 Fluorene ND 590 Phenanthrene ND 590 Anthracene ND 590 Fluoranthene ND 590 \ Pyrene ND 590 ) Benzo(a)anthracene ND 590 Chrysene ND 590 Benzo(b) Fluoranthene ND 590 Benzo(k)Fluoranthene ND _ 590 Benzo(a)pyrene ND 590 Indeno(1,2,3-cd)pyrene ND 590 Dibenzo(a,h)anthracene ND 590 Benzo(ghi)perylene ND 590 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 70% o-Terphenyl 61%. 2-Fluorobiphenyl 96% 2-Bromonaphthalene 100% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1453-04D i i CORPORATIO4 Analysis Report: Extractable Petroleum Hydrocarbons Client TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/.17/04 Client ID: SB5-2 Date Received: 11/18/04 Lab-ID: C1453-06D Date Extracted: 11/27/04 Matrix: Soil, 92%Solid Date Analyzed:12R/04 F1, 1217/04 F2 Concentration in:ug/kg,dry weight basis Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics ND 11,000 C19-C36 Aliphatics 120,000 22,000 CI -C22 Aromatics 59,000 11,000 Target Analvtes Naphthalene ND 540 2-Methylnaphthalene ND 540 Acenaphthylene NO, 540 Acenaphthene ND 540 Fluorene ND 540 Phenanthrene ND 540 Anthracene ND 540 Fluoranthene 660 540 Pyrene 710 540 Benzo(a)anthracene ND 540 Chrysene ND 540 Benzo(b)Fluoranthene ND 540 Benzo(k)Fluoranthene NO 540 Benzo(a)pyrene ND 540 Indeno(1,2,3-cd)pyrene ND 540 Dibenzo(a,h)anthracene ND 540 Benzo(ghi)perylene ND 540 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 83% o-Terphenyl -80% 2-Flu6robiphenyl 98% 2-Bromonaphthalene 98% ND-Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were Achieved- EPHranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1453-06D CORPORATION-] Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/17/04 Client ID: SB-X Date Received: 11/18/04 Lab ID: C1453-09D Date Extracted: 11/27/04 Matrix:Soil,86%Solid Date Analyzed:12[7/04 Fi., 12I7/04 F2 Concentration in:ug/kg, dry weight basis Dilution:) Reporting EPH Ranges Results Limits C9-CI Aliphatics ND 12,000 CI-C36 Aliphatics 35,000 23,000 CI -C22 Aromatics 30,000 12,000 Target Analvtes Naphthalene ND 580 2-Methylnaphthalene ND 580 Acenaphthylene ND 580 Acenaphthene ND 580 Fluorene ND 580 Phenanthrene ND 580 'Anthracene ND 580 Fluoranthene ND 580 \ Pyrene ND 580 J Benzo(a)anthracene ND 580 Chrysene ND 580 Benzo(b)Fluoranthene ND 580 Benzo(k)Fluoranthene ND 580 Benzo(a)pyrene ND 580 Indeno(1,2,3-cd)pyrene ND 580 Dibenzo(a,h)anthracene ND 580 Benzo(ghi)perylene ND 580 Surrogate Recovery: QC Batch: MB-15859 Chlorooctadecane 67% o-Terphenyl 62% 2-Fluorobiphenyl 98% 2-Bromonaphthalene 100% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C 1453-09D / i. Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/17/04 Client ID: SB8-2 Date Received: 11/18/04 Lab ID: C1453-10D Date Extracted: 11127/04: Matrix:Soil,87%Solid Date Analyzed--217/04 F1, 12/7/04 F2 Concentration in:ug/kg, dry weight basis Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics 14,060 11,000 CI-C36 Aliphatics 70,000 23,000 CI -C22 Aromatics 130,000 11,000 Target Analyles Naphthalene ND 580 2-Methylnaphthalene NO 580 Acenaphthylene - ND 580. Acenaphthene ND 580 Fluorene ND 580 Phenanthrene 5,000 580' Anthracene. 1,800 580 Fluoranthene 8,600 580 Pyrene 8,000 580 Benzo(a)anthracene 3,800 580 Chrysene 4,200 580 Benzo(b) Fluoranthene 4,500 580 Benzo(k) Fluoranthene 1,700 580. Benzo(a)pyrene 3,300 580 Indeno(1,2,3-cd)pyrene 1,600 580 Dibenzo(a,h)anthracene ND 580 Benzo(ghi)perylene 1,400 580 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 52% o-Terphenyl 55% 2-Fluorobiphenyl 96% 2-Bromonaphthalene 97% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved_ EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1453-10D IT K Ell CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/17/04 Client ID: SB8-2 RE Date Received: 11/18/04 Lab ID: C1453-10D RE Date Extracted: 11/27/04 Matrix: Soil,87%Solid Date Analyzed: 12/20/04 F2 Concentration in:ug/kg, dry weight basis Dilution: 1 Reporting EPH Ranges Results Limits C11 -C22 Aromatics 130,000 11,000 Target Analytes Naphthalene ND 580 2-Methylnaphthalene ND 580 Acenaphthylene ND 580 Acenaphthene ND 580 Fluorene ND 580 Phenanthrene 5,000 580 Anthracene 1,700 580 Fluoranthene 8,500 580 Pyrene 7,900 580 Benzo(a)anthracene 3,700 580 Chrysene 4,100 580 Benzo(b)Fluoranthene 4,300 580 Benzo(k)Fluoranthene 1,700 580 Benzo(a)pyrene 3,300 580 Indeno(1,2,3-cd)pyrene 1,900 580 Dibenzo(a,h)anthracene ND 580 Benzo(ghi)perylene 1,700 580 Surrogate Recovery: QC Batch: MB-15859 o-Terphenyl 55% 2-Fluorobiphenyl 96% 2-Bromonaphthalene 97% ND= Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved_ EPH ranges are adjusted to exclude concentration of target and QC (surrogate)analytes. Page 1 of 1 C1453-1 OD RE J i i MIT KE -11 O.P O I Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/17/04 Client ID: SB3-6 Date Received: 11/18/04 Lab 10: C1453-12D Date Extracted: 11/27/04 Matrix:Soil, 91%Solid Date Analyzed:1217/04 F1, 1217104 F2 Concentration in:ug/kg, dry weight basis Dilution: 1 Reporting EPH Rand Results limits C9-C18 Aliphatics- 57,000 11;000 C19-C36 Aliphatics 53,000 22,000 C11 -C22 Aromatics 61,000 11,000 Tart Analytes Naphthalene ND 550 2-Methylnaphthalene ND 550 Acenaphthylene ND 550 Acenaphthene ND 550 Fluorene ND 550 Phenanthrene ND 550 Anthracene ND 550 Fluoranthene ND 550 Pyrene ND 550 Benzo(a)anthracene ND 550 Chryserie ND 550 Benzo(b) Fluoranthene ND 550 Benzo(k) Fluoranthene ND 550- Benzo(a)pyrene ND 550 lndeno(1,2,3-cd)pyrene ND 550 Dibenzo(a,h)anthracene ND 550 Benzo(ghi) perylene ND 550 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 53% o-Terphenyi 56% 2-Fluorobiphenyl 100% 2-Bromonaphthalene 104% ND=Not Detected Except where noted in the Project Narrative,all QAIQC procedures required by the EPH methoct were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved_ EPH ranges are adjusted to exclude concentration of target and QG(surrogate)analytes- Page 1 of 1 C1453-12D CORPORATIO . Analysis Report_ Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected:11/18/04 Client ID: S84-14 Date Received: 11A9/04 . Lab ID: C1453-14D Date Extracted:11/27/04 Matrix:Soil,97%Solid Date Analyzed:12/7/04 F1, 1217/04 F2 Concentration in: ug/kg,dry.weight basis Dilution: 1 Reporting. EPH Ranges Results Limits C9-C18 Aliphatics 28,000. 10,000 C19-C36 Aliphatics 62,000 20,000 C11 -C22 Aromatics 65,000 10,000 Target Analytes Naphthalene ND 520 2-Methylnaphthalene ND 520 Acenaphthylene ND 520 Acenaphthene ND 520 Fluorene ND 520 Phenanthrene ND 520 Anthracene ND 520 Fluoranthene ND 520 Pyrene ND 520 Benzo(a)anthracene ND 520 Chrysene ND 520 Benzo(b)Fluoranthene ND 520 Benzo (k)Fluoranthene ND. 520 Benzo(a)pyrene ND 520 Indeno(1,2,3-cd)pyrene ND 520 Dibenzo(a,h)anthracene ND 520 Benzo(ghi)perylene ND 520 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 71% o-Terphenyl 72% 2-Fluorobiphenyl 98% 2-Bromonaphthalene 99% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1453-14D CORPORATION i Analysis Report: Extractable Petroleum Hydrocarbons Client TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/18/04. Client ID: SB2-2 Date Received: 11/19/04 Lab ID: C1453-15A Date Extracted: 11/27/04 Matrix:Soil,.96%Solid Date Analyzed:l217/04F1, 12f7/04-F2 Concentration in:ug/kg,dry weight basis Dilution: 1 i I Reporting EPH Ranges Results Limits C9-CI Aliphatics ND 10,000 C19-C36 Aliphatics 45,000 21,000 C11 -C22 Aromatics -31,000 10,000 Target Analytes _ Naphthalene ND 520 .2-Methyfnaphthalene ND 520 Acenaphthylene ND 520 Acenaphthene ND 520 Fluorene ND 520 Phenanthrene ND 520 Anthracene ND 520 Fluoranthene ND 520 Pyrene ND 520 Benzo(a)anthracene ND 520 Chrysene ND 520 Benzo(b)Fluoranthene NO 520 Benzo(k) Fluoranthene" ND 520 Benzo(a)pyrene ND 520 Indeno(1,2,3-cd)pyrene ND 520 Dibenzo(a,h)anthracene ND 520 Benzo(ghi) perylene ND 520 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 63% o-Terphenyl 68% 2-Fluorobiphenyl 101% 2-Bromonaphthalene 105% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the.required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1453-15A MITKEM CORPORATION Analysis Report:.Extractable Petroleum Hydrocarbons Client- TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/18/04 Client ID: SB10-2 Date Received: 11/19/04 Lab ID: C1453-16D Date Eztfacted: 11/27/04 Matrix:Soil, 94%SoGd Date Analyzed:1217/04 F1, 12/7/04 F2 Concentration in:ug/kg, dry weight basis Dilution_1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics 15,000 11,000 C19-C36 Aliphatics 80,000 20,000 C11 -C22 Aromatics 93,000 11,000 Target Analytes Naphthalene ND 530 2-Methylnaphthalene ND 530 Acenaphthylene ND 530 Acenaphthene ND 530 Ftuorene ND 530 Phenanthrene ND 530 Anthracene ND 530 Fluoranthene 980 530 1 Pyrene 970 530 Benzo(a)anthracene Nb 530 Chrysene ND 530 Benzo(b)Fluoranthene ND 530 Benzo(k)Fluoranthene ND 530 Benzo(a)pyrene ND 530 Indeno(1,2,3-cd)pyrene ND 530 Dibenzo(a,h) anthracene ND 530 Benzo(ghi)perylene ND 530 Surrogate Recovery: QC Batch:MB-15859 Chlorooctadecane 49% o-Terphenyl 52% 2-Fluorobiphenyl 95% 2-Bromonaphthalene 98% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1453-1613 l r CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 11/18/04 Client ID: SB10-2 RE Date Received: 11/19/04 Lab ID: C1453-16D RE Date Extracted: 11/21/04 Matrix:Soil,94%Solid Date Analyzed: 12/20/04 F2 Concentration in:ug/kg;dry weight basis Dilution: 1 . Reporting EPH Ranges Results .Limits i C11-C22 Aromatics. 160,000 11,000 Target Analytes Naphthalene ND 530 2-Methy1naphthalene ND 530 Acenaphthylene ND 530 Acenaphthene ND 530 Fluorene ND 530 Phenanthrene ND 530 Anthracene ND 530 Fluoranthene 950 530 j Pyrene 950 530 Benzo(a)anthracene ND 530 Chrysene ND 530 i Benzo(b) Fluoranthene ND 530 Benzo(k)Fluoranthene. ND 530 Benzo(a)pyrene ND 530 Indeno(1,2,3-cd)pyrene ND 530 Dibenzo(a,h)anthracene ND 530 Benzo(ghi)perylene ND 530 Surrogate Recovery: QC Batch: MB-15859 o-Terphenyl 52% 2-F1uorobiphenyl 93% 2-Bromonaphthatene 95% ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved_ EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1453-16D RE CORPORATION Analysis Report: Matrix Spike Client TRC Date Extracted for MS/MSD: 11/27/04 Matrix: Soil: Date Analyzed for MS: 12/7/04 Client ID_ SB5-2 Date Analyzed for MSD: 12f7/04 Lab 1D for Matrix Spike(MS):C1453-06DMS Lab ID for Matrix Spike Duplicate(MSD):C1453-06DMSD Analysis: MADEP EPH 04-1.1 MADEP EPH - F1 -ALIPHATICS Anal e %Recovery MS MSD %RPD Naphthalene 50 56 10 2-Methylnaphthalene .53 59 10 Acenaphthylene 59 64 8 Acenaphthene .63 69 8 Fluorene 69 76 9 Phenanthrene 82 91 10 Anthracene 78 88 11 Fluoranthene 77 84 9 Pyrene 76 83 9 Benzo(a)anthracene 85 91 8 Chrysene 85 92 8 Benzo(b) Fluoranthene 92 101 9 Benzo(k)Fluoranthene 79 86 9 Benzo(a)pyrene 89 94 5 Indeno(1,2,3-cd)pyrene 77 83 7 Dibenzo(a,h)anthracene 66 73 10 Benzo(ghi)perylene 69 74 8 C11 -C22 Aromatics 74 80 9 Surrogate Recovery. MS MSD o-Terphenyl 76% 84% 2-Fluorobiphenyl 98% 99% 2-Bromonaphthalene 102% 96% Page 2 of 2 eph.ms/msd Quantitation Report p (Not -Reviewed) Data File C:\HPCHEM\l\DATA\SEP64\0.4.0921\F1D7337.D Vial: 98 Ac.q On 9-21-04 11:53 :45 PM Operator: TT Sample FRACT CHECK AROMATICS' F2 '' Inst : F1' Misc : 25ug/ml Multiplr: 1.00 ) IntFile : autointl_e Quant Time: Sep 21 13 :00 19104 Quant Results File: PAH0825F.RES Quant Method : C:\HPCHEM\1\QMETHODS\PAH0825F.M (Chemstation Integrator) Title. : EPH PAH Fraction Last Update : Mon Sep 13. 10:37:42 2004 Response. via : Initial Calibration C A2&, ,06(f, DataAcq Meth EPH2 .M g6ej� � Volume Inj . : 1 UI, � . z Signal Phase DB-5MS Signal Info 0.25 MM - Compound R-T. Response Conc Units ----------------------------------------------------------- Internal Standards 1) I 5a-Androstane 22 .59 35419720 40.000 ng/ul System Monitoring Compounds 2) S ortho-Terphenyl 0.00 0 N.D. ng/ui Spiked Amount 20. 000 Recovery = 0 .000 6) S FRAC S 2-FLUOROBIPHENYL 13 .25 14795071 17.760 ng/ul Spiked Amount 20.000 Recovery = 88_80g 8) S FRAC S 2-BROMONAPHTHALENE 15. 15 10002168 17.750 ng/ul Spiked Amount 20.000 Recovery = 88.75% Target Compounds 3) Contaminant - BHT 15.37 36474576 NoCal ng/ul 4) Naphthalene 1.0. 16 13136698 14.610 ng/ul 5) 2-Methy1naphthalene 12. 13 13779718 15.594 ng/ul 7) Acenaphthylene 14. 73 14844052 16.428 ng/ul 9) Acenaphthene . 15.26 16264305 17. 685 ng/ul 10) Fluorene 16. 79 17395964 19.066 ng/ul 11) Phenanthrene 19.63 19112286 20.785 ng/ul 12) Anthracene 19. 78 19014497 21. 708 ng/ul 13) Fluoranthene 23 . 17 19880104 21.395 ng/ul 14) Pyrene 23 . 83 20250434 21. 184 ng./ul 15) Benzo (a) anthracene 27.43 19909872' 21.201 ng/ul 16) Chrysene 27.53 20085047 21. 564 ng/ul 17) Benzo (b) Fluoranthene 30 .46 21492363 23 .335 ng/ul 18) Benzo (k) Fluoranthene 30.55 20380435 21. 610 ng/ul 19) Benzo (a) pyrene 31.47 19097103 22.277 ng/ul 20) Indeno (1, 2, 3-cd) pyrene 35. 97 18591048' 23 .34.7 ng/ul 21) Dibenzo (a,h) anthracene 36. 14 18387678 21. 159 ng/ul 22) Benzo (ghi) perylene 37. 04 19205057 22 .700 ng/ul to C1 tR-co - ------------------------------------------------------------- (f) =RT Delta > 1/2 Window (m) =manual int. F1D7337 :D AL0312R.M Tue Sep 21 13 :05 :20 2004 HPDOS9 Page 1 Quantitation Report . (QT Reviewed) Data File : C:\HPCHEM\1\DATA\SEP04\040921.SEC\F1D7336.D Vial: 96 Acq On 9-21-04 11:53 :-45 . PM Operator: TT Sample FRACT CHECK ALIPHATICS F1 Inst F1 Misc 25ug/ml Multiplr: 1.00 IntFile autointl.e Quant Time: Sep 21 13 :02 19104 Quant Results File: AL0312R.RES Quant Method : C:\HPCHEM\1\QMETHODS\AL0312R.M (Chemstation Integrator) Title : EPH Aliphatic Hydrocarbon Fraction i Last Update : Thu Aug 26 09:17:32 2004 Response via : Initial_ Calibration DataAcq Meth : EPH2.M '�f _Volume Inj . : I UL /r Signal Phase DB-SMS ' Signal Info : 0.25 MM Compound R.T. Response Conc Units ----------------------------------------------------------------------_-- Internal Standards 1) I 5a-Androstane 22 .40 50391176 40 .000 ng/ul System Monitoring Compounds 2) S 1-Chlorooctadecane 0.00 0 N.D. ng/ul Spiked Amount 20.000 Recovery = 0 .000 i Target Compounds 3) Contaminant - BHT 15.20 22253329 NoCal ng/ul Nonane C9 4.62 13040226 10 .669 ng/ulm,3 5) Decane C10 6.38 _16958492 13 _718 ng/ul 6) Dodecane C1.2 10.07 19178539 16.776 ng/ul 7) 2-Fluorobiphenyl 0.00 6 N:D_ ng/uld 8) Tetradecane C14 13.50 20582457 18 .113 ng/ul 9) 2=Bromonaphthalene 0.00 0 N.D. ng/ul 10.) Hexadecane C16 16.58 24225068 19 .484 ng/ul 11) Octadecane C18 19.35 26305068 20 .566 ng/ul 12) Nonadecane C19 20 .64 25861272 20 .238 ng/ul 13) Eicosane C20 21.87 26490090 21 .313 -ng/ul 14) Docosane C22 24 .18 27296338 21 .053 ng/ul 15) Tetracosane C24 26.30 27045065 20 .756 ng/ul 16) Hexacosane C26 28.26 26835480 20 .410 ng/ul 17) Octacosane C28 30 .09 26535569 20.305 ng/ul 18) Triacontane C30 32 .33 26281020 20 .222 ng/ul 19) Hexatriacontane C36 41.49 23489150 18 .974 ng/ul 1 Otc,� lLe Cow _ 51 9 �Zl !n4 i ----------------------------------------------------------------------------- (f) =RT Delta > 1/2 Window (m) =manual int. F1D7336.D AL0312R.M Tue Sep 21 13 :04 :02 2004 HPDOS9 Page 1 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS -No. : SDG No. : MC1453 / Matrix: (soil/water) SOIL Lab Sample ID: C1453-09A Sample wt/vol: 6.4 (g/mL) G Lab File ID: V2G5931 Level: (low/med) IOW Date Received: 11/18/04 Moisture: not dec. 14 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:^ (ML) Soil Aliquot Volume: __(uL) CONCENTRATION UNITS• CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 4 U 74-87-3---------Chloromethane 4 U 75-01-4---------Vinyl Chloride 4 U 74-83-9---------Bromomethane 4 U 75-00-3---------Chloroethane 4 U 75-69-4---------Trichlorofluoromethane 2 J 75-35-4---------1,1-Dichloroethene 4 U 67-64-1---------Acetone 35 75-15-0---------Carbon Disulfide 4 U 75-09-2---------Methylene Chloride 12 156-60-5--------trans-1,2-Dichloroethene 4 U 1634-04-4-------Methyl tert-butyl ether 4 U 75-34-3---------1;1-Dichloroethane 4 U 78-93-3--- ------2-Butanone 7 156-59-2--------cis-1,2-Dichloroethene 4 U 590-20-7--------2,2-Dichloropropane 4 U 74-97-5---------Bromochloromethane 4 U 67-66-3---------Chloroform 4 U 109-99-9--------Tetrahydro uran . 4 U 71-55-6---------1, 1,1-Trichloroethane 4 U. 563-58-6--------1, 1-Dichloropropene 4 U 56-23-5---------Carbon Tetrachloride 4 U 107=06-2--------1,2-Dichloroethane 4 U 71-43-2---------Benzene 4 U 79-01-6---------Trichloroethene 4 U 78-87-5---------1,2-Dichloropropane 4 U 74-95-3---------Dibromomethane 4 U 75-27-4---------Bromodichloromethane 4 U 10061-01-5------cis-1,3-Dichloropropene 4 U 108-10-1--------4-Methyl-2-pentanone 4 U 108-88-3--------Toluene 4 U 10061-02-6------trans-1,3-Dichloropropene 4 U 79-00-5---------1,1,2-Trichloroethane 4 U 142-28-9--------1,3-Dichloropropane 4 U FORM I VOA OLM03.0 lA EPA SAMPLE No.- VOLATILE ORGANICS ANALYSIS DATA SHEET SB=X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM . Case No. : SAS No. : SDG No : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-09A Sample wt/vol 6.4 (g/mL) G Lab File ID: V2G5931 Level: (low/med) LOW Date Received: ll/18/04 . Moisture: not. dec.. 14 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (man) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: _(U;) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q J 127-18-4--------Tetrachloroethene 10 591-78-6--------2-Hexanone 4 U 124-48-1--------Dibromochloromethane 4 U 106-93-4---------1,2-Dibromoethane 4 U 108-90-7--------Chl:orobenzene 4 U 630-20-6--------1,1,1,2-Tetrachloroethane 4 U 100-41-4--------Ethylbenzene 4 U ----------------m,p-Xylene _ 1 J 95-47-6---------o-Xylene 4 U 1330-20-7-------Xylene (TOtal) 1 J 100-42-5--------Styrene 4 U 75-25-2---------Bromoform_ 4 U 98-82-8-------- Isopropylbenzene 4 U 79-34=5---------1,1,2,2-Tetrachloroethene 4 U 108-86-1--------Bromobenzene 4 U 96-18-4---------1,2,3-Trichloropropane 4 U 103-65-1--------n-Propylbenzene 4 U 95-.49-8---------2-Chlorotoluene 4 U 108-67-8--------1,3,5-Trimethylbenzene 4 U 106-43-4--------4-Chlorotoluene 4 U 98-06-6---------tert-Butylbenzene 4 U . 95-63-6---------1,2,4-Trimethylbenzene 4 U 135-98-8--------sec-Butylbenzene 4 U 99-87-6---------4-Isopropyltoluene 4 U 541-73-1--------1,3-Dichlorobenzene 4 U 106-46-7--------1,4-Dichlorobenzene 4 U 104-51-8--------n-Butylbenzene _ 4 U 95-50-1---------1,2-Dichlorobenzene 4 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 4 U 120-82-1--------1,2,4-Trichlorobenzene 4 U 87-68-3---------Hexachlorobutadiene_ 4 U 91-20-3---------Naphthalene 4 U 87-61-6---------1,2,3-Trichlorobenzene 4 U 60-29-7---------Ether 4 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET. SB-X Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-09A Sample wt/vol: 6.4 (g/mL) G Lab File ID: V2G5931 Level: (low/med) IOW Date Received: 11/18/04 ?k Moisture: not decl 14 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: _WL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 4 U 637-92-3--------Ethyl tert-butyl ether 4. 0 994-05-8--------tert-Amyl methyl ether 4 U 123-91-1--------1,4-Dioxane 91 U FORM I VOA OLM03 .0 lA . EPA SAMPLE. NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB1-8 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG .No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-OIA Sample wt/vol: 6.8 (g/mL) G Lab File ID: V2G5929 Level: (low/med) LOW Date Received: 11/18/04 Moisture: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1..0 Soil Extract Volume:_ (ML) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 4 U 74-87-3---------Chloromethane 4 U 75-01-4---------Vinyl Chloride 4 U 14-83-9---------Bromomethane 4 U 75-00-3---------Chloroethane 4 U 75-69-4---------Trichlorofluoromethane 2 J 75-35-4---------1,1-Dichloroethene _ 4 U 67-64-1---------Acetone. 42 75-15-0---------Carbon Disulfide_ 4 U 75-09-2---------Methylene Chloride 8 156-60-5--------trans-1,2-Dichloroethene 4 U 1634-04-4-------Methyl tert-butyl ether 4 U 75-34-3---------1,1-Dichloroethane_ 4 II 78-93-3---------2-Butanone 4 U 156-59-2--------cis-1,2-Dichloroethene 4 U 590-20-7--------2,2-Dichloropropane 4 U 74-97-5---------Bromochloromethane 4 U 67-66-3---------Chloroform 4 U 109-99-9---------Tetrahydrofuran 4 U 71-55-6---------1,1,1-Trichloroethane _ 4 U 563-58-6--------1,1-Dichloropropene 4 U 56-23-5---------Carbon Tetrachloride 4 U 107-06-2--------1,2-Dichloroethane 4 U 71-43-2--- -------Benzene _ 8 79-01-6---------Trichloroethene 4 U 78-87-5---------1,2-Dichloropropane_ 37 74-95-3---------Dibromomethane 4 U 75-27-4---------Bromodichloromethaane 4 U 10061-01-5-------cis-1,3-Dichloropropene 4 U 108-10-1--------4-Methyl-2-pentanone 4 U 108-88-3--------Toluene 4 U 10061-02-6------trans-1,3-Dichloropropene 4 U 79-00-5---------1,1,2-Trichloroethane 4 U 142-28-9--------1,3-Dichloropropane 4 U j FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SBl-8 -Lab Name: MITKEM CORPORATION Contract- Lab. Code: MITiCEM Case No. SAS No. SDG No. : MC14 S 3 / Matrix: (soil/water) SOIL Lab Sample ID: C1453-01A Sample wt/vol: 6.8. (g/mL) G Lab File ID: V2G5929 Level: (low/med) LOW Date .Received: 11/18/04 o Moisture: not dec. 8 Date Analyzed 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 127.-18-4---=----Tetrachloroethene 40 591-78-6--------2-Hexanone 4 U 124-48-1--------Dibromochloromethane 4 U 106-93-4--------1,2-Dibromoethane 41 U 108-90-7--------Chlorobenzene 4 U 63-0-20-6---------1,1,1,2-Tetrachloroethane 4 U 100-41-4--------Ethylbenzene 98 ----------------m,p-Xylene 130 95-47-6---------o-Xylene 27 1330-20-7-------Xylene (Total) 160 100-42-5--------Styrene 4 U 75-25-2---------Bromoform 4 U 98-82-8----------Isopropyl zene 730 E 79-34-5---------1,1,2,2-Tetrachloroethane 4 U 108-86-1--------Bromobenzene 4 U 96-18-4----------1,2,3-Trichloropropane - 4 U 103-65-1--------n-Propylbenzene 20000 E 95-49-8---------2-Chlorotoluene 4 U 108-67-8--------1,3,5-Trimethylbenzene 4 U 106-43-4--------4-Chlorotoluene 4 U 98-06-6---------tert-Butylbenzene 980 E 95-63-6---------1,2;4-Trimethylbenzene 5300 E 135-98-8--------sec-Butylbenzene 16000 E 99-87-6---------4-Isopropyltoluene 5300 E 541-13-1--------1,3-Dichlorobenzene 4 U -106-46.7--------1,4-Dichlorobenzene 4 U 104-51-8--------n-Butylbenzene 10000 E 95-50-1---------1,2-Dichlorobenzene 4 U 96-12-8---------1,2-Dibromo-3-chloropropane 4 U 120=82-1--------1,2,4-Trichlorobenzene 4 U 81-68-3---------Hexachlorobutadiene 4 U 91-20-3---------Naphthalene 140 87-61-6---------1,2,3-Trichlorobenzene 4 U 60-29-7---------Ether 4 U FORM I VOA OLM03.0 1 I . . lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET i SB1-8 i Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No_ : MC1453 Matrix:. (soil/water) SOIL Lab Sample ID: C1453-OIA Sample wt/vol: 6.8 (g/mL) G Lab File ID: V2G5929 Level: (low/med) LOW Date Received.: 11/18/0' %- Moisture.: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uh) CONCENTTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 168-20-3--------Diisopropyl Ether. 4 U 637-92-3--------Ethyl tert-butyl ether 4 U 994-05-8--------tert-Amyl methyl ether 4 II 123-91-1--------1,4-Dioxane 80 U i FORM I VOA OLM03.0 lA EPA SAMPLE NO.. VOLATILE ORGANICS ANALYSIS DATA SHEET SBl-8 Lab Name: MITKEM CORPORATION Contract: Lab.Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 J Matrix-. (soil/water) SOIL 'Lab Sample ID: C1453-01B Sample wt/vol: 6.5 (g/mL) G _ Lab File ID VSF6826 . Level: (low/med) MED Date Received: 11/18/04 W Moisture: not .dec. 8 . Date Analyzed: 12/01/04 GC Column: DE-624 ID: 0.25 (am) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Sail Aliquot Volume: 100.0(UL) C70NCE2TTRATION UNITS: CAS NO. (FOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 230 U 74-87-3----=----Chloromethane 230 U 75-01-4---------Vinyl Chloride 230 U 74-83-9---------Brcuomethane 230 U 75-00-3---------Chloroethane - 230 U 75-69-4---------TrichlorofluoromeL ane 230 U 75-35-4---------1,1-Dichloroethene 230 U 67-64-1---------Acetone 230 U 75-15-0---------Carbon 1isu-1fide 230 U 75-09-2---------Methylene Chloride 200 J 1 156-60-5--------trans-1,2-Dichloroethene 230 U J 1634-04-4-------Methyl tert-butyl ether 230 U 75-34-3---------1,1-Dichloroethane _ _ 230 U 78-93-3---------2-Butanone 230 U 156-59-2--------cis-1,2-Dic oroe a 230 U 590-20-7--------2,2=Dichloropropane__ 230 U 74-97-5-------- Bromochloromethane 230 U 67-66-3---------Chloroform 230 U 109-99-9--------Tetrahydrofuran 230 U 71-55-6---------1,1,1-Trichloroethane 230 U 563-58-6--------1,1-Dichloropropene 230 U 56-23-5---------Carbon Tetrachloride _ 230 U 107-06-2--------1,2-Dichloroethane 230 U 71-43-2---------Benzene 230 U 79-01-6---------Trichloroet ene 230 U 78-87-5---------1,2-Dichloropropane 230 U 74-95-3------.---Dibr-no thane 230 U 75-27-4---------Bromodichlorome a 230 U 10061-01-5------cis-1,3-Dichloropropene 230 U 108-10-1--------4-Methyl-2-pentanone 230 U 108-88-3---------Toluene 230 U 10061-02-6------trans-1,3-Dic-oropropene 230 U 79-00-5---------1,1,2-Trichloroethane 230 U 142-28-9--------1,3-Dichloropropane - 230 U FORM I VOA OLM03.0 1A EPA SAMPLE No. VOLATILE. ORGANICS ANALYSIS DATA SHEET i - - SB1-8 Lab Name: MITKEK CORPORATION Contract: Lab Code: MITK M Case No. : SAS No. : SDG No. : MC1453 I Matrix: (soil/water) SOIL Lab Sample ID: C1453-01B j Sample wt/vol: 6.5 (g/mL) G Lab File ID: VSF6826 Level: (low/med) MED' Date Received: 11/18/04 Moisture:: not dec. 8m Date Analyzed: 12/01/04 CC Column: DB-624 ID 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(ML) Soil Aliquot Volume: 100.0(uL) S CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/K 4 127-18-4--------Tetrachloroethene 230 U 591-•78-6--------2-Hexanone 230 U I 124-48-1--------Dibro6aochlorome thane 230 U 106-93-4--------1,.2-Dibromoethane 230 U 108 90-7--------Chloroberizene 230 U 630-20-6--------1,1;1,2-Tetrachloroethane 230 U 100-41-4--------Eutylbenzene 98 J ----------------m,p-Xylene 160 J 95-47-6---------o-Xylene 46 J 1330-20-7-------Xylene (Totalf 210 J 100-42-5--------Styrene_ _ 23.0 U 75-25-2---------Bromoform 230 U 98-82-8---------Isopropyl enzene 1200 79-34-5---------1,1,2,2-Tetrachloroethane 230 U 108-86-1--------Bromobenzene 230 U 96-18-4---------1,2,3-Trichloropropane 230 U 103-65-1--------n-Propylbenzene 2200 95-49-8---------2-Chlorotoluene 230 U 108-67-8------ 1,3,5-Trimethylbenzene 960 106-43-4--------4-Chlorotoluene 230 U 98-06-6----------tert-Butylbenzene 150 J 95-63-6---------1,2,4-Trimethylbenzene 1100 135-98-8--------sec-Butylbenzene 2900 99-87-6---------4-Isopropyltoluene 1400 541-73-1--------1,3-Dichlorobenzene 230 U 106-46-7-----m---1,4-Dichlorobenzene 230 U 104-51-8--------n-Butylbenzene 3100 95-50-1---------1,2-Dichlorobenzene 230 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 230 U 120-82-1--------1,2,4-Trichlorobenzene 230 U 87-68-3---------Hexachlorobutadierle 73 J 91-20-3---------Naphthalene 230 U x 87-61-6---------1,2,3-Trichloro ,nzene 170 J 60-29-7---------Ether 230 U FORM I VOA 0LM03.0 lA EPA SAMPLE NO. _4---- -- -�' '.VOLATILE ORGANICS ANALYSIS DATA SHEET SBl-8 Lab Name.- MITKII4 CORPORATION Contract: -Lab Code: MITREM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID.: C1453-01B Sample -wt/vol: 6.5 (g/mL) G Lab File ID: V5F6826 Level: (low/med) MED- Date Received: -11/18/04 Moisture: not dec. . 8. Date Analyzed: 12/01/04 GC Column: DB-624 ID:- 0.25 (mm) Dilution Factor. 1.0 Soil Extract Volume: 5(ML) Soil Aliquot Volume: 10G.0(uL) CONCENTRATION UNITS: + CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 230 U 637-92-3--------Ethyl .tert-butyl ether 230 U 994-05-8--------tern-Amyl methyl ether 230 U 123-91-1--------1,4-Dioxane 4600 U .f� I FORM I VOA OIM03.0 1' 1A EPA .SAMPLE NO_ VOLATILE ORGANICS ANALYSIS DATA SHEET SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No..: SAS No SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16A. Sample wt/vol: 5.4 (g/mL) G Lab File ID: V2G5935 Level: (low/med) LOW Date Received: 11/19/04 !k Moisture: not dec. 6 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: (uL) CONCEWRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 i7 75-01-4---------Vinyl Chloride 5. U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 5 u 67-64-1---------Acetone 5 U 75-15-0---------Carbon Disulfide 5 II 75-09-2---------Methylene Chloride_ 7 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 II 78-93-3---------2-Butanone 5 II 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5----------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene ' 5 U 78-87-5---------1,2-Dichlorcpropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 II FORM I VOA 01EM03.0 ILA EPA SAMPLE .NO. VOLATILE ORGANICS 'ANALYSIS DATA SHEET SB10-2 Lab Name: 14ITKEK CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No- : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C145.3-16A Sample wt/vol: 5.4 (g/mL) G Lab File ID: V2G5935 Level: (low/med) IOW Date Received: 11/19/04 Moisture: not dec. 6 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (min) Dilution Factor: 1.0 :Soil Extract Volume: (mL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: .CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4---------Tetrachlor-oethene 4 J 591-78-6--------2-Hexanone 5 U 124--48-1--------Dibroanochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U - 108-90-7--------Chlorobenzene 5 U 630=20-6--------1,1,1,2-Tetra oroethane 5 U 100-41-4------- -Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1 1330-20-7-------Xylene (Total 5 U l 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropy nzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 3 J 106=43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6--------=1,2,4-Trimethylbenzene 6 135-98-8---------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,.3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--- - ----1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Tri orobenzene 5 U 60-29-7---------Ether 5 U FORM I VOA OLM03.0 i 1A EPA SAMPLE NO. VOLATILE-ORGANICS ANALYSIS DATA SHEET SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No- : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16A Sample wt/vol: 5.4 (g/mL) G Lab File ID: V2G5935 Level: (low/med) LOW Date Received: 11/19/04 Moisture: not dec. 6 Date Analyzed: 11/26./04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:_ (ML) Soil Aliquot Volume: (UL) CONCENTRATION UNITS: CAS NO- COMPOUND (ug/L or ug/Kg) UG/KG Q i 108-20-3--------Diisopropyl Ether 5 II. 637-92-3--------Ethyl tert-butyl ether 5 II .994-05-8--------tert-Amyl methyl ether 5 II 123-91-1--------1,4-Dioxane 98 II FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB10-2RE Lab-Name: -1i[ITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16ARE Sample wt/vol: 5.7 (g/mL) G Lab File ID: V2G5990 Level: (low/med) LOW Date Received: 11/19/04 Moisture: not dec. 6 Date Analyzed: 12/01/04. _: GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L. or ug/Kg) UG/KG Q 75-71-8--------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride_ 5 U 74-83-9---------Bromoanethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromet e 5 U 75-35-4---------1,1-Dichloroethene 5 U 67-64-1---------Acetone 8 75-15-0---------Carbon Disulfide 5 U 1 75-09-2---------Methylene Chloride 4 J 1 156-60-5--------trans-1,2-Dichloroet ene 51 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3-------- 1,1-Dichloroethane 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroet ene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydro uran 5 U 71-55=6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6--- -------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane_ 5 U FORM I VOA OLM03.0 !. lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB10-2RE Lab Name: MITKEK CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample.-ID: C1453-16ARE Sample wt/vol: ' 5.7 (g/mL) G Lab File ID: V2G5990 Level: (low/med) IOW Date Received: 11/19/04 Moisture: not dec. 6. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume -(UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 121-18-4--------.-Tetrachloroethene 4 J 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane - 5 U 106-93-4----=- 1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 II 95-47-6---------o-Xylene 5 II 1330-20-7-------Xylene (Total 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane� 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3 -5-Trimethylbenzene 1 J 106-43-4--------4-Chlorotoluene 5 U 98-06-6---= ----tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene . 2 J 135-98-8--------sec-Butylbenzene _ 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene_ 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1----------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U_ 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Tric orobenzene 5 U 60-29-7---------Ether 5 U FORM I VOA O1,M03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB10-2RE Lab Name: MITKEK CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16ARE Sample wt/vol: 5.7 (g/mL) G Lab File ID: V2G5990 Level: (low/med) LOW Date Received: 11/19/04 Moisture: not dec. 6 Date Analyzed: 12/01/04 GC Column.: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume:. J(tit) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or.ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 93 U FORM I VOA 01EM03.0 ) 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEEP i SB3-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12A Sample wt/vol: - 6.7 (g/mL) G 'Lab File ID: . V2G5933 Level: (low/med) LOW Date Received: 11/18/04 Moisture: not dec. 9 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume:. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 4 U 74--87-3-------- -Chloromethane . - 4 U 75-01-4---------Vinyl Chloride 4 U 74-83-9---------Bromomethane 4 U 75-00-3---------Chloroethane 4 U 75-69-4------- Trichlorofluoromethane 1 J 75-35-4---------1,1-Dichloroethene 4 U 67-64-1---------Acetone 94 75-15-0---------Carbon Disulfide 4 U 75-09-2---------Methylene Chloride 7 156-60-5--------trans-1,2-Dichloroethene 4 U 1634-04-4-------Methyl tert-butyl ether 4 U 75-34-3---------1,1-Dichloroethane 4 U 78-93-3---------2-Butanone. 22 156-59-2--------cis-1,2-Dichloroethene 4 U 590-20-7--------2,2-Dichloropropane 4 U 74-97-5---------Bromochloromethane. 4 U 67-66-3---------Chloroform 4 U 109-99-9--------Tetrahydrofuran 4 U 71-55-6---------1,1,1-Trichloroethane 4 U 563-58-6--------1,1-Dichloropropene 4 U 56-23-5---------Carbon Tetrachloride 4 U 107-06-2--------1,2-Dichloroethane 4 U 71-43-2----------Benzene 4 U 79-01-6---------Trichloroethene 2 J 78-87-5--------=-1,2-Dichloropropane 4 U 74-95-3---------Dibromomethane 4 U 75-27-4---------Bromodichloromethane 4 U 10061-01-5------cis-1,3-Dichloropropene 4 U 108-10-1--------4-Methyl-2-pentanone 4 U 108-88-3--------Toluene 7 10061-02-6------trans-1,3-Dichloropropene 4 U 79-00-5---------1, 1,2-Trichloroethane 4 U 142-28-9--------1,3-Dichloropropane 4 U FORM I VOA OLM03.0 lA EPA SAMPLE W. VOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6 Lab -Name. MITKEM CORPORATION Contract: Lab Code:. MITKEM Case No..: SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453712A Sample wt/Vol: 6.7 (g/mL) G Lab File ID: V2G5933 - Level: (low/med) LOW Date Received: 11/18/04 Moisture: not dec. 9 Date Analyzed: 11/26/04. GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8------- Dichlorodifluoromethane 4 U 74-87-3---------Chloromethane 4 U 75-01-4---------Vinyl Chloride 4 U 74-83-9---------Brcmomethane 4 U 75-00-3---------Chloroethane 4 U 75-69-4---------Trichlorofluoromethane 1 J 75-35-4---------1,1-Dichloroethene 4 U 67-64-1---------Acetone 94 75-15-0---------Carbon Disulfide 4 U 75-09-2---------Methylene Chloride 7 156-60-5--------trans-1,2-Dichloroethene 4 U 1634-04-4-------Methyl tert-butyl ether 4 U 75-34-3---------1,1-Dichloroethene 4 U 78-93-3---------2-Butanone 22 156-59-2---------cis-1,2-Dichloroethene 4 U 590-20-7--------2,2-Dichloropropane 4 U 74-97-5---------Bromochloromethane 4 U 67-66-3---------Chloroform 4 U 109-99-9--------Tetrahydrofuran 4 U 71-55-6---------1,.1,1-Trichloroethane 4 U 563-58-6--------1,1-Dichloropropene 4 U 56-23-5---------Carbon Tetrachloride 4 U 107-06-2--------1,2-Dichloroethene 4 U 71-43-2---------Benzene 4 U 79-01-6---------Trichloroethene 2 J 78-87-5---------1,2-Dichloropropane_ 4 U 74-95-3-------=-Dibromomethane. 4 U 75-27-4---------Bromodichloromethane 4 U 10061-01-5------cis-1,3-Dichloropropene 4 U 108-10-1--------4-Methyl-2-pentanone 4 U 108-88-3--------Toluene 7 10061-02-6------trans-1,3-Dichloropropene 4 U 79-00-5---------1,1,2-Trichloroethane 4 U 142-2.8-9--------1,3-Dichloropropane 4 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6 Lab Name: MITIUiZI CORPORATION Contract: Lab Code: MITICEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-'12A Sample wt/vol: . 6.7 (g/mL) G Lab File ID: V2G5933 -Level: (low/med) LOW Date Received: 11/18/64 i Moisture: not dec. 9 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract- Volume: (ML) Soil Aliquot Volume: JUL,) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 34 591-78-6--------2-Hexanone . 4 U 124-48-1--------Dibromochlaromethane 4 U 106-93-4---------1,2-Dibromoethane 4 U 108-90-7--------Chlorobenzene 4 U 630-20-6--------1 1 1 2-Tetrachloroethane 4 U 100-41-4--------Ethylbenzene 4 U ----------------m,p-Xylene 240 -47-6---------o-Xylene 62 1330-20-7-------Xylene (Total 300 100-42-5--------Styrene 4 U 75-25-2---------Bromoform 4 U 98-82-8---------Isopropyl.benzene 15 79-34-5---------1,1,2,2-Tetrachloroethane 4 U 108-86-1--------Bromobenzene 4 U 96-18-4---------1,2,3-Trichloropropane 4 U 103-65-1--------n-Propylbenzene 4 U 95-49-8---------2-Chlorotoluene 4 U 108-67-8--------1,3,5-Trimethy ene 1200 E 106-43-4--------4-Chlorotoluene . 4 U 98-06-6---------tert-Butylbenzene 4 U 95-63-6---------1,2,4-Trimethylbenzene 1100 E 135-98-8--------sec-Butylbenzene 23 99-87-6---------4-Isopropyltoluene 160 541-73-1--------1,3-Dichlorobenzene 4 U 106-46-7---------1,4-Dichlorobenzene 4 U 104-51-8--------n-Butylbenzene 4 U 95-50-1---------1,2-Dichlorobenzene_ 4 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 4 U 120-82-1--------1,2,4-Trichlorobenzene ___ 4 U 87-68-3---------Hexachlorobutadiene 4 U 91-20-3---------Naphthalene 22 87-61-6---------1,2,3-Trichlorobenzene 4 U 60-29-7---- :- -Ether 4 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET. SB3-6 Lab Name: MITIM4 CORPORATION Contract: Lab Code: MITKEK Case No. : SAS No. : SDG No. : :MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12A Sample wt/vol:- 6.7 (g/mL) G Lab File ID: V2G5933 Level: (low/med) LOW Date Received: 11/18/04 Moisture: not,dec. 9 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution.Factor: 1.0 Soil Extract. Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 4 U 637-92-3--------Ethyl tert-butyl ether 4 U 994-05-8--------tert-Amyl methyl ether 4 U 123-91-1--------1,4-Dioxarie 82 U 1 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOI TILE ORGANICS ANALYSIS DATA .SHEET V SB3-6 Lab .Name: MITKEM. CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12B Sample wt/vol: S.4 (g/mL) G Lab File ID:. V5F6827 Level: (low/med) MEN Date Received: 11118/04 %. Moisture: not dec. 9 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 {mm) Dilution Factor: 1.0 Soil Extract Volume: 5.(mL) Soil Aliquot Volume: 1.00.0(uL) CONC NT ATION UNITS.: CAS NO. COMPOUND (ug/L or ug/Kg) UG/IGG Q 75-71-8---------Dichloroc3ifluoromethane 280 U 74-87-3---------Chloromethane 280 U 75-01-4-----_---Vinyl Chloride 280 U 74-83-9---------Bromomethane 280 U 75-00-3---------Chloroethane 280 U 75-69-4---------Trichlorofluoromethane 280 U 75-35-4---------1,1-Dichloroethene 280 U 67-64-1---------Acetone _ 280 U 75-15-0---------Carbon Disulfide - 280 U 75-09-2---------Methylene -Chloride__'_ 240 J 156-60-5--------trans-1,2-Dichlor6e ne _ 280 U 1634-04-4-------Methyl tert-butyl .ether 280 U 75-34-3---------1,1-Dichloroethane. 280 U 78-93-3------- 2-Butanone 280 U 156-59-2--------cis-1,2-Dichloroethene 280 U 590-20-7--------2,2-Dichloropropane 280 U 74-97-5---------Bromochloromethane 280 U 67-66-3---------Chloroform 280 U 109-99-9--------Tetrahydrofuran 280 U 71-55-6---------1,1,1-Trichloroethane 280 U 563-58-6--------1,1-Dichloropropene 280 U 56-23-5---------Carbon Tetrachloride 280 U 101-06-2--------1,2-Dichloroethane 280 U 71-43-2---------Benzene 280 U 79-01-6---------Trichloroethene 280 U 78-87-5---------1,2-Dichloropropane 280 U 74-95-3---------Dibromomethane .280 U 75-27-4---------Bromodichloromethane 280 U 10061-01-5------cis-1,3-Dichloropropene 280 U 108-10-1--------4-Methyl-2-pentanone 280 U 108-88-3--------Toluene 280 U 10061-02-6------trans-1,3-Dichloropropene 280 U 79-00-5---------1,1,2-Trichloroethane 280 U 142-28-9--------1,3-Dichloropropane 280 U FORM I VOA OLM03 .0 lA EPA SAMPLE NO. VOLATILE. ORGANICS ANALYSIS DATA .SHEET SB3-6 Lab Name: MITKE24 CORPORATION Contract-. Lab Code: .MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453=12B Sample wt/vol: 5.4 (g/mL) G Lab File ID: V5F6827 Level: (low/vied) MED Date Received: 11/1$/04 Moisture: not dec. 9 Date Analyzed:: 12/01/04 GC Column: DB-624 ID: 0.25. (mvi) Dilution Factor: 1.0 Soil Extract Volume: 5(ML) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 280 U 591-78-6--------2-Hexanone 280 U 124-48-1--------Dibromochlorome a 280 U 106-93-4--------1,2-Dibromoethane 280 U 108-90-7--------Chlorobenzene 280 U 630-20-6--------1,1,1,2-Tetrachloroet a 280 U 100-41-4--------Ethylbenzene 280 U ----------------m,p-Xylene 980 95-47-6---------o-Xylene 290 1330-20.-7-------Xylene (Total) 1300 100-42-5--------Styrene 280 U 75-25-2---------Bromoform 280 U 98-82-.8---------Isopropy nzene i70 J 79-34-5-------- 1,1,2,2-Tetrachlor0ethane 280 U. 108-86-1-----=--Bromobenzene 280 U 96-18-4---------1,2,3-Trichloropropane 280 U 103-65-1--------n-Propylbenzene 280 U 95-49-8---------2-Chlorotoluene 280 U 108-67-8--------1,3,5-Trimethylbenzene 56000 E 106-43-4--------4-Chlorotoluene 280 U 98-06-76---------tert-Butylbenzene 2800 95-63-6---------1,2,4-Trimethylbenzene 62000 E 135-98-8--------sec-Butylbenzene 1800 99-87-6---------4-Isopropyltoluene- 16000 E 541-73-1--------1,3-Dichlorobenzene 110 J 106-46-7--------1,4-Dichlorobenzene 190 J 104-51-8--------n-Butylbenzene 280 U 95-50-1---------1,2-Dichlorobenzene 280 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 280 U 120-82-1--------1,2,4-Trichlorobenzene 280 U 87-68-3---------Hexachlorobutadiene 280 U 91-20-3---------Naphthalene 2700 87-61-6---------1,2,3-Tric oro nzene 280 U 60-29-7---------Ether 280 U FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA .SHEET SB3-6 Lab Name: MITKEm CORPORATION Contract: Lab Code.: MincEm ' Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12B f Sample wt/vol: 5.4 (g/mL) .G Lab File ID: V5F6827 Level: (low/med) MED Date Received: 11/18/04 g Moisture: hot. dec. 9 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q. 108-20-3--------Diisopropyl Ether 280 U 637-92-3--------Ethyl tert-butyl ether 280 U 994=05-8--------tert-Amyl methyl ether 280 U 123=91-1--------1,4-Dioxane 5600. 0 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SFR':ET SB3-6DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12BDL Sample wt/vol: 5.4 (g/mL) G Lab- File ID: = V5F6830 Level: (lbw/med) MED - Date Received: 11/18/04 k Moisture: not.dec. 9 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 20.0 Soil Extract volume: 5(ML) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane . 5600 U 74-87-3---------Chloromethane 5600 U 75-01-4---------Vinyl Chloride 5600 U 74-83-9---------Branomethane 5600 U 75-00-3---------Chloroethane 5600 U 75-69-4---------Trichlorofluoromethane5600 U 75-35-4-=-------1,1-Dichloroethene 5600 U 67-64-1---------Acetone 5600 U 75-15-0---------Carbon Disulfide 5600 U 75-09-21---------Methylene Chloride 5600 U 156-60-5-:------trans-1,2-Dichloroe ene 5600 U 1634-04-4-------Methyl tert-butyl ether 5600 U 75-34-3----------1,1-Dichloroethane 5600 U 78-93-3---------2-Butanone 5600 U 156-59-2--------cis-1,2-Dichloroe ene 5600 U 590-20-7--------2,2-Dichloropropane _ 5600 U 74-97-5---------Bromochloromethane 5600 U 67-66-3----------Chloroform -5600 U 109-99-9--------Tetrahydro uran 5600 U 71-55-6---------1,1,1-Trichloroethane 5600 U 563-58-6--------1,1-Dichloropropene 5600 U 56-23-5---------Carbon Tetrachloride 5600 U 107-06-2--------1,2-Dichloroethane 5600 U 71-43-2---------Benzene 5600 U 79-01-6---------Trichloroet ene 5600 U 78-87-5---------1,2-Dichloropropane 5600 U 74-95-3---------Di.bromomethane 5600 U 75-27-4-------- Bromodichloromethane 5600 U 10061-01-5------cis-1,3-Dichloropropene 5600 U 108-10-1--------4-Methyl-2-pentanone 5600 U 108-88-3--------Toluene 5600 U 10061-02-6------trans-1,3-Dichloropropene 5600 U 79-00-5---------1,1,2-Trichloroethane_ 5600 U 142-28-9--------1,3-Dichloropropane 56001U FORM I VOA OLM03 .0 l IA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6DL Lab Name: MITKEM CORPORATION Contract: j Lab Code: MITKEM Case No. : SAS No. SDG No. : MC1453 I Matrix: (soil/water) SOIL Lab Sample ID: C1453-12BDL Sample wt/vol: 5.4 (g/mL) G Lab File ID: V5F6830 I - Level: (low/med) MED Date.Received: - 11/18/04 g Moisture:' not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0:25 .(mm). Dilution Factor: 20.0 Soil Extract Volume:- 5(mL) Soil Aliquot Volume. 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4' 127-18-4--------Tetrachloroethene 5600. U 591-78-6---------2-Hexanone 5600: U 124-48-1--------Dibromochlorome a 5600 U 106-93-4--------1,2=Dibromoethane 5600 U 108-90-7---- Chlorobenzene 5600 U 630-20-6-----7--1,1,1,2-Tetrac oroethane 5600 U 100-41-4--------Ethylbenzene 5600 U ----------------m,p-Xylene 5600 U 95-47-6---------o-Xylene 5600 U 1330-20-7-------Xylene (Total) 5600 U 100-42-5--------Styrene 5600 U 75-25-2---------Bromoform 5600 U 98=82-8---------Isopropy zene 5600 U 79=34-5-----.----1,1,2,2-Tetrachloroethane 5600 U 108-86-1--------Bromobenzene 5600 U 96-18-4---------1,2,3-Trichloropropane 5600 U 103-65-1--------n-Propylbenzene 5600 U 95-49-8---------2-Chlorotoluene 5600 U 108-67-8------ 1,3,5-Trimethylbenzene 84000 D 106-43-4--------4-Chlarotoluene 5600 U 98-06-6---------tert-Butylbenzene 2500 DJ 95-63-6---------1,2,4-Trimethylbenzene 120000 D 135-98-8--------sec-Butylbenzene 5600 U 99-87-6---------4-Isopropyltoluene 14000 D 541-73-1--------1,3-Dichlorobenzene 5600 U 106-46-7--------1,4-Dichlorobenzene 5600 U 104-51-8--------n-Butylbenzene . 5600 U 95-50-1---------1,2-Dichlorobenzene 5600 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5600 U 120-82-1--------1,2,4-Trichlorobenzene 5600 U 87-68-3---------Hexachlorobutadiene 5600 U 91-20-3---------Naphthalene 4200 DJ 87-61-6---------1,2,3-Tri oro zene 5600 U 60-29-7---------Ether 5600 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6DL Lab Name: MITIM4 CORPORATION Contract: Lab Code: MITKER Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) .SOIL Lab Sample ID: C1453-12BDL Sample wt/vol-:. .5.4 (g/cnL) G Lab File ID: - V5F6830 Level: (low/med) MID Date Received: 11/18/04 g Moisture: n -t- dec.. 9 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 20.0 Soil Extract.Volume: 5(mL) Soil Aliquot.Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-.3---- -----Diisopropyl Ether 5600 U 637-92-3--- ----Ethyl tert-butyl ether 5600 U 994-05-8---------tert-Amyl methyl ether 5600 U 123-91-1--------1,4-Di:oxane 110000 U FORM I VOA OLM03.0 \ lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET ! SB4-14 Lab Name: MITKEM CORPORATION Contract: r Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 i Matrix: (soil/water)-.SOIL Lab Sample ID: C1453=14A Sample wt/vol: 5.2 (g/mL) G Lab File ID: V2G5989 Level:. (low/med) LOW Date Received: 11/19/04 Moisture: not dec. 3 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (rpm) Dilution Factor: 1.0 -Soil Extract. Volume: (ML) Soil Aliquot Volume: _ :( ,) CONCENTRATION UNITS: CAS NO. COMPOUND .(ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane . 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 5 U 74-83-9----------Bromomethane 5 U 75-00-3---------Chloroethane. 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 5 U 67-64-1---------Acetone 12 75-15-0---------Carbon Disulfide 5 U 75-09-2----------Methylene Chloride 6 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether. 5 U 75-34-3---------1,1-Dichloroethene 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------.cis-1,2-Dichloroethene 5 U 590=20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109=99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichioroethene 5 U 78-87-5----------1,2-Dichloropropane 5 U 74-95-3-------- Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 .0 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U FORM I VOA OLM03.0 lA EPA SAMPLE No, VOLATILE ORGANICS ANALYSIS DATA SHEET SB4-14 Lab Name: 14ITKENI CORPORATION. Contracts _ Lab Code: MITKEM Case No. . SAS No. . SDG No. .. MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-14A Sample wt/vol: 5.'2 (g/mL) G Lab File ID: V205989 Level: (low/med) IOW Date Received: 11/19/04 % Moisture: not dec. 3 Date Analyzed:. 12/01/04 GC Column: DB-624 ID: 0.25 (min) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 10 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromet a 5. 0 106-93-4---------1,2-Dibromoethane 5 U 108-90=7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 1GO-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 1 J 95-47-6---------o-Xylene 5 U \ 1330-20=7-------Xylene (Total) 1 J 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5. 0 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U .108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Triz ethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isoprcpyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Di.bromo-3-chlorcpropane 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U FORM I VOA 0IM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB4-14 Lab Name: . MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-14A Sample wt/vol: . . 5.2 (g/mL) G Lab File ID: V2G5989 Level: (low/med) LOW Date Received: 11/19/04 Moisture: not dec. 3 Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor:. 1.0 Soil Extract-Volume: (ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether _ _ 5 U -994-05-8- ------tert-Amyl methyl ether 5 U 123-9.1-1--------1,4-Dioxane 99 U FORM I VOA OLM03.0 lA. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2 Lab Name: MITKEM CORPORATION Contract Lab Code: MITKEM Case No. : SAS No. : SDG No.. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-06A Sample wt/vol: 4.3 (g/mL) G Lab File ID: V2G5936 - Level: -(low/med) LOW Date Received: 11/18/04 Moisture: not dec.. 8 Date Analyzed: 11/26/04 GC Colum: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: - uw CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane . 6 U 74-87-3---------Chloronethane 6 U 75-01-4---------Vinyl Chloride 6 U 74-83-9------ Bromomethane 6 U 75-00-3---------Chloroethane 6 U 75-69-4---------Trichlorofluoromethane 3 J 75-35-4---------1,1-Dichloroethene 6 U 67-64-1---------Acetone 14 75-15-0---------Carbon Disulfide 6 U 75-09-2---------Methylene Chloride 10 156-60-5--------trans-1,2-Dichloroethene 6 U 1634-04-4-------Methyl tert-butyl ether 6 U 75-34-3---------1,1-Dichloroethane 6 U 78-93-3---------2-Butanone 6 U 156-59=2--------cis-1,2-Dichloroethene 6 U 590-20-7--------2,2-Dichloropropane 6 U 74-97-5---------Bromochloromethane 6 U 67-66-3---------Chloroform 6 U 109-99-9--------Tetrahydrofuran 6 U 71-55-6---------1,1,1-Trichloroethane 6 U 563-58-6--------1,1-Dichloropropene 6 U 56-23-5---------Carbon Tetrachloride 6 U 107-06-2--------1,2-Dichloroethene 6 U 71-43-2---------Benzene 6 U 79-01-6---------Trichloroethene 6 U 78-87-5---------1,2-Dichloropropane 6 U 74-95-3---------Dibromomethane 6 U 75-27-4-=-------Bromodichloromethane 6 U 10061-01-5------cis-1,3-Dichloropropene 6 U 108-10-1--------4-Methyl-2-pentanone 6 U 108-88-3--------Toluene 6 U 10061-02-6-------trans-1,3-Dichloropropene 6 U 79-00-5---------1,1,2-Trichloroethane 6 U 142-28-9--------1,3-Dichloropropane 6 U FORM I VOA OLM03.0 / 1A EPA SAMPLE NO. ! VOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2 Lab Name.: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : .MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-06A Sample wt/vol: 4.3 (g/mL) G Lab File ID: V2G5936 Lever: (low/med) LOW Date Received: 11/18/04 Moisture:. not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil .Aliquot. Volume: —JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4------- Tetrachloroethene 25 591-78-6--------2-Hexanone 6 U 124-48-1--------Dibromochloromethane 6 U 106-93-4---------1,2-Dibromoethane 6 U 108-90-7--------Chlorobenzene 6 U 630-20-6--------1,1,1,2-Tetrachloroethane 6 U 100-41-4------- Ethylbenzene. 6 U ----------------m,p-Xylene 3 J 95-47-6---------o-Xylene 6 U 1330-20-7-------Xylene (Total) 3 J 100-42-5--------styrene_ 6 U 75-25-2---------Bromoform 6 U 98-82-8---------Isopropylbenzene 6 U 79-34-5---------1,1,2,2-Tetrachloroethane 6 U 108-86-1--------Bromobenzene 6 U 96-18-4---------1,2,3-Trichloropropane 6 U 103-65-1--------n-Propylbenzene 6 U 95-49-8---------2-Chlorotoluene 6 U 108-67-8--------1,3,5-Trimethylbenzene 6 U 106-43-4--------4-Chlorotoluene 6 U 98-06-6---------tert-Butylbenzene 6 U 95-63-6---------1,2,4-Trimethylbenzene 2 J 135-98-8--------sec-Butylbenzene_ 6 U 99-87 6---------4-Iscpropyltoluene 6 U 541-73=1--------1,3-Dichlorobenzene _ 6 U 106-46-7---------1,4-Dichlorobenzene 6 U 104-51-8--------n-Butylbenzene 6 U 95-50-1---------1,2-Dichlorobenzene 6 U 96-12-8---------1,2-Dibromo-3-chlorcpropane_ 6 U 120-82-1--------1,2,4-Trichlorobenzene 6 U 87-68-3----------Hexachlorobutad.iene 6 U 91-20-3---------Naphthalene 6 U 87-61-6---=-----1,2,3-Trichlorobenzene 6 U 60-29-7---------Ether 6 U FORM I VOA 01EM03.0 lA EPA SAMPLE 140. VOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. :. SAS No. : SDG No. : MC1453 -� Matrix: (soil/water) SOIL Lab Sample ID: C1453-06A Sample wt/vol: . 4.3 (g/mL) G Lab File ID: V2G5936 Level: (low/med) IOW Date Received: 11/18/04 Moisture: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (min) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: _ -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 6 U 637-92-3--------Ethyl tert-butyl ether 6 U 994-05-8--------tert-Amyl methyl ether 6 U . 123-91-1--------1',4-Dioxane 130 U FORM I VOA OLM03.0 / lA EPA- SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 I Matrix:. (soil/water) SOIL Lab Sample ID: C1453-06AMS Sample wt/vol: 5.1 (g/mL) G Lab File ID: V2G5937 Level: (low/coed) LOW Date Received: 11/18/04 o Moisture: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract. Volume: (ML) Soil Aliquot Volume: _WL). CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 45 7.4-87-3---------Chloromethane 49 75-01-4---------Vinyl Chloride 45 74-83-9---------Bromomethane 50 75-00-3---------Chloroethane 49 75-69-4---------Trichlorofluoromethane 60 75-35-4---------1,1-Dichloroethene__ 50 67-64-1---------Acetone 88 75-15-0---------Carbon Disulfide 32 75-09-2------=--Methylene Chloride 48 156-60-5--------trans-1,2 Dichloroethene 45 1634-04-4-------Methyl tert-butyl ether 110 75-34=3---------1,1-Dichloroethane 48 78-93-3---------2-Butanone 72 156-59-2--------cis-1,2-Di oroethene 51 590-20-7--------2,2-Dichloropropane 50 74-97-5---------Bromochloromethane 50 67-66-3----------Chloroform 45 109-99-9--------Tetrahydrofuran 85 71-55-6---------1,1,1-Trichloroethane 50 563-58-6--------1,1-Dichloropropene 47 56-23-5---------Carbon Tetrachloride 49 107-06-2--------1,2-Dichloroethane 52 71-43-2---------Benzene 49 79-01-6---------Trichloroethene 50 78-87-5---------1,2-Dichloropropane 50 74-95-3---------Dibromomethane 52 75-27-4---------Bromodichlorcmethane 51 10061-01-5------cis-1,3-Dichloropropene 52 108-10-1--------4-Methyl-2-pentanone 64 108-88-3--------Toluene _ 51 10061-02-6------trans-1,3=Dichloropropene 53 79-00-5---------1,1,2-Trichloroethane 52 142-28-9--------1,3-Dichloropropane _� 54 FORM I VOA OLM03.0 1 lA EPA SAMPLE NO. VOLATILE ORGANICS,ANALYSIS DATA SHEET SB5-2MS Lab Name: MIZK! CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix:. (soil/water) SOIL Lab Sample ID: C1453-06AMS Sample wt/vol 5.1 (g/mL) G Lab File ID: V2G5937 Level: (low/med) LOW Date Received: :11/18/04 t Moisture: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (man) Dilution. Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/YG Q 127-18-4--------Tetrachloroethene 78 591-78-6------ 2-Hexanone 72 124-48-1=-------Dibromochloromet a 53 106-93-4--------1,2=Dibromoethane ' 55 108-90-7--------Chloroberizene 5o 630-20-6--------1,1,1,2-Tetrachloroethane 51 100-41-4--------Ethylbenzene 53 ----------------m,p-Xylene. 110 95-47-6---------o-Xylene 56 1330-20-7-------Xylene (Total) 160 100-42-5--------Styrene 54 . 75-25-2---------Bromofonn 56 98-82-8---------Isopropy zene 52 79-34-5---------1,1,2,2-Tetrachloroethane 60 108-86-1--------Bromobenzene 55 96-18-4---------1,2,3-Trichloropropane 61 103-65-1--------n-Propylbenzene 51 95-49-8---------2-Chlorotoluene 52 108-67-8--------1,3,5-Trimethyl zene 54 106-43-4--------4-Chlorotoluene 53 98-06-6---------tert-Butylbenzene 51 95-63-6---------1,2,4-Trimethylbenzene 55 135-98-8--------sec-Butylbenzene 49 99-87-6---------4-Isopropyltoluene 48 541-73-1--------1,3-Dichlorobenzene 50 106-46-7--------1,4-Dichlorobenzene 48 164-51-8--------n-Butylbenzene 45 95-50-1---------1,2-Dichlorobenzene 53 96-12-8----------1,2-Dibromo-3-chloropropane_ 65 120-82-1--------1,2,4-Trichlorobenzene 44 87-68-3---------Hexachlorobutadiene 26 91-20-3---------Naphthalene 56 87-61-6---------1,2,3-Trichlorobenzene 41 60-29-7---------Ether 57 FORM I VOA OLM03.0 ) 1A EPA SAMPLE NO. VOLATILE .ORGANICS ANALYSIS DATA SHEET SB5-2MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.-: MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-06AMS Sample wt/vol:. 5.1 (g/mL) G .Lab File ID: ' V2G5937 Level: (low/med) LOW Date Received: 11/18/04 Moistures not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uLr) CONCENTRATION UNITS:. CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3-=------Diisopropyl Ether_ 61 637-92-3--------Ethyl tert-butyl ether 63 994-05-8--------tert-Amyl methyl .ether _ 70 123-91-1--------1,4-Dioxane 1200 FORM I VOA OLM03:0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA. SHEET SB5-2MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM . Case No. : SAS No. : SDG No. : MC1453 ) Matrix: (soil/water) SOIL Lab Sample -ID: C1453-06AMSD Sample wt/vol: - 3.9 (g/mL) G Lab File ID: V2G5938 Level: (low/med) LOW Date Received: 11/18/04 o Moisture: not dec. 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 . (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) uG/KG Q - 75-71-8---------Dichlorodifluoromethane 59 74-87-3---------Chloromethane 56 75-01-4---------Vinyl Chloride 58 74-83-9---------Bromomethane 62 75-00-3---------Chloroethane 60 75-69-4--.-------Trichlorofluoromethane 58 75-35-4---------1,1-Dichloroethene 62 67-64-1---------Acetone 130 75-15-0---------Carbon Disulfide 37 75-09-2---------Methylene Chloride 60 156-60-5--------trans-1,2-Dichloroethene 60 J 1634-04-4-------Methyl tert-butyl ether 15.0 75-34-3------- 1,1-Dichloroethene 65 78-93-3---------2-Butanone 100 156-59-2--------cis-1,2-Dichloroethene 69. 590-20-7--------2,2-Dichloropropane 65 74-97-5---------Bromochloromethane 67 67-66-3----------Chloroform 59 10.9-99-9--------Tetrahydrofuran 110 71-55-6---------l,l,l-Trichloroethane 65 563-58-6--------1,1-Dichloroprcpene 63 56-23-5---------Carbon Tetrachloride 63 107-06-2--------1,2-Dichloroethene 70 71-43-2---------Benzene 67 79-01-6---------Trichloroethene 110 78-87-5---------1,2-Dichloropropane 66 74-95-3---------Dibromomethane 68 75-27-4---------Bromodichloromethane 66 10061-01-5------cis-1,3-Dichloropropene 69 108-10-1--------4-Methyl-2-pentanone 86 108-88-3--------Toluene 67 10061-02-6------trans-1,3-Dichloroprcpene 69 79-00-5----------1,1,2-Trichloroethane 66 142-28-9--------1,3-Dichloropropane 74 FORM I VOA OLM03.0 ) lA EPA SAMPLE W. VOLATILE ORGANICS ANALYSIS DAM SHEET SB5-2MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS. No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-06AMSD. Sample wt/vol: 3.9 (g/mL) G Lab File ID: V2G5938 j Level: (low/med) LOW Date Received: 11/18/04 i %-..Moisture.: not dec. . 8 Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: { ) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q i 127-18-4--------Tetrachloroethene_ 140 591-78-6--------2-Hexanone 110 124-48-1------- Dibronx>chloromethane 72 106-93-4--------1,2-Dibromoethane 76 108-90-7--------Chlorobenzene T 67 630-20-6--------1,1,1,2-Tetrachloroeth nE 69 100-41-4--------Euhylbenzene----------------m,p-Xylene 1 72 72 95-47-6-------=-o-Xylene 75 1330-20-7-------Xylene (Total 220 100-42-5--------Styrene 70 75-25-2---------Bromoform , 74 98-82-8---- - ----Isopropylbenzene 7 79-34-5---------1,1,2,2-Tetrachloroethane 7 108-86-1--------Bromobenzene 76 96-18-4---------1,2,3-Tr'ichl.oropropane 89 103-65-1--------n-Propylbenzene 73 95-49-8---------2-Chlorotoluene 73 108-67-8--------1,3,5-Trimethylbenzene 74 106-43-4--------4-Chlorotoluene 72 98-06-6---------tert-Butylbenzene 61 95-63-6---------1,2,4-Trimethylbenzene 75 135-98-8--------sec-Butylbenzene 67 99-87-6---------4-Isopropyltoluene 66 541-73-1--------1,3-Dichlorobenzene 66 106-46-7--------1,4-Dichlorobenzene 64 104-51-8--------n-Butylbenzene 61 95-50-1---------1,2-Dichlorobenzene 68 96-12-8---------1,2-Dibromo-3-chloropropane_ 90 120-82-1--------1,2,4-Trichlorobenzene 53 87-68-3---------Hexachlorobutadiene - 36 91-20-3---------Naphthalene 73 87-61-6---------1,2,3-Trichlorobenzene 53 60-29-7---------Ether 76 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS.DATA SHEET SB5-2MSD Lab Name: MITKEM CORPORATION Contract: 11 Lab Code: :MITKEM Case No. : SAS No. : SDG-No. : MC1453 J Matrix: (soil/crater) SOIL Lab Sample ID: C1453-06AMSD Sample wt/vol: 3.9 (g/mL) G Lab File. IDz V2G5938 Level: .(low/med) LOW Date Received: 11/18/04 Moisture: not dec. 8 . Date Analyzed: 11/26/04 -- GC. Column: , DB-624. . ID_: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: ,(ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS. NO. CONFOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 80 637-92-3--------Ethyl tert-butyl ether 85 994-05-8--------tert-Amyl methyl.ether 92 123-91-1--------1,4-Dioxane 1600 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS. ANALYSIS DATA SHEET SB8-2 Lab Name: MITICEM CORPORATION Contract: F Lab Code: MITKEM Case No. : SAS No. : SDG No.: MC1453 S' l� Matrix: (soil/water) SOIL Lab- Sample ID: C1453-10A Sample wt/vol: 7.9 (g/mL) G Lab File ID: V2G5932 Level: (low/med) LOW Date Received: 11/18/04 . t Moisture: not dec'. 13 Date Analyzed: 11/26/04, �t GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 T;. Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) IN CONCENTRATION UNITS:- CAS NO. COMPOUND, (ug/L or .ug/Kg) UG/KG Q r 75-71-8---------Dichlorodifluoromethane 4 U f. 74-87-3---------Chloromethane 4 U 75-01-4---------Vinyl Chloride _. 4 U 74-83-9---------Bromomethane 4 U 75-00-3---------Chloroethane 4 U r 75-69-4---------Trichlorofluoromethane 1 J 75-35-4---------1,1-Dichloroethene 4 U 67-64-1---------Acetone 6 75-15-0---------Carbon Disulfide __ _ 4 U 75-09-2---------Methylene Chloride 4 156-60-5--------trans-1,2-Dichloroethene 4 U 1634-04-4-------Methyl tert-butyl .ether 4 U 75-34-3---------1,1-Dichloroethane 4 U 78-93-3---------2-Butanone 4 U .. 156-59-2--------cis-1,2-Dichloroethene _ 4 U 590-20-7--------2,2-Dichloropropane 4 U 74-97-5---------Bromochloromethane 4 U 67-66-3---------Chloroform 4 U 109-99-9--------Tetrahydrofuran 4 U 71-55-6---------1,1,1-Trichloroethane 4 U 563-58-6--------1,1-Dichloropropene _ 4 U 56-23-5---------Carbon Tetrachloride 4 U 107-06-2--------1,.2-Dichloroethane 4 U 71-43=2---------Benzene 4 U 79-01-6---------Trichloroethene 4 U 78-87-5---------1,2-Dichloropropane 4 U 74-95-3---------Di.bromomethane 4 U 75-27-4---------Bromodichloromethane 4 U 10061-01-5------cis-1,3-Dichloropropene 4 U 108-10-1--------4-Methyl-2-pentanone 4 U 108-88-3--------Toluene 4 U 10061-02-6------trans-1,3-Dichloropropene 4 U 79-00-5---------1,1,2-Trichloroethane 4 U 142-28-9--------1,3-Dichloropropane 4 .0 FORM I VOA OLM03.0 IA EPA SAMPLE NO. VOI•ATI E ORGANICS ANALYSIS DATA SHEEP TRIP Lab Name: MITKEm CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix:-(Soil/water) SOIL Lab Sample ID:. C1453-08A Sample wt/vol:_ 5.0 (g/mL) G Lab File ID: V2G5986 Level: (low/[ned} LOW Date Received: 11/18/04 Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: --(uL-) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 17 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochlorome 5 U 106-93-4=-------1,2-Dibromoethane 5 :U 108-.90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5. 0 100=41-4--------Ethylbenzene '5 U ----------------m,p-Xylene 2 J 95=47-6---------o-Xylene . 5 U 1330--20-7-------Xylene (Total) 2 J 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropy ene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethy zene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5. U 104-51-8--------n-Butylbenzene 5 U 95-50-1----------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 ,U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-.20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Tric orobenzene 5 U 60-29-7---------Ether 5 U FORM I VOA 01,M03..0 / 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET' TRIP Lab Name: MITKEK CORPORATION Contract: .Lab Code:. MITKEM Case No. : SAS No- : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-08A Sample wt/vol.: 5.0 (g/mL) G Lab File ID: V2G5986 Level: (low/med) LOW Date Received: 11/18/04 $ Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: _(ML) Soil Aliquot Volume: ( ,) CONCENITRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 10.8-20-3--------Diisopropyl Ether .5 U 631-92-3--------Ethyl tert-butyl ether -5 U '994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 II t FORM I VOA 0LM03:0 lA -EPA SAMPLE NO: VOLATILE. ORGANICS ANALYSIS-DATA SHEET TRIP Lab Name:. MITIM4 CORPORATION Contract: Lab Code: MI Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-17A Sample wt/vol: 5:0 :(g/mL) G Lab File ID: V2G5987 Level: (low/med) LOW Date Received: 11/19/04 W Moisture: not -dec. Date Analyzed: 12/01/04 . GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) .UG/KG Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 5- 1-4---------Vinyl Chloride 5 U 74-83-9---------Bromomethane 5 U . 75-00-3---------Chloroethane -~ 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene _ _ 5 U 67-64-1---------Acetone 14 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 156-60-5--------trans-l;2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 78-93-3----------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-.97-5---------Bromochloromethane 5 U "67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6.--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2------ Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U 79-00-5---------1,1,2-Trichloroethane 5 U. 142-28-9--------1,3-Dichloropropane 5 U FORM I VOA 0IM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS 'DATA SHEET TRIP Lab Name: MITKE2I CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix:. (soil/water) SOIL Lab Sample ID: C1453-17A Sample wt/vol:. 5.0 (g/mL) G Lab File ID: V2G5987 Level: (low/med) IOW Date Received: 11/19/04 o Moisture: not dec. Date Analyzed: 12/01/04- GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: :1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 11 591-78-6--------2-Hexanone _ 5 u 124-48-1--------Dibromochloromet e 5 U 106-93-4------ 1,2-Dibromoethane- 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U -=--------------m,p-Xylene 1 J 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total 1 J 100-42-5-------=-Styrene 5 U 75-25-2----'-----Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5. U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene� 5 U 108-67-8--------1;3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3=Dichlorobenzene 51U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2;4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Trichlorobenzene. 5 U 60-29-7---------Ether 5 .0 FORM I VOA OLM03 A lA EPA SAMPLE NO.. VOLATILE ORGANICS.ANALYSIS DATA.SHEET TRIP Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-17A Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5987 Level: (low/med) LOW Date Received: 11/19/04 Moisture: .not dec. Date Analyzed: 12/0.1/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:_ (ML) Soil Aliquot Volume: {U,) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisbpropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA 0LM03.0 J lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2KLCS Lab Name: MITKEM CORPORATION Contract:. Lab Code: MITfM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15858 Sample wt/vol: .5_.0 (g/mL) G Lab File ID: V2G5926 Level: - (low/med) LOW Date Received: 11/18/04 Moisture: not dec. Date Analyzed: 11/26/04 i GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) IIG/KG Q 75-71-8---------Dichlorodifluoromethane 42 74-87-3---------Chloromethane 42 75-01-4---------Vinyl Chloride 44 74-83-9------ Bromomethane 45 75-00-3---------Chloroethane 44 75-69-4---------Trichlorofluoromethane 53 75-35-4---------1,1-Dichloroethene 46 67-64-1---------Acetone 64 75-15-0---------Carbon Disulfide. _ 46 75-09-2---------Methylene Chloride 35 156-60-5-------- trans-1,2-Dichloroethene 46 1634-04-4-------Methyl tert-butyl ether 99 -75-34-3---------1,1-Dichloroethane 46 78=93-3---------2-Butanone 58 156-59-2--------cis-1,2-Dichloroethene 48 590-20=7--------2,2-Dichloropropane 49 74_-97-5---------Bromochloromethane _ 44 67-66-3---------Chloroform 42 .109-99-9--------Tetrahydrofuran _ 70 71-55-6---------1,1,1-Trichloroethane 47 563-58-6--------1,1-Dichloropropee_ _ 47 56-23-5---------Carbon Tetrachloride 47 107-06-2--------1,2-Dichloroethane 46 71-43-2---------Benzene 47 '79-01-6---------Trichloroethene 47 18-87-5---------1,2-Dichloropropane 46 74-95-3---------Dibromomethane 46 75-27-4---------Bromodichloromethane 45 10061-01-5------cis-1,3-Dichloropropee 49 108-10-1--------4-Methyl-2-pentanone 55 108-88-3--------Toluene 49 10061-02-6-=--.--trans-1,3-Dichloropropee 5.0 79-00-5---------1,1,2-Trichloroethane 46 142-28-.9--------1,3-Dichloropropane 49 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2KLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No.. : SAS No. : SDG No MC145.3 ) Matrix: (soil/water) SOIL Lab Sample ID: LCS-15858 Sample wt/vol: . 5.0 (g/mL) G Lab File ID: V2G5926 Level: (low/med). IOW Date Received: 11/18/04 Moisture: not dec.. Date Analyzed: 11/26/.04 GC Column: DB-624 ID:- 0.25 (man) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 48 591-78-6--------2-Hexanone 66 124-48-1--------Dibromochloromethane 48 106-93-4--------1,2-Dibromoethane 50 108-90-_7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetra oroethane 46 100-41-4--------Euhylbenzene 53 ----------------m,p-Xylene 100 95-47-6---------o-Xylene 54 1330-20-7-------Xylene (Total) 160 1 100-42-5--------Styrene 52 75-25-2---------Bromoform 49 98-82-8---------Isopropylbenzene 56. 79-34-5---------1,1,2,2-Tetrachloroethane 50 108-86-1--------Bromobenzene 49 96-18-4---------1,2,3-Trichloroprcpane 52 103-65-1--------n-Propylbenzene 52 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 53 106-43-4--------4-Chlorotoluene 50 98-06-6-------- tert-Butylbenzene 53 95-63-6---------1,2,4-Trimethylbenzene 53 135-98-8--------sec-Butylbenzene 54, 99-87-6---.------4-Isopropyltoluene 52 541-73-1--------1,3-Dichlorobenzene 49 106-46-7--------1,4-Dichlorobenzene. 47 104-51-8--------n-Butylbenzene 55 95-50-1---------1,2-Dichlorobenzene 49 96-12-8---------1,2-Dibromo-3-chloropropane 52 120-82-1--------1,2,4-Trichlorobenzene 54 87-68-3---------Hexachlorobutadiene 50 91-20-3---------Naphthalene _ 58 87-61-6---------1,2,3-TrichloroBenzene 54 . 60-29-7---------Ether 50 FORM I VOA OLM03 .0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2KLCS Lab Name: MITICU4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: . (soil/water) SOIL Lab Sample ID: LCS-15858 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5926 Level: (low/med) LOW Date Received: 11/18/04 o Moisture: . not dec. Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl:.Ether 58 637-92-3--------Ethyl tert-butyl ether - 56 994-05-8--------tert-Amyl methyl ether 62 123-91-1--------1,4-Dioxane 960 FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA V2KLCSD Lab Name: HITICEM CORPORATION Contract: Lab Code:. MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15858 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V265925 Level: (low/med) LOW Date Received: 1; Moisture: not dec. Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.2.5 (min) Dilution Factor: .1.0 Soil Extract Volume: (ML) Soil Aliquot Volumev -{uL) CONCEIITRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluorcmethane 41 74-87-3---------Chloromthane 40 75-01-4---------Vinyl, Chloride 43 74-83-9=--------Bromomethane 44 75-00-3---------Chloroethane _ 43 75-69-4---------Trichlorofluoromethane 41 75-35-4---------1,1-Dichloroethene 45 67-64-1---------Acetone _ 52 75-15-0------ Di--Carbon sulfide 45 75-09-2---------Methylene Chloride 35 156-60-5--------trans-1,2-Dichloroethene 45 1634-04-4-------Methyl tert-butyl ether 92 75-34-3---------1,1-Dichloroethene 45 78-93-3---------2-Butanone 53 156-59-2--------cis-1,2-Dichloroethene 48 590-20-7--------2,2-Dichloropropane 49 74-97-5--=------Bromochloromethane 43 67-66-3---------Chloroform 41 109-99.-9--------Tetrahydrofuran 61 71-55-6---------1,1,1-Trichloroethane 46 563-58-6--------1,1-Dichloropropene 46 56-23-5---------Carbon Tetrachloride 45 107-06-2--------1,2-Dichloroethane 45 71-43-2---------Benzene 47 79-01-6---------Trichloroethene 46 78-87-5---------1,2-Dichloropropane 46 74-95-3---------Di.bromomethane 44 75-27-4---------Bromodichloromethane 45 10061-01-5------cis-1,3-Dichloropropene 48 108-10-1--------4-Methyl-2-pentanone 48 108-88-3--------Toluene 49 10061-02-6------trans-1,3-Dichloropropene 47 79-00-5---------1, 1,2-Trichloroethane 44 142-28-9--------1,3-Dichloropropane 49 FORM I VOA OLM03.0 l lA EPA SAMPLE No. VOLATILE ORGANICS ANALYSIS DATA SHEET V2KLCSD Lab Name: MITKEM- CORPORATION Contract: Lab Code: MITKEK Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15858 Sample wt/vol: 5.0 (g/mL) G Lab File ID: ' V2G5925 i Level: (low/med) LOW- Date Received: Moisture.: not dec. Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (inm) Dilution Factor: 1.0 Soil Extract Volume:. (ML) Soil Aliquot Volume: -(uL) i CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/xg) uG/xG Q 127-18-4--------Tetrachloroethene 49 591-78-6--------2-Hexanone 56 124-48-1--------Dibromochloromethane 47 106-93-4--------1,,2-Dibromoethane 47 108-90-7--------Chlorobenzene 48 630-20-6--------1,1A,1,2-Tetrachloroethane 4.7 100-41-4--------Ethylbenzene 53 ----------------m,p-Xylene 110 95-47-6---------o-Xylene 55 1330-20-7-------Xylene (Total) 160 100-42-5--------Styrene 53 75-25-2---------Bromoform 47 98-82-8----------Isoprcpylbenzene 56 79-34-5---------1,1,2,2-Tetrachloroethane 47 108-86-1--------Bromobenzene_ _ 49 96-18-4---------1,2,3-Trichloropropane 48 103-65-1--------n-Propylbenzene 51 95-49-8---------2-Chlorotoluene 51 108-67-8--------1,3,5-Trimethylbenzene 52 106-43-4--------4-Chlorotoluene 50 98-06-6---------tert-Butylbenzene 53 95-63-6---------1,2,4-Trimethylbenzene 53 135-98-8--------sec-Butylbenzene 54 99-87-6---------4-Isopropyltoluene 52 541-73-1--------1,3-Dichlorobenzene 49 106-46-7--------1,4-Dichlorobenzene 47 104-51-8--------n-Butylbenzene 55 95-50-1---------1,2-Dichlorobenzene 49 96-12-8---------1,2-Dibromo-3-chloropropane 46 120-82-1--------1,2,4-Trichlorobenzene 52 87-68-3---------Hexachlorobutadiene 49 91-20-3---------Naphthalene 53 87-61-6------ --- 1,2,3-Trichlorobenzene 51 60-29-7---------Ether 48 FORM I VOA OLM03:0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET: V2KLCSD _ Lab Name: MITKEM CORPORATION Contract: Lab Code: NITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15858 Sample wt/vol: . 5.0 (g/mL) G Lab File ID: V2G5925 Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (ten) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume:. -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 56 637-92-3--------Ethyl tert-butyl ether 54 994-05-8--------tert-Amyl methyl ether 57 123-91-1--------1,4-Dioxane 680 FORM I VOA OLM03.0 VOLATILE EPA SAMPLE NO. ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: V2SLCS Lab. Code: MITKEM Case No. : SAS No. : 4 SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5984 i Level: (low/med) LOW Date Received-: _ Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: .1.0 Soil Extract Volume: _(ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-.8---------Dichlorodifluoromethane 58 74-87-3---------Chloromethane 47 75-01-4---------Vinyl Chloride 48 74=83-9---------Bromomethane_ 46 75-00-3---------Chloroethane 47 75-69-4------- Trichlorofluoromethane 46 75-35-4---------1,1-Dichloroethene 46 67-64-1---------Acetone 67 75-15-0---------Carbon Disulfide 47 75-09-2---------Methylene Chloride 39 156-60-5--------trans-1,2-Dichloroethene 46 1634-04-4-------Methyl tert-butyl ether 94 75-34-3---=--- 1,1-Dichloroethane 45 78-93-3---------2-Butanone 64 156-59-2--------cis-1,2-Dichloroethene 48 590-20-7--------2,2-Dichloropropane 52 74-97-5------... Bromochloromethane. 45 67-66-3---------Chloroform 42 109-99-9--------Tetrahydrofuran 70 71-55-6---------1,1,1-Trichloroethane 48 563-58-6--------1,1-Dichloropropene 49 56-23-5---------Carbon Tetrachloride 49 107-06-2--------1,2-Dichloroethane 46 71-43-2---------Benzene 47 79-01-6-------- Trichloroethene 47 78-87-5----------1,2-Dichloropropane 45 74-95-3---------Dibromomethane 45 75-27-4---------Bromodichloromethane 45 10061-01-5------cis-1,3-Dichloropropene 48 108-10-1--------4-Methyl-2-pentanone_ 56 108-88-3--------Toluene 50 10061-02-6------trans-l,3-Dichloropropene 49 79-00-5---------1,1,2-Trichloroethane 45 142-28-9--------1,3-Dichloropropane_ 48 FORM I VOA 01-M03.0 lA EPA SAMPLE NO. 7� VOLATILE ORGANICS ANALYSIS. .DATA SHEET V2SLCS Lab Name: -MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5984. Level: (low/med) Low Date Received: o Moisture: not dec... . Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: lut) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 50 591-78-6--------2-Hexanone 69 124-48-1--------Dibromochloromethane 47 106-93-4--------1,2-Dibromoethane 49 108-90-7--------Chlorobenzene 48 630-20-6--------1;1,1,2-Tetra oroethane 47 100-41-4--------Ethylbenzene 54 ----------------m,p-Xylene 100 95-47-6---------o-Xylene 53 1330-20-7-------Xylene (Total) 160 100-42-5--------Styrene 53 75-25-2---------Bromoform 49 98-82-8---------Isopropylbenzene 57 79-34-5------- 1,1,2,2-Tetrachloroethane 47 108-86-1--------Bromobenzene 48 96-18-4---------1,2,3-Trichloroprcpane 49 103-65-1--------n-Propylbenzene _ 52 95-49-8---------2-Chlorotoluene 49 108-67-8--------1,3;5-Trimethy ene 52 106-43-4--------4-Chlorotoluerie 49 98-06-6---------tert-Butylbenzene 52 95-63-6----------1,2,4-Trimethylbenzene 52 135-98-8--------sec-Butylbenzene 52 99-87-6---------4-Isopropyltoluene 52 541-73-1--------1,3-Dichlorobenzene 48 106-46-7--------1,4-Dichlorobenzene 46 104-51-8--------n-Butylbenzene 54 95-50-1---------1,2-Dichlorobenzene 48 96-12-8---------1,2-Dibromo-3-chlorcprcpane_ 52 120-82-1--------1,2,4-Trichlorobenzene 52. 87=68-3---------Hexachlorobutadiene 50 91-20-3---------Naphthalene 56 87-61-6---------1,2,3-Tri oro zene 52 60-29-7---------Ether 50 FORM I VOA OLM03.0 i lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2SLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM _ Case No. : SAS No. : SDG No. : MC1453 r Matrix: (soil/water) SOIL Lab Sample ID: LCS-15905 Sample wt/vol: 5.0 (g/miL) G Lab File ID: V2G5984 Level: (low/med) LOW Date Received: $ Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ' ID: 0.25 (man) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 54 637-92-3--------Ethyl tert-butyl ether 53 994-05-8--------tert-Amyl methyl ether '58 123-91-1------ 1,4-Dioxane 1000 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2SLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5985 Level: (low/med) IOW Date Received: Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 67 74-87-3------=--Chloromethane . 48 75-01-4---------Vinyl Chloride f 48 74-83-9---------Bromomethane _ 47 75-00-3---------Chloroethane 47 75-69-4---------Trichlorofluoromethane 40 75-35-4---------1,1-Dichloroethene 47 67-64-1---------Acetone 57 75-15-0---------Carbon Disulfide 48 75-09-2----------Methylene Chloride 40 156-60-5--------trans-1,2-Dichloroethene 47 1634-04-4-------Methyl tert-butyl ether 95 .75-34-3---------1,1-Dichloroethane 45 78-93-3---------2-Butanone 54 156-59-2--------cis-1,2-Dichloroethene 49 590-20-7--------2,2-Dichloropropane 51 74-97-5---------Bromochloromethane 44 67-66-3---------Chloroform 42 109-99=9--------Tetrahydrofuran 67 71-55-6---------1,1,1-Trichloroethane 48 563-58-6--------1,1-Dichloropropene 48 56-23-5---------Carbon Tetrachloride 47 107-06-2--------1,2-Dichloroethane 45 71-43-2---------Benzene 47 79-01-6---------Trichloroethene 48 78-87-5---------1,2-Dichloropropane 45 74-95-3---------Dibromomethane 44 75-27-4---------Bromodichloromethane 44 10061-01=5------cis-1,3-Dichloropropene 48 108-10-1--------4-Methyl-2-pentanone 49 108-88-3--------Toluene 49 10061-02-6------trans-1,3-Dichloropropene 44 79-00-5---------1,1,2-Trichloroethane 44 142-28-9--------1,3-Dichloropropane 48 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2SLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No.-: SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5985 Level: (low/med) LOW Date Received! a Moisture: not dec. Date Analyzed: 12/01/04 'r GC Column: DB-624 ID: 8.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene _ 51 591-78-6--------2-Hexanone 58 124-48-1--------Dibromochloromethane_ _ 46 106-93-4--------1,2-Dibromoethane 48 108-90-7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetrachloroethane 47 .100-41-4---'-=---Ethylbenzene_ 54 ----------------m.p-Xylene 100 95-47-6---------o-Xylene 53 1330-20-7-------Xylene (Total) 160 100-42-5--------Styrene 52 75-25-2---------Bromoform 47 98-82-8---------Isopropylbenzene 56 79-34-5---------1,1,2,2-Tetrachloroethane 45 108-86-1--------Bromobenzene . 50 96-18-4---------1,2,3-Trichloropropane 45 103-65-1--------n-Propylbenzene 51 95-49-8----------2-Chlorotoluene 49 108-67-8--------1,3,5-Trimethy nzene 52 106-43-4--------4-Chlorotoluene 48 98-06-6---------tert-Butylbenzene 53 95=63-6---------1,2,4-Trimethylbenzene 53 135-98-8--------sec-Butylbenzene 53 99-87-6---------4-Isopropyltoluene 52 541-73-1--------1,3-Dichlorobenzene 48 106-4.6-7--------1,4-Dichlorobenzene 47 104-51-8--------n-Butylbenzene 53 95-50-1---------1,2-Dichlorobenzene� 48 96-12-8---------1,2-Dibromo-3-chloropropane_ 50 120-82-1--------1,2,4-Trichlorobenzene 54 87-68-3---------Hexachlorobutadiene__ 50 91-20-3---------Naphthalene 57 87-61-6---------1,2,3-Trichlorobenzene 53 60-2.9-7---------Ether 49 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V2SLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 ) Matrix: - (soil/water) SOIL Lab .Sample ID: LCSD-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5985 Level: (low/med). LOW Date Received: %; Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uL-) CONCENTRATION UNITS: CAS NO. CQMPOUM (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 55 637-92-3--------Ethyl tert-butyl ether 55 994-05-8--------tert-Amyl methyl ether 59 123-91-1--------1,4-Dioxane 980 } FORM I VOA 0LM03.0 ) EPA SAMPLE NO: VOLATILE ORGANICS ANALYSIS DATA SHEET VSALCS. Lab Name: MITIM4 CORPORATION Contract: Lab Code: MITKE2I Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15904 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V5F6824 Level: (low/med) MED Date Received: o Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 2300 74-87-3---------Chloromethane 2400 75-01-4---------vinyl Chloride---- 2400 74-83=9----------Bromomethane 2300 75-00-3---------Chloroethane -2400 15-69-4---------Trichlorofluoromethane 2400 75-35-4---------1,1-Dichloroethene 2400 67-64-1-------=-Acetone 1900 75-15-0------- --Carbon Disulfide 2400 75-09-2---------Methylene Chloride 2400 156-60-5--------trans-1,2-Dichloroe�ene 2500 1634-04-4-------Methyl tert-butyl ether 4560 75-34-3-------- 1,1-Dichloroethane 2500 78-93-3---------2-Butanone 3000 156-59-2--------cis-1,2-Dichloroethene 2400 590-20-7--------2,2-Dichloropropane 2800 74-97-5---------Bromochloromethane 2900 67-66-3---------Chloroform 3100 109-99-9-=------Tetrahydrofuran 3600 71-55-6---------1,1,1=Trichloroethane 2900 563-58-6--------1,1-Dichloropropene 2800 56-23-5---------Carbon Tetrachloride 2500 107-06-2--------1,2-Dichloroethane 2300 71-43-2---------Benzene 2500 79-01-6---------Trichloroethene 2500 78-87-5---------1,2-Dichloropropane 2400 74-95-3---------Dibromomethane 2400 75-27-4---------Bromodichloromethane 2400 10061-01-5------cis-1,3-Dichloropropene 2400 108-10-1--------4-Methyl-2-pentanone 2000 108-88-3--------Toluene _ 2500 10061-02-6------trans-1,3-Dichloropropene 2200 79-00-5---------1', 1,2-Trichloroethane 2200 142-28-9---------1,3-Dichloropropane 2400 FORM I VOA OLM03.0 ) _ a -- - 'r �. r l EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VSALCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : "MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15904 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V5F6824 Level: (low/med) NED Date Received: g Moisture: not dec. Date Analyzed: 12/O1/04 GC Column: DB-624 ID.- 0.25 (mm) Dilution Factor: 1:0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(ut) CONCENTRATION. UNITS: CAS -NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 2500. 591-78-6--------2-Hexanone 2200 124-48-1--------Dibromochloromethane 2400 106-93-4--------1,2-Dibromoethane 2300 108-90-7--------Chlorobenzene 2500 "630-20-6--------1,1,1,2-Tetrachloroethane 2600 100-41-4--------Euhylbenzene 2600 --=-------------m,p-Xylene 5100 95-47-6---------o-Xylene 2600 1330-20-7-------Xylene Total 7800 100-42-5--------Styrene 260.0 75-25-2---------Bromoform 2300 98-82-8---------Isopropylbenzene 2600 79-34-5---------1,1,2,2-Tetrachloroethane 2300 108-86-1-------- Bromobenzene 2500 96-18-4---------1,2,3-Trichloropropane 2300 103-65-1--------n-Propylbenzene 2700 95-49=8---------2-Chlorotoluene 2700 108-67-8--------1,3,5-Trimethylbenzene 2700 106-43-4--------4-Chlorotoluene 2700 98-06-6---------tent-Butylbenzene _ 2600 95-63-6---------1,2,4-Trimethylbenzene 2700 135-98-8--------sec-Butylbenzene 2600 99-87-6---------4-Isopropyltoluene 2600 541-73-1--------1,3-Dichlorobenzene 2600 106-46-7--------1,4-Dichlorobenzene 2500 104-51-8--------n-Butylbenzene 2600 -95-50-1---------1,2-Dichlorobenzene 2600 96-12-8---------1,2-Dibromo-3-chloropropane 2100 120-82-1--------1,2,4-Trichlorobenzene 2200 87-68-3---------Hexachlorobutadiene 2400 91-20-3---------Naphthalene 2000 87-61-6---------1,2,3-Trich.lorobenzene 2100 60-29-7---------Ether 2300 FORM I VOA OLM03.0 lA EPA SAMPLE NO: VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: VSALCS Lab Code: MITI03K Case No. : SAS No. : SDG No. : MC1453 Matrix: . (soil/water) SOIL Lab Sample ID: LCS-15904 Sample. wt/vol: 5.0 (g/mL) G Lab File ID: V5F6824 Level: (low/med) MED Date Received: Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5.(mL) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 2200 637-92-3---------Ethyl tert-butyl ether . 2200 994-.05-8--------tert-Amyl methyl ether, 2500 123-91-1--------1,4-Dioxane 39000 l FORM I VOA 0LM03.0 ILA. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET ` V5ALCSD j Lab Name: MITKEM CORPORATION Contract: Lab .Code: MITKEK Case No. : SAS No. . SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15904 Sample wt/vol: 5-0 (g/mL) G Lab File ID: V5F6825 Level: (low/med) HIED. Date Received: a Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mn) Dilution Factor: 1.0: Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100:Q{u;) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or :ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 2300 74-87-3-----=---Chloromethane 2700. 75-01-4---------Vinyl Chloride 2700 74-83-9---------Bromomethane 2500 75-00-3---------Chloroethane 2500 75-69-4---------Trichlorofluoromethane 2500 75-35-4---------1,1=Dichloroethene -2500 67-64-1---------Acetone 2000 75-15-0---------Carbon Disulfide 2600 75-09-2---------Methylene Chloride 2600 156-60-5--------trans-1,2-Dichloroethene 2600 1634-04=4-------Methyl tert-butyl ether 5600 75-34-3---------1,1-Dichloroethane 2600 78-93-3_-----=--2-Butanone 2400 156-59-2--------cis-1,2-Dichloroethene 2600 590-20-7--------2,2-Dichloropropane 2500 74-97-5---------Bromochloromethane 2500 67-66=3---------Chloroform 2500 109-99-9--------Tetrahydrofuran 2900 71-55-6---------1, 1,1-Trichloroethane 2900 563-58-6--------1,1-Dichloropropene 2700 56-23.-5---------Carbon Tetrachloride 2500 107-06-2--------1,2-Dichloroethane 2400 -71-43-2---------Benzene 2700 79-01-6---------Trichloroethene 2600 78-81-5---------1,2-Dichloropropane 2600 74-95-3---------Dibromomethane 2500 75-27-4---------Bromodichloromethane 2500 10061-01-5------cis-1,3-Dichloropropene 2500 108-10-1---------4-Methyl-2-pentanone 2300 108-88-3--------Toluene 2600 10061-02-6------trans-1,3-Dichloropropene. * 2500 79-00-5---------1, 1,2-Trichloroethane 2500 142-28-9--------1,3-Dichloropropane 2500 FORM I VOA OLM03.0. EPA SAMPLE I9O. VOLATILE ORGANICS ANALYSIS DATA SHEET VSALCSD Lab Name: MITKFM CORPORATION Contract: Lab Cade; MITI+! Case No. : -SAS No. : SDG No. : MC1453. Matrix: (soil/water) SOIL Lab Sample ID: .LCSD-15904 . Sample. wt/vol: 5.0 (g/mL) G Lab File ID: V5F6825 Level.: (low/med) MED Date Received: %- Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 . ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene_ 2600 591-78-6--------2-Hexanone 2300 124-48-1--------Dibrogochloromethane 2500 106-93-4--------1,2-Dibromoethane 2500 108-90-7--------Chlorobenzene 2600 630-20-6--------1,1,1,2-Tetrachloroethane 2600 100-41-4--=-----Ethylbenzene 2700 ----------------m,p-Xylene 5400 95-47-6---------o-Xylene 2700 -1330-20-7--=----Xylene (Total) 8200 100-42-5-------- Styrene 2700 . 75-25-2---------Bromoform 2400 98-82-8---------Isoprcpylbenzene 2600 79-34-5---------1,1,2,2-Tetrachloroethane 2500 --108-86-1 ------Bromobenzene 2600 96-18-4---------1,2,3-Trichloropropane 2500 103-65-1--------n-Propylbenzene 2700 95-49-8---------2-Chlorotoluene 2700 108-67-8--------1,3,5-Trimethylbenzene 2700 106-43-4--------4-Chlorotoluene 2800 98-06-6---------tert-Butylbenzene 2700 95-63-6----------1,2,4-Trimethylbenzene _2800. 135-98-8--------sec-Butylbenzene 2700 99-87-6---------4-Isoprcpyltoluene 2700 541-73-1-------- 1,3-Dichlorobenzene 2600 166-46-7--------1,4-Dichlorobenzene 2600 104-.51-8--------n-Butylbenzene 2600 95-50-1---------1,2-Dichlorobenzene 2700 96-12-8---------1,2-Dibrcmo-3-chlorapropane_ 2400 120-82-1--------1,2,4-Trichlorobenzene 2400 87-68-3---------Hexachl.orobutadiene 2500 91-20-3---------Naphthalene 2300 87-61-6---------1,2,3-Tric orobenzene 2300 60-29-7---------Ether 2600 FORM I VOA OLM03.0 / i EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA. SHEET VSALCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. . SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15904 Sample wt/vol: 5.0. (g/mL) G Lab File ID: V5F6825 Level:. . (low/med) MED . Date Received: %- Moisture: not dec. _ Date Analyzed: 12/01/04 GC Column: DB-624 _ ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(uL). CONCENTRATION UNITS: CAS. NO- COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisopropyl Ether 2400 637-92-3--------Ethyl tert-butyl ether 2400 994-05-8--------tert-Amyl methyl ether 2700 123-91-1--------1,4-Dioxane 45000 FORM I VOA OLM03.0 S 1B EPA SAMPLE -NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB-X Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG .No. : MC1453 J ` z Matrix: (soil/water) SOIL Lab Sample ID:- C1453-09E Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2660 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 14 .decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/oi/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 380 U 111-44-4--------bis(2-Chloroethyl Ether 380 U 95-57-8---------2-Chlorophenol 380 U 541-73-1--------1,3-Dichlorobenzene 380 U 106-46-7--------1,4-Dichlorobenzene 380 U 95-50-1---------1,2-Dichlorobenzene 380 U 95-48-7---------2-Methylphenol 380 U \ 108-60-1--------2,2' -oxybis(1-Chloropropan-eT 380 U 106-44-5--------4-Methylphenol 380 U 621-64-7--------N-Nitroso-di-n-propylamine 380 U 67-72-1---------Hexachloroethane 380 U 98-95-3---------Nitrobenzene . 380 U 78-59-1---------Isophorone 380 U 88-75-5---------2-Nitrophenol 380 U 105-67-9--------2,4-Dimethylphenol 380 U 120-83-2--------2,4-Dichlorophenol 380 U 120-82-1--------1,2,4-Trichlorobenzene 380 U 91-20-3---------Naphthalene 380 U 106-47-8--------4-Chloroanili.ne 380 U 111-91-1---------bis(2-Chloroethoxy methane_ 380 U 87-68-3---------Hexachlorobutadiene 380 U 59-50-7---------4-Chloro-3-Methylphenol 380 U 91-57-6---------2-Methylnaphthalene 380 U 77-47-4---------Hexachlorocyclopentadie�ne 380 U 88-06-2---------2,4,6-Trichlorophenol 380 U 95-95-4---------2,4,5-Trichlorophenol 780 U 91-58-7---------2-Chl.oronaphthalene 380 U 88-74-4---------2-Nitroaniline 780 U 131-11-3--------Dimethylphthalate 380 U 208-96-8--------Acenaphthylene_ 380 U 606-20-2---------2,6-Dinitrotoluene 380 U 99-09-2---------3-Nitroaniline _ 780 U 83-32-9---------Acenaphthene 380 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-09E Sample. wt/vol: 30.0 (g/mL) G Lab File ID: S2E2660 Level: (low/med) LOW Date Received: 11/18/04. g Moisture: 14 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed; 12/01/04 Injection Volume 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol_ 780 U 100-02-7--------4-Nitrophenol 780 U 132-64-9--------Dibenzofuran 380 .0 121-14-2--------2,4-Dinitrotoluene 380 U 84-66-2---------Diethylphthalate 380 U 7005-72-3-------4-Chlorophenyl-phenylether 380 U 86-73-7---------Fluorene 380 U 100-01-6--------4-Nitroaniline - 780 U 534-52-1--------4,6-Di.nitro-2-methylphenol 780 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 380 U 101-55-3--------4-Bromophenyl-phenylether 380 U 118-74-1--------Hexachlorobenzene 380 U 87-86-5---------Pentachlorophenol 780 U 85-01-8---------Phenanthrene 300 U 120-12-7--------Anthracene 380 U 86-.74-8---------Carbazole 380 U 84-74-2---------Di-n-butylphthalate 380 U 206-44-0--------Fluoranthene 380 U 129-00-0--------Pyrene_ 380 U 85-68-7---------Butylbenzylphthalate 380 U 91-94-1---------3,3'--Dichlorobenzidine 380 U 56-55-3---------Benzo(a)anthracene .380 U 218-01-9--------Chrysene 380 U 117-81-7--------bis(2-Ethylhexyl phthalate_ 69 LT117-84-0--------Di-n-octylphthalate _ 380 U 205-99-2--------Benzo(b) fluoranthene 380 U 207-08-9--------Benzo(k)fluoranthene _ 380 U 50-32-8.---------Benzo(a)pyrene_ 380 U 193-39-5--------Indeno(112,3-cd p ene 380 U 53-70-3---------Dibenzo(a,h)anthracene 380 U 191-24-2--------Benzo(g,h,i)perylene 380 U. (.1 - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB1-8 Lab Name: MITKEM CORPORATION Contract: _ Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-01E Sample wt/vol: 30.1 (g/mL) G Lab File ID:. S2E2669 Level: (low/med) IOW Date Received: 11/18/04 !k Moisture: 8 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04. Injection. Volume:. 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 360 U 111-44-4--------bis(2-Chloroethy Ether 360 U 95-57-8---------2-Chlorophenol. 360 U 541-73-1--------1,3-Dichlorobenzene 360 U 106-46-7--------1,4-Dichlorobenzene 360 U 95-50-1---------1,2-Dichlorobenzene 360 U 95-48-7---------2-Methylphenol_ 360 U \ 108-60-1--------2,2'-oxybis(1-Chloropropane 360 U 106-44-5--------4-Methylphenol 360 U 621-64-7--------N-Nitroso-di-n-propylamine 360 U 67-72-1---------Hexachloroethane 360 U 98-95-3---------Nitrobenzene 360- U 78-59-1---------Isophorone 360 U 88-75-5---------2-Nitrophenol 360 U 105-67-9--------2,4-Dimethylp enol 360 U 120-83-2--------2,4-Dichlorophenol 360 U 120-82-1--------1,2,4-Trichlorobenzene 360 U 91-20-3---------Naphthalene 360 U 106-47-8--------4-Chloroaniline 360. U` 111-91-1--------bis(2-Chloroethoxy)methane _ 360 U 87-68-3---------Hexachlorobutadiene 360 U 59-50-7---------4-Chloro-3-Methylphenol 360 U 91-57-6---------2-Methylnaphthalene 17000 E 77-47-4---------Hexachlorocyclopentadie�ne 360 U 88-06-2---------2,4,6-Trichlorophenol 360 U 95-95-4---------2,4,5-Trichlorophenol 720 U 91-58-7---------2-Chloronaphthalene 360 U 88-74-4---------2-Nitroaniline 720 U 131-11-3--------Dimethylphthalate 360 U 208-96-8--------Acenaphthylene 360 U 606-20-2--------2,6-Dinitrotoluene 360 U 99-09-2---------3-Nitroaniline _ 720 U 83-32-9---------Acenaphthene 360 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB1-8 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No_ : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-OIE Sample wt/vol: 30.1 (g/n-L) G Lab File ID: S2E2669 Level: ' (low/med) LOW Date Received: 11/18/04 Moisture: 8 decanted: (Y/N). N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol�_ 720 U 100-02-7--- -----4-Nitrophenol _ 720 U 132-64-9--------Dibenzofuran 750 121-14-2--------2,4-Dini.trotoluene 360 U 84-66-2---------Diethylphthalate 360 U 7005-72-3-------4-Chlorophenyl-phenylether. 360 U 86-73-7-------- Fluorene _ 1500 100 01-6-----=--4-Nitroaniline 720 U 534-52-1--------4,6-Dinitro-2-met ylphenol 720 U 86-30-6---------N-Nitrosodiphenylamine (1) 360 U 101-55=3---------4-Bromophenyl.=phenylether 360 U 118-74-1--------Hexachlorobenzene 360 U 87-86-5---------Pentachlorophenol 720 U 85-01-8---------Phenanthrene 3900 120-12-7--------Anthracene 360 U 86-74-8---------Carbazole 360 U 84-74-2---------Di-n-butylpht late 360 U 206-44-0--------Fluoranthene 220 J 129-00-0--------Pyrene 1300 85-68-7---------Butylbenzylphthalate 360 U 91-94-1---------3,3' -Dichlorobenzidirie 360 U 56-55-3---------Benzo(a)anthracene 260 J 218-01-9---------Chrysene 790 117-81-7--------bis(2-Ethylhexyl)phthalate_ 360 U 117-84-0-----.---Di-n-octylphthalate 360 U 205-99-2--------Benzo(b)fluoranthene _ 160 J 207-08-9--------Benzo(k).fluoranthene 360 U . 50-32-8---------Benzo(a)pyrene . 360 U 193-39-5--------Indeno(1,2,3-cd)pyrene 360 U 53-70-3---------Dibenzo(a,h)anthracene 360 U 191-24-2--------Benzo(g,h,i)perylene 360 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 �ll�� lg EPA SAMPLE NO. SEMIVOLATILR ORGANICS ANALYSIS DATA SHEET SB1-8DL Lab Name: MITKEM CORPORATION Contract: \ Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 /1 Matrix: (soil/water) SOIL Lab Sample ID: C1453-01EDL Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2707 Level: (low/med) LOW Date Received: 11/18/04 I; Moisture: 8 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 4.0 - GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. GROUND (ug/L or .,ug/Kg) UG/KG Q 108-95-2--------Phenol 1400 U 111-44-4--------bis(2-Chloroethyl Ether 1400 U 95-57-8---------2-Chlorophenol 1400 U 541-73-1--------1,3-Dichlorobenzene 1400 U 106-46-7--------1,4-Dichlorobenzene 1400 U 95-50-1---------1,2-Dichl.orobenzene 1400 U 95-48-7---------2-Methylphenol 1400 U \ 108-60-1--------2,2'-oxybis(1-Chlorcpropane) 1400 U J 106-44-5--------4=Methylphenol 1400 U 621-64-7--------N-Nitroso-di-n-propylamine_ 1400 U 67-72-1---------Hexachloroethane 1400 U 98-95-3---------Nitrobenzene 1400 U 78-59-1---------Isophorone_ _ 1400 U 88-75-5---------2-Nitrophenol 1400 U 105-67-9--------2,4-Dimethylphenol 1400 U 120-83-2--------2,4-Dichlorophenol- 1400 U 120-82-1--------1,2,4-Trichlorobenzene 1400 U 91-20-3---------Naphthalene 1400 U 106-47-8--------4-Chloroaniline 1400 U 111-91-1--------bis(2-Chloroethoxy)methane_ 1400 U 87-68-3---------Hexachlorobutadiene 1400 U 59-50-7---------4-Chloro-3-Methylphenol 1400 U 91-57-6---------2-Methylnaphthalene _ 16000 D- 77-.47-4---------Hexachlorocyclopentadiene 1400 U 88-06-2---------2,4,6-Trichlorophenol 1400 U 95-95-4---------2,4,5-Trichlorophenol_ 29.00 U 91-58-7---------2-Chloronaphthalene 1400 U 88-74-4---------2-Nitroaniline 2900 U 131-11-3--------Dimethylphthalate 1400 U 208-96-8--------Acenaphthylene 1400 U 606-20-2--------2,6-Dinitrotoluene 1400 U 99-09-2---------3-Nitroaniline 2900 U 83-32-9---------Acenaphthene 1400 U l FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. 'SEMIVOLATILE ORGANICS ANALYSIS DATA- SHEET SB1-8DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case- No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-01EDL Sample wt/vol: 3 0.1 (g/mL) G Lab File ID: S2E2707 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 8 decanted: (YIN) N Date Extracted:11/24/04 Concentrated. Extract Volume: 1000(uL) Date Analyzed: 12/03/04 Injection Volume:. 1.0(uL) Dilution Factor: 4.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5----------2,4-Di dtrophenol` 2900 U 100-02-7--------4-Nitrophenol 2900 U 132-64-9--------Dibenzofuran 1400 U 121-14-2--------2,4-Dinitrotoluene 1400 U 84-66-2---------Diethylphthalate 1400 U 7005-72-3-------4-Chlorophenyl-phenylether 1400 U 86-73-7------ ---Fluorene 1800 D 100-01-6--------4-Nitroa==ne 2900 U 534-52-1--------4,6-Dinitro-2-methylphenol 2900 U 86-30-6---------N-Nitrosodiphenylamine_(1)_ 1400 U 101-55-3--------4-Bromophenyl-phenylether 1400 U 118-74-1--------Hexachlorobenzene 1400 U 87-86=5---------Pentachlorophenol 2900 U 85-01-8---------Phenanthrene 4100 D 120-12-7--------Anthracene 1400 U 86-74-8---------Carbazole 1400 U 84-74-2---------Di-n-butylphthalate 1400 U 206-44-0--------Fluoranthene 310 DJ 129-00-0--------Pyrene 790 DJ 85-68-7---------Butylbenzylphthalate 1400 U 91-94-1---------3,3'-Dichlorobenzidine 1400 U 56-55-3---------Benzo(a)anthracene 1400 U 218-01-9------.--Chrysene 1400 U 117-81-7--------bis(2-Ethylhexyl}phthalate_ 1400 U 117-84-0--------Di-n-octylphthalate . 1400 U 205=99-2--------Benzo(b) fluoranthene 1400 U 207-08-9--------Benzo(k) fluoranthene 1400 U 50-32-8---------Benzo(a)pyrene 1400 U 193-39-5--------Indeno(1,2,3-cd)pyrene 1400 U 53-70-3---------Dibenzo(a,h)anthracene 1400 U ' 191-24-2--------Benzo(g,h,i)perylene 1400 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET; SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 } Matrix: (soil/water) SOIL Lab Sample ID: C1453-16E Sample wt/vol: 30.2 (g/mL)_ G Lab File ID: S2E2668 Level: (low/med) IOW Date Received: 11/19/04 Moisture: 6 decanted:. (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 . GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol _ 350 U Eth 111-44-4--------bis(2-Chloroethyl er 350 U 95-57-8---------2-Chlorophenol 350 U 541-73-1--------1,3-Dichlorobenzene 350 U 106.-46-7--------1,4-Dichlorobenzene 350. 0 95-50-1---------1,2-Dichlorobenzene 350 U 95-48-7---------2-Methylphenol 350 U 108-60-1--------2,2 - -oxybis(1-diloropropane 350 U 106-44-5--------4-Methylphenol 350 U 621-64-7--------N-Nitroso-di-n-propylamLne_ 350 U 67-72-1---------Hexachloroethane 350 U 98-95-3-- =-----Nitrobenzene 350 U 78-59-1---------Isophorone 350 U 88-75-5---------2-Nitrophenol_ 350 U 105-67-9--------2,4-Dimethylphenol 350. 0 120-83-2--------2,4-Dichlorophenol 350 U 120-82-1--------1,2,4-Trichlorobenzene 350 U 91-20-3---------Naphthalene 350 U 106-47-8--------4-Chloroanif3 e 350 U 111-91-1---------bis(2-Chloroethoxy methane_ 350 U 87-68-3---------Hexachlorobutadiene 350 U 59-50-7---------4-Chloro-3-Methylphenol 350 U 91-57-6---------2-Methylnaphthalene 350 U 77-47-4---------HexachlorocyclopenCa e 350 U 88-06-2---------2,4,6-Trichlorophenol 350 U 95-95-4---------2,4,5-Trichlorophenol 710 U 91-58-7---------2-Chloronaphthalene 350 U 88-74=4---------2-Nitroanili.ne 710. 0 131-11-3------ Dimethylphthalate 350 U 208-96-8--------Acenaphthylene 350 U 606-20-2--------2,6-Dinitrotoluene 350 U 99-09-2---------3-Nitroaniline 710 U 83-32-9---------Acenaphthene 350 U FORM I SV-1 OLM03.0 / 1C : EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16E Sample wt/vol: 30.2 (g/mL) G Lab File ID: S2E2668 Level: (low/med.) LOW Date Received: 11/19/04 o Moisture: 6 decanted: (Y/N) N Date Extracted:ll/24/04 Concentrated Extract Volume: 1000(UL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCE2 TRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 710 U 100-02-7--------4-Nitrophenol 710 U 132-64-9--------Dibenzofuran f 350 U 121=14-2--------2,4-Dini.trotoluene 350 U 84-66-2---------Diethylphthalate 350 U 7005-72-3-------4-Chlorophenyl-phenylether 350 U 86-73-7---------Fluorene 350 U 100-01-6--------4-Nitroanile 710 U 534-52-1--------4;6-Dinitro-2-methylphenol 710 U 86-30-6---------N-Nitrosodi_ph6nylamine (1)__ 350 U 101-55-3--------4-Bromophenyl-phenylether 350 U 118-74-1--------Hexachlorobenzene 350 U 87-86-5---------Pentachlorophen0l_ 710 U 85-01-8---------Phenanthrene 360 120-12-7--------Anthracene _ 100 J 86-74-8---------Carbazole 350 U 84-74-2---------Di-n-butylphthalate 350 U 206-44-0--------Fluoranthene 720 129-00-0--------Pyrene 830 85-68-7---------Butylbenzylphthalate J 350 U 91-94-1---------3,3'-Dichlorobenzidine 350 U 56-55-3---------BenZo-W anthracene 450 218-01-9-=------Chrysene 530 117-81-7--------bis(2-Ethylhexyl)phthalate_ 78 J 117-84-0--------Di-n-octylphthalate 350 U 205-.99-2--------Benzo(b)fluoranthene 600 207-08-9--------Benzo(k) fluoranthene 330 J 50-32-8---------Benzo(a)pyrene 420 193-39-5--------Indeno(1,2,3-cd pyrene 120 J 53-70-3---------Dibenzo(a,h)anthracene 350 U 191-24-2--------Benzo(g,h,i)perylene 140 J (l�annot be separated fromDiphenylamine FORM I SV-2 OLMO3.0 1B" EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2 Lab Name: MITKEM CORPORATION Contract: _ 1 Lab Code: MITKEM Case No. : SAS No. .- SDG No. : MC1453 / Matrix. (soil/water) SOIL Lab Sample. ID: C1453-15C Sample wt/vol: 30.0 '(g/mL) G Lab File ID: S2E2664 Level: (low/med) LOW Date Received: 11/19/04 Moisture: 4 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 340 U 111-44-4--------bis(2-Chloroethyl)Ether 340 U 95-57-8---------2-Chlorcphenol 340 U 541-73-1--------1,3-Dichlorobenzene 340 U 106-46-7--------1,4-Dichlorobenzene 340 U 95-50-1---------1,2-Dichlorobenzene 340 U 95-48-7---------2-Methylphenol 340 U . 108-60-1--------2,2' -oxybis(1-Chloropropane) 340 U 106-,44-5---------4-Methylphenol 340 U 621-64-7--------N-Nitroso-di-n-propylamine_ 340 U 67-72=1---------HexachlOroethane 340 U 98-95-3---------Nitrobenzene 340 U 78-59-1---------Isophorone 340 U 88-75-5---------2-Nitrophenol 340 U 105-67-9--------2,4-Dimethylphenol 340 U 120-83-2--------2,4-Dichlorophenol _ 340 U 120-82-1--------1,2,4-Trichlorobenzene 340 U 91-20-3---------Naphthalene 340 U 106-47-8--------4-Chloroaniline 34.0 U Ill-91-1--------bis(2-Chloroethoxy methane. 340 U 87-68-3---------Hexachlorobutadiene , 340 U 59-50-7---------4-Chloro-3-Methylphenol 340 U 91-57-6---------2-Methylnaphthalene 340 U 77-47-4---------Hexachlorocyclopentadie�ne 340 U 88-06-2---------2;4,6-Trichlorophenol 340 U .95-95-4---------2,4,5-Trichlorophenol 700 U 91-58-7---------2-Chloronaphthalene 340 U 88-74-4---------2-Nitroaniline 700 U 131-11-3--------Dimethylphthalate 340 U 208-96-8--------Acenaphthylene 340 U 606-20-2--------2,6-Dinitrotoluene 340 U 99-09-2---------3-Nitroaniline 700 U 83-32-9---------Acenaphthene 340 U 1 FORM I SV-1 OLM03.0 1 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS- DATA SHEET' SB2-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-15C Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2664 Level: (low/med) LOW Date Received: 11/19/04 o Moisture: 4 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dini.trophenol _ _ 700 U 100-02-7--------4-Nitrophenol 700 U 132-64-9--------Dibenzofuran 340 U 121-14-2--------2,4-Dinitrotoluene 340 U 84-66-2---------Diethylphthalate 340 U 7005-72-3-------4-Chlorophenyl-phenylether 340 U 86-73-7---------Fluorene 340 U 100-01-6--------4-Nitroaiuline 700 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 700 U 86.-30-6---------N-Nitrosodiphenylamine (1) 340 U 101-55-3--------4-Bromophenyl-phenylether .340 U 118-74-1--------Hexachlorobenzene 340 U 87-86-5---------Pentachlorophenoly 700 U 85-01-8---------Phenanthrene 340 U 120-12-7--------Anthracene 340 U 86-74-8---------Carbazole 340 U 84-74-2---------Di-n-butylphthalate 340 U 206-44-0--------Fluoranthene 340 U 129-00-0---------Pyrene 340 U 85-68-7---------Butylbenzylphthalate 340 U 91-94-1---------3,3'-Dichlorobenzidine_ 340 U 56-55-3---------Benzo(a)anthracene 340 U 218-01-9--------Chrysene 340 U 117-81-7--------bis(2-Ethylhexyl phthalate_ 71 J 117-84-0--------Di-n-octylphthalate 340 U 205-99-2--------Benzo(b) fluoranthene 340 U 207-08-9--------Benzo(k) fluoranthene 340 U 50-32-8-=-------Benzo(a)pyrene__ 340 U 193-39-5--------Indeno(1,2,3-cd)pyrene 340 U 53-70-3---------Dibenzo(a,h)anthracene 340 U 191-24-2--------Benzo(g,h,i)perylene 340 U (1�Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SENaVOLATILE ORGANICS ANALYSIS DATA SHEET. SB2-2M5 Lab Name: MITKFM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 / Matrix: (soil/water) SOIL Lab Sample ID: C1453-15CMS Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2665 Level: (low/med) LOW Date Received: 11/19/04 o Moisture: 4 decanted: (Y/N) N Date .Extracted:11/24/04 Concentrated Extract Volume: 1000.(uL) Date Analyzed:. 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1..0 - - GPC Cleanup: (Y/N) N pH:. CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 1400 111-44-4--------b1s(2-Chloroethyl Ether 1300 95-57-8---------2-Chlorophenol 1400 541-73-1--------1,3-Dichlorobenzene 1200 106-46-7--------1,4-Dichlorobenzene 1300 95-50-1---------1,2-Dichlorobenzene 1300 95-48-7---------2-Methylphenol 14.00 108-60-1--------2,2'-oxybis(1-Chloropropane 1400 106-44-5--------4-Methylphenol 1400 621-64-7--------N-Nitroso-di-n-propylamine_ 1500 67-72-1---------Hexachloroethane 1200 98-95-3---------Nitrobenzene 1400 78-59-1-=-------Isophorone 1400 88-75-5---------2-Nitrophenol 1300 105-67-9--------2,4-Dimethylp eno1 1600 120-83-2--------2,4-Dichlorophenol 1400 120-82-1--------1,2,4-Trichlorobenzene 1300 91-20-3---------Naphthalene 1400 106-47-8--------4-Chloroani i.ne 1000 111-91-1--------bis(2-Chloroethoxy methane_ 1400 87-68-3---------Hexachlorobutadiene 1300 59-50-7---------4-Chloro-3-Methylphenol 1400 91-57-6---------2-Methylnaphthalene 1400 77-47-4---------Hexachlorocyclopentadiene 870 88-06-2---------2,4,6-Trichlorophenol 1300 95-95-4---------2,4,5-Trichlorophenol 1400 91-58-7---------2-Chloronaphthalene 1400 88-74-4---------2-Nitroaniline 1400 131-11-3--------Dimethylphthalate l 1400 208-96-8--------Acenaphthylene 1500. 606-20-2--------2,6-Dinitrotoluene 1400 99-09-2---------3-Nitroaniline 1100 83-32-9---------Acenaphthene 1400 l FORM I SV-1 — OL403.0 / 1C EPA SAMPLE NO. SEMIVOLATILE, ORGANICS ANALYSIS DATA SHEET SB2-2MS Lab Name.: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-15CMS Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2665 Level: (low/med) LOW Date Received: 11/19/04 `s Moisture: 4 . decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L .or ug/Kg) UG/KG Q 51-28-5---------2,4-Dini.trcphenol 500 J 100-02-7--------4-Nitrcphenol 1200 132-64-9--------Dibenzofuran 1400 121-14-2--------2,4-Dinitrotoluene _ 1400 84-66-2---------Diethylphthalate 1100 7005-72-3-------4-Chlorophenyl-phenylether 1400 86-73-7--.-------Fluorene _ 1400 100-01-6--------4-Nitroaniluie 1400 534-52-1--------4,6-Dinitro-2-methylphenol 790 86-30-6---------N-Nitrosodiphenylamine (1) 1800 101-55-3--------4-Bromopheriyl-phenylet�ier 1400 118-74-1--------Hexachlorobenzene 1400 87-86-5---------Pentachlorophenol 580 J 85-01-8---------Phenanthrene _ 1400 120-12-7--------Anthracene _ 1500 86-74-8-=-------Carbazole 1500 84-74-2---------Di-n-butylphthalate 1500 206-44-0--------Fluoranthene 1400 129-00-0--------Pyrene _ 1500 ylphthalate 85-68-7---------Butylbenz 1600 91-94-1----------3,3 ' -Dichlorobenzidine 1300 56-55-3---------Benzo(a)anthracene 1400 218-01-9------- Chrysene _ 1600 117-81-7--------bis(2-Ethylhexyl phthalate_ 1600 117-84-0--------Di-n-octylphthaiate 1900 205-99-2--------Benzo(b)fluoranthene 1400 207-08-9--------Benzo(k)fluoranthene 1600 50-32-8---------Benzo(a)pyrene . 1400 193-39-5--------Indeno(1,2,3-cam pyrene 93.0 53-70-3---------Dibenzo(a,h)anthracene 970 191-24-2--------Benzo(g,h,i)perylene_ 850 (I - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453715CMSD Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2666 Level: (low/med) LOW Date Received: 11/19/04 !k Moisture: 4 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04. Injection Volume: 1.0(uL) Dilution Factor: 1.0. -" GPC Cleanup: (Y/N) N pH: CONCENTRATION ONITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 1500 111-44-4--------bis(2-Chloroethyl)Ether 1400 95-57-8---------2-Chlorophenol 1500 541-73-1=-------1,3-Dichlorobenzene _ 1300 106-46-7--------1,4-Dichlorobenzene 1400 95-50-1---------1,2-Dichlorobenzene 1400 95-48-7---------2-Methylphenol 1500 108-60-1--------2,2'-oxybis(1-Chloropropane) 1500 106-44-5--------4-Methylphenol_ 1600 621-64-7--------N-Nitroso-di-n-propylamine_ 1600 67-72-1---------Hexachloroethane 1400 98-95-3---------Nitrobenzene 1400 78-59-1------- Isophorone 1500 88-75-5---------2-Nitrophenol 1400 105-67-9--------2,4-Dimethylphenol 1800 120-83-2--------2,4-Dichlorophenol 1500 120-82-1--------1,2,4-Trichlorobenzene 1400 91-20-3---------Naphthalene 1500 106-47-8--------4-Chloroaniline 1000 111-91-1--=-----bis(2-Chloroethoxy methane_ 1500 87-68-3---------Hexachlorobutadiene 1400 59-50-7---------4-Chloro-3-Methylphenol 1600 91-57-6---------2-Methylnaphthalene 1500 77-47-4---------Hexachlorocyclopentadiene 880 88-06-2---------2,4,.6-Trichlorophenol 1400 95-95-4---------2,4,5-Trichlorophenol 1500 91-58-7---------2-Chloronaphthalene 1500 88-74-4---------2-Nitroaniline 1600 131-11-3----- Dime thylphthalate 160.0 208-96-8--------Acenaphthylene 1600 606-20-2--------2,6-Dinitrotoluene 1600 99-09-2---------3-Nitroaniline_ _ 1200 83-32-9---------Acenaphthene 1600 FORM I SV-1 OLM03.0 ) 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2MSD Lab Name: MITICHM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.: MC1453 Matrix; (soil/water) SOIL Lab Sample ID: C1453-15CMSD Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2666 Level: (low/med) LOW Date Received: 11/19/04 % -Moisture: 4 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol .440 J 100-02-7--------4-Nitrophenol . 1400 13.2-64-9--------Dibenzofuran 1500 121-14-2--------2,4-Dinitrotoluene 1600 84-66-2----------Diethylphthalate 1200 7005=72-3-------4-Chlorophenyl-phenylether— 1600 86=73-7---------Fluorene 1600 100-61-6--------4-Nitroaniline 1700 534-52-1--------4,6-Dinitro-2-methylphenol 740 86-30-6---------N-Nitrosodiphenylamine (1)__ 2000 101-55-3--------4-Bromophenyl-phenylether 1500 118-74-1---------Hexachlorobenzene 1600. 87-86-5---------Pentachlorophenol 640 J 85-01-8---------Phenanthrene 1600 120-12-7--------Anthracene 1600 86-74-8---------Carbazole 1700 84-74-2---------Di-n-butylphthalate 1.600 206-44-0--------Fluoranthene 1600 129-00-0---------Pyrene 1600 85-68-7---------Butylbenzylphthalate 1700 91-94-1---------3,3 --Dichlorobenzidine 1500 56-55-3---------Benzo(a)anthracene 1600 218-01-9--------Chrysene -- 1700 117-81-7--------bis(2=Ethylhexyl)phthalate_ 1700 117-84-0--------Di-n-octylphthalate 2000 205-99-2--------Benzo(b) fluoranthene 1500 207-08-9--------Benzo(k) fluoranthene 1800 50-32-8---------Benzo(a)pyrene 1500 193-39-5--------Indeno(1,2,3-cdFpyrene 1000 53-70-3---------Dibenzo(a;h)anthracene 1100 191-24-2--------Benzo(g,h,i)perylene 940 (1) - Cannot be separated from Diphenylamine FORM' I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITICEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12E Sample wt/vol: 30.0 (g/mL) G Lab File ID: - S2E2661 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 9 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: " CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 360 U 111-44-4--------bis(2-Chloroethyl}Ether 360 U 95-57-8---------2-Chlorophenol 360 U 541-73-1--------1,3-Di chlorobenzene 360 U .106-46-7--------1,4-Dichlorobenzene 360 U 95=50-1---------1,2-Dichlorobenzene 360 U 95-48-7---------2-Methylphenol 360 U 108-60-1--------2,2--oxybis(1-Chloropropane 360 U 106-44 5--------4-Methylphenol_ 360 U ropylmi e 621-64-7--------N-Nitroso-di-n-pa 360 U 67-72-1---------Hexachloroethane 360 U 98-95-3---------Nitrobenzene 360 U 78-59-1---------Isophorone 360 U 88-75-5---------2-Nitrophenol� 360 U 105-67-9--------2,4-Dimethylphenol 360 U 120-83-2--------2,4-Dichlorophenol 360 U 120-82-1--------1,2,4-Trichlorobenzene 360 U 91-20-3---------Naphthalene 800 106-47-8--------4-Chloroaniline 360 U 111-91-1--------bis(2-Chloroethoxy methane "360 U 87-68-3---------Hexachlorobutadiene— 360 U 59-50-7---------4-Chloro-3-Methylphenol 360 U 91-57-6---------2-Methylnaphthalene 180 J 77-47-4---------Hexachlorocycicpentadiene 360 U 88-06-2---------2,4,6-Trichlorophenol 93 J 95-95-4---------2,4,5-Trichlorophenol 740 U 91-58-7---------2-Chloronaphthalene 360 U 88-74-4---------2-Nitroaniline 740 U 131-11-3--------Dimethylphthalate _ 360 U 208-96-8--------Acenaphthylene 360 U 606-20-2--------2,6-Dinitrotoluene 360 U 99-09-2---------3-Nitroaniline 740 U 83-32-9---------Acenaphthene 360 U FORM I SV-1 OLM03.0 l 1C . EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB3-6 Lab Name: 14ITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. :: SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453.-12E. Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2661 Level: (low/med) LOW Date Received: 11/18/04 g Moisture: 9 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N)' N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 740 U 100-02-7---------4-Nitrophenol 740 U 132-64-9--------Dibenzofuran 360 U 121-14-2--------2,4-Dinitrotoluene 360 U 84-66-2---------Diethylphthalate 360 U 7005-72-3-------4-Chlorophenyl-phenylether - 360 U 86-73-7---------Fluorene 360 U 100-01-6--------4-Nitroaniline 740 U 534-52-1--------4,6-Dinitro-2-methylphenol 740 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 360 U 101-55-3--------4-Bromophenyl-phenylether 360 U 118-74-1--------Hexachlorobenzene 360 U 87-86-5---------Pentachlorophenol 740 U 85-01-8-------- -Phenanthrene 74 J. 120-12-7--------Anthracene 360 U 86-74-8---------Carbazole 360 U 84-74-2---------Di-n-butylphthalate 360 U 206-44-0--------Fluoranthene 360 U 129-00-0--------Pyrene 85 J 85-68-7---------Butylbenzylphthalate 360 U 91-94-1---------3,3'-Dichlorobenzidine 360 U 56-55-3---------Benzo(a)anthracene 360 U 218-01-9--------Chrysene 360 U 117-81-7--------bis(2-Ethylhexyl)phthalate_ 120 J 117-84-0--------Di-n-octylphthalate 360 U 205-99-2--------Benzo(b) fluoranthene 360 U 207-08-9--------Benzo(k).fluoranthene 360 U 50-32-.8---------Benzo(a)pyrene 360 U 193-39-5--------Indeno(1,2,3-cd)pyrene 360 U 53-70-3---------Dibenzo(a,h)anthracene 360 U 191-24-2--------Benzo(g,h,i)perylene 360 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SE41VOIATTLE ORGANICS ANALYSIS DATA SHEET SB4-14 . Lab Name: MITKEM CORPORATION Contract: _ 1 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-14E Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2662 Level: (low/med) LOW Date Received: 11/19/04 Moisture: .3 decanted: (Y/N) N Date Extracted:11/24/04. Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor:. 1-0 -- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 340 U 111-44=4--------bis(2-Chloroethyl)Ether 340 U 95-57-8---------2-Chlorophenol 340 U 541-73-1--------1,3-Dichlorobenzene 340 U 106-46-7--------1,4-Dichlorobenzenef 340 U 95-50-1---------1,2-Dichlorobenzene 340 U 95-48-7---------2-Methylphenol 340 U 108-60-1--------2,2--oxybis(1-Chloropropan6) 340 U 106-44-5--------4-Methylphenol _ 340 U 621-64-7--------N-Nitroso-di-n-propylamine 340. U` 67-72-1---------Hexachloroethane 340 U 98-95-3---------Nitrobenzene 340 U 78-59-1---------Isophorone 340 U 88-75-5---------2-Nitrophenol_ 340 U 105-67-9--------2,4-Dimethylphenol - 340 U 120-83-2--------2,4-Dichlorophenol 340 U 120-82-1--------1,2,4-Trichlorobenzene 34.0 U 91-20-3---------Naphthalene 340 U 106-47-8--------4-Chloroanlline 340 U 111-91-1--------bis(2-Chloroetbo- y)methane 340 U 87-68-3---------Hexachlorobutadiene 340 U 59-50-7---------4-Chloro-3-Methylphenol 340 U 91-57-6---------2-Methylnaphthalene 340 U 77-47-4---------Hexachlorocyclopentadierie 340 U 88-06-2---------2,4,6-Trichlorophenol 340 U 95-95-4---------2,4,5-Trichlorophenol 690 U 91-58-7---------2-Chloronaphthalene 340 U 88-74-4---------2-Nitroaniline 690 U 131-11-3--------Dimethylphthalate_ 340 U 208-96-8--------Acenaphthylene_ 340 U 606-20-2--------2,6-Dinitrotoluene 340 U 99-09-2---------3-Nitroaniline 690 U 83-32-9---------Acenaphthene 340 U FORM I SV-1 OLM03:0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET. SB4-14 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No.. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-14E Sample wt./vol_,- 30.1 (g/mL) G Lab File ID: S2E2662. . Level: (low/med) LOW Date Received: 11/19/04 %Moisture: 3 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date .Analyzed: 12/01/04 Injection Volume: 1.0 (uL) Dilution Factor: 1-.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 690. 0 100-02-7--------4-Nitrophenol 690 U 132-64-9--------Dibenzofuran 340 U 121-14-2--------2,4-Dinitrotoluene 340 U 84-66-2---------Diethylphthalate _ 340. 0 7005-72-3-------4-Chlorophenyl-phenylether— 340 U .86-73-7---------Fluorene 340 U 100-01-6--------4-Nitroaniline 690 U` 534-52-1--------4,6-Dinitro-2-methylphenol_ 690 U 86-30-6---------N-Nitrosodiphenylamine (1) 340 U 101-55-3--------4-Bromophenyl-phenylether 340 U 118-74-1--------Hexachlorobenzene 340 U 87-86-5---------Pentachlorophenol 690 U 85-01-8---------Phenanthrene 95 J 120-12-7--------Anthracene 340 U 86-74-8---------Carbazole 340 U 84-74-2---------Di-n-butylphthalate 340 U 206-44-0--------Fluoranthene 110 J 129-00-0--------Pyrene_ 86 J 85-68-7---------Butylbenzylphthalate 340 U 91=94:-1---------3,3'-Dichlorobenzidine 340 U 56-55-3---------Benzo(a)anthracene 340 U 218-01-9--------Chrysene 340 U 117-81-7--------bis(2-Ethylhexyl phthalate_ 73 J 117-84-0--------Di-n-octylphthalate 340 U 205-99-2--------Benzo(b)fluoranthene 46 J 207-08-9--------Benzo(k)fluoranthene 340 U 50-32-8---------Benzo(a)pyrene 340 U 193-39-5--------Indeno(1,2,3-cd)pyrene 340 U 53-70-3---------Dibenzo(a,h)anthracene 340 U 191-24-2--------Benzo(g,h,i)perylene 340 U (1 - -Cannot be separated from Dipphenylamine i FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA. SHEET. SB5-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID C1453-06E Sample wt/vol: 30.2 (g/mL) G Lab File ID: S2E2663 Level: (low/med) LOW Date Received: 11/18/04 % Moisture: 8 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENrRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 360 U 111-44-4--------bis(2-Chloroethyl)Ether. 360 U 95-57-8---------2-Chlorophenol 360 U 541-73-1--------1,3-Dichlorobenzene 360 U 106-46-7--------1,4-Dichlorobenzene 360 U 95-50-1---------1,2-Dichlorobenzene_ 360 U 95-48-7---------2-Methylphenol 36.0 U 108-60-1--------2,2'_-oxybis(1-Chloropropane) .360 U 106-44-5--------4-Methylphenol 360 U 621-64-7--------N-Nitroso-di-n-propylamine_ 360 U 67-72-1---------Hexachloroethane 360 U 98-95-3---------Nitrobenzene 360, U 78-59-1---------Isophorone 360 U 88-75-5---------2-Nitrophenol 360 U 105-67-9--------2,4-Dimethylphenol 360 U 120-83-2--------2,4-Dichlorophenol 360 U 120-82-1--------1,2,4-Trichlorobenzene 360 U 91-20-3---------Naphthalene 360 U 106-47-8--------4-Chloroaniline 360 U 111-91-1--------bis(2-Chloroethoxy)met hane_ 360 U 87-68-3---------Hexachlorobutadiene _ 360 U 59-50-7---------4-Chloro-3-Methylphenol 360 U 91-57-6---------2-Methylnaphthalene 360 U 77-47-4---------Hexachlorocyclopentadiene 360 U 88-06-2---------2,4,6-Trichlorophenol_ 360 U 95-95-4---------2,4,5-Trichlorophenol 720 U 91-58-7---------2-Chloronaphthalene 360 U 88-74-4---------2-Nitroaniline 720 U 131-11-3--------Dimethylphthalate 360 U . 208-96-8--------Acena hth lene 95 J P Y -- 606-20-2--------2,6-Dinitrotoluene _ 360 U 99-09-2---------3-Nitroaniline 720 U 83-32-9---------Acenaphthene 360 U FORM I SV-1 OLM03.0 ) 1C EPA SAMPLE'NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. :. MC1453 Matrix: (soil/water) SOIL Lab Sample. ID: C1453-06E Sample wt/vol: . 30.2 (g/mL) G Lab File ID: S2E2663 Level: (low/med) IOW Date Received: 11/18/04 o Moisture: 8 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04' Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: CONCENTRATION-UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 720 U 100-02-7--------4=Nitrophenol _ 720 U 132-64-9--------Dibenzofuran 360 U 121-14-2--------2,4-Dinitrotoluene 360 U 84-66-2----------Diethylphthalate 360 U 7005-72-3-------4-Chlorophenyl-phenylether_ 360 U 86-73-7---------Fluorene 38 J 100-01-6--------4-Nitroaniline 720 U 534-52-1--------4,6-Dinitro-2-methylphenol 720 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 360 U 101-55-3--------4-Bromophenyl-phenylether 360 U 118-74-1--------Hexachlorobenzene 360 U 87-86-5---------Pentachlorophenol_ 720 U 85-01-8---------Phenanthrene_ 280 J 120-12-7--------Anthracene 250 J 86-74-8---------Carbazole 360 U 84-74-2---------Di-n-butylphthalate 360 U 206-44-0--------Fluoranthene 2600 129-00-0--------Pyrene 2400 85-68-7---------Butylbenzylphthalate 360 U 91-94-1---------3,3 '-Dichlorobenzidine__ _ 360 U 56-55-3---------Benzo(a)anthracene 2200 218-01-9--------Chrysene 2400 117-81-7--------bis(2-EthylhexylTphthalate_ 70 J 117-84-0--------Di-n-octylphthalate 360 U 205-99-2--------Benzo(b)fluoranthene 270.0 207-08-9--------Benzo(k)fluoranthene 1300 50-32-8---------Benzo(a)pyrene 2400 193-39-5--------Indeno(1,2,3-c�yrene 960 53-70-3---------Dibenzo(a,h)anthracene 320 J 1.91-24-2--------Benzo(g,h,i)perylene 990 W - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS `ANALYSIS DATA SHEET.- -- SB8-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-10E.. Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2667 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 13 decanted:. (YIN) N Date Extracted:1-1/24/04 Concentrated Extract Voles: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N PH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 380 U 111-44-4--------bis(2-Chloroethyl)Ether 380 U 95-57-8---------2-Chlorophenol 380 U 541-73-1--------1,3-Dichlorobenzene 380 U 106-46-7--------1,4-Dichlorobenzene 380 U 95-50-1---------1,2-Dichlorobenzene 380 U 95-48-7---------2-Met-oxybishylpheno1 380 U 108-60-1--------2,2' (1-Chloropropane 380 U 106-44-5--------4-Methylphenol 380 U 621-64-7--------N-Nitroso-di-n-propylamine 380 U 67-72-1---------Hexachloroethane_ 380 U 98-95-3---------Nitrobenzene 380 U 78-59-1---------Isophorone 380 U 88-75-5---------2-Nitrophenol 380 U 105-67-9--------2,4-D!Zethylphenol 380 U 120-83-2--------2,4-Dichlorophenol 380 U 120-82-1--------1,2,4-Trichlorobenzene 380 U 91-20-3---------Naphthalene _ 380 U 106-47-8--------4-Chloroaniline 380 U 111-91-1--------bis(2-Chloroethoxy methane_ 380 U 87-68-3---------Hexachlorobutadiene 380 U 59-50-7---------4-Chloro-3-Methylphenol 380 U 91-57-6---------2-Methylnaphthalene 73 J 77-47-4---------Hexachlorocycicpentad e a 380 D 88-06-2---------2,4,6-Trichlorophenol 380 U 95-95-4---------2,4,5-Trichlorophenol 770 U 91-58-7---------2-Chloronaphthalene 380 U 88-74-4---------2-Nitroanniline 770 U 131-11-3--------Dimethylphthalate 380 U 208-96-8--------Acenaphthylene _ ^ 380 U 606-20-2--------2,6-Dinitrotoluene 380 U 99-09-2---------3-Nitroaniline 770 U 83-32-9---------Acenaphthene— 600 FORM. I SV=1 OLM03.0 SAMPLE NO. 1C. EPA' SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB8-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case-No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-10E Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2667 Level: (low/med) LOW Date Received: 11/18/04 o Moisture: 13 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC .Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 770 U 100-02-7--------4-Nitrophenol 770 U 132-64-9--------Dibenzofuran 340 LT 121-14-2--------2.,4-Dinitrotoluene 380 U. 84-66-2---------Diethylphthalate 380 U 7005-72-3-------4-Chlorophenyl-phenylether 380 U 86-73-7---------Fluorene 830- 10.0-01-6------=-4-Nitroaniline 770 II 534-52-1------ 4,6-Dinitro72-methylphenol 770 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 380 U 101-55-3--------4-Bromophenyl-phenylether 380 U 118-74-1--------Hexachlorobenzene 380 U 87-86-5---------Pentachlorophenol 770 U 85-01-8---------Phenanthrene 6600 E 120-12-7--------Anthracene 2700 86-74-8---------Carbazole 950 84-74-2---------Di-n-butylphthalate 380 U 206-44-0=-------Fluoranthene 9500 E 129-00-0--------Pyrene 8500 E 85-68-7---------Butylbenzylphthalate 380 U 91-94-1-------- 3,31-Dichlorobenzidine 380 U 56-55-3---------Benzo(a)anthracene 4700 218-01-9--------Chrysene 4800 117-81-7--------bis(2-Ethylhexyl)phthalate_ . 88 J 117-84-0--------Di-n-octylphthalate 380 U 205-99-2--------Benzo(b)fluoranthene 5100 207-08-9---------Benzo W fluoranthene 2200 50-32-8-7------=Benzo(a)pyrene 3600 193=39-5--------Indeno(1,2,3-cd)pyrene 1000 53-70-3---------Dibenzo(a,h)anthracene 360 J 191-24-2--------Benzo(g,h,i)perylene 970 (l�annot be separated from Diphenylamtne FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB8-2Dt Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : .MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453710EDL Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2706 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 13 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 2.0 - GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2---------Phenol _ 760 U 111-44-4---------bis(2- loroethyl) Ether 760 U 95-57-8---------2 Ch-Chlorophenol_ 760 U 541-73-1--------1,3-Dichlorobenzene 760 U 106-46-7--------1;4-Dichlorobenzene 760 U 95-50-1---------1,,2-Dichlorobenzene 760 U 95-48-7---------2-Methylphenol 760 U 108-60-1---------2,2' -oxybis(1-Chloropropane) 760 U 106-44-5--------4-Methylphenol 760 U 621-64-7--------N-Nitroso-di-n-propylamine_ 760 U 67-72-1---------Hexachloroethane 760 U 98-95-3---------Nitrobenzene 760 U 78-59-1---------Isophorone 760 U 88-75-5---------2-Nitropheiiol 760 U 105-67-9--------2,4-Dimethylphenol 760 U 120-83-2--------2,4-Dichlorophenol_ 760 U 120-82-1--------1,2,4-Trichlorobenzene 760 U 91-20-3---------Naphthalene 760 U 106-47-8--------4-Chloroanili.fie- 760 U 111-91-1--------bis(2-Chloroethoxy methane_ 760 U 87-68-3---------Hexachlorobutadiene 760 II 59-50-7---------4-Chloro-3-Methylphenol 760 U 91-57-6---------2-Methylnaphthalene 760 U 77-47-4---------Hexachlorocycicpentadien 760 U 88-06-2---------2,4,6-Trichlorophenol. 760 U 95-95-4---------2,4,5-Trichlorophenol 1500 U 91-58-7---------2-Chloronaphthalene 760 U 88-74-4---------2-Nitroaniline 1500 U 131-11-3--------Dimethylphthalate 760 U 208-96-8--------Acenaphthylene 760 U 60.6-20-2--------2,6-Dinitrotoluene 760 U 99-09-2---------3-Nitroaniline 1500 U 83-32-9---------Acenaphthene 600 DJ FORM I SV-1 OLNI03.0 1C EPA SAMPLE NO. SENIVDLATILE`ORGANICS ANALYSIS DATA'SHEET` SB8-2DL Lab Name: MITXEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-10EDL Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2706 Level: (low/med) IOW Date Received: 11/18/04 o Moisture: 13 decanted: (Y/N) .N Date Extracted:11/24/04 ` Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 2.0 - GPC Cleanup: (Y/N) N pH: _ CONCENTRATION UNITS CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 51-28-5----------2,4-Dinitrophenol 1500 U 100-02-7--------4-Nitrophenol—_ 1500 U 132-64-9--------Dibenzofuran 340 DJ 121-14-2--------2,4-Dinitrotoluene 760 U 84=66-2---------Diethylphthalate 760 U 7005-72-3-------4-Chlorophenyl-phenylether 760 U 86-73-7---------Fluorene 810 D 100-01-6--------4-Nitroaniline 1500 U 534-52-1--------4,6-Dinitro-2-methylphenol 1500 U 86-30-6---------N-Nitrosodiphenylamine (1) 760 U 101-55-3--------4-Bromophenyl-phenylether 760 U 118-74-1--------Hexachlorobenzene 760 U 87-86-5---------Pentachlorophenol 1500 U 85-01-8---------Phenanthrene 7000 D 120-12-7--------Anthracene 2800 D 86-74-8---------Carbazole 950 D 84-74-2---------Di-n-butylphthalate 760 U 206-44-0--------Fluoranthene_ 10000 D 129-00-0--------Pyrene 8000 D 85-68-7---------Butylbenzylphthalate 760 U 91-94-1---------3.,3'-Dichlorobenzidine 760 U 56-55-3---------Benzo(a)anthracene 4800 D 218-01-9--------Chrysene 4700 D 117-81-7--------bis(2-Ethylhexyl}phthalate_ 760 U 117-84-0--------Di-n-octylphthalate 760 U 205-99-2--------Benzo(b)fluoranthene 4200 D 207-08-9--------Benzo(k)fluoranthene 2300 D 50-32-8---------Benzo(a)pyrene 3400 D 193-39-5--------Indeno(1,2,3-cd)pyrene 1400 D 53-70-3---------Dibenzo(a,h)anthracene 460 DJ 191-24-2--------Benzo(g,h,i)perylene: 1400 D (1) Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1C EPA SAMPLE NO. SE TVOLATILE ORGANICS ANALYSIS DATA SHEET S2BLCSD Lab Name: MITKEM CORPORATION Contract: _ Lab Code: MTTKEM Case No. 4. SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2658 Y . Level: (low/med) IOW Date Received: ; Moisture: 0 decanted: (YIN) N Date Extracted:11/24/00 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 k Injection Volume: 1.OWL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol_ 950 100=02-7------- 4-Nitrophenol 1500 132-64-9--------Dibenzofuran 1500, 121-14-2--------2,4-Dinitrotoluene 1600 84-66-2---------Diethylphthalate 1300 7005-72-3-------4-Chlorophenyl-phenylether_ 1600. 86-73-7---------Fluorene 1600 100-01-6--------4-Nitroaniline 1.600 j 534-52-1--------4,6-Dinitro-2-methyiphenol 1200 86-30-6---------N-Nitrosodiphenylamine (1)_ 2000 101-55-3--------4-Bromophenyl-phenylether 1600 118-74-1--------Hexachlorobenzene 1600 87-86-5---------Pentachlorophenol 1300 85-01-8---------Phenanthrene _ 1600 120-12-7--------Anthracene 1600 86-74-8---------Carbazole 1800 84-74-2---------Di-n-butylphthalate 1700 206-44-0--------Fluoranthene 1600 129-00-0--------Pyrene 1500 85-68-7---------Butylbenzylphthalate 1600 91-94-1-------=-3,3' =Dichlorobenzidine 1200 56-55-3---------Benzo(a)anthracene 1600 218-01-9--------Chrysene 1800 117-81-7--------bis(2-Ethylh xyl)phthalate_ 1600 117=84-0--------Di-n-octylphthalate 1500 205-99-2--------Benzo(b) fluoranthene 1500 207-08-9--------Benzo(k) fluoranthene 160.0 50-32-8---------Benzo(a)pyrene 1600 193-39-5--------Indeno(1,2,3-cddpyrene 1600 53-70-3---------Dibenzo(a,h)anthracene 1600 191-24-2--------Benzo(g,h,i)perylene - 1600 (1) - Cannot be separated from Diphenylamne FORM I SV-2 OLM03.0 I' DATA PACKAGE ADDENDUM SEMIVOLATILE ORGANICS C 1453 Data Summary Forms, followed by Full Data Package Pages. 1B EPA SAMPLE NO. � SEMIVOLATILE ORGANICS ANALYSIS DATA-SHEET SB-X Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 / Matrix: (soil/water) SOIL Lab Sample ID: C1453-09E Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2660 Level: (low/med) LOW Date Received: 11/18/04 o Moisture: 14 decanted: (Y/N) N Date Extracted:11/24/04 r Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 380 U 103-33-3--------Azobenzene 380 U 98-86-2---------Acetophenone 380 U FORM .I SV-1 OLM03.0 1B EPA SAMPLE NO. SE4IVOLATILE ORGANICS ANALYSIS DATA SHEET. SB1-8 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM . Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-01E Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2669 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 8 decanted: (YIN), N ' Date Extracted:11/24/04-. i Concentrated Extract Volume: 1000(uL) Date Analyzed: 12'/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND _ (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 360 U 103-33-3--------Azobenzene 360 U 98-86-2---------Acetophenone` 360 U FORM I SV-1 OLM03 .0 EPA SAMPLE NO. SEMIVOLATILE ORGANICS.. ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: SB1-8DL _ 1 Lab Code: MITKEM Case No..: SAS No. : SDG No_ : MC1453 Matrix: (sail/water) SOIL Lab Sample ID: C1453-01EDL Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2707 Level: (low/med) IOW Date Received: 11/18/04 `6 Moisture: 8 decanted: (Y/N) N Date Extracted:11/24/04. Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/03/04 Injection Volume:' 1.0(uL) Dilution Factor: 4.0 -- GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 1400 U 103-33-3--------Azobenzene _ 1400 U 98=86-2---------Acetophenone 1400 U FORM I SV-1 OLM03.0 EPA.SAMPLE NO SEMIVOLATILE ORGANICS ANALYSIS DATA.'SHEE SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16E Sample wt/vol: . 30.2 (g/mL) G Lab File ID: S2E2668 Level: (low/med) LOW Date Received: 11/19/04 5 Moisture: . 6 decanted: (YIN) N Date. Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N. pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53=3---------Aniline 350 U 103=33-3----- Azobenzene 350 U 98-86-2---------Acetophenone 350 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2 Lab Name: MITKEM CORPORATION Contract: . Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-15C Sample wt/vol: 30.0 -(g/mL) G Lab File ID: S2E2664 Level: (low/med) LOW. Date Received: 11/19/04 Moisture: 4 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL). Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS• CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 340 U 103-33-3--------Azobenzene 340 U 98-86-2---------Acetophenone 340 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2MS Lab Name: MITKEM. CORPORATION Contract: Lab Code: MITKEM- Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453--1SCMS Sample wt/vol: 30.0. (g/mL) G Lab File ID: S2E266S Level: (low/med) LOW Date Received: 11/19/04 s Moisture: 4 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume- 1000 (uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 1100 E 103-33-3--------Azobenzene 1500 98-86-2---------Acetophenone 340 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB2-2MSD g Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MCI453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-15CMSD Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2666 Level: (low/med) LOW Date Received: 11/19/04 Moisture: 4 decanted: (YIN) N Date 'Extracted:11/24/04 Concentrated Extract Volume: 1000(UL) Date Analyzed: 12/02/04 Injection Volume: 1.0(UL) Dilution Factor: 1.0 -- GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 1200 E 103-33-3-------=Azobenzene 1600 98-86-2---------Acetophenone 340 U FORM I SV-1 OLMO3.0 IB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA. SHEET SB3-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-12E Sample wt/vol: 30.0 (g/mL) G Lab File. ID: S2E2661 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 9 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL)- Dilution Factor:. 1.0 . GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 360 U 103-33-3--------Azobenzene 360 U 98-86=2---------Acetophenone .360 U FORM I SV-1 OLM03.0 .1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA .SHEET SB4-14 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 matrix:-(soil/water) SOIL Lab Sample ID: C1453-14E Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2662. Level: (low/med) LOW Date Received: 11/19/04 Moisture: 3 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: . 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS.: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 340 U 103-33-3--------Azobenzene 340 U 98-86-2---------Acetophenone 340 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB5-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL. Lab Sample ID: C1453-06E Sample wt/vol: 30.2 (g/mL)- G Lab File ID: S2E2663 Level: (low/med) LOW Date Received: 11/18/04 o Moisture: . 8 decanted: (Y/N) N Da:te -Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1..0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: .CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 62-53-3---------Aniline 360 U 103-33-3--------Azobenzene 360 U 98-86-2---------Acetophenone 360 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB8-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-10E Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2667 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 13 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline _ 380 U 103-33-3--------Azobenzene 380 U 98-86-2---------Acetophenone 380 U . l FORM I SV-1 OLM03.0 lB EPA SAMPLE No SEM1VOLATILE ORGANICS ANALYSIS -DATA SHEET Lab Name: MITKEM CORPORATION• Contract: SB8-2DL Lab Code: MITT<EM Case' No. : SAS No. ; SDG No_ : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-10EDL Sample wt/vol: 30.0 -(g/mL) G Lab File ID: S2E2706 Level: (low/med) LOW Date Received: 11/18/04 Moisture: 13 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: - 1000(uL) Date Analyzed: 12/03/04 Injection Volume: : .1.0(uL) Dilution Factor: 2.0 - GPC-Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 760 U 103-33-3--=-----Azobenzene 760 U 98-86-2---------Acetophenone 760 U FORM I SV-1 0LM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SB9-8 Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample iD: C1453-04E Sample wt/vol: 30.1 (g/mL) G Lab File ID: S2E2659 Level: (low/med) IOW Date- Received: .11/18/04 Moisture: 15 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000 (uL) Date Analyzed:. 12/01/04 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 390 U 103-33-3--------Azobenzene 390 U 98-86-2----=----Acetophenone 390 U J FORM I SV-1 OLM03.0 ) 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2BLCS Lab Name: .MITKEM CORPORATION. Contract: Lab Code: -MITKEM Case No SAS No: : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2657 Level: (low/med) LOW Date Received: Moisture: 0 decanted: (YIN) N Date EXtracted:11/24/00 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N_. pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3----------Aniline 1000 E 103-33-3--------Azobenzene 1600 98-86-2---------Acetophenone 330 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO'. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2BLCSD Lab. Name.: MITKEM CORPORATION Contracts 1 Lab Code: MITKEM. Case No. : SAS No. : SDG No'. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCSD-15845 Sample wt/vol: 3.0.0 {g/mL) G Lab File ID: S2E2.658 Level: (low/med) LOW Date Received: o Moisture: 0 decanted: (YIN) N Date Extracted:11/24/00 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L. or ug/Kg) UG/KG Q 62-53-3---------Aniline: 1000 E 103-33-3--------Azobenzene 1700 98-86-2----------Acetophenone 330 U FORM I SV-1 OLM03.0 1 3D SOIL.SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.: MC1453 Matrix Spike -' EPA Sample No. : SB2-2 Level: (low/med) LOW SPIKE SAMPLE. MS MS QC. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. Aniline 1700 0.0 1100 65 40-140 Azobenzene 1700 0.0 1500 88 40-140 SPIKE MSD MSD ADDED CONCENTRATION o °s QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ---------------- --------- ------------- ------ ------ ------ ------ Aniline 1700 1200 70 7 30. 40-140 Azobenzene 1700 1600 94 6 30 40-140 # Column. to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out-of 4 outside limits CON24ENTS: FORM III SV-2 OLM03.0 FORM 3 SOIL SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No_ : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : S2BLCS Level: (low/med) LOW -- - SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. Aniline 1700 1000 59 40-140 Azobenzene 1700 1600 94 40-140 SPIKE LCSD LCSD ADDED CONCENTRATION o a QC LIMITS ==COMPOUND _(ug/Kg) = ===(ug/Kg)=== =REC-# -RPD-# -RPD== =REC. == Aniline 1700 1000 59 0 30 40-140 / Azobenzene 1700 1700 100 6 30 40-140 # Column to be used .to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out of 4 outside limits CONIl4ENTS: FORM III SV 4B . EPA SAMPLE NO. SEMIVOLATILE METHOD BLANK SL44MARY SBLK2B Lab Name: -MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File ID: S2E2656 Lab_ Sample ID: MB-15845 Instrument ID: S2 Date Extracted: 11/24/04 Matrix: (soil/water) SOIL Date Analyzed: 12/01/04 Level: (low/med) LOW Time. Analyzed: 1933 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD-: EPA LAB LAB DATE SAMPLE NO; SAMPLE ID FILE ID ANALYZED - -------------- -------------- ---------- :. 01 S2BLCS LCS-15845 S2E2657 12/01/04 02 S213LCSD LCSD-15845 S2E2658 12/01/04 03 SB9-8 C1453-04E S2E2659 12/01/04 04 SB-X C1453-09E S2E2660 12/01/04 05 SB3-6 C1453-12E S2E2661 12/01/04 06, SB4-14 C1453-14E S2E2662 12./01/04 07 SB5-2 C1453-06E S2E2663- 12/01/04 08 SB2-2 C1453-15C S2E2664 12/02/04 09 SB2-2MS C1453-ISCMS S2E2665 12/02/04 10 SB2-2MSD C1453-15CMSD S2E2666 12/02/04 11 SB8-2 C1453-10E S2E2667 12/02/04 12 SB10-2 C1453-16E. S2E2668 12/02/04 13 SB1-8 C1453-01E S2E2669 12/02/04 14 SB8-2DL C1453-10.EDL S2E2706 12/03/04 15 9B1-8DL C1453-01EDL S2E2707 12/03/04 16 17 - 18 - 19 - 20 - 21 22 23 24 25 26 27 28 - - 29 30 CONMENTS: page 1 of 1 FORM IV SV OLM03 .0 113 EPA.SAMPLE NO: SEMIVOLATILE ORGANICS ANALYSIS DATA `SHEET SBLK2B rt Lab Name: MITKEM CORPORATION Contract: l - Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2656 - Level: "(low/med) LOW Date Received: Ig Moisture: 0 decanted: (YIN) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000.(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - .GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 62-53-3---------Aniline 330 U 103-33-3--------Azobenzene 330 U 98-86-2---------Acetophenone 330 U FORM I SV-1 OLM03 .0 FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET SB-X Lab Name:. MITIC2K CORPORATION Contract: Lab Code: MITKE4 .Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-09E Sample wt/vol: . 30.0 (g/mL) G Lab File ID:'. E2E2655F t Moisture: 14 decanted: (YIN) N Date Received: 11/18/04 Extraction: (SepF/Cont/Sonc) SONG Date Extracted:11/30/04 Concentrated Extract Volume: 10000(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: , 1.0 GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 12674-11-2------Aroclor-1016 38 U 11104-28-2------Aroclor-1221 38 U 11141-16-5------Aroclor-1232 38 'U 53469-21-9------Aroclor-1242 38. U 12672-29-6------Aroclor-1248 38 U 11097-69-1------Aroclor-1254 38 U 11096-82-5------Aroclor-1260 38 U FORM I PCB FORM 1 CLIENT SAMPLE NO. - PCB ORGANICS ANALYSIS DATA SHEET._ -- SB1-8 Lab Name: MITKEK CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : .MC1453 Matrix: -(soil/water) SOIL Lab Sample ID: C1453-01E Sample wt/vol: 30.1 (g/mL) G Lab File ID: E2E2651F Moisture: 8 decanted: (Y/N) N Date Received: 11/18/04 Extraction: (SepF/font/Sonc) SONC Date Extracted:.11/30/04 Concentrated Extract Volume: 10000.(uL) Date Analyzed: 12/02/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 12674-11-2------Aroclor-1016 36 U 11104-28-2------Aroclor-1221 -36 U 11141-16-5------Aroclor-1232 36 U 53469-21-9------Aroclor-1242 36 U 12672-29-6------Aroclor-1248' 36 U 11097-69-1------Aroclor-1254 36 U 11096-82-5------Aroclor-1260 36 U 1 FORM I PCB FORM 1._ CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET SB10-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-16E. Sample wt/vol: 30.1 (g/mL) G' Lab. File ID: E2E2666F Moisture: 6 decanted: (YIN). N Date Received: 11/19/04 Extraction:. '(SepF/font/Sonc)- SONC Date Extracted:11/30/04 Concentrated Extract Volume: 10000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 _ GPC Cleanup: (Y/N) N PH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 4 12674-11-2------Aroclor-1016 35 U 11104-28-2---=--Aroclor-1221 35- U 11141-16-5------Aroclor-1232 35 U 53469-21-9------Aroclor-1242 35 U 12672-29-6------Aroclor-1248 35 U. 11097-69-1------Aroclor-1254 48 11096-82-5------Aroclor-1260 35. U FORM I -PCB FOR 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET - SB2-2 Lab Name: MITKEM CORPORATION Contract: Lab Code MITKEM Case No. : SAS No. : . .SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: C1453-15C Sample wt/vol: 30.0- (g/mL) G Lab File ID: E2E2.663F Moisture: 4 decanted: (YIN) N Date Received: 11/19/04 Extraction: (SepF/font/Sonc) SONG Date Extracted:11/30/04 Concentrated Extract Volume: 10000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 12674-11-2------Aroclor-1016 34 U 11104-28-2------Aroclor-1221 34 U 11141-16-5------Aroclor-1232 34 U 53469-21-9------Aroclor-1242 34 U 12672-29-6------Aroclor-1248 34 U 11097-69-1------Aroclor-1254 34 U 11096-82-5------Aroclor-1260 34 U FORM I PCB FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET SB2-2MS Lab Name: MITKEM CORPORATION Contract: !Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: -C1453-15CMS Sample wt/vol: 30.0 (g/mL) G Lab .File ID: E2E2664F Moisture: 4 decanted: (Y/N) N Date Received: 11/19/04 Extraction: (SepF/font/Sons) SONC Date Extracted:ll/30/04 Concentrated Extract Volume: 10000(uL) Date Analyzed: 12/03/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG C2 12674-11-2------Aroclor-1016 _ 290 11104-28-2------Aroclor-1221 34 U 11141-16-5------Aroclor-1232 34 U 53469-21-9------Aroclor-1242 34 U 12672-29-6------Aroclor-1248 34 U 11097-69-1------Aroclor-1254 34 U 11.096-82-5------Aroclor-1260 300 FORM I PCB U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET SBS-2 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No. SAS No. : SDG No_ : MC1453 Matrix (soil/water) : SOIL Lab Sample ID: C1453-06 Level (low/med) : MED Date Received: 11/18/04 ' % Solids: 92.0 Concentration Units (ug/L or mg/kg dry weight) : MG/KG CAS No. Analyte Concentration C Q M 7440-36-0 Antimony 1.1 U P 7440-38-2 Arsenic 2.1 P 7440-39-3 Barium 25.4 P 7440-41-7 Beryllium 0.32 U1 P 7440-43-9 Cadmium 1.2 P 7440-47-3 Chromium 243 P 7439-92-1 Lead 40.5 P 7440-02-0 Nickel 8.6 P 7782-49-2 Selenium 1.6 U P 7440-22-4 Silver 4.0 P 7440-28-0 Thallium 1.1 U p 7440-62-2 Vanadium 12.3 * P 7440-66-6 Zinc 52.2 * P 7439-97-6 Mercury 0.044 * CV Cyanide N CA PiO 6-4146Y 1 Comments: i it i FORM I - IN SW846 f, - 1 _ U.S_ EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET 1 SB-X Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No. SAS No. : SDG No_: MC1453 Matrix {soil/water) : SOIL Lab. Sample ID: C1453-09 Level (low/med) : MED Date Received: 11/18/04 Solids: 86.0 Concentration Units (ug/L or mg/kg dry weight) : MG/KG CAS No_ Analyte Concentration C Q M 7440-36-0 Antimony 1.1 U P 7440-38-2 Arsenic 2.1 P 7440-39-3 Barium 13_5 P 7440-41-7 Beryllium 0.33 U P 7440-43-9 Cadmium 1.1 P 7440-47-3 Chromium 564 P 7439-92-1 Lead . 7:6 P 7440-02-0 Nickel 8.0 P 7782-49-2 Selenium 1.6 U P 7440-22-4 Silver 4.1 P 7440-28-0 Thallium. 1.1 U P 7440-62-2 Vanadium 13.4 * P 7440-66-6 Zinc 30.9 * P 7439-97-6 Mercury 0.035 U * Cv Cyanide N CA Comments: FORM I - IN SW846. 2D SOIL SFIKIVOLATILE SURROGATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No_ : SDG No. : MC1453 Level: (low/med) LOW EPA SI S2 S3 S4 S5 S6 S7 S8 TOT SAMPLE NO. (NBZ)# (FBP)# (TPH)# (PHL)# (2FP)# (TBP)# # # OUT ------------ ------ ------ ------ - 01 SBLK2B 88 90 97 86 85 95. 0 02 S2BLCS 91 92 94 92 89 98 0. 03 S2BLCSD 88 93 90 90 88 99 0 04 SB9-8 68 71 73 69 68 74 0 05 SB-X 79 81 82 78 79 82 0 06 SB3-6 106* 81 81 -88 98* 82 2 07 SB4-14 80 82 86 78 80 83 0 08 SB5-2 73 76 80 73 71 60 0 09 SB2-2 81 86 90 81 80 80 0 10 SB2-2MS 77 81 83 76 76 79 0 11 SB2-2MSD 75 80 84 75 76 80 0 12 SB8-2 86 90 108 82 81 89 0 13 SB10-2 85 89 112 86 84 81 0 14 SB1-8 123* 89 167* 96 93 90 2 . 15 SB8-2DL 90 91 87 84 85 84 0 16 SB1-8DL 124D 90 101 84 81 86 0 17 18 19 20 21 22 23 24 25 26 27 2829 f 30 QC LIMITS S1 (NBZ) = Nitrobenzene-d5 (46-102) S2 (FBP) = 2-Fluorobiphenyl (52-107) S3 (TPH) = Terphenyl-d14 (61-113) S4 (PHL) = Phenol-d5 (45- 99) - S5 (2FP) = 2-Fluorophenol (44- 95) S6 (TBP) = 2,4,6-Tribromophenol (50-111) # Column to be used to flag recovery values. * Values outside of contract required QC limits D Surrogate diluted out page 1 of 1 FORM II SV-2 OLM03.0 x: FORM 2 SOIL PCB SURROGATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 GC Column(1) : RTXCLPPEST ID: 0.53. (mm) GC Column(2) RTXCLPPEST 2 ID: 0.53 (mm) CLIENT TCX 1 TCX 2 DCB 1 DCB 2 OTHER OTHER TOT SAMPLE NO. %-REC # oREC # %REC # %REC # (1) - (2) OUT ------------ ------ ------ ------ ------ ------ ------ --- 01. PBLK2A 79 79 74 69 0 02 P2ALCS 86 86 80 76 0 03 P2ALCSD. 87 87 82 77 -- -- — 0 04 SB1-8 54 136 46 45 0 05 SB7-2 54 129 169* 56 _ 1 06 SB9-8 80 79 65 62 0 07 SB5-2 78 78 71 66 0 08 SB-X 69 70 64 60 _ 0 09 SB8-2 70 103 115 74 0 10 SB2-2 82 83 74 72 0 11 SB2-2MS 83 83 73 72 0 12 SB2-2MSD 87 87 72 72 _0 13 SB10-2 70 72 58 56 . 0 14 15 16 17 18 19 _ 20 21 22 23 24 25 - 26 27 28 29 30 ADVISORY QC LIMITS S1 (TCX) = Tetrachloro-m-xylene , (42-147) S2 (DCB) = Decachlorobiphenyl (29-155) # Column to be used to flag recovery values * Values outside of QC limits D Surrogate diluted out page 1 of 1 FORM II PCB _ - x- T' . 1. 3B SOIL VOLATILE MATRIX SPIRE/MATRIX SPIRE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITREM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - EPA Sample No. : SB5-2 Level: (low/med) IOW SPIRE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUDID (ug/Kg) (ug/Kg) (ug/Kg) REC ## REC. _______________ _________ _____________ _____________ ______ _____ Dichlorodifluoromethane 53 0.0 45 85 58-131 Chloromethane 53 0.0 49 92 63-120 Vinyl Chloride 53 0.0 45 85 61-134 Bromomethane 53 0:0 50 94 10-2-15 Chloroethane 53 0.0 49 92 55-146 Trichlorofluoromethane 53 3 60 108 63-126 1,1-Dichloroethene 53 0.0 50 94 67-127 Acetone 53 14 88 140 0-154 Carbon Disulfide 53 0.0 32 60* 63-126 Methylene Chloride 53 10 48 72 62-128 trans-1,2-Dichloroethen 53 0.0 45 85 76-120 Methyl tert-butyl ether . 110 0.0 110 100 52-130 1,1-Dichloroethane 53 0.0 48 90 74-118 2-Butanone 53 0..0 72 136 14-154 cis-1,2-Dichloroethene 53 0.0 51 96 83-115 ,2,2-Dichloropropane 53 0.0 50 94 64-125 Bromochloromethane 53 0.0 50 94 70-119 Chloroform 53 0.0 45 85 77-120 Tetrahydrofuran 53 0.0 85 160* 70-130 1,1,1-Trichloroethane 53 0.0 50 94 72-126 1,1-Dichloropropene 53 .0.0 47 89 71-132 Carbon Tetrachloride 53 0.0 49 92 69-135 1,2-Dichloroethane 53 0.0 52 98 65-126 Benzene 53 0.0 49 92 78-121 Trichloroethene. 53 0.0 50 94 75-125 1,2-Dichloropropane 53 0.0 50 94. 78-111 Dibromomethane 53 0.0 52 98 65=125 Bromodichloromethane 53 0.0 51 96 75-118 Column to be used to flag recovery and RPD Values with an asterisk * Values outside of QC limits COY24ENTS: page 1 of 6 FORM III VOA-2 OLM03.0 3B SOIL VOLATILE MATRIX SPIRE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453. Matrix Spike - EPA Sample No. : SB5-2 Level: (low/coed) LOW SPIRE SAMPLE MS MS QC. ADDED. CONCENTRATION CONCENTRATION !k LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. ------------------------ -------- -- cis-1,3-Dichloropropene 53 0.0 52 98 78-120 4 Methyl-2-pentanone 53 0.0 64 121 45-141 Toluene 53 0.0 51 96 80-126 trans-1,3-Dichloroprope 53 0.0 53 100 73=123 1,1,.2-Trichloroethane 53 0.0 52 98 66-125 1,3-Dichloropropane 53 0.0 54 102 76-119 Tetrachloroethene 53 25 78 100 65-134 2-Hexanone 53 0.0 72 136 37-136 Dibromochloromethane 53 0-0 53 100 76-115 1,2-Dibromoethane 53 0.0 55 104 72=117 Chlorobenzene .53 0:0 50 94 78-117 1,1,1,2-Tetrachloroetha 53 0.' 0 51 96 80-115 Ethylbenzene 53 o.0 53 160 19-129 Xylene (Total) 160 3 160 98 83-125 Styrene 53 0.0 54 102 83-122 Bromoform 53 0.0 56 106 67-126 Isopropylbenzene 53 0.0 52 98 80-135 1,1;2,2-Tetrachloroetha 53 0.0 60 113 70-117 \ Bromobenzene 53 0.0 55 104 79-119 1-,2,3-Trichloropropane 53 0.0 61 115 0.-154 n-Propylbenzene 53 0.0 51 96 64-141 2-Chlorotoluene 53 0.0 52 98 70-132 1,3,5-Trimethylbenzene 53 0.0 54 102 72-133 4-Chlorotoluene 53 0.0 53 100 77-122 tert-Butylbenzene 53 0.0 51 96 31-159 1,2,4-Trimethylbenzene 53 2 55 100 73-126 sec-Butylbenzene 53 0.0 49 92 68-137 4-Isopropyltoluene 53 0.0 48 90 66-131 Column to be used to flag recovery- and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III VOA-2 OLM03.0 3B SOIL VOLATILE MATRIX SPIKE/MATRIX 'SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - EPA Sample No. :. SB5-2 Level: (low/med) LOW SPIKE SAMPLE MS MS QC ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC ## REC. ------------ --------- ------------- ------------- ------ ------ 1,3-Dichlorobenzene 53 0.0 50 94 75-115 1,4-Dichlorobenzene. 53 0.0 48 90 72-110 n-Butylbenzene 53 0.0 45 85 66-130 1,2-Dichlorobenzene 53 0.0 53 100 78-113 1,2-Dibromo-3-chloropro 53 0.0 65 123 52-128 1,2,4-Trichlorobenzene 53 0.0 44 83 49-126 Hexachlorobutadiene 53 0.0 26 49* 58-115 Naphthalene 53 0.0 56 106 45-130 1,2,3-Trichlorobenzene 53 0.0 41 77 44-131 Ether 53 0.0 57 108 70-130 Diisopropyl Ether 53 0.0 61 115 70-130 Ethyl tert-butyl ether 53 0.0 63 119 70-130 tert-Amyl methyl ether 53 0.0 70 132* 70-130 1,4-Dioxane 1100 0.0 1200 109 65-135 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III VOA-2 OLM03.0 3B SOIL VOLATILE MATRIX -SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - EPA Sample No. : SB5-2 Level: (low/med) LOW -- SPIKE MSD MSD ADDED CONCENTRATION % w QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ------ --------- ------------- ------ ------ ------ ------ Dichlorodifluoromethane 70 59 84 1 40 58-131 Chloromethane 70 56 80 14 40 63-120 Vinyl Chloride 70 58 83 2 40 61-134 Bromomethane 70 62 88 6 40 10=215 - Chloroethane 70 60 86 7 40 55-146 Trichlorofluoromethane 70 58 78 32 40 63-126 1,1-Dichloroethene 70 62 88 6 40 67-12.7 Acetone 70 130 166* 17 40 0-154 Carbon Disulfide 70 37 53* 12 40 63-126 Methylene Chloride 70 60 71 1 40 62-128 trans-1,2-Dichloroethen ..70 60 86 1 40 76-120 Methyl tert-butyl ether 140 150 107 7 40 52-130 1,1-Dichloroethane 70 65 93 3. 40 74-118 2-Butanone 70 100 143 5 4.0 14-154 cis-1,2-Dichloroethene 70 69 98 2 40 83-115 2,2-Dichloropropane 70 65 93 1 40 64-125 Bromochloromethane 70 67 96 2 40 70-119 Chloroform 70 59 84 1 40 77-120 Tetrahydrofuran 70 110 157* 2 40 70-130 1,1,1-Trichloroethane 70 65 93 1 40 72-126 1,1-Dichloropropene 70 63 90 1 40 71-132 Carbon Tetrachloride 70 63 90 2 40 69-135 1,2-Dichloroethane 70 70 100 2 40 65-126 Benzene 70 67 96 4 40 78-121 Trichloroethene 70 110 157* 50* 40 75-125 1,2-Dichloropropane 70 66 94 0 40 78-117 Dibromomethane 70 68 97 1 40 65-125 Bromodichloromethane 70 66 94 2 40 75-118 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III. VOA-2 OLM03.0 3B SOIL VOLATILE MATRIX SPIKE/MATRIX 'SPIKE DUPLICATE.RECOVERy Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. ,.; SDG No. : MC1453 Matrix Spike - EPA Sample No. : SB5.-2 Level: (low/med) LOW -- SPIKE MSD MSD ADDED CONCENTRATION o %- QC LIMITS COMPOUM (ug/Kg.) (ug/Kg). REC # RPD .# RPD REC. cis-1,3-Dichloropropene 70 69 98 0 40 78-120 4-Methyl-2-pentanone 70 86 123 2 40 45-141 Toluene 70 67 96 0 40 80-126 trans-.1,3-Dichloroprope 70 69 98 2 40 73=123 1,1,2-Trichloroethane 70. 66 94 4 - 40 66-125 1,3-Dichloropropane 70 74 106 4 40. 76-119 Tetrachloroethene 70 140 164* 48* 40 65-134 2-Hexanone 70 110 157* 14 40 37-136 Dibromochloromethane 70 72 103 3 40 76-115 1,27Dibromoethane 70 76 108 4 40 72-117 Chlorobenzene 70 67 96 2 40 78-117 1,1,1,2-Tetrachloroetha 70 69. 98 2 40 80-115 Ethylbenzene 70 72 103 3 40 79=129 Xylene (Total) 210 220 103 5 40 83-125 Styrene 70 70 100 2 40 83-122 Brom,oform 70 74 106 0. 40 67-126 Isopropylbenzene 70 71 101 3 40 80-135 1,1;2,2-Tetrachloroetha 70 7 10* 167* 40 70-117 Bromobenzene 70 76 108 4 40 79-119 1,2,3-Trichloropropane 70 89 127 10 40 0-154. n-Propylbenzene 70 73 104 8 40 64-141 2-Chlorotoluene 70 73 104 6 140 70-132 1,3,5-Trimethylbenzene 70 74 106 4 40 72-133. 4-Chlorotoluene 70 72 103 3 40 77-122 tert-Butylbenzene 70 .61 87 10 40 31-159 1,2,4-Trimethylbenzene 70 75 104 4 40 73-126 sec-Butylbenzene 70 67 96 4 40 68-137 4-Isopropyltoluene 70 66 94 4 40 66-131 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COM ENTS: page 5 of 6 FORM III VOA-2 OLM03.0 3B SOIL VOLATILE MATRIX SPIKE/MATRIX SPIRE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 J Matrix Spike - EPA Sample No. : SB5-2 Level:_(low/med) LOW SPIKE MSD MSD ADDED ' CONCENTRATION QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. _________ _____________ ______ _____= ====== ====== z- 1,3-Dichlorobenzene 70 66 .94. 0 40 75-115 1,4-Dichlorobenzene 70 64 91 1 40 72-110 n-Butylbenzene 70 61 87 2 40 66-130 1,2-Dichlorobenzene 70 68 97 3 40 78-113 1,2-Dibromo-3-chloropro 70 90 128 4 40 52-128 1,2,4-Trichlorobenzene 70 53 76 9 40 49-126 Hexachlorobutadiene 70 36 51* 4 40 58-115 .Naphthalene 70 73 104 2 40 45-130 1,2,3-Trichlorobenzene 70 53 76 1 40 44-131 Ether . 70 76 108 0 40 70-130 Diisopropyl Ether 70 80 114 1 40 70-130 Ethyl tert-butyl ether 70 85 121. 2 40 70-130 tert-Amyl methyl ether 70 92 131* 1 40 70-130 1,4-Dioxane 1400 1600 114 4 40 65-135 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 3 out of 70 outside limits Spike Recovery: 13 out of 140 outside limits COMMENTS: 1 page 6 of 6 FORM III VOA-2 OLM03.0 FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITICEM CORPORATION Contract: Lab Code: MITICEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V2.SLCS Level: (low/med) LOW SPIRE SAMPLE LCS LCS QC. ADDED- CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Rg) (ug/Rg) (ug/Rg) REC # REC. i Dichlorodifluoromethane 50 58 116 58-131 Chloromethane 50 47 94 63-120 Vinyl Chloride 50 48 96 61-134- Bromomethane 50 46 92 10=215 Chloroethane 50 47 94 55-146 -Trichlorofluoromethane 50 46 92 63-126 1.,.l-Dichloroethene 50 46 92 67-127 1�cetone 50 67 134 0454 Carbon Disulfide 50 47 94 - 63-126 Methylene Chloride . 50 39 78 62-128 trans.-1,2-Dichloroethen 50 46 .92 76-120 Methyl tert-butyl ether .100 94 94 52-130 1,1-Dichloroethane 50 45 90 74-118 2-Butanone 50 64 128 14-154 cis-1,2-Dichloroethene 50 48 96 83-115 2,2-Dichloropropane 50 52 104 64-125 Bromochloromethane 50 45 90 70-119 Chloroform 50 42 84 77-120 Tetrahydrofuran 50 70 140* 70-130 1,1,I-Trichloroethane 50 48 96 72-126 1,1-Dichloropropene 50 49 98 71-132 Carbon Tetrachloride 50 49 98 69-135 1,2-Dichloroethane 50 46 92 65-126 Benzene 50 47 94 78-121 Trichloroethene 50 47 94 75-125 1,2-Dichloropropane 50 45 90 78-117 Dibromomethane 50 45 90 65-125 Bromodichloromethane 50 45 90 75-118 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 1 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MITK M Case No. : SAS No. : SDG No. : MC1453 / Matrix Spike - Sample No. : V2SLCS Level: (low/med) LOW SPIRE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION %, LIMITSI COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. ------- --------- ------------- ------------- ------ ------ cis-1,3-Dichloropropene 50 48 96 78-120 4-Methyl-2-pentanone 50 56 112 45-141 Toluene 50 50. 100 80-126 trans-1,3-Dichloroprope 50 49 98 73-123 .1,1,2-Trirhloroethane 50 45 90 66-125 1,3-Dichloropropane 50 48 96 76-119 Tetrachloroethene 50 50 100 .65-134 2-Hexanone 50 69 138* 37-136 Dibromochloromethane 50 47 94 76-115 1,2.-Dibromoethane 50 49 98' 72-117 Chlorobenzene 50 48 96 78-117 1,1,1,2-Tetrachloroetha 50 47 94 80-115 Ethylbenzene 50 .54 108 79-129 Xylene (Total) 150 160 107 83-125 Styrene 50 53 106 83-122 Bromoform 50 49 . 98 67-126 Isopropylbenzene 50 57 114 80-135 1,1,2,.2-Tetrachloroetha 50 47 94 70-117 Bromobenzene 50 48 96 79-115 1,2,3-Trichloropropane 50 49 98 0-154 n-Propylbenzene 50 52 104 64-141 2-Chlorotoluene 50 49 98 70-132 1,3,5-Trimethylbenzene 50 52 104 72-133 4-Chlorotoluene 50 49 98 77-122 tert-Butylbenzene 50 52 104 31-159 1,2.,4-Trimethylbenzene 50 52 104 73-126 sec-Butylbenzene 50 52 104 68-137 4-Isopropyltoluene 50 52 104 66-131 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON24ENTS: page 2 of 6 FORM III VOA FORM 3 . SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V2SLCS Level: (low/med) LAW SPIRE SAMPLE LCS LCS QC� ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. -------------- _____________ ------ ---------- --------- ------------- ------ ______ 1,3-Dichlorobenzene 50 5 48 96 75-11 1,4-Dichlorobenzene 50 46 92 .7 -11 n-Butylbenzene 50 54 108. 66-130 1,2-Dichlorobenzene 50 48 96 '78-113 1,2-Dibromo-3-chloropro .50 52 104 52-128 1,2,4-Trichlorobenzene 50 52 104 49-126 Hexachlorobutadiene 50 50 100 58-115 Naphthalene 50 56 112 45-130 1,2,3-Trichlorobenzene 50 52 104 44-131 Ether 50 50 100 70-130 Diisopropyl Ether 50 54 108 70-130 Ethyl tert-butyl ether 50 53 106 70-130 tert-Amyl methyl ether 50 58 116 70-130 1,4-Dioxane 1000 1000 100 65-135 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE. Lab Name: MITKEM CORPORATION Contract: Lab- Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike Sample No. : V2SLCS Level: (low/med) IOW SPIKE LCSD LCSD ADDED CONCENTRATION %- . %; QC LIMITS COMPOUND (ug/Kg) (ug/Kg) RFC # RPD ## RPD REC. - ----------------- --------- ------------ ------ ------ ------ ------ - Dichlorodifluorcmethane 50 67 134* 14 40 58-131 Chloromethane 50 48 96 2 40 63-120 Vinyl Chloride 50 48 96 0 40 61-134` Bromomethane 50 47, 94 2 40 10-215 Chloroethane 50 47 94. 0 40 55-146 Trichlorofluoromethane 50 40 80 14 40 63-126 1,1-Dichloroethene 50 47 94 2 40 67-127 Acetone 50 57 114 16 40 0-154 Carbon.Disulfide 50 48 96 2 40 63-126 Methylene" Chloride 50 40 80 2 40 62-128 trans-1,2-Dichloroethen 50 47 94 2 40 76-120 Methyl tert-butyl ether 100 95 95 1 40 52-130 1,1-Dichloroethane 50 45 90 0 40 74-118 2-Butanone 50 54 108 17 40 14-154 cis-1,2-Dichloroethene 50 49 98 2 40 83-115 .2,2-Dichloropropane 50 51 102 2 40 64-125 Brcmochloromethane 50 44 88 2 40 70-119 Chloroform 50 42 84 0 40 77-120 Tetrahydrofuran 50 .67 134* 4 40 70-130 1,1,1-Trichloroethane 50 48 96 0 40 72-126 1, 1-Dichloropropene 50 48 96 2 40 71-132 Carbon Tetrachloride 50 47 94 4 40 69-135 1,2-Dichloroethane 50 45 90 2 40 65=126 Benzene 50 47 94 0 40 78-121 Trichloroethene 50 48 96 2 40 75-125 1,2-Dichloropropane 50 45 90 0 40 78-117 Dibromomethane 50 44 88 2 40 65-125 Bromodichloromethane 50 44 88 2 40 75-118 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CONP+IE24TS page 4 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V2SLCS Level: (low/med) LOW SPIKE LCSD LCSD ADDED CONCENTRATION % % QC LIMITS COMPOUND ADDED Aug/Kg) REC # RPD # RPD REC.. cis-1,_3-Dichloropropene 50 48. 96 0 40 78-120 4-Methyl-2-pentanone 50 49 98 13 40 45-141 Toluene 50 49 98 2 40 80-126 trans-1,3-Dichloroprope 50 44 88 11 40 73-123 1,1,2-Trichloroethane 50 44 88_ 2 40 66-125 1,3-Dichloropropane 50 48 96 0 40 76-119 Tetrachloroethene 50 51 102 2 40 65-134 2-Hexanone 50 58 116 17 40 37-136 Dibromochloromethane 50 46 92 2 40 76-115 1,2-Dibromoethane 50 48 96 2 40 72-117 Chlorobenzene 50 48 96 0 40 78-117 1,1,1,2-Tetrachloroetha 50 47 94 0 40 80-115 Ethylbenzene 50 54 108 0 40 -79-129 Xylene (Total) 150 160 107 0 40 83-125 Styrene 50 52 104 2 40 83-122 Bromoform. 50 47 94 4 40 67-126 Isopropylbenzene 50 56 112 2 40 80-135 1,1,2,2-Tetrachloroetha 50 45 90 4 40 '70-117 Bromobenzene 50 50 100 4 40 79-119 1,2,3-Trichloropropane 50 45 90 8 40 0-154 n-Propylbenzene 50 51 102 2 40 64-141 2-Chlorotoluene 50 49 98 0 40 70-132 1,3,5-Trimethylbenzene 50 52 104 0 40 72-133 4-Chlorotoluene 50 48 96 2 40 77-122 tert-Butylbenzene 50 53 106 2 40 31-159 1,.2,4-Trimethylbenzene 50 53 106 2 40 73-126 sec-Butylbenzene 50 53 106 2 40 68-137 4-Isopropyltoluene 50 52 104 0 40 66-131 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB .CONTROL SAMPLE. Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 / Matrix Spike Sample No. : V2SLCS Level: (low/crud) IOW SPIKE LCSD LCSD ADDED CONCENTRATION . W QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ----------- --------- ------------- ------ ------ ------ ------ 1,3-Dichlorobenzene 50 48 96 0 40 75-115 1,4-Dichlorobenzene 50 47 94 2 40 72-110 n-Butylbenzene 50 53 106 2 40 66-130 1,2-Dichlorobenzene 50 48 96 0 40 78-113 1,2-Dibromo-3-chloropro 50 50 100 4 40 52-128 1,2,4-Trichlorobenzene 50 54 108 4 40 49-126 Hexachlorobutadiene 50 50 100 0 40 58-115 Naphthalene 50 57 114 2 40 45-130 1,2,3-Trichlorobenzene 50 53 106 2 40 44-131 Ether 50 49 98 2 40 70-130 Diisopropyl Ether 50 55 110 2 40 70-130 Ethyl .tert-butyl ether 50 55 110 4 40 70-130 tert-Amyl methyl ether 50 59 118 2 40 70-130 1,4-Dioxane 1000 980 98 2 40 65-135 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 70 outside limits Spike Recovery: 4 out of 140 outside limits COMMENTS: page 6 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SW No..: MC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) LOW — SPIKE SAMPLE LCS LCS . ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/Kg). (ug/Kg) (ug/Kg) REC #k REC. Dichlorodi.fluoromethane 50 42 84 58-131 Chloromethane 50 42 84. 63-120 Vinyl Chloride 50 44 88 61-134 Bromomethane 50 45 90 10-215 Chloroethane 50 44 88 55-146 Tr .chlorofluoromethane . 50 53 106 63-126 1,1-Di.chloroethene 50 46 92 67-127 Acetone 50 64 128 0-154 Carbon Disulfide 50 46 92 63-126 Methylene. Chloride 50 35 70 62-128 trans-1,2-Dichloroethen 50 46 92 ' 76-120 Methyl tert-butyl ether 100 99 99 .52-130 1,1-Dichloroethane 50 46 92 74-118 2-Butanone 50 58 116 14-154 cis-1,2-Dichloroethene 50 48 96, 83-115 2,2-Dichl- oropropane 50 49 98 64-125 Bromochloromethane 50 44. 88 70-119 Chloroform 50 42 84 77-120 Tetrahydrofuran 50 70 140* 70-130 1,1,1-Trichloroethane 50 47 94 72-126 1,1-Dichloropropene 50 47 94 71-132 Carbon Tetrachloride 50 47 94. 69-135 . 1,2-Dichloroethane. 50 46 92 65-126 Benzene 50 47 94 78-121 Trichloroethene 50 47 94 75-125 1,2-Dichloropropane 50 46 92 78-117 Dibromomethane 50 46 92 65-125 Bromodichloromethane 50 45 90 75-118 Column to be used to flag recovery RPD values with an asterisk * Values outside of QC limits COMMENTS: page 1 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: l Lab Code: 1ITICEM! ' Case No. .-; SAS No. SDG No.' : MC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) LOW SPIRE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION %- LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC REC. cis-1,3-Dichloropropene 50 49 98 78-120 4-Methyl-2-pentanone 50 55 110 45-141 Toluene 50 49 98 80-126 trans-1,3-Dichloroprope 50 50 100 73=123 1,1,2-Trichloroethane 50 46 92 66-125 1,3-Dichloropropane 50 49 98 76-119 Tetrachloroethene 50 48 96 65-134 2-Hexanone 50 66 132 37-136 Dibrornochloromethane 50 48 96 76-115 1,2-Dibromoethane 50 .50 100 72-117 Chlorobenzene 50 48 96 78-117 1,1,1,2-Tetrachloroetha 50 46 92 80-115 Ethylbenzene 50 53 106 79-129 Xylene (Total) 150 160 107 83-125 Styrene 50 52 104 83-122 Bromoform 50 49 9.8 67-126 Isopropylbenzene 50 56 112 80-135 1,1,2,2-Tetrachloroetha 50 50 100 70-117 Bromobenzene 50 49 98 79-119 1,2,3-Trichloropropane 50 52 104 0-154 n-Propylbenzene 50 52 104 64-141 2-Chlorotoluene 50 50 i00 70-132 1,3,5-Trimethylbenzene 50 53 106 72-133 4-Chlorotoluene 50 50 100 77-122 tert-Butylbenzene 50 53 106 31-159 1,2,4-Trimethylbenzene 50 53 106 73-126 sec-Butylbenzene 50 54 108 687137 4-Isopropyltoluene 50 52 104 66-131 Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON04ENTS: page 2 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE. Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No: : NIC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) LOW SPIKE SAMPLE LCS LCS QC� ADDED CONCENTRATION FCONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) ug/Kg) REC # REC. _________ .1,3-Dichlorobenzene 50 49 98 75-115 1,4-Dichlorobenzene 50 47 94 72-110 n-Butylbenzene 50 55 110 66-130 .1,2-Dichlorobenzene 50 49 98 78-113 1,2-Dibromo-3-chloropro 50 52 104 52-128 1,2,4-Trichlorobenzene '50 54 108 49-126 Hexachlorobutadiene 50 50 100 58-115 Naphthalene 50 58 116 45-130 1,2,3-Trichlorobenzene 50 54 108 44-131 Ether 50 50 100 70-130 Diisopropyl Ether 50 58 116 70-130 Ethyl tent-butyl ether- 50 56 112 70-130 tert-Amyl methyl ether 50 62 124 70-130 1,4-Dioxane 1000 960 96 65-135 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CONIl�NTS: page 3 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB -CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MI- Case No. : SAS No. . SDG No. : MC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) TOW SPIKE LCSD LCSD ADDED CONCENTRATION ! QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. --=--------------------- -----=--- ------------- ------ ------ ------ ------ ------------------------ --------- ------------- ------ ------ ------ ------ Dichlorodifluoromethane 50 41 82 2 40 58-131 Chloromethane 50 40 80 , 5 40 63-120 Vinyl Chloride 50 43 86 2 40 61-13.4 . Bromomethane 50 44 88 2 40 10-215 Chloroethane. 50 43 86 2 40 55-146 Trichlorofluoromethane 50 41 .82 26 40 63-126 1,1-Dichloroethene 50 45 90 2 40 67-127 Acetone 50 52 104 21 40 0-154 Carbon Disulfide 50 45 90 2 40 63-126 Methylene Chloride 50 .35 70 0 40 62-128 trans-1,2-Dichloroethen 50 45 90 2 40 76-120 Methyl tert-butyl ether 100 92 92 7 40 52-130 1:,1-Dichloroethene 50 45 90 2 40 74-118 2-Butanone 50 53 106 9 40 14-154- cis-1,2-Dichloroethene 50 48 96 0 40 83-115 2,2-Dichloropropane 50 49 98 0 40 64-125 Bromochloromethane 50 43 86 2 40 70-119 Chloroform 50 41 .82 2 40 77-120 Tetrahydrofuran 50 61 122 14 40 70-130 1,1,1-Trichloroethane 50 46 92 2 40 72-126 1,1-Dichloropropene 50 46 92 2 40 7.1-132 Carbon Tetrachloride 50 45 90 4 40 69-135 1,2-Dichloroethene 50 45 90 2 40 65-126 Benzene 50 47 94 0 40 78-121 Trichloroethene 50 46, 92 2 40 75-125 1,2-Dichloropropane 50 46 92 0 40 78-117 Dibromomethane 50 44 88 4 40 65-125 Bromodichloromethane 50 45 90 0 40 75-118 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE' Lab Name: MITKEM CORPORATION Contract: Lab Code MITIM -Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) LOW ~� SPIKE LCSD LCSD ADDED CONCENTRATION $ QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. cis-1,3-Dichloropropene 50 48 1 96 2 40 78-120 4-Methyl-2-pentanone 50 48 96 14 40 45-141 Toluene 50 49 98 0 40 80-126 trans-1,3-Dichloroprope 50 47 94 6 40 73-123 - 1,1,2-Trichloroethane 50 44 88 4 40 66-125 1,.3-Dichloropropane 50 49 98 0 40 76-119 Tetrachloroethene 50 49 98 2 40 65-134 2-Hexanone 50 56 112 16 40 37-136 Dibromochloromethane 50 47 94 2 40 76-115 1,2-Dibromoethane 50 47 94 6 40 72-117 Chlorobenzene 50 48 96 0 40 78-117 1,1,1,2=Tetrachloroetha 50 47 94 2 -40 80-115 Ethylbenzene. 50 53 106 0 40 79-129 . Xylene (Total) 150 160 107 0 40 83-125 Styrene 50 53 106 2 40 83-122 Bromoform 50 47 94 4 40 67-126 Isopropylbenzene 50 56 112 0 40 80-135 1,1,2,2-Tetrachloroetha 50 47 94 6 40 70-117 Bromobenzene 50 49 98 0 40 79-119 1,2,3-Trichloropropane 50 48 96 8 40 0-154 n-Propylbenzene 50 51 102 2 40 ' 64-141 2-Chlorotoluene 50 51 .102 2 40 70-132 1,3,5-Trimethylbenzene 50 52 104 2 40 72-133 4-Chlorotoluene 50 50 100 0 40 77-122 tert-Butylbenzene 50 53 106 0 40 31-155 1,2,4-Trimethylbenzene 50 53 106 0 40 73-126 sec-Butylbenzene 50 54 108 0 40 68-137 4-Isopropyltoluene 50 52 104 0 40 66-131 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB .CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V2KLCS Level: (low/med) IOW SPIKE LCSD LCSD ADDED CONCENTRATION t % QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC ## RPD ## RPD REC. ------------ ----------------- ------------- ------ ------ ------ ------ 1,3-Dichlorobenzene 50 49 98 0 40 75-115. 1,4-Dichlorobenzene 50 47 94 0 40 72=110 n-Butylbenzene 50 55 110 0 40 66-130 1,2-Dichlorobenzene 50 49 98 0 40 78-113. 1,2-Dibromo-3-chloropro 50 46 92. 12 40 52-128 1,2,4-Trichlorobenzene 50 52 104 4 40 49-126 Hexachlorobutadiene 50 49 98 2 40 58-115 Naphthalene 50 53 106 9 .40. 45-130 1,2,3-Trichlorobenzene 50 51 102 6 40 44-131 Ether 50 48 96 4 40 70-130 Diisopropyl Ether 50 56. 112 4 40 70-130 Ethyl tert-butyl ether 50 54 108 4 40 70-130 ) tert-Amyl methyl ether 50 57 114 8 40 70-130 1,4-Dioxane 1000 680 68 34 40 65-135 # Column to be used to flag recovery and RPD values with an asterisk. * Values outside of QC limits RPD: 0 out of 70 outside limits Spike Recovery: 1 out of 140 outside limits COMMENTS page 6 of 6 FORM III VOA FORM 3 i SOIL VOLATILE LAB CONTROL SAMPLE Lab Name- MITREM CORPORATION Contract Lab Code: MITKEM . Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V5ALCS Level: (low/med) M D ti SPIKE SAMPLE_ LCS LCSf QC. ADDED- CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. Dichlorodifluoromethane 2500 2300 92 48-135 Chloromethane 25k00 2400 96 60=118 Vinyl .Chloride 2560 2400 96 65-113 Bromomethane 2500 2300 92_ 73-122 Chloroethane 2500 2400 96 72-118 Trichlorofluoromethane 2500 2400 96 68-129 1,1-Dichloroethene 2500 2400 96 .67-121 Acetone 2500 1900 76 .38-161 Carbon Disulfide 2500 2400 96 53-137 Methylene Chloride 2500 2400 96 59-132 trans-1,2-Dichloroethen 2500 2500 100 71-124 Methyl tert-butyl ether 2500 4500 180* .75-123 1,1-Dichloroethane 2500 2500 100 83'-116 2-Butanone 2500 3000' 120 64-139 cis-1,2-Dichloroethene 2500 2400 96 83-120 2,2-Dichloropropane 2500 2800 112 70-129 BromDchloromethane 2500 290.0 116 85-124 Chloroform . 2500 3100 124* 89-118 Tetrahydrofuran 2500 3600 144* 76-126 1,1,1-Trichloroethane 2500 2900 116 81-122 1,1-Dichloropropene 2500 2800 112 76-122 Carbon Tetrachloride 2500 2500 100 79=125 1,2-Dichloroethane 2500 2300 92 83-123 Benzene 2500 2500 .100 81-120 Trichloroethene 2500 2500 100 77-121 1,2-Dichloropropane 2500 2400 96 a1-116 .Dibromomethane 2500 2400 96 86-124 Bromodichloromethane 2500 2400 96 90-114 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CJOD24ENTS: page 1 of 6 FORM III VOA FORM 3 . SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case-No. : SAS No. : SDG No_ : MC1453 Matrix Spike - Sample No. : VSALCS Level: (low/med) MED SPIRE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION %- LIMITS -COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. --------------- --------- ------------- ------------- ------ ------ cis-1,3-Dichloropropene 25.00 2400 96 78-119 4-Methyl-2-pentanone 2500 2000 80 57-138 Toluene 2500 2500 100 81-121 trans-1,3-Dichloroprope 2500 2200 88 85-118 1,1,2-Trichloroethane 2500 2200 88 44-159 1,3=Dichloropropane 2500 2400 96 79-125 Tetrachloroethene 2500 2500 100 73-121 2-Hexanone 2500 2200 88 53-145 Dibromochloromethane 2500. 2400 96 80-124 1,2-Dibromoethane 2500 2300 92 80-124 Chlorobenzene 2500 2500 100 82-118 1,1,1,2-Tetrachloroetha 2500 2600 104 84-121 Euhylbenzene 2500 2600 104 80-122 _Xylene (Total) 7500 7800 104 81-121 Styrene 2500 2600 104 77-128 Bromoform 2500 2300 . 92 77-130 Isopropylbenzene 2500 2600 104 58-148 1,1,2,2-Tetrachloroetha 2500 2300 92 76-125 Bromobenzene 2500 2500 100 16-124 1,2,3-Trichloropropane 2500 2300 92 57-140 n-Propylbenzene 2500 2700 108 72-119 2-Chlorotoluene 2500 2700 108 75-120 1,3,.5-Trimethylbenzene 2500 2700 108 76- 116 4-Chlorotoluene 2500 2100 108 78-116 tert-Butylbenzene 2500 2.600 104 71-115 1,2,4-Trimethylbenzene 2500 2700 108 77-117 sec-Butylbenzene 2500 2600 104 67-117 4-Isopropyltoluene 2500 2600 104 68-118 Column to be used to flag recovery and RPD values with an aste4ri sk * Values outside of QC limits C 44ENTS: page 2 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. SDG No. : MCI453 Matrix Spike - Sample No. : .V5ALCS Level: (low/med) MED SPIKE SAMPLE LCS LCS QC; ADDED CONCENTRATION CONCENTRATION 's LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. 1,3-Dichlorobenzene 2500 2600 104 80-116 1,4-Dichlorobenzene 2500 2500 100 80-114 n-Butylbenzene 2500 2600 104 58-121 1,2-Dichlorobenzene 2500 2600 104 81-116 1,2-Dibromo-3-chloropro 2500 2100 84 71-126 1,-2,4-Trichlorobenzene 2500 2200 88 67=11.4 Hexachlorobutadiene 2500 2400 96 50-111 Naphthalene 2500 2000. 80 58-133 1,2,3-Trichlorobenzene 2500 2100. 84 64-118 Ether 2500 2300 92 70-130 Diisopropyl Ether 2500 2200 88 70-130 Ethyl tert-butyl- ether 2500 2200 88 70-130 tert-Amyl methyl ether 2500 2500 100 70-130 1,4-Dioxane 50000 39000 78 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V5ALCS Level: (low/med) MED SPIKE LCSD LCSD ADDED CONCENTRATION g QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. Dichlorodifluorcmethane 2500 2300 92 . . 0 40 48-135 Chloroanethane 2500 2700 108 12 40 60-118 Vinyl Chloride 2500 2700 108 12 40 65-113 Bromomethane 2500 2500 100 8 40 73-122 Chloroethane 2500 2500 100 4 40 72-118 Trichlorofluoromethane 2500 2500 100 4 40 68-129 1,1-Dichloroethene 2500 2500 100 4 40 67-121 Acetone 2500 2000 80 5 40 38-161 Carbon Disulfide 2500 2600 104. 8 40 53-137 Methylene Chloride 2500 2600 104 8 40 59-132 trans-1,2-Dichloroethem 2500 2600 104 4 40 71-124 Methyl tert-butyl ether 2500 . 5000 200* 10 40 75-123 1.,1-Dichloroethane 2500 2600 104 4 40 83-116 2-Butanone 2500 2400 96 22 40 64-139 cis-1,2-Dichloroethene 2500 2600 104 8 40 83-120 2,2-Dichloropropane 2500 2500 100 11 40 70=129 Bromochloromethane 2500 2500 100 15 40 85-124 Chloroform 2500 2500 100 21 40 89-118 Tetrahydrofuran 2500 2900 116 .22 40 76-126 ) 1,1,1-Trichloroethane 2500 2900 116 0 40 81-122 1,1-Dichloropropene 2500 2706 108 4 40 76-122 Carbon Tetrachloride 2500 2500 100 0 40 79-125 1,2-Dichloroethane 2500 2400 96 4 40 83-123 Benzene 2500 2700 108 8 40 81-120 Trichloroethene 2500 2600 104 4 40 77-121 1,2-Dichloropropane 2500 2600 1.04 8 40 81-116 Dibromomethane 2500 2500 100 4 40 86-124 Bromodichloromethane 2500 2500 100 4 40 90-114 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III VOA FORM 3 SOIL VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No: : MC1453 Matrix Spike - Sample No. : VSALCS Level: (low/med.) .MED SPIRE LCSD LCSD ADDED CONCENTRATION o QC.LIMITS COMPOUND (ug/Kg) . (ug/Kg) REC # RPD # RPD REC. -------- - .-------- ------------- ------ ------ ------ ------ cis-1,3-Dichloropropene 2500 2500 100 4 40 178-11-9 4-Methyl-2-pentanone 2500 2300 92 14 40 57-138 Toluene 2500 2600 104 4 40 81-121 trans-1,3-Dichloroprope 2500 2500 100 13 40 85-118 1,1.,2-Trich.loroethane 2500 2500 100 13 40 44-159 1.,3-Dichloropropane 2500 2500 100 4 40 79-125 Tetrachloroethene 2500 2600 104 4 40 73-121 2=Hexanone 2500 2300 92 4 40 53-145 Dibromochloromethane 2500 2500 100 4 40 80-124 1,2-Dibromoethane 2500 2500 100 8 40 80-124 Chlorobenzene 25.00 2600 104 4 40 82-118 1,1,1,2-Tetrachloroetha 2500 2600 104 0 40 84-121 Ethylbenzene 2500 2700 108 4 40 80-122 Xylene (Total) 7500 8200. 109 5 40 81-121 Styrene 2500 2700 108 4 40 77-128 Bromoform 2500 2400 96 4 40 77-130 Isopropylbenzene 2500 2600 104 0 40 58-148 1,1,2,2-Tetrachlbroetha 2500 2500 100 8 40 76-125 Bromobenzene 2500 2600 104 4 40 .76-124 1,2,3-Trichloropropane 2500 2500 100 8 40 57-140 n-Propylbenzene 2500 2700 108 0 40 .72-119 2-Chlorotol.uene 2500 2700 108 0 40 75-120 1,3,..5-Trimethylbenzene 2500 2700 108 0 40 76-116 47Chlorotoluene 2500 2800 112 4 40 78-116 tent-Butylbenzene 2500 2700 108 4 40 71-115 1,2,4-Trimethylbenzene 2500 2800 112 4 40 77-117 sec-Butylbenzene 2500 2700 108 4 40 67-117 4-Isopropyltoluene 2500 2700 108 4 40 68-118 # Column- to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: ,)age 5 of 6 FORM III VOA FORM 3 SOIL VOI ATI_LE LAB CONTROL SAMPLE Lab Name: MI CE24 CORPORATION Contract: Lab Code: MITKEM " Case No SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : V5ALCS Level: (low/med) MED SPIRE LCSD LCSD ADDED CONCENTRATION %- %- QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. ------ --------- ------------- ------ ------ ------ ------ 1,3-Dichlorobenzene 2500 2600 104 0 40 80-116 1,4-Dichlorobenzene 2500 2600 104 4 40 80.114 n-Butylbenzene 2500 2600 104 0 40 58-121 1,2-Dichlorobenzene 2500 2700 108 4 40 81-116 1,2-Dibromo-3-chlorcpro 2500 2400 96 13 40 71-126 1,2,4-Trichlorobenzene 2500 2400 96 9. 40 67-114 Hexachlorobutadiene 2500 2500 100 4 40 50-111 'Naphthalene 2500 2300 92. 14 40 58-133 1,2,3-Trichlorobenzene 2500 2300 92 9 40 64-118 Ether 2500 2600 104 12 40 70-130 Diisopropyl Ether 2500 2400 96 9 40 70-130 Ethyl tert-butyl ether 2500 2400 96 9 40 70-130 1' tert-Amyl methyl ether 2500 2700 108 8 40 70-130 1,4-Dioxane 50000 45000 90 14 40 70-130I # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 70 outside limits Spike Recovery: 4 out of 140 outside limits COMMENTS: page 6 of 6 FORM III VOA 3D SOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No..:. MC1453 Matrix Spike - EPA Sample No. : SB2-2 Level: (low/med) LOW SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/Kg)'• (ug/Kg) (ug/Kg) REC ## REC. Phenol 1800 0.0 1400 78 45-109 bis(2-Chloroethyl)Ether 1806 0.0 1300 72 43-104 2-Chlorophenol 1800 0.0 1400 78 43-107 1,3-Dichlorobenzene 1800 0.0 1300 72 40-101 1,4-Dichlorobenzene 1800 0.0 1300 72 41-102 1,2-Dichlorobenzene '1800 0.0 1300 72. 41-105 2--Methylphenol 1800 0.0 1400 78 45-108 2,21 -oxybis(1-Chloropro 1800 0.0 1400 78 41-105 4-Methylphenol 1800 0.0 1400 78 48-109 N-Nitroso-di-n-prop. (1) 1800 0.0 1500 83 44-111 .. Hexachloroethane 1800 0.0 1300 72 40-102 Nitrobenzene 1800 0:0 1400 78 44-108 Isophorone 1800 0'.0- 1400 78 42-113 2-Nitrophenol 1800 0.0 1300 72 42-111 2,4-Dimethylphenol 1800 0.0 1700 94 37-107 2,4-Dichlorophenol 1800 0.0 1400 -78 49-110 1,2,4-Trichlorobenzene 1800 0.0 1400 78 42-107 Naphthalene 1800 0.0 1400 78 44-112 4-Chloroaniline 1800 0.0 1000 56 4-102 bis(2-Chloroethoxy)meth 1800 0.0 1400 78 467108 Hexachlorobutadiene 1800 0.0 1400 78 41-108 4-Chloro-3-Methylphenol .1800 0.0 1500 83 56-117 2-Methy1naphthalene 1800 0.0 1400 78 46-110 Hexachlorocyclopentadie 1800 0.0 890 49 10-118 2,4,6-Trichlorophenoi 1800 0.0 1400 78 53-115 2,4,5-Trichlorophenol 1800 0.0 1400 78 59-113 2-Chloronaphthalene 1800 0.0 1400 78 52-112 2-Nitroaniline 1800 0.0 1400 78 63-117 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: -- - page 1 of 6 FORM III SV-2 0LM03.0 3D SOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIRE DUPLICATE RECDVERY Lab Name: MITKEM -CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.: MC1453 Matrix Spike - EPA Sample No. : .SB2-2 Level: (low/med) IOW - SPIRE SAMPLE. MS MS QC. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC ## REC. Dimethylphthalate 1800 0.0 1400 78 62-117 Acenaphthylene 1800 0.0 .1500 83 58-112 2,6-Dinitrotoluene 1800 0.0 .1400 78 60-118 3-Nitroaniline ' 1800 0.0 1100 61 30-117 Acenaphthene 1800 0.0 1500 83 53-116 2,4-Dinitrophenol 1800 0.0 510 28 15-136 4-Nitrophenol 1800 0.0 1200 67 50-12.9 Dibenzofuran 1800 .0.0 1500 83 61-112 2,4-Dinitrotoluene 1800 0,.0 1400 78 59-123 Diethylphthalate . 1800 0.,0 1100 61 61-120 4-Chlorophenyl-phenylet 1800 0.0 1400 78 59-116 Fluorene 18.00 0.0 1500 83 63-115 4-Nitroaniline 1800 0.0 1500 83 35-124 4,6-Dinitro-2-methylphe 1800 0.0 810 45 33-130 N-Nitrosodiphenylamine 1800 0.0 1800 100 50-150 4-Bromophenyl-phenyleth 1800 0.0 1400 78 66-110 Hexachlorobenzene 1800 0.0 1400 .78 67-112 Pentachlorophenol 1800 . 0.0 600 33 19-130 Phen.anthrene 1800 0..0 1400 78 70-115 Anthracene 1800 0.0 1500 83 63-117 Carbazole 1800 0.0 1600 89 62-122 Di-n-butylphthalate 1800 0.0 1500 83 70-120 Fluoranthene 1800 0.0 1400 78 64-121 Pyrene 1800 0.0 1600 89 66-120 Butylbenzylphthalate 1800 .0.0 1600 89 63-123 3,31-Dichlorobenzidine 1800 0.0 1300 72 8-124 Benzo(a)anthracene 1800 0.0 1400 78 50-129 Chrysene 1800 0.0 1600 89 41-150 (1) N-Nitroso-di-n-propylamine ## Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: -- - page 2 of 6 FORM III SV-2 OLM03.0 3D SOIL. SEMIVOLATILE MATRIX SPIRE/MATRIX SPIKE- DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No..: SDG No.-: MCIA53 Matrix Spike - EPA Sample No. : SB2-2 Level: (low/med) LOW — -- SPIKE SAMPLE MS MS QC, ADDED CONCENTRATION CONCENTRATION !W LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC #: REC.' ------------------------ --------- ------------- -- b is(2-Ethylhexyl)phthal 1800 72 1600 85 64-115 Di-n-octylphthalate 1800 0.0 1900 106 69-137 Benzo(b) fluoranthene 1800 0.0 1400 78 61-129 Benzo(k)fluoranthene 1800 0.0 1600 89 62-130 Benzo(a)pyrene 1800 0.0 1400 78 66-119 Indeno(1,2,3-cd)pyrene 1800 0.0 950 53* 56-128 Dibenzo(a,h)anthracene 1800 0.0 1000 56* 58-128 Benzo(g,h,i)perylene 1800 0.0 870 48 32-149 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits C 24MEMS: - - — page 3 of 6 FORM III SV-2 OLM03.0 3D SOIL SEMIVOLATILE MATRIX�SPIKE/Mn=: SPIKE- DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. . SAS No. : SDG No. : MC1453 Matrix Spike - EPA Sample No. : SB2-2 Level: (low/med) IOW SPIKE MSD MSD — - ADDED CONCENTRATION g- %- QC LIMITS COMPOUND (ug/Kg) (uJ/K9) REC # RPD # RPD REC.. ------------------------ --------- ------------- Phenol 1800 1500 83 6 40 45-109 bis(2-Chloroethyl)Ether 1800 1400 78 8 40 43-104 2-Chlorophenol 1800 1500 83 6 40 437107 1,3-Dichlorobenzene 1800 1400 78 8 40 40--"l 1,4-Dichlorobenzene 1800 1400 78 8 40 41-102 1,2-Dichlorobenzene 1800 1400 78 8 40 41-105 2-Methylphenol 1800 1500 83 6 40 45-108 2,21-oxybis(1-Chloropro 1800 1500 83 6 40 41-105 4-Methylphenol 1800 1600 89 13 40 48-109 N-Nitroso-di-n-prop. (1) 1800 1700 94 12 40 44-111 Hexachloroethane 1800 . 1400 78 8 40 40-102 Nitrobenzene 1800 1500 83 6 40 44-108 Isophorone 1800 1500 83 6 40 42-113 2-Nitrophenol 1800 1400 78 8 40 42-111 2,4-Dimethylphenol 1800 1800 100 6 40 37-107 2,4-Dichlorophenol 1800 1500 83 6 40 49-110 1,2,4-Trichlorobenzene 1800 1500 83 6 40 42-107 Naphthalene . 1800 1500 83 6 40 44-112 4-Chloroaniline 1800 1100 61 8 40 4-102 bis(2-Chloroethoxy)meth 1800 1500 83 6 40 46-108 Hexachlorobutadiene 1800 1400 78 0 40 41-108 4-Chloro-3-Methylphenol 1800 1600 89 7 40 56-117 2-Methylnaphthalene 1800 1600 89 13 40 46-110 Hexachlorocyclopentadie 1800 890 49 0 40 10-118 2,4,6-Trichlorophenol 1800 1500 83 6 40 53-115 2,4,5-Trichlorophenol 1800 1600 89 13 40 59-113 2-Chloronaphthalene 1800 1600 89 13 40 52-112 2-Nitroaniline 1800 1700 94 19 40 63-117 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: — — page 4 of 6 FORM III SV-2 OIM03.0 3D SOIL -SIIKIVOLATILE MATRIX SPIKE/MA.TRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Codes MITKEM Case No. : SAS No._: SDG No. : MC1453 Matrix Spike - EPA Sample No. : SB2-2 Level: (low/med) LOW - - SPIKE MSD MSD - ADDED CONCENTRATION - % QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. --------- ------------- ------ --- Dimethylphthalate 1800 1600 89 13 40 62-117 Acenaphthylene 1800 1600 89 7 40 58-112 2,6-Dinitrotoluene 1800 1600 89 13 40 60-118 3-Nitroaniline 1800 1200 67 9 40 30-117 Acenaphthene 1800 1600 89 7 40 53-116 2,4-Dinitrophen0l 1800 450 25 11 40 15-136 4-Nitrophenol 1800 1400 78 15 40 50-129 Dibenzofuran . 1800 1600 89 7 40 61-112 2,4-Dinitrotoluene 1.800 1600 89 13 40 59-123 Diethylphthalate 1800 1200 67 9 40 61-120 4-Chlorophenyl-phenylet 1800 1600 89 13 40 59-116 Fluorene 1800 1600 89 7 40 63-115 4-Nitroaniline 1800 1700 94 12 40 35-124 4,6-Dinitro-2-methylphe. 1800 750 42 7 40 33-130 N-Nitrosodiphenylamine 1800 2000 111 10 40 50-150 4-Bromophenyl-phenyleth 1800 1500 83 6 40 66-110 Hexachlorobenzene 1600 1600 89 13 40 67-112 Pentachlorophenol 18.00 660 37 11 40 19-130 Phenanthrene 1800 1600 89 13 40 70-115 Anthracene 1800 1600 89 7 40 63-117 Carbazole 1800 1800 100 12 40 62-122 Di-n-butylphthalate 1800 1700 94 12 40 70-120 Fluoranthene 1800 1600 89 13 40 64-121 Pyrene 1800 1600 89 0 40 66-120 Butylbenzylphthalate 1800 1800 100 12 40 63-123 3,31-Dichlorobenzidine 1800 1500 83 14 .40 8-124 Benzo(a)anthracene 1800 1600 89 13 40 50-129 Chrysene 1800 1800 100 12 40 41-150 (1) N-Nitroso-di-n-propylami.ne # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: — --- - page 5 of 6 FORM III SV-2 OLM03.0 3D SOIL SEMIVOLATILE MATRIX SPIKE/MATRIK SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - .EPA Sample No. : SB2-2 Level: (low/med) LOW SPIRE MSD MSD ADDED CONCENTRATION %- -1 QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. bis(2-Ethylhexyl")phthal 1800 1800 96 12 40 64-115 Di-n-octylphthalate 1800 2100 117 10 40 69-137 Benzo(b)fluoranthene 1800 1600 89 13 -.40 61-129 Benzo(k)fluoranthene 1800 1800 100 12 40 62-130 Benzo(a)pyrene 1800 1600 89 13 40 66-119 Indeno(1,2,3-cd)pyrene 1800 1100 61 14 40 56-128 Dibenzo(a,h)anthracene 1800 1100 61 8 40 58-128 Benzo(g,h,i)perylene 1800 960 53- 10 40 32-149 1 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 64 outside limits Spike Recovery: 2 out of 128 outside limits COMME T!'S: —- page 6 of 6 FORM III SV-2 OLM03.0 FORM 3 SOIL SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : S2BLCS Level: (low/med) LOW SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUM (ug/Kg) (ug/Kg) (ug/Kg) RE # REC. Phenol 1700 1500 88 45-109 bis(2-Chloroethyl)Ether 1700 1400 82 43-104 2-Chlorophenol 1700 1500 88 43-107 1,3-Dichlorobenzene 1700 1400 82 40-101 1,4-Dichlorobenzene 1700 1400 _ 82 41-102 -1,2-Dichlorobenzene 1700 140.0 82 41-105 2-Methylphenol 1700 1500 88 45-108 2,21-oxybis(1-Chloropro 1700 1500 88 .41-105 4-Methylphenol 1700 1600 94 48-109 N-Nitroso-di-n-prop. (1) 1700 1600 94 44-111 Hexachloroethane 1700 1400 82 40-102 Nitrobenzene 1700 1500 88 44-168 Isophorone 1700 1500 88 42-113 2-Nitrophenol 1700 1500 88 42-111 2,4-Dimethylphenol 1700 1600 94 37-107 2,4-Dichlorophenol 1700 1600 94 49-110 1,2.,4-Trichlorobenzene 1700 1500 88 42-107 Naphthalene 1700 1500 88. 44-112 4-Chloroaniline 170.0 810 48 4-102 bis(2-Chloroethoxy)meth 1700 1600 94 46-108 Hexachlorobutadiene 1700 1400 82 .41-108 4-Chloro-3-Methylphenol 1700 1600 94 56-117 2-Methy1naphthalene 1700 1500 88 46-110 Hexachlorocyclopentadie 1700 1800 106 10-118 2,4, 6-Trichlorophenol 1700 1500 88 .53-115 2,4, 5-Trichlorophenol 1700 1500 88 59-113 2-Chloronaphthalene 1700 1500 88 52-112 2-Nitroaniline 1700 1600 94 63-117 (1) N-Nitroso-di-n-propylamine # Column. to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COAMVNTS: page 1 of 6 FORM III SV FORM 3 SOIL SE IIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix Spike - Sample No. : S2BLCS Level: (low/med) LOW SPIKE SAMPLE LCS Les Ste- ADDED. CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. Dimethylphthalate 1700 1600 94 62-117 Acenaphthylene 1700 1600 94 58-112 2,6-Dinitrotoluene 1700 1600 94 60-118 3-Nitroaniline 1700 1000 59 30--117 Acenaphthene 1700 1600 94 537116 21 4-Dinitrophenol 1700 1000 59 15-136 4-Nitrophenol 1700 1500 88 50-129 Diben:zofuran 1700 1600 94 61-112 2,4-Dinitrotoluene 1700 1600 94 59-123 Diethylphthalate. 1700 1300 .76. 61-120 4-Chlorophenyl-phenylet 1700 1600 94 59-116 Fluorene 1700 1600 94- 63-115 4-Nitroaniline 1700 1600 94' 35-124 4,6-Dinitro-2-methylphe 1700 1200 70 33-130 N-Nitrosodiphenylamine 1700 2000 118 50-150 4=Bromophenyl-phenyleth 1700 1600 94 66-110 Hexachlorobenzene 1700 1600 94 67-112 Pentachlorophenol 1700 1400 82 19-130 . Phenanthrene 1700 1600 94 70-115 Anthracene 1700 1700 100 63-117 Carbazole 1700 1800 .106 62-122 Di-n-butylphthalate 1700 1600 94 70-120 Fluoranthene 1700 1600 94 64-121 Pyrene 1700 1600 94 667120 Butylbenzylphthalate 1700 1600 94 63-123 3,31-Dichlorobenzidine 1700 1100 65 8-124 Benzo(a)anthracene 1700 1600 94 50-129 Chrysene 1700 1800 106 41-150 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * values outside of QC limits COMMENTS: page 2 of. 6 FORM III SV FORM 3 SOIL SEMIVOLATILE LAB' CONTROL SAMPLE Lab Name: M CEM CORPORATION Contract: gab Code: MITKEM Case No. : SAS No: : SDG No. : MC1453 Matrix Spike - Sample No. : S2BLCS Level:_(low/med) LOW SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. - bis(2-Ethylhexyl)phthal 1700 1600 94 64-115 Di-n-octylphthalate 1700 1500 88 69-137 Benzo(b) fluoranthene 1700 1400 82 61-129 Benzo(k)fluoranthene 1700 1700 100 62-130 Benzo(a)pyrene 1700 1600 94 66-119 Indeno(1,2,3-cd)pyrene 1700 1600 94 56-128 Dibenzo(a,h)anthracene 1700 1600 94 58-128 Benzo(g,h,i)perylene 1700 1600 94 32-149 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III SV 4A -EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY - Lab Name MITKFM CORPORATION Contract: VB1K2K Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File -ID: V2G5923 Lab Sample ID: MB-15858 Date Analyzed: . 11/26/04 Time Analyzed: 1442 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (YIN) Y Instrument ID: V2 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB -- TSAR TIME' SAMPLE NO. SAMPLE ID FILE ID ANALYZED ------------ ---- --------- =- 01 V2KLCSD LCSD-15858 V2G5925 1546 02 V2KLCS LCS-15858 V2G5926 1614 03 SB1-8 C1453-01A V2G5929 1750 04 SB-X C1453-09A V2G5931 1843 05 SB8-2 C1453-10A V2G5932 1909 i 06 SB3-6 C1453-12A V2G5933 1934 07 .SB10-2 C1453-16A V2G5935 2027 08 SB5-2 C1453-06A V2G5936 2053 ` 09 SB5-2MS C1453-06AMS V2G5937 2119 10 SB5-2MSD C1453-06AMSD V2G5938 2145 11 12 - - ' 13 14 — - 15 -- — - 16 17 18 19 — 20 21 22 - 23 24 25 _ 26 27 28 29 30 COPM]aus: page 1 of 1 FORM IV VOA OLM03.0 } lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK2K Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15858 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5923 Level: (low/med) LOW Date Received: o Moisture: not dec. Date Analyzed: 11/26/04. GC Column: DB-624 ID: 0.25 (mm) Dilution-Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 5 .0 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 5 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69=4---------Trichlorofluoromethane 5 U 75-35-4---------1;1-Dichloroethene 5 U 67-64-1---------Acetone 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethene 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane .5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U .10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1-------- 4-Methyl-2-pentanone .5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropane 5 U 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U FORM I VOA OLM03.0 lA EPA SAMPLE Np. VOLATILE_ ORGANICS ANALYSIS DATA SHEET VBLK2K Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15858 Sample wt/vol: .5.0 (g/mL) G Lab File ID: V2G5923 Level: (low/med) LOW Date Received: o Moisture: not dec. _ Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: -(mL) Soil Aliquot Volume: -("uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane - 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethene 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5. 0 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene. 5 U 95-50-1---------1,2-Dichlorobenzene 5 U. 96-12-8---------1,2-Dibromo-3-chloropropane. 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87=61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether- 5 U FORM I VOA OLM03.0 ' 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK2K Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15858 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5923 Level: (low/med) Low Date Received: - - o Moisture: not dec. Date Analyzed: 11/26/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (mL) Soil Aliquot Volume: _ JUL-) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) 'IIG/KG Q 108-20-3--------Diisopropyl Ether 5 II 637=92-3--------Ethyl tert-butyl ether 5 II 994-05-8--------tert-Amyl methyl ether 5 U 123=91-1--------1,4-Dioxane 100 U r FORM I VOA O1,M03.0 4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY VBLK2S Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MITKEM. Case No. : SAS No. : SDG No. : MC1453 ! Lab File ID: V2G5983 Lab Sample ID: MB-15905 Date Analyzed: 12/01/04 Time Analyzed: 1224 GC Column: .DB-624 ID: 0.25 (mm) Heated Purge: (Y/N) Y Instrument ID: V2 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE-ID ANALYZED ------------ -------------- -------------- ---------- ------------ -------------- -------------- ---------- 01 V2SLCS LCS-15905 V2G5984 1302 02 V2SLCSD LCSD-15905 V2G5985 1332 03 TRIP C1453-08A V2G5986 1411 04 TRIP C1453-17A V2G5987 1441 05 SB9-8 C1453-04A V2G5988 1512 06 SB4-14 C1453-14A V2G5989 1542 07 SB10-2RE C1453-16ARE V2G5990 1612 08 09 _ 10 11 — 12 I 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 - - -^- 28 29 30 ~- COMMENTS: page 1 of 1 FORM IV VOA OLM03 .0 lA EPA SAMPLE NO: VOLATILE ORGANICS ANALYSIS DATA SHEET' VBLK2S Lab Name: MITKEM CORPORATION Contract: lab. Code MITKEM ' Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5983 Level: (low/med). LOW Date Received: %- Moisture: not dec. _ Date.Analyzed: 12/01/04 GC Column: DB-624. . ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO.. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4----------Vinyl Chloride 5 U 74-83-9=-----7--Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 5 U 67-64-1---------Acetone .5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4--------Methyl tert-butyl ether 5 U 75-34=3---------1,1-Dichloroethane 5 U 78-93-3--------=2-Butanone 5 U 156-59-2---------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3-----=---Chloroform 5 U 109--99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---=-----1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: VBLK2S Lab Code: MITKEM Case No. : SAS No.-: SDG No. : MC1453 Matrix: (soil/water) .SOIL Lab Sample ID: MB-15905 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V2G5983 Level: (low/med) LOW Date Received: %- Moisture: not dec.. Date Analyzed., 12/01/04 GC Column: DB-624 . . ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:' (ML) Soil Aliquot Volume: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochlor ethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethyl zene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene .5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK2 S Lab Name: MITKEH CORPORATION Contract: Lab Code: MITKEK Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15905 .Sample. wt/vol: 5:0 (g/mL) G Lab File ID: V2G5983 Level: (low/med) LOW Date Received: s Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (ML) Soil Aliquot Volume: _ (L) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3--------Diisoprcpyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether _ . 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 4A EPA SAMPLE NO.. VOLATILE METHOD BLANK SUMMARY VBLKSA Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File ID: V5F6823 Lab Sample ID: MB-15904 Date Analyzed: 12/01/04 Time Analyzed: 1150 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (Y/N) N Instrument ID: V5 THIS METHOD BLANK APPLIES TO THE FOLLOWIM SAMPLES, MS and MSD: EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED O1 VSALCS LCS-15904 V5F6824 1227 02 VSALCSD LCSD-15904 V5F6825 1253 03 SB1-8 C1453-OIB V5F6826 1338 04 SB3-6 C1453-12B V5F6827 1404 05 SB3-6DL C1453-12SDL V5F6830 1554 06 07 08 09 10 11 } 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 COMMENTS: page 1 of 1 FORM IV VOA OLM03.0 IA. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK5A Lab Name: MITKEM CORPORATION Contract: Lab. Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: M8-15904 Sample wt/vol: 5.0 (g/mL) G Lab File ID: V5F6823 Level: (low/med) :MED Date Received: g Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB7624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100:0(UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 75-71-8---------Dichlorodifluoromethane 250 U 74-87-3---------Chloromethane 250 U 75-01-4---------Vinyl Chloride 250 U 74-83-9-------=-Bromomethane 250 U 75-00-3.---------Chloroethane 250 U 75-69-4---------Tri.chlorofluoromethane 250 U 75-35-4---------1,1-Dichloroethene 250 U 67-64-1---------Acetone 250 U 75-15-0---------Carbon Disulfide 250 U 75-09-2---------Methylene Chloride_ __ 250 U 156-60-5--------trans-1,2-Dichloroethene 250 U 1634-04-4-------Methyl tert-butyl ether 250 U 75=34-3.---------1,1-Dichloroethane 250 U 78-93-3---------2-Butanone .250 U 156-59-2-.-------cis-1.,2-Dichloroethene_ 250 U 590-20-7--------2,2-Dichlorcpropane 250 U 74-97-5---------Bromochloromethane 250 U 67-66-3---------Chloroform 250 U 109-99-9--------Tetrahydrofuran _ 250 U 71-55-6---------1.,1,1-Trichloroethane_ 250 U 563-58-6--------1,1-Dichloropropene 250 U 56-23.-5---------Carbon Tetrachloride 250 U 107-06-2--------1,2-Dichloroethane 250 U 71-43-2---------Benzene 250 U 79-01-6---------Trichloroethene _ 250 U 78-87-5---------1,2-Dichloropropane_. 250 U 74-95-3---------Dibromomethane 250 U 15-27-4---------Bromodichloromethane 250 U 10061-01-5------cis-1,3-Dichloropropene 250 U 108-10-1--------4-Methyl-2-pentanone 250 U 108-88-3--------Toluene 250 U 061-02-6------trans-1,3-Dichlorcpropene 250 U 79-00-5---------1,1,2-Trichloroethane 250 U 142-28-9--------1,3-Dichloropropane 250 U FORM I VOA OLM03.'0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET : VBLK5A Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case-No. : SAS No. : SDG No. : MC1453 Matrix:: (soil/water) SOIL Lab Sample ID: MB-15904 Sample wt/vol: 5_0 (g/mL) G Lab File ID:, V5F6823 Level: (low/med) MID Date Received: !k Moisture: not dec. Date. Analyzed: 12/01/04 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100-.6-WL CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 127-18-4--------Tetrachloroethene 250 U 591-78-6--------2-Hexanone, - 250 U 124-48-1--------Dibromochloromethane : 250 U 106-93-4--------1,2-Dibromoethane 250 U 108=90-7--------Chlorobenzene 250 U 630-20-6--------1,1,1,2-Tetrachloroethane 250 U 100-41-4--------Ethylbenzene 250 U ----------------m,p-Xylene 250 U 95-47-6---------o-Xylene 250 U 1330=20-7-------Xylene (Total) 250 U 1/ 100-42-5--------Styrene 2.50 U 75-25-2---------Bromoform 250 U 98-82-8---------Isopropylbenzene 250 U 79-34-5---------1,1,2,2-Tetrachloroethane 250 U 108-86-1--------Bromobenzene 250 U 96-18-4---------1,2,3-Trichloropropane 250 U 103-65-1--------n-Propylbenzene 250. 0 95-49-8---------2-Chlorotoluene 250 U 108-67-8--------1,3,5-Trimethylbenzene 250 U 106-43-4--------4-Chlorotoluene 250 U 98-06-6---------tert-Butylbenzene 250 U 95-63-6---------1,2,4-Trimethylbenzene 250 U 135-98-8--------sec-Butylbenzene 250 U 99-87-6---------4-Isopropyltoluene 250 U 541-73-1--------1,3-Dichlorobenzene 250 U 106-46-7--------1,4-Dichlorobenzene 250 U 104-51-8--------n-Butylbenzene 250 U 95-50-1---------1,2-Dichlorobenzene 250 U 96-12=8---------1,2-Dibromo-3-chloropropane 250 U 120-82-1--------1,2,4-Trichlorobenzene 250 U 87-68-3---------Hexachlorobutadiene 250 U 91-20-3---------Naphthalene_ 250 U 87-61-6---------1,2,3-Trichlorobenzene 250 U 60-29-7---------Ether 250 U FORM I VOA OLM03.0 lA EPA SAMPLE NO_ VOLATILE ORGANICS ANALYSIS DATA SHEET VBLKSA Lab Name: MITKEK CORPORATION Contract: Lab Code: MITKEM' Case No. : SAS No. : SDG No MC1453 Matrix: (soil/water) SOIL Lab- Sample ID: MB-15904 Sample wt/vol: 5.0 (g/mL) G Lab File ID: VSF6823 Level: (low/med) MM Date Received: !k Moisture: not dec. Date Analyzed: 12/01/04 GC Column: DB-624 ID: .0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: 5(mL) Soil Aliquot Volume: 100.0(UL) CONCENTRATION UNITS: CAS -.NO.. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-20-3-- -----=Diisopropyl Ether 250 U 637-92-3--=-----Ethy1 tert-butyl ether 250 U 994-05-8--------tent-Amyl methyl ether 250 U 123-91-1--------1,4-Dioxane 5000 U FORM I VOA OLM03.0 4B EPA SAMPLE NO. SEMIVOLATILE. METHOD BLANK. SUMMARY SBIMB Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM . Case No. : SAS No. : SDG No_ : MC1453 Lab File ID: S2E2656 Lab Sample ID: MB-15845 - Instrument ID: S2 Date Extracted: 11/24/04 Matrix: .(soil/water) SOIL Date Analyzed:. 12/01/04 Level: (low/med) LOW Time Analyzed:: 1933 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB --- DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED ------------ -------------- -------------- ---------- 01 S2BLCS LCS-15845 S2E2657 12/01/04 02 S2BLCSD LCSD-15845 S2E2658 12/01/04 03 SB9=8 C1453-04E S2E2659 12/01/04 04 SB-X C1453-09E S2E2660 12/01/04 05 SB3-6 C1453-12E S2E2661 12/01/04 06 SB4-14 C1453-14E S2E2662 12/01/04 07 SB5-2 C1453-06E S2E2663 12/01/04 08 SB2-2 C1453-15C S2E2664 12/02/04 09 SB2-2MS C1453-15CMS S2E2665 12/02/04 10 SB2-2MSD C1453-ISCMSD S2E2666 12/02/04 11 SB8-2 C1453-10E S2E2667 12/02/04 12 SB10-2 C1453-16E S2E2668 12/02/04 13 SB1-8 C1453-01E S2E2669 12/02/04 14 SB8-2DL C1453-10IDL S2E2706 12/03/04 15 SB1-8DL C1453-01EDL S2E2707 .12/03/04 16 17 _ 18 19 20 21 22 23 24 25 26 27 28 29 30 COMMENTS: page 1 of 1 FORM IV SV OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORCWCS ANALYSIS DATA SHEET SBLK2B Lab Name: MITKEM CORPORATION Contract: _ Lab Code: MITREM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2656 Level: (low/med) LOW Date Received: o Moisture: 0 decanted: (YIN) N Date Extracted:ll/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1:0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95-2--------Phenol 330 U 111-44-4--------bis(2-Chloroethyl}Ether 330 U 95-57-8---------2-Chlorophenol 330 U 541-73-1--------1,3-Dichlorobeiizene 330 U 106-46-7------.--1,4-Dichlorobenzene 330 U 95-50-1------- 1,2-Dichlorobenzene 330 U 95-48-7---------2-Methylphenol 330 U 108-60-1--------2,2'-oxybis(1-Chloropropane) 330 U 106-44-5--------4-Methylphenol 330 U 621-64-7--------N-Nitroso-di-n-propylamine_ 330 U 67-72-1---------Hexachloroethane 330 U 98-95-3---------Nitrobenzene 330 U 78-59-1---------Isbphorone - 330 U 88-75-5---------2-Nitrophenol 330 U 105-67-9--------2,4-Dimethylphenol 330 U 120-83-2------- 2,4-Dichlorophenol 330 U 120-82-1--------1,2,4-Trichlorobeiizene 330 U 91-20-3---------Naphthalene J 330 U 106-47-8--------4-Chloroanillne 330 U 111-91-1--------bis(2-Chloroethoxyy methane_ 330 U 87-68-3---------Hexachlorobutadiene 330 U 59-50-7---------4-Chloro-3-Methylphenol 330 U 91-57-6---------2-Methylnaphthalene 330 U 77-47-4---------Hexachlorocyclopentadlene 330 U 88-06-2---------2,4,6-Trichlorophenol 330 U 95-95-4---------2,4,5-Trichlorophenol_ 670 U 91-58-7---------2-Chloronaphtha.lene 330 U 88-74-4--------- 2-Nitroaniline 670 U 131-11-3--------Dimethylphthalate 330 U 208-96-8--------Acenaphthylene— 330 U 606-20-2--------2,6-Dinitrotoluene 330 U 99-09-2---------3-Nitroaniline 670 U 83-32-9---------Acenaphthene 330 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SENIIVOLATILE ORGANICS ANALYSIS DATA SHEET SBLK2B Lab Name: MIZKE2 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL. Lab Sample ID: MB-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2656 Level: (low/med) LOW Date Received: Moisture: 0 decanted: (Y/N) N Date Extracted:11/24/04 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (Y/N) N pH: CONC 24TRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5---------2,4-Dinitrophenol 670 U 100-02-7--------4-Nitrcphenol 670 U 132-64-9--------Dibenzofuran 330 U 121-14-2--------2,4-Dinitrotoluene 330 U 84-66-2---------Diethylphthalate 330 U 7005-72-3-------4-Chlorophenyl-phenylether- 330 U 86-73-7---------Fluorene 330 U 100-01-6--------4-Nitroaniline 670 U ) 534-52-1--------4,6-Dinitro-2-methylphenol 670 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 330 U 101-55-3--------4-Bromophenyl-phenylether 330 U 118-74=1--------Hexachlorobenzene 330 U 87-86-5---------Pentachlorophenol 670 U 85-01-8---------Phenanthrene 330 U. 120-12-7--------Anthracene 330 U 86-74-8---------Carbazole 330 U 84-74-2---------Di-n-butylphthalate 330 U 206-44-0--------Fluoranthene _ 330 U 129-00-0--------Pyrene f 330 U' 85-68-7---------Butylbenzylphthalate 330 U 91-94-1---------3,3'-Dichlorobenzidine 330 U 56-55-3---------Benzo(a)anthracene 330 U 218-01-9--------ChYysene 330 U 117-81-7--------bis(2-Ethylhe)qyl phthalate 330 U 117-84-0--------Di-n-octylphthalate _ 330 U 205-99-2--------Benzo(b)fluoranthene 330 U 207-08-9--------Benzo(k)fluoranthene _ 330 U 50-32-8---------Benzo(a)pyrene 330 U 193-39-5--------Indeno(1,2,3-cd_)pyrene 330 U 53-70-3------- Dibenzo(a,h)anthracene- 330 U 191-24-2--------Benzo(g,h,i)perylene 330 U (1 - Cannot be separated from Diphenylamtne FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS' ANALYSIS 'DATA SHEET . S2BLCS Lab Name: MITKEM CORPORATION Contract Lab Code: MITREM Case No. : SAS No. : SDG No. :` MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2657 Level: (low/med) LOW Date. R.eceived: o Moisture: 0 decanted: (Y/N) N Date Extracted:11/24/00 Concentrated Extract Volume: 1000(uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/RG Q 108-95-2--------Phenol 1500 111-44-4--------bis(2-Chloroethyl)Ether 1400 95-57-8---------2-Chloroph6nol 1500 541-73-1--------1,3-Dichlorobenzene 1400 106-46-7--------1,4-Dichlorobenzene 1400 95-50-1---------1,2-Dichlorobenzene 1400 95-48-7---------2-Methylphenol _ 1500 108-60-1--------2,2'-oxybis(1-Chloropropan 1500 106-44-5--------4-Methylphenol 1600 621-64-7--------N-Nitroso-di-n-propylam nne_ 1600 67-72-1---------Hexachloroethane_ 1400 98-95-3---------Nitrobenzene 1500 78-59-1---------Isophorone 1500 88-75-5---------2-Nitrophenol 1500 105-67-9--------2,4-Dimethylphenol 1600 120-83-2--------2,4-Dichlorophenol 1600 120-82-1--------1,2,4-Trichlorobenzene_ 1500 91-20-3---------Naphthalene 1500 106-47-8--------4-Chloroaniline 810 111-91-1--------bis(2-Chlorobthoxy methane 1600 87-68-3---------Hexachlorobutadiene 1400 59-50-7---------4-Chloro-3-Methylphenol 1600 91-57-6---------2-Methylnaphthalene 1500 77-47=4---------Hexachlorocyclopentadiene 1800 88-06-2---------2,4,6-Trichlorophenol 1500 95-95-4---------2,4,5-Trichlorophenol 1500 91-58-7---------2-Chloronaphthalene _ 1500 88-74-4---------2-Nitroaniline 1600 131-11-3----=---Dimethylphthalate_ 1600 208-96-8--------Acenaphthylene 1600 606-20-2--------2,6-Dinitrotoluene 1600 99-09-2---------3-Nitroaniline 1000 83-32-9---------Acenaphthene 1600 FORM I SV-1 OLM03.0 1C _ EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2BLCS Lab Name: MITKEM CORPORATION Contract: r Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: LCS-15845 Sample wt/vol: 30.0 (g/mL) G Lab File ID: S2E2657 Level: (low/med) LOW Date Received: Moisture: 0 decanted: (Y/N) N Date Extracted:ll/24/00 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 12/01/04 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG. 4 51-28-5---------2,4-Dinitrophenol 1000 100-02-7--------4-Nitrophenol 7 1500 132-64-9--------Dibenzofuran 1600 121-14-2--------2,4-Dinitrotoluene 1600 84-66-2---------Diethylphthalate 1300 7005-72-3-------4-Chlorophenyl-pheriylether 1600 86-73-7---------Fluorene 1600 100-01-6--------4-Nitroa=—Une 1600 ) 534-52-1--------4,6-Dinitro-2-methylphenol 1200 86-30-6---------N-Nitrosodiphenylamine (1) 2000 101-55-3--------4-Bromophenyl-phenylether 1600 118-74-1--------Hexachlorobenzene __ 1600 87=86-5---------Pentachlorophenol 1400 85-01-8---------Phenanthrene 1600 120-12-7--- - ----Anthracene 1700 86-74-8---------Carbazole 1800 84-74-2---------Di-n-butylphthalate 1600 206-44-0--------Fluoranthene 1600 129-00-0--------Pyrene 1600 85-68-7---------Butylbenzylphthalate 1600 91-94-1---------3,3--Dichlorobenzidine- 1100 56-55-3---------Benzo(a)anthracene 1600 218-01-9--------Chrysene 1800 117-81-7--------bis(2-Et ylhexyl phthalate_ 1600 117-84-0--------Di-n=octylphthalate_._ 1500 205-99-2--------Benzo(b) fluoran-then 1400 207-08-9--------Benzo(k) fluoranthene 1700 50-32-8---------Benzo(a)pyrene 1600 193-39-5--------Indeno(1,2,3-cd pyrene 1600 53-70-3---------Dibenzo(a,h)anthracene 1600 191-24-2--------Benzo(g,h,i)perylene 1600 (1) Cannot be separated from DiphenylamLne FORM I SV-2 OLM03.0 FORM 4 CLIENT SAMPLE NO. PCB METHOD BLANK SUMMARY PBIMA Lab Name: _MITKEM CORPORATION Contract:. Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1453 Lab Sample ID: MB-15882 Lab File ID: 'E2E2648F Matrix (soil/water) SOIL Extractions (SepF/Copt/Sonc). SONC Sulfur Cleanup (Y/N) Y Date. Extracted: 11/30/04 Date Analyzed (1) : 12/02/04 Date. Analyzed (2).: 12/02/04 Time Analyzed .(1) : 1447 Time Analyzed (2) : 1447 Instrument ID (1) : E2 Instrument ID (2) : E2 GC Column (1) : RTXCLPPEST ID: 0.53 (mm) GC Column (2) : -RTXCLPPEST 2 ID: 0.53 (mm) THIS METHOD BLANKAPPLIES TO THE FOLLOWING SAMPLES, MS and MSD: LAB DATE DATE - SAMPLE NO. SAMPLE ID ANALYZED 1 ANALYZED 2 ------------ -------------- ----------. ---------- 01 P2ALCS LCS-15882 12/02/04 12/02/04 02 P2ALCSD LCSD-15882 12/02/04 :12/02/04 03 SB1-8 C1453-01E 12/02/04 12/02/04 04 SB7-2 C1453-03A 12/02/04 12/02/04 05 SB9-8 C1453-04E 12/02/04 12/02/04 06 SB5-2 C1453-06E 12/02/04 12/02/04 07 SB-X C1453-09E 12/02/04 12/02/04 08 SB8-2 C1453-10E 12/02/04 12/02/04 09 SB2-2 C1453-15C 12/03/04 12/03/04 10 SB2-2MS C1453-15CMS 12/03/04 12/03/04 11 SB2-2MSD C1453-15CMSD 12/03/04 12/03/04 12 SB10-2 C1453-16E 12/03/04 12/03/04 13 _ 14 � J 15 16 17 18 19 20 21 22 23 24 25 26 COMMED]TS: page 1 of 1 FORM IV PCB FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET _ PBLK2A Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No..: SAS No. : SDG No. : MC1453 Matrix: (soil/water) SOIL Lab Sample ID: MB-15882 Sample wt/vol: 30.0 (g/mL) G Lab File ID: E2E2648F Moisture: 0 decanted: (YIN) N Date Received: Extraction: (SepF/Cont/Sonc) SONC Date Extracted:11/30/04 Concentrated Extract Volume: 10000(uL) Date Analyzed: 12/02/04 Injection Volume• 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 12674-11-2------Aroclor-1016 33 U 11104-28-2------Aroclor-1221 33 U 11141-16-5------Aroclor-1232 33 U 53469-21-9------Aroclor-1242 33 U 12672-29-6------Aroclor-1248 33 U 11097-69-1------Aroclor-1254 33 U 11096-82-5------Aroclor-1260 33 U FORM I PCB U-Sr EPA - CLP 3. i BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1453 Preparation Blank Matrix (soil/water) : SOIL Preparation Blank Concentration Units (ug/L or mg/kg) : MG/KG Initial Calib_ Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Mercury 0.0 U 0.0 U 0.0 U 1 0.007 U CV FORM III - IN SW846 • T' U-S_ EPA CLP 3 BLANKS. Lab Name: Mitkem Corporation Contract: 28367-0650-00000 Lab Code: MITKEM Case No. SAS. No. : SDG No. : MC1453 Preparation Blank Matrix (soil/water) : SOIL Preparation Blank Concentration Units (ug/L or mg/kg) : MG/KG Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U 9.1 lul 9.1 U 0.120 U CA FORM III - IN SW846 U.S. EPA - CLP 3 BLANKS i Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No. SAS No. : SDG No.': MC1453 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or. mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C I Blank. C M Cyanide 9.1 U Y CA FORM III - IN SW846 U.S: -EPA CLP \ 3 ) _ BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No, SAS No. : SDG No. : MC1453 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U 9.1 U -11.1 B 1 9.1 1 U CA FORM III - IN SW846 U-S_ EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No_ SAS No. : SDG No._: MC1453 Preparation Blank Matrix (soil/water) : SOIL Preparation Blank Concentration Units (ug/L or mg/kg) : MG/KG Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U 9.1 U 9.1 U 9.1 U 0.120 U CA .1 FORM III - IN SW846 U-S_ EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: - MITKEM Case No_ SAS No_ : SDG`No:: MC1453 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib_ Continuing Calibration Prepa- Blank. Blank {ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U CA I FORM III - IN SW846 U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No. SAS No_ : SDG No.. : MC1453 Preparation Blank Matrix (soil/water) : SOIL Preparation Blank Concentration Units (ug/L or mg/kg) . MG/KG Initial Calib_ . Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank. C M Antimony 6.5 B 2.6 B 1.7 B 2.3 B 0.273 B P Arsenic i.6 U. 1.6 U 1.6 U 1.6 U 0.093 B P Barium 2.1 U 2.1 U 2.1 U 2.1 U 1.062 B P Beryllium 0.2 U 0.4 B 0.1 U 0.1 U 0.006 U P Cadmium 0.1 U 0.1 U 0.1 U 0.1 lu 0.005 U P Chromium 0.4 U 0.5_ B 0.4 U 0.4 U 0.044 B P. Lead 0.5 U 0.7 B 0.9 B 0.5. U 0.041 U P Nickel 1.3 B 0.9 B 1.3 B 0.6 U 0.165 B P Selenium 1.0 U 1.0 U 1.0 U 1.0 U 0.100 B P Silver 0.9 B 0.9 U 0.9 U 0.9 U 0.019 U P Thallium 4.8 B 4.3 B 3.3 B 4.4 B 0.202 B P Vanadium 0.5 U 0.5 U 0.5 U 0.5 U 0.021 U. P Zinc 6.1 B 3.9 B 3.4 B 6.1 B 1.188 B P FORM III - IN SW846. U-S_ EPA CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-00000 Lab Code: MITKEM Case No. SAS No_ : SDG.No. : NC1453 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Antimony 1.2 U 1.2 U 1.2 U P Arsenic 1.6 U 1.6 U 1.6 U P Barium 2.1 U 2.1 U 2.1 U P Beryllium 0.1 U 0.1 U 0.1 U P Cadmium 0.1 U 0.1 U 0.1 U P Chromium 0.4 U 0.7 B 0.4 U P Lead 1.1 B 0.7 B 0.5 U P Nickel 0.6 U 0.6 U 0.6 U P Selenium -2.1 B 1.0 U 1.0 U P Silver 0.9 B 0.9 U 0.9 U P Thallium 3.3 B 2.4 B 3.0 B P vanadium 0.5 U 0.5 U 0.5 U P Zinc 3.3 B 4.9 B 3.1 B P FORM III - IN SW846 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY ; Lab Name: MITKEM CORPORATION Contract: Lab Code: MITIM4 Case No. : SAS No. : SDG No. : MC1453 Lab File ID (Standard) : V2G5922 Date Analyzed: 11/26/04 Instrument ID: V2 Time Analyzed: 1352 GC Column: DB-624 ID: 0.25 (mn) Heated Purge: (YIN) Y ISi IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT # .12 HOUR STD 2404603 6.10 1571838 9.72 977366 12.64 UPPER LIMIT 4809206 6.60 3143676 10.22 1954732 13.14 LOWER LIMIT 1202302 5.60 785919 9.22 . 488683 12.14 EPA SAMPLE - ------- NO. ---- ------- ---------- ------- ---------- ------- 01 VBLK2K 2261024 -6.09 1475226 - 9.72 805180 12.65 02 V2KLCSD 2365693 6.09 1498458 9.72 929266 12.64 03 V2KLCS 2297347 6.09 1474369 9.72 919145 :12.b4 04 SB1-8 1422812 6.09. 426007* 9.72 10811* 12 .67 05 SB-X 1859656 6.09 1223327 9.71 760577 12.63 06 SB8-2 1701402 6.08 1066010 9.71 556714 12.64 07 SB3-6 1563945 6.10 565217* 9.74 405359* 12.61 08 SB10-2 1413269 6.08 80.0202 9.71 353371* 12.63 09 SB5-2 1309037 6.08 845014 9.71 472319* 12.64 10 SB5-2MS 1616105 6.08 1058746 9.71 603031 12.63 11 SB5-2MSD 1731897 6.08 1076918 9.71 577860 12.64 12 13 14 15 16 17 18 19 20 21 22 IS1 = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 IS3 (DCB) = 1,4-Dichlorobenzene-d4 AREA UPPER LIMIT = +100%- of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag values outside QC 'limits with an asterisk. * Values outside of QC limits. page l of 1 FORM VIII VOA OLM03.0 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITIE4 CORPORATION Contract: Lab Coder MITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File ID (Standard) : V2G5981 Date Analyzed: 12/01/04 Instrument ID: V2 Time Analyzed: 1106 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (Y/N) Y IS1 IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT # 12 HOUR STD 2187351 6.13 1418472 9.76 884073 12.67 UPPER LIMIT 4374702 6.63 2836944 10.26 1768146 13.17 LOWER LIMIT 1093676 5.63 709236 9.26 442031 12417 -------- ------- EPA SAMPLE NO. 01 VBIMS 1881849 6.13 1211484 9.76 717640 12.68 02 V2SLCS 2058493 6.14 1327256 9.77 842643 12.68 03 V2SLCSD 1980204 6.14 1266913 9.77 792973 12.68 04 TRIP 14.10366 6.14 922722 9.77 540651 12.68 05 TRIP 1483834 6.14 1003667 9.77 594943 12.68 06 SB9-8 1509311 6.14 1038206 9.77 695977 12.68 07 SB4-14 1796860 6.14 1200938 9.76 705734 12.68 08 SB10-2RE 1432760 6.13 763722 9.76 286634* 12.68 69 10 11 _ 12 13 14 15 16 _ 17 18 19 20 21 22 ISi = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 IS3 (DCB) = 1,4-Dichlorobenzene-d4 AREA UPPER LIMIT = +100t of internal standard area AREA LOWER LIMIT = - 50!k of internal standard area RT .UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal- standard RT # Column used to flag values outside QC limits with an asterisk.. * Values outside of QC limits. page 1 of 1 � FORM VIII VOA OLM03.0 8A VOLATILE INTERNAL STANDARD AREA AMID RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File ID (Standard) : VSF6822 Date Analyzed: 12/01/04 Instrument ID: V5 Time Analyzed: 1107 GC Column: DB-624 ID: 0.25 (mm) Heated.Purge: (YIN) N IS1 AREA # RT # AREA # RT # AREA # RT # 12 HOUR STD 1404163 6.03 . UPPER LIMIT 2808326 6.53 LOWER LIMIT 702082 5.53 ---------- ------- ---------- ------- ------- ------- ------- EPA SAMPLE NO. O1 VBLKSA 1382808 6.02 02 VSALCS 1316502 6.04 03 VSALCSD 1213915 6.02 04 SB1-8 1213679 6.02 _ 05 SB3-6 1195155 6.03 06 SB3-6DL 1574935 6.03 07 08 09 10 11 12 -13 14 15 16 17 18 19 20 21 22 IS1 = Fluorobenzene AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk_ * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03.0 8B SEMIVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEK Case No. : SAS No SDG No.: MC1453 Lab File ID (Standard) : S2E2651 Date Analyzed: 12/01/04 Instrument ID: S2 Time Analyzed: 1640 ' IS1 DCB IS2 {NPT 7_S3AREA # RT # AREA # RT # RT ##12 HOUR STD 308569 7.65 1183975 9.64 12.51 UPPER LIMIT 617138 8.15 2367950 10.14 13..01 LOWER LIMIT 154285 7.15 591988 9.14 341358 12.01 EPA SAMPLE NO. 01 SBLK2B 275212 7.65 997962 9.63 586853 12.49 02 S2BLCS 264951 7.65 993261 9.64 587266 12.49 03 S2BLCSD 268133 7.64 1027659 9.63 592921 12.50 04 SB9-8 270102 7.64 996628 9.63 579366 12.49 05 SB-X 261244 7.64 967533 9.63 562095 12.48 06 SB3-6 207745 .7.66 907541 9.64 566981 12.49 07 SB4-14 251180 7.64 922522 9.63 551271 12:49 08 SB5-2 264313 7.64 985891 9-63 573759 12.49 09 SB2-2 256863 7.64 942639 9.63 557677 12.48 10 SB2-2MS 269660 7.64 1003549 9.63 578460 12.49 11 SB2-2MSD 258305 7.64 984473 9.63 572065 12.49 1 12 SB8-2- 269420. 7.64 997353 9.63 581762 12.48 13 SB10-2 255191 7.64 944034 9.63 553419 12.48 14 SB1-8 215064 7.65 734224 9.65 476653 12.55 15 _ 16 - - 17 -- 18 -- 19 20 21 _ 22 ISl (DCB) = 1,4-Dichlorobenzene-d4 IS2 (NPT) = Naphthalene-d8 IS3 (ANT) = Acenaphthene-d10 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50%- of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal .standard RT RT LOWER LIMIT 0.50 minutes of internal standard RT # Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of i OLM03.0 PORN! VIII SV-1 8C SEMIVOLATILE n TP'RNAL` STADIDARD AREA AND RT SUMMARY Lab Name: MITREM CORPORATION Contract: Lab Code: -MITKEM Case No. : SAS No. : SDG No MC1453 Lab File ID (Standard) : S2E2651 Date Analyzed: 12/01/04 Instrument ID:. S2 Time Analyzed: 1640 IS4 PHUT IS5 CRY IS6 PRY AREA # RT # AREA # RT # AREA # RT # 12 HOUR STD 114.4304 14.90 982601 18.19 868879 20.67 UPPER LIMIT 2288608 15.40 1565202 18.69 1737758 21.17 LOWER LIMIT 572152 14.40 491301 17.69 434440 20.17 EPA SAMPLE NO. 01 SBLK2B - 977082 14.88 890666 18.17 873182 20.65 02 S2BLCS 974894 14.88 883429 18.18 864157 20.-66 03 S2BLCSD 985051 14.89 896716 18.18 881845 20.65 04 SB9-8 963813 14.88 896831 18.17 865309 20.65 05 SB-X 931.959 14.89 871978 18.17 843134 20.64 06 SB3-6 951629 14.89 851224 18.17 817953 20.65 07 SB4-14 885813 14.88 806333 18.17 723663 20.65 08 SB5-2 964116 14.88 811114 18.18 701152 .20.66 09 SB2-2 928105 14.88 754720 18.17 567377 20.64 10 SB2-2MS 952153 14.88 741440 18.18 523184 20.64 11 SB2-2MSD 955612 14.88 770708 18.18 565767 20.63 12 SB8-2 965973 14.88 672575 18.19 423222* 20.66 13 SB10-2 897187 14.88 560562 18.17 269153* 20..64 14 SB1-8 573311 14.94 160170* 18.20 71706* 20.67 15 1.6 17 18 19 20 21 22 IS4 (PHU) = Phenanthrene-d10 IS5 (CRY) = Chrysene-d12 IS6 (PRY) = Perylene-d12 AREA UPPER LIMIT = +1009. of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT ## Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-2 OLM03.0 8B SEMIVOI,ATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITIEM CORPORATION Contract: Lab Code: MITIEM Case No. : SAS No. : SDG No. : MC1453 )` Lab File ID (Standard) S2E2701 Date Analyzed: 12/03/04 Instrument ID: S2 Time Analyzed: 0750 IS1 DCB IS2 NPT IS3 ANT AREA # RT # AREA # RT # AREA # RT # 12 HOUR STD 300976 7.55 1141451 9.53 649316 . 12.40 UPPER LIMIT 601952 8.05 2282902 10.03 1298632 -12.90 LOWER. LIMIT 150488 7.05 570726 9.03 324658 11.90 - -.- EPA SAMPLE NO. 01 SB8-2DL 230261 7.55 853939 9.53 491144 12.40 02 SB1-8DL. 211622 7.55 757279 - 9.54 419672 12.41 03 _ 04 05 _ 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 IS1 (DCB)- = 1,4-Dichlorobenzene-d4 IS2 (NPT) = Naphthalene-d8 IS3 (ANT) = Acenaphthene-d10 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-1 01EM03.0 8C SEMIVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: 14ITKEM Case No. : SAS No. : SDG No. : MC1453 Lab File ID (Standard) : S2E2701 Date Analyzed:. 12/03/04 Instrument ID: S2 Time Analyzed: 0750 IS4 PHN IS5 CRY IS6 PRY AREA # RT # # RT # AREA # RT � # ------------ ---------- ------- ---------- - 12 HOUR STD 1093443 14.80 984296 18.09 926949 20.50 UPPER LIMIT 2186886 15.30 1968592 18.59 1853898 21.00 LOWER LIMIT 546722 14.30 492148 - 17.59 463475 20.00 EPA SAMPLE NO. ------------ ---------- ------- ---------- ------- _ 01 SB8-2DL 816503 14.80 724713 18.08 651752 20.50 02 SB1-8DL 662964 14.81 487917* 18.10 284048* 20.52 03 64 05 _ 06 07 - - 08 09 10 11 12 -- 13 14 15 16 17 -- 18 -- - - - 19 20 21 -- - - 22 IS4 (PHN) =- Phenanthrene-d10 IS5 (CRY) =.Chrysene-d12 IS6 (PRY) = Perylene-d12 AREA UPPER LIMIT = +1000-. of internal standard area AREA LOWER LIMIT = - 501k of internal standard area RT UPPER LIMIT .= + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-2 OLM03.0