Loading...
70-92 Boston Street - Phase 1 Initial Site Investigation and Tier Classification - Aqueous Samples Data Report - January 2005 I, l ' a CORPORATION "En-vironmental Testing For The New Millennium" c i January 27,2005 TRC Solutions, Inc. Foot of John Street Lowell, MA 01852 Attn: Ms. Liz Denly - i, i RE: Client Project: Flynn Tan, Salem, Aqueous Samples Lab Project#: C1600 . Dear Ms. Denly: Enclosed please find the data report of the required analyses for the samples associated fJ with the above referenced project. If you have any questions regarding this report,please call me. i We appreciate your business_ Sinc el , Edward A. Lawler Laboratory Operations Manager 175 Metro Center Boulevard • Warwick, Rhode Island 02886-1755 (401) 732-3400 • Fax (401) 732-3499 • wwwmitkem.com SDG Narrative Mitkem Corporation.submits the enclosed data package in response to TRC Solutions' Flynn Tan aqueous sample project. Under this deliverable, analysis results are presented for five samples that were received on December 28 and 29, 2004 and logged in under Mitkem Work Order Number C1600. Analyses were performed per instruction in the chain of custody form. For reference, a copy of the Mitkem Work Order form is included for cross-referencing the client sample ID and laboratory sample ID. The analyses were performed according to Massachusetts DEP and EPA SW-846 methods,with results presented in a Level 4 format deliverable. The following observation and/or deviations are observed for the following analyses: 1. Volatile Organic Analyses: Samples were analyzed by Method 8260B. 1 Surrogate standards: four surrogate standards were spiked into each analysis. Surrogate / recoveries were within the MADEP and Mitkem QC limits. Mitkem's statistical QC limits listed on the surrogate report.form are wider than the MADEP 70%-130% limits for d4-1,2-dichloroethane. Lab control sample/lab control sample duplicate: spike recoveries were within the MADEP 70%- 130%limits with the exception of low recovery for 1,4-dioxane in V6WLCS and its duplicate and V6XLCS and its duplicate. This compound is also outside of the calibration acceptance criteria. A few compounds were recovered outside of the Mitkem statistical QC limits in V6XLCS and its duplicate. Lab fortified blank: laboratory fortified blanks at the 1 ug/L concentration level were analyzed to support a reduced reporting limit for vinyl chloride and 1,1-dichloroethene. Percent recoveries for both compounds in both LFB were within the QC limits. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Percent recoveries and replicate RPDs were within the MADEP 70%- 130% limits, as well as the Mitkem statistical QC limits, with the exception of low recovery for for styrene in both the MS and MSD. Replicate RPD exceeded the MADEP 30% limit for vinyl acetate. Sample analysis: samples MW-2 and MW-3 were reanalyzed at 2X and 1 OX dilutions respectively. No other unusual occurrences were noted during sample analysis. ©boje- r (i k, li- 2. MADEP VPH Analysis: Samples were analyzed by VPH Method 1.1. All samples were properly preserved. Surrogate standards:percent recoveries were within the QC limits. Lab control sample:spike_recoveries were within the QC limits for the lab control sample and duplicate lab control sample. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Percent recoveries and replicate RPDs were within the QC limits. Sample analysis:no unusual occurrences were.noted during sample analysis. 3. Semivolatile Organic Analyses: Samples were extracted by Method 3520C continuous liquid-liquid extraction, and analyzed by Method 8270C. Surrogate standards: six surrogate standards were spiked into each analysis. All . surrogate recoveries were within the Mitkem QC.limits. All compounds are within the MADEP 30-130%limits for base/rieutral and 15-110% limits for acid compounds with the exception of tribromophenol in samples MW-5, MW-6MS and MW-X recovered above the MADEP 110%QC limit. Lab control sample: spike recoveries were within the MADEP well as the Mitkem statistical QC limits with the exception of hexachlorocyclopentadiene recovered above the Mitkem limit but within the MADEP limit. Mitkem LCS QC limits are generally within the MADEP 40-140%limits for base/neutral and 30-136% limits for acid compounds with the exception of:difficult analytes. These QC limits and the difficult compounds have been statistically determined per method requirements. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Percent recoveries were within the MADEP 40-140%limits for base/neutral and 30-130%limits for acid compounds with the exception of unusually low recovery for 3,3'dichlorobenzidirie in the MS and MSD. A few compounds were outside of the Mitkem statistical QC limits. Replicate RPDs were within the MADEP and Mitkem limits with the exception of 3,3'-dichlorobenzidine- Sample analysis: the compounds aniline, azobenzene and acetophenone were not included on the analyte list for this project. No other unusual occurrences were noted during sample analysis. �03� Al IT K ENT CORPORATION Analysis Report:Volatile Petroleum Hydrocarbons Client TRC MA Analysis MADEP VPH 1.1 Client ID: VBLK4H Date Analyzed: 12/29/2004 Lab ID: MB-16283 Aliquot Used for Analysis:5 ml Matrix: Aqueous Concentration in:ug/L Dilution Factor. 1 Reporting Target Anal tomes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND' 5 Naphthalene ND 5 QC Batch: 16283 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9'-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 97 2,5-Dibromotoluene(PID) 93 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performancefacceptance standards for the required.0A1QC procedures were achieved. No significant modifications were made to this method_ VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-MB CORPORATION i Analysis Report: Volatile Petroleum Hydrocarbons i Client TRC MA Analysis: MADEP VPH 1.1 Client ID: V13LK4J Date Analyzed: 12/30/2004 Lab ID: MB-16311 Aliquot Used for-Analysis: 5 ml Matrix Aqueous Concentration in: ug/L Dilution Factor. 1 Reporting Target Anal�tes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene NO 5 QC Batch: 16311 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12.Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 106 2,5-Dibromotoluene(PID) 107 ND=Not Detected Except where noted in'the Project Narrative, all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved, No significant modifications were made to.this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1600-MB CORPOIR ON Analysis Report:Volatile Petroleum Hydrocarbons 1 Client: TRC MA Analysis: MADEP VPH 1-1 Client ID: VBLK4L Date Analyzed: 12/31/2004 Lab ID: MB-16321 Aliquot Used for Analysis: 5 ml Matrix:- Aqueous Concentration in:ug/L Dilution Factor_ 1 Reporting Target Analvtes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 -Naphthalene ND 5 QC Batch: 16321 VPH Rannes C5 C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 102 2,-5-Dibromotoluene(PID) 96 ND= Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method_ VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C 1600-MB I CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Matrix Spike Summary i Client; TRC MA Client ID:- MW-6 Matrix: Aqueous Lab ID for Matrix Spike: C1600-02BMS Analysis Date for Matrix Spike: 12/3012004 Lab ID for MS Duplicate: C1600-02BMSD Analysis Date for MS Duplicate: 12/30/2004 Analysis: MADEP VPH 1.1 %o Recovery Analyte Matrix Spike Matrix Spike Duplicate RPD[%] Benzene 93 92 1 Ethylbenzene 88 90 2 Toluene 88 90 2 o-Xylene 90 91 1 m-and p-Xylenes 86 87 1 MTBE 100 101 0 Naphthalene 98 102 4 VPH Ranges C5-C8 Aliphatics 111 113 2 C9--C10 Aromatics 109 104 5 C9-C12 Aliphatics 71 70 1 Page 1 of 1. C1600-MS/MSD CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client: TRC MA Matrix: Aqueous Lab ID for Blank Spike: LCS-16283 Analysis Date for Blank Spike: 12/29/2004 __- Lab ID for BS Duplicate: LCSD-16283 Analysis Date for BS Duplicate: 12/29/2004 Analysis: MADEP VPH i:1 %Recover, Analyte Blank Spike Blank Shrike Duplicate RPD Benzene 106 98 7 Ethylbenzene 103 96 7 Toluene 105 97 7 o-Xylene 103 96 7 m-and p-Xylenes 104 97 6 MTBE 106 99 6 Naphthalene 92 82 11 VPH Ranges C5-C8 Aliphatics 118 108 9 C9 -C10 Aromatics 100 95 5 C9-CI Aliphatics 99 90 10 QC Batch: 16283 Page 1 of 1 C1600-LCS CORPORATION Analysis Report: Volatile.Petroleum Hydrocarbons Lab Control Summary Client TRC MA Matrix: Aqueous Lab ID for Blank Spike: LCS-16311 Analysis Date for Blank Spike: 12/30/2004 Lab ID foe BS Duplicate: . LCSD-16311 Analysis Date for BS Duplicate: 12130/2004 Analysis: MADEP VPH 1.1 % Recovery Anal a Blank SLAP Blank Spike Duplicate RP_ D(%) Benzene 104 96 g Ethylbenzene 104 96 g Toluene 104 95 9 o-Xylene 104 97' 6' m-and p-Xylenes 105 97 7 MTBE 111 106 4 Naphthalene 116 115 0 VPH Ranges C5-C8 Aliphatics 116 103 12 C9-C10 Aromatics 103 97 6 C9-C12 Ariphatics 99 90 10 QC Batch: 16311 Page 1 of 1 C1600-LCS CORPORATION— Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client TRC_MA Matrix: Aqueous Lab.ID for Blank Spike: LCS-16321 Analysis_Date for Blank Spike: 12/31/2004 Lab ID for BS Duplicate: LCSD-16321 Analysis Date for BS Duplicate: 12/31/2004 . Analysis: MADEP VPH 1.1 % Recovear Analyte, Blank Spike Blank Spike Du Acate RPD Benzene 105 100 4 Ethylbenzene 104 100 3 Toluene 104 100 3 j o-Xylene 104 100 3 m-and p-Xylenes 104 101 2 MTBE 106 107 0 Naphthalene 103 112 8 VPH Ranges C5-C8 Aliphatics 119 111 7 C9-C10 Aromatics 102 101 1 C9-C12 Aliphatics 105 100 5 QC Batch: 16321 Page 1 of 1 C1600-LCS CORPORATION I Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/28/04 Client ID: MW-5 Date Received: 12/28/04 Lab ID: C1600-01C Date Extracted: 1/10/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17/05 F2 Concentration in:ug/L Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics ND .200 C19-C36 Aliphatics. ND 200 . C11 -C22 Aromatics 260-- 100 Target Analytes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5. Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a)anthracene ND 5 Chrysene -ND 5 Benzo(b)Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5. Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo (ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 78% o-Terphenyl 80% 2-Fluorobiphenyl 79% 2-Bromonaphthalene 68% ND= Not Detected Except where noted in the Project Narrative,.all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate) analytes. Page 1 of 1 C1600-01C CORPORATIO. Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA' Analysis: MADEP EPH 04/1.1 Date Collected: 12/29/04 Client ID: MW-6 Date Received:.12129/04 Lab ID. C1600-02C Date Extracted: 1/1.0/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17105 F2 Concentration in:ug/L Dilution: 1 Reporting EPH Ranges Results Limits C9-CI Aliphatics ND 200 C19-C36 Aliphatics ND 200 C11 -C22 Aromatics. 120 100 Target Anahrtes Naphthalene ND 5 2-Methyinaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 ) Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi) perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 78% o-Terphenyl 78% 2-Fluorobiphenyl 74% 2-Bromonaphthalene 67% ND= Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1600-02C 1 i CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client TRC MA Analysis: MADEP EPH 0411.1 Date Collected: 12/29/04 Client ID: MW X Date-Received: 12/29/04 Lab ID: C1600-03C Date Extracted:1/10/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17/05 F2 Concentration in: ug/L Dilution:.1 Reporting EPH Ranges Results Limits C9-CI Aliphatics ND 200 CI C36 Aliphatics ND 200 CI -C22 Aromatics ND 100 Target Analytes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND - 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd) pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 83% o-Terphenyl 84% 2-Fluorobiphenyl 77% 2-Bromonaphthalene 72% ND=Not Detected Except where noted in the Project Narrative, all QAIQC procedures required by the EPH method were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-03C M ITKE -Ai CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons j Client: TRCMA . Analysis: MAD_EP EPH 04/1.1 Date Collected.: 12/28104 Client ID: Date Received: 12/28/04 Lab ID: MB-16432 Date Extracted: 1/10/05 Matrix Aqueous Date Analyzed: 1/17/05 F1,1/17/05 F2 Concentration in:ug/L Dilution: 1 Reporting EPH Ranggs Results Limits C9-C18 Aliphatics ND 200 C19-C36 Aliphatics ND 200 CI.-C22 Aromatics 310 100 Target Anabdes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5' Acenaphthene ND 5 Fluorene ND 5 Phenanthrene. ND 5 Anthracene . ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi) perylene ND 5 QC Batch: MB-16432 Surrogate.Recovery: Chlorooctadecane 92% o-Terphenyl 92% 2-Fluorobiphenyl 72% 2-Bromonaphthalene 69% ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required.by the EPH method were followed, and all performancelacceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC (surrogate)analytes. Page 1 of 1 MB-164K CORPORATION Analysis Report: Lab Control Sample Client TRC Date Extracted for LCS/LCSD: 1/10/05 Matrix: Aqueous Date Analyzed for LCS: 1/17105 Lab ID for Lab Control Sample(LCS): LCS-16432 Date Analyzed for LCSD: 1/17/05 Lab ID for Lab Control Sample Duplicate(LCSD): LCSD-46432 . Analysis: MADEP EPH 04-1.1 MADEP EPH - F1 -ALIPHATICS Ana We %Recovery LCS LCSD % RPD Nonane C9 32 39 20 Decane C10 41 44 9 Dodecane C12 -50 51 1 Tetradecane C14 60 61 2 Hexadecane C16 72 71 1 Octadecane C18 79 76 4 Nonadecane C19 81 78 4 Eicosane C20 87 84 4 Docosane C22 85 82 4. Tetracosane C24 83 79 . 5 Hexacosane C26 84 80 5 Octacosane C28 84 80 5 Triacontane.C30 83 79 5 Hexatnacontane C36 82 78 5 C9-C18 Aliphatics 56 57 3 C19-C36 Aliphatics 84 80 5 Surrogate Recovery LCS LCSD Chlorooctadecane 100% 92% % Naphthalene Breakthrough: 0.0 0.0 % 2-methylnaphtalene Breakthrough: 0.0 0.0 Page 1 of 2 eph.Ics MIT KE -NI CORPORATION Analysis Report: Lab Control Sample Client TRC Date Extracted for LCS/LCSD: 1110/05 Matrix: Aqueous Date Analyzed for LCS: 1/17/05 Lab ID for Lab Control Sample(LCS): LCS-16432 Date Analyzed for LCSD: 1/17/05 Lab ID for Lab Control Sample Duplicate(LCSD): LCSD-16432 Analysis: MADEP EPH 04-1.1 MADEP EPH - F2 -AROMATICS Anal e % Recovery LCS LCSD % RPD Naphthalene 50 53 7 2-Methylnaphthalene 50 52 5 Acenaphthylene 63 63 1 Acenaphthene 70 71 1 Fluorene 72 72 1 Phenanthrene 80 80 1 Anthracene 80 82 1 Fluoranthene 83 84 0 Pyrene 83 83 0 Benzo(a)anthracene 80 80 1 Chrysene 87 87 1 Benzo(b)Fluoranthene 82 80 1 Benzo(k) Fluoranthene 82 81 2 Benzo(a).pyrene 84 83 1 Indeno(1,2,3-cd)pyrene al 80 1 Dibenzo(a,h)anthracene 74 73 1 Benzo(ghi)perylene 79 78 1 C11 -C22 Aromatics 75 76 0 Surrogate Recovery. LCS LCSD o-Terphenyl 91% 89% 2-Fluorobiphenyl 76% 76% 2-Bromonaphthalene 72% 71% Page 2 of 2 eph.lcs i 1 I • ' I ' L i i Analysis Report: Matrix Spike Client TRC Date Extracted for MS/MSD: 1/10/05 Matrix: Aqueous Date Analyzed for MS: 1/17/05 i Client ID: MW-6 Date Analyzed for MSD: 1/17/05 Lab ID for Matrix Spike(MS): C1600-02CMS Lab ID for Matrix Spike Duplicate(MSD):C1600-02CMSD Analysis: MADEP EPH 04-1.1 MADEP EPH - F1 -ALIPHATICS Anal e %Recovery - MS MSD % RPD i Nonane C9 30 19 45 Decane C10 39 27 38 Dodecane C12 51 43 17 Tetradecane C14 58 50 15 Hexadecane C16 70 65 8 Octadecane C18 77 73 5 Nonadecane C19 79 76 4 i Eicosane C20 86 84 2 Docosane C22 86 84 2 Tetracosane C24 83 82 1 Hexacosane C26 84 83 1 Octacosane C28 83 82 1 Triacontane C30 83 82 1 Hexatriacontane C36 83 81 2 C9-C18 Aliphatics 54 46 16 C19-C36 Aliphatics 83 82 2 Surrogate Recovery MS MSD Chlorooctadecane 97% 95% Pagel of 2 eph.ms/msd. lA EPA SAMPLE NO-. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.': MC1600 Matrix: (soil/water) WATER Lab Sample ID-:. C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5105 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONC19 TRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5- U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 0 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromet e 5 U 75-35-4-----=---1,1-Dichloroethene 1 U 67-64-1---------Acetone 2 J 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U ) 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 1 1 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---=-----2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran S U 71-55-6---------1,1,1-Trichloroethane S U 563-58-.6--------1,1=Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride S U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5-------- 1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl_-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEEP MW-2 lab Name: MITFEm CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. :, MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID; V6D5105 Level: (low/med) IOW Date Received: 12/29/04 1 Moisture: not dec. _ Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 - Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) ---------------- CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane S. U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene _ 5 U 591-78-6--------2-Hexanone 5 U 124-48-1- - ------Dibromochloromethane _ 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 64 630-20-6=-------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-.5---------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 15 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 24 95-49-8----------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 8 95-63-6---------1,2,4-Trimethylbenzene 180 135-98-8--------sec-Butylbenzene 14 99-87-6---------4-Isopropyltoluene 4 J 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7---------1,4-Dichlorobenzene 1 J 104-51-8--------n-Butylbenzene 9 95-50-1---------1,2-Dichlorobenzene 2 J 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1----=-7-1,-2,4-Trichlorobenzene 5 U 87=68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 13 FORM I VOA OLM03.'0 lA EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5105 Level: (low/med) IOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624: ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87.-61-6---------1,2,3-Trichlorobenzene 5 U . 60-29-7----------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U .637-92-3--------Ethyl tert=butyl ether .5 U 994-05-8--------tert-Amyl methyl ether 5. 0 123-91-1--------1,4.-Dioxane 100 U FORM I VOA OLM03-0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2DL Lab. Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL- Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5139 Level: (low/med) LOW Date Received: 12/29/04. Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 2.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume: AUL) CONCE24'I'f2ATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 10 U 74-87-3---------Chloromethane 10 U 75-01-4---------Vinyl Chloride 4 U 74-83-9---------Bromomethane 10 U 75-00-3---------Chloroethane 10 U 75-69-4---------Trichlorofluoromethane 10 U 75-35-4---------1,1-Dichloroethene 2 .0 67-64-1---------Acetone 10 U 74-88-4---------Iodomethane 10 U 75-15-0---------Carbon Disulfide 10 U 15-09-2---------Methylene, Chloride 10 U 156-60-5--------trans-1,2-Dichloroethene 10 U 1634-04-4-------Methyl tert-butyl ether 10 U 75-34-3---------1,1-Dichloroethane 10 U 108-05-4--------Vinyl acetate 10 U 78-93-3---------2-Butanone 10 U 156-59-2--------cis-1,2-Dichloroethene 10 U 590-20-7--------2,2-Dichloropropane 10 U 74-97-5---------Bromochloromethane 10 U 67-66-3---------Chloroform 10 U 109-99-9--------Tetrahydrofuran 10 U 71-55-6---------1,1,1-Trichloroethane 10 U 563-58-6--------1,1-Dichloropropene 10 U 56-23-5----------Carbon Tetrachloride 10 U 107-06-2--------1,2-Dichloroethane 10 U 71-43-2---------Benzene 10 U 79-01-6---------Trichloroethene 10 U 78-87-5---------1,2-Dichloropropane 10 U 74-95-3---------Dibromomethane 10 U 75-27-4---------Bromodichloromethane 10 U 10061-01-5------cis-1,3-Dichloropropene 10 U 108-10-1--------4-Methyl-2-pentanone 10 U 108-88-3--------Toluene 10 U 10061-02-6------trans-1,3-Dichloropropene 10 U FORM I VOA OLM03.0 IA. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2DL Lab Name: MITKEK CORPORATION Contract: Lab Code: MITKEK Case No. : SAS No. : SDG No. : MC1600 ) Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5139 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. _ Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution .Factor: 2.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2.Trichloroethane 10 U 142-28-9--------1,3-Dichloropropane 10 U 127-18-4--------Tetrachloroethene 10 U 591-78-6--------2-Hexanone 10 U 124-48-1--------Dibromochloromethane 10 U 106-93=4-------=1,2-Dibromoethane 10 U 108-90-7--------Chlorobenzene 57 D 630-20-6--------1,1,1,2-Tetrachloroethane 10 U 100-41-4--------Ethylbenzene 10 U ----------------m,p-Xylene 10 U \ 95-47-6---------o-Xylene 10 U 1330-20-7-------Xylene (Total) 10 U 100-42-5--------Styrene 10 U 75-25-2---------Bromoform 10 U 98-82-8---------Isopropylbenzene 13 D 79-34-5---------1,1,2,2-Tetrachloroethane 10 U 108-86-1--------Bromobenzene 10 U 96-18-4---------1,2,3-Trichloropropane_ 10 U 103-65-1--------n-Propylbenzene 23 D 95-49-8---------2-Cblorotoluene 10 U 108-67-8---------1,3,5-Trimethylbenzene 10 U 106-43-4--------4-Chlorotoluene 10 U 98-06-6---------tert-Butylbenzene . .6 DJ 95-63-6---------1,2,4-Trimethylbenzene 220 D 135-98-8--------sec-Butylbenzene 13 D 99-87-6---------4-Isopropyltoluene 4 DJ 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 104-51-8--------n-Butylbenzene 9 DJ 95-50-1---------1,2-Dichlorobenzene 10 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 87-68-3---------Hexachlorobutadiene 10 U 91-20-3----------Naphthalene 14 D FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSISDATA SHEEP MW-2DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5139 Level: -(low/med) IOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 2.0 Soil Extract Volume: (uL) Soil Aliquot Volume:. uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 81-61-6---------1-,2,3-Trichlorobenzene 10 U 60-29-7---------Ether 10 U 108-20-3--------Dlisopropyl Ether 10 U 637-92-3------=-Ethyl tent-butyl ether 10 U 994-OS-8--------tert-Amyl methyl ether 10 U 123-91-1--------1,4-Dioxane 200 U FORM I VOA OLMO3.0 iA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG: No. : MC1600 ) Matrix: (soil/water) WATER Lab Sample .ID: C1600-04A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5104 Level: . (low/med) LOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: . DB-624 ID: 0.25 (mn) Dilution Factor: .1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: __(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 1 J 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone 4 J 74-88-4---------Iodomet e 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene. Chloride 5 U ) 156-60-5--------trans-l;2-Dichloroethene 5 U 1634-04-4-------Methyl: tert=butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4-----=--Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dic oroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5----------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6------ 1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2---------1,2-Dichloroethane 5 U 71-43-2---------Benzene, 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03. l YA EPA SAMPLE NO_ VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKE4 Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04A. Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5104 Level: (low/med) Low Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0:25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _ _ UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3=Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7----------Chlorobenzene - 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Eutylbenzene 5 U ----------------m,p-Xylene 34 95-47-6---------o-Xylene 11 1330-20-7-------Xylene (Total) 45 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 4 J 79-34-5---------1,1,2,2-Tetrachloroethene 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 310 E 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 10 95-63-6---------1,2,4-Trimethylbenzene 480 E 135-98-8--------sec-Butylbenzene 10 99-87-6---------4-Isopropyltoluene. 44 541-73-1--------1;3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 2 J 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 6 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 54 FORM I VOA OLM03.0 :CA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5104 Level: .(low/med) IOW Date Received: 12/29/04 45 Moisture: not .dec_ Date Analyzed: 01/04/05 GC Column: DB-624 ID:. 0.25 (mm) Dilution Factor: IA Soil Extract Volume: (uL) Soil Aliquot Volume: _ -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7----------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl .tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03:0 ) IA. EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3DL Lab. Name: MITKEM CORPORATION Contract: Lab Code:_ MITKEM Case' No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5145 Level: (low/med) LOW Date Received: 12/29/04 a Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (nun) Dilution Factor: 10.0 Soil Extract Volume:-_ (uL) Soil Aliquot Volume: �UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug%Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 50 U 74-87-3---------Chloromethane 50 U 75-01-4---------Vinyl Chloride 20 U 74-83-9---------Bromomethane 50 U 75-00-3---------Chloroethane 50 U 75=69-4---------Trichlorofluoromethane 50 U 75-35-4---------1,1-Dichloroethene 10 U 67-64-1---------Acetone' 50 U 74-88-4---------Iodomethane 50 U 75-15-0-------2-Carbon Disulfide -50 U 75-09-2---------Methylene Chloride 50 U 156-60-5--------trans-1,2-Dichloroethene 50 U 1634-04-4-------Methyl tert-butyl ether 50 U 75-34-3---------1,1-Dichloroethane 50 U 108-05-4---------Vinyl acetate 50 U 78-93-3---------2-Butanone 50 U 156-59-2--------cis-1,2-Dichloroethene 50 U 590-20-7--------2,2-Dichloropropane 50 U 74-97-5---------Bromochloromethane 50 U 67-66-3---------Chloroform_ 50 .0 109-99-9--------Tetrahydrofuran 50 U 71-55-6---------1,1,1-Trichloroethane 50 U 563-58-6--------1,1-Dichloropropene 50 U 56-23-5---------Carbon Tetrachloride 50 U 107-06=2--------1,2-Dichloroethane 50 U 71-43-2---------Benzene 50 U 79-01-6---------Trichloroethene 50 U 78-87-5---------1,2-Dichloropropane 50 U 74-95-3---------Dibromomethane 50 U 75-27-4---------Bromodichloromethane 50 U 10061-01-5------cis-1,3-Dichloropropene 50 U 108-10-1--------4-Methyl-2-pentanone 50 U 108-88-3----- ----Toluene 50 U 10061-02-6------trans-1,3-Dichloropropene 50 U FORM I VOA OLM03.0 lA _ EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET. MW-3DL Lab Name: MITKEM CORPORATION Contract: Lab Code:. MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600704ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5145 Level: (low/med) LOW Date Received: 12/29/04 's Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 10.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO, COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 50 U 142-28-9--------1,3-Dichloropropane 50 U 127-18-4--------Tetrachloroethene 50 U 591-78-6--------2-Hexanone 50 U 124-48-1--------Dibromochloromethane 50 U 106-93-4--------1,2-Dibromoethane 50 U 108-90-7--------Chlorobenzene 50 U 630-20-6--------1,1,1,2-Tetrachloroethane 50 U 100-41-4--------Eutylbenzene 50 U ----------------m,p-Xylene 26 DJ 95-47-6---------o-Xylene _ 50 U 1330-20-7-------Xylene (Total) 26 DJ 100-42-5--------Styrene 50 U 75-25-2---------Bromoform 50 U 98-82-8---------Isopropylbenzene 50 U 79-34-5---------1,1,2,2-Tetrachloroethane 50 U 108-86-1--------Bromobenzene 50 U 96-18-4---------1,2,3-Trichloropropane 50. 0 103-65-1--------n-Propylbenzene 50 U 95-49-8---------2-Chlorotoluene 50 U 108-67-8--------1,3,5-Trimethy nzene 470 D 106-43-4--------4-Chlorotoluene 50 U 98-06-6---------tert-Butylbenzene 50 U 95-63-6---------1,2,4-Trimethylbenzene 1200 D 135-98-8--------sec-Butylbenzene 50 U 99-87-6---------4-Isopropyltoluene 50 U 541-73-1--------1,3-Dichlorobenzene 50 U 106-46-7--------1,4-Dichlorobenzene 50 U 104-51-8--------n-Butylbenzene 50 U 95-50-1---------1,2-Dichlorobenzene 50 U 96-12-8---------1,2-Dibromo-3.-chloropropane_ 50 U 120-82-1--------1,2,4-Trichlorobenzene 50 U 87-68-3---------Hexachlorobutadiene 50 U 91-20-3---------Naphthalene 58 D FORM I VOA OZM03.0 1A EPA SAMPLE NO: VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5145 Level: (low/med) LOW Date- Received: 12/29/04 1 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 10.0 Soil Extract Volume: _(uL) Soil Aliquot Volume: _ (UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 4 87-61-6----------1,2,3-Trichlorobenzene. 50 U 60-29-7---------Ether 50 U 108-20-3--------Diisopropyl Ether 50 U 631-92-3--------Ethyl tert-butyl ether 50 U 994-05-8--------tert-Amyl methyl ether 50 U 123-91-1--------1,4-Dioxane 1000 U FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET. MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A. Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5099 Level: (low/med) LOW Date Received: 12/28/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane T 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride. 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3------- 1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dic loroethene 5 LT 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrah, ofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6-------- 1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethene 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM . Case No. : SAS No. : SDG No. : - MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5099 Level: (low/med) IOW Date Received: 12/28/04 o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution .Factoi-:- 1.0 Soil Extract Volume: —(uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U - 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochlorome e 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene 5 U ----------------m,p-Xylene 5 .0 95-47-6--------70-Xylene_ 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1, 1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U. 108-67-8--------1,3;5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 2 J 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane _ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene _ 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03.0 1A EPA SAMPLE .NO.= VOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITI! CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A Sample.wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5099 Level: (low/med) LOW Date Received: 12/28/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot. Volume: JUL) .CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 6.0-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 1 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5100 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. _ Date Analyzed:, 01/04/05 GC Column: DB-624 ID:. 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene .1 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3--=-------1,1-Dichloroethene 5 U 108-05-4-- -----Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1, 1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2------=-1,2-Dichloroethene 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74.-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6-------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0. lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 ) Matrix: (soil/water) WATER Lab Sample ID: C1600-02A Sample wt/vol: -5.000 (g/mL) ML Lab File' ID: V6D5100 Level: (low/med) LOW Date Received: 12./29/04 Moisture: not dec. Date Analyzed. 01/04/05 GC Column: DB-624 . ID: 0.25 (am) Dilution- Factor; 1.0 Soil Extract Volume: _ (uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127 18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2=Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroeth.ane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropy nzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3, 5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3=chloropropane_ 5 U 120-82-1--------1;2,4-Trichiorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE-ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM. CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02A .Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5100 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1'.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U- 60-29-7---------Ether _ 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 15 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane .100 U FORM I VOA OLM03:0 3.A EPA- SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample 'ID: C1600-02AMS Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5143 Level: (low/med) LOW Date Received: 12/29/04 U Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _ _ UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ' UG/L Q 75-71-8---------Dichlorodifluoromethane 48 74-87-3---------Chloromethane 49 75-01-4---------Vinyl Chloride 48 74-83-9---------Bromomethane 55 75-00-3---------Chloroethane _ 46 75-69-4---------Trichlorofluoromethane _ 58 75-35-4---------1, 1-Dichloroethene 50 67-64-1---------Acetone 30 74-88-4---------Iodomethane 55 75-15-0---------Carbon Disulfide 43 \ 75-09-2---------Methylene Chloride 51 ) 156-60-5--------trans-1,2-Dichloroethene 40 1634-04-4-------Methyl tert-butyl ether 78 75-34-3---------1,1-Dichloroethene 39 108-05-4--------Vinyl acetate 66 78-93-3---------2-Butanone 33 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropane 37 74-97-5---------Bromochloromethane 44 67-66-3---------Chloroform 42 109-99-9--------Tetrahydrofuran 54 71-55-6---------1, 1,1-TYichloroethane 40 563-58-6--------1,1-Dichloropropene _ 43 56-23-5---------Carbon Tetrachloride 39 107-06-2--------1,2-Dichloroethane 42 71-43-2---------Benzene 43 79-01-6---------Trichloroethene 43 78-87-5---------1,2-Dichloropropane 42 74-95-3---------Dibromomethane 45 75-27-4---------Bromodichloromethane 39 10061-01-5------cis-1,3-Dichloropropene 38 108-10-1--------4-Methyl-2-pentanone 37 108-88-3--------Toluene 44 10061-02-6------trans-1,3-Dichloropropene 371 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALLYSIS DATA .SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: 'Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMS Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5143 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: _ (uL) Soil .Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 45 142-28-9--------1,3-Dichloropropane 46 127-18-4--------Tetrachloroethene_ -51 591-78-6--------2-Hexanone 35 124-48-1--------Dibromochloromethane 40 106-93-4--------1,2-Dibromoethane 48 108-90-7--------Chlorobenzene 49 630-20-6--------1,1,1,2-Tetrachloroethane 44 100-41-4--------Ethylbenzene 47 ----------------m,p-Xylene 92 95-47-6---------o-Xylene 46 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 31 75-25-2---------Bromoform 35 98-82-8---------Isopropylbenzene 46 79-34-5---------1,1,2,2-Tetrachloroethane 52 108-86-1--------Bromobenzene 50 96-18-4---------1,2,3-Trichloropropane 44 103-65-1--------n-Propylbenzene 50 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 44 106-43-4--------4-Chlorotoluene 51 98-06-6---------tert-Butylbenzene 50 95-63-6---------1,2,4=Trimethylbenzene 44 135-98-8--------sec-Butylbenzene 50 99-87-6---------4-Isopropyltoluene 50 541-73-1--------1,3-Dichlorobenzene 51 106-46-7--------1,4-Dichlorobenzene _ 52 104-51-8--------n-Butylbenzene 52 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3-chloropropane_ 45 120-82-1--------1,2,4-Trichlorobenzene 50 87-68-3---------Hexachlorobutadiene 47 91-20-3---------Naphthalene 52 FORM I VOA OLM03:0 1A EPA SAMPLE NO: VOLATILE ORGANICS ANALYSIS DATA SHEET , V6WLCSD Lab Names MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No: : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5095 Level: (low/med) LOW Date Received: o Moisture: not dec. -Date Analyzed: 01/04/05 GC Coles: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 i Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane. 48 142-28-9--------1,3-Dichloropropane 47 127-18-4--------Tetrachloroethene 49 591-78-6--------2-Hexanone - .37 124-48-1--------Dibromochlorome e 44 fr 106-93-4--------1,2-Dibromoethane 48 108-90-7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetrachloroethane 45 a 100-41-4--------Ethylbenzene 47 ----------------m,p-Xylene 94 95-47-6---------o-Xylene 48 _ 1330-20-7-------Xylene (Total)- 140 100-42-5---------Styrene 48 75-25-2---------Bromoform 43 98-82-8---------Isopropyl nzene 47 79-34-5---------1,1,2.,2-Tetrachloroethane 45 108-86-1--------Bromobenzene 46 96-18-4---------1,2,3-Trichloropropane 43 103-65-1--------n-Propylbenzene 46 95-49-8---------2-Chlorotoluene 47 108-67-8--------1,3,5-Trimethylbenzene 46 106-43-4--------4-Chlorotoluene 46 98-06-6---------tert-Butylbenzene 45 95-63-6---------1,2,4-Trimethylbenzene 46 135-98-8--------sec-Butylbenzene 46 99-87-6------- 4-Isopropyltoluene . 46 541-73-1--------1,3-Dichlorobenzene 47 106-46-7--------1,4-Dichlorobenzene 47 104-51-8--------n-Butylbenzene 46 1" 95-50-1---------1,2-Dichlorobenzene 47 96-12-8---------1,2-Dibromo-3-chloropropane_ 39 120-82-1--------1,2,4-Trichlorobenzene 46 87-68-3---------Hexachlorobutadiene 43 91-20-3---------Naphthalene 46 fi FORM I VOA OLM03 .0 ) 1A. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITIEM. Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: -LCSD-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5095 Level: (low/med) LOW Date Received: - Moisture: not dec. Date Analyzed: 01/04/05 GC.Column: DB-624 ID:. 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: _ (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg_) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 46 60-29-7---------Ether 53 108-20-3--------Diisopropyl Ether 50 637-92-3--------Ethyl tert-butyl ether 50 994-05-8--------tert-Amyl methyl ether 52 123-91-1--------1,4-Dioxane 540 FORM I VOA OLM03.0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS. DATA SHEET V6WLFB Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LFB.-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5096 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB=624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-01-4---------Vinyl Chloride 0.8 1 75-35-4---------1, 1-Dichloroethene 1 FORM I VOA OLM03.0 ) lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5134 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Coles: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: —JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 48 74-87-3---------Chloromethane 43 75-01-4---------Vinyl Chloride 45 74-83-.9---------Bromomethane 58 75-00-3---------Chloroethane 47 75-69-4---------Trichlorofluoromethane 59 75-35-4---------1,1-Dichloroethene 50 67-64-1---------Acetone 46 74-88-4----------Iodomet e 55 75-15-0---------Carbon Disulfide 48 75-09-2---------Methylene Chloride 51 156-60-5--------trans-1,2-Dichloroethene 42 1634-04-4-------Methyl tert-butyl ether 79 75-34-3---------1.,1-Dichloroethane _ 40 108-05-4--------Vinyl acetate 69 78-93-3---------2-Butanone 38 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropane 38 .74-97-5---------Bromochloromethane 45 67-66-3---------Chloroform 44 109-99-9--------Tetrahydrofuran 52 71-55-6---------1,1,1-Trichloroethane 41 563-58-6--------1,1-Dichloropropene 44 56-23-5---------Carbon Tetrachloride 42 107-06-2.--------1,2-Dichloroethane 43 71-43-2---------Benzene 44 79-01-6---------Trichloroethene 44 78-87-5---------1,2-Dichloropropane _ 43 74-95-3---------Dibromomethane 45 75-27-4---------Bromodichloromethane 41 10061-01-5------cis-1,3-Dichloropropene 40 108-10-1--------4-Methyl-2-pentanone 36 108-88-3--------Toluene 45 10061-02-6------trans-1,3-Dichloropropene 40 FORM I VOA OLM03:0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No: : SAS No. : SDG No:: MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16380 Sample wt/vol: 5,000 (g/mL) ML Lab File ID: V6D5135 y Level: (low/med) LOW DAte "Received: o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENiRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 44 74-87-3---------Chloromethane 44 75-01-4---------Vinyl Chloride 47 74-83-9---------Bromomethane 58 75-00-3----------Chloroethane 48 75-69-4---------Trichlorofluoromethane 58 75-35-4---------1,1-Dichloroethene 51 67-64-1---------Acetone 41 74-88-4---------Iodomethane` 55 75-15-0---------Carbon Disulfide 48 75-09-2---------methylene Chloride 51 156-60-5--------trans-1,2-Dichloroethene 41 1634-04-4-------Methyl tert-butyl ether 79 75-34-3---------1,1-Dichloroethane 39 108-05=4--------Vinyl acetate 39 78-93-3---------2-Butanone 36 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropane 38 74-97-5---------Bromochloromethane 45 67-66-3---------Chloroform 43 109-99-9--------Tetrahydrofuran 52 71-55-6---------1,1,1-Trichloroethane 41 563-58-6--------1,1-Dichloropropene 44 56-23-5---------Carbon Tetrachloride 40 107-06-2--------1,2-Dichloroethane 42 71-43-2---------Benzene 43 79-01-6---------Trichloroethene _ 43 78-87-5---------1,2-Dichloropropane 42 74-95-3---------Dibromomethane 44 75-27-4---------Bromodichloromethane 41 10061-01-5------cis-1,3-Dichloropropene 40 108-10-1--------4-Methyl-2-pentanone 36 108-88-3--_-----Toluene 44 10061-02-6------trans-1,3-Dichloropropene. 39 FORM I VOA OLM03:0 ) IA. EPA SAMPLE No. VOLATILE ORGANICS ANALYSIS DATA..SHEET VGXLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: . (soil/water) WATER Lab Sample ID: LCSD-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5135 Level: (low/med) LOW Date Received: Moisture: not dec. _ Date Analyzed. 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 44 142-28-9--------1,3-Dichloropropane 46 127-18-4--------Tetrachloroethene 52 $91-78-6--------2-Hexanone 37 .. 124-48-1--------Dibromochloromethane 43 106-93-4--------1,2-Dibromoethane 47 108-90-7--------Chlorobenzene 48 630-20-6--------1;1,1,2-Tetrachloroethane 44 100-41-4--------Euhylbenzene 48 ----------------m,p-Xylene 97 95-47-6---------o-Xylene 48 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 49 75-25-2---------Bromoform 40 98-82-8---------Isopropylbenzene 47 79-34-5---------1,1,2,2=Tetrachloroethane 50 108-86-1--------Bromobenzene 5.0 96-18-4---------1,2,3-Trichloropropane 46 103-65-1--------n-Propylbenzene 50 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3, 5-Trimethyl nzene 51 106-43-4--------4-Chlorotoluene 52 98-06-6---------tert-Butylbenzene 49 55-63-6---------1,2,4-Trimethylbenzene 50 135-98-8--------sec-Butylbenzene 51 99-87-6---------4-Isopropyltoluene 51 541-73-1--------1,3-Dichlorobenzene 52 106-46-7--------1,4-Dichlorobenzene 51 104-51-8--------n-Butylbenzene 52 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3-chloropropane 42 120-82-1--------1,2,4-Trichlorobenzene 49 87-68-3---------Hexachlorobutadiene 47 91-20-3---------Naphthalene 50 FORM I VOA OLM03:0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600, Matrix: (soil/water) WATER Lab Sample ID C1606-01D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3107 Level: (low/med) LOW Date Received-: 12/28/04 Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume:, 1000(14L) Date Analyzed: 01/05/05 injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol . 10 U 111-44-4--------bis(2-Chloroethyl) Ether 10 U 95-57-8---------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108-60-1--------2,2 ' -oxybis(1-Chioropropane 10 U ) 106-44-5--------4-Methylphenol 10 U 621-64-1--------N-Nitroso-di-n-propylamine_ 10 U 67-72-1---------Hexachloroethane _ 10 U 98-95-3---------Nitrobenzene _ 10 U 78-59-1---------Isophorone _ 10 U 88-75-5----------2-Nitrophenol 10 U 105-67-9---------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U• 120-82-1--------1,2,4-Trichlorobenzene` 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy methane_ 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------HexachlorocyclopentadT ene 10 U 88-06-2---------2,4,6-Trichlorophenol 19 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene 10 U 606-20-2--------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 ) 1C EPA SAMPLE NO. SEMIVOLATILE. ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case .No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2.E3107 Level: (low/med) LOW Date Received: 12/28/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05- Injection Volume: 1.6(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether_ 10 U 86-73-7---------Fluorene 10 U 100-01-6--------4-Nitroani.line 20 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 20 U 86-30-6---------N-Nitrosodiphenylamine (1) 10 U 101-55-3--------4-Bromophenyl-phenylether 10 U '118-74-1--------Hexachlorobenzene 10 U 87-86-5---------Pentachlorophenol 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene 10 U 129-00-0--------Pyrene 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3' -Dichlorobenzidine 10 U 56-55-3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis(2-Ethylhexyl)phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b)fluoranthene 10 U 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene 10 U 193-39-5--------Indeno(1,2,3-cd pyrene 10 U 53-70-3----------Dibenzo(a,h)anthracene 10 U 191-24-2--------Benzo(g,h,i)perylene 10 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET I- MW_6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : 'MC1600 Matrix: (soil/water) WATER Lab Sample ID. C1600-02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3108 Level: (low/med) LOW Date Received: 12/29/.04 o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume:. 1000 (uL) Date Analyzed: 01./05/05 Injection Volume: 1..0(uL) Dilution 'Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 10 U 111-44-4--------bis(2-Chloroethyl)Ether . 10 U 95-57-8---------2-Chlorophenol 10. 0 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-1---------2-Methylphenol 10 U 108-60-1--------2,2' -oxybis(1-Chloropropane) 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylp?yenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy)methane_ 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 10 U 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene ' 10 U 606-20-2--------2,6-Dinitrotoluene__ 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMNOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: - S2E3108 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: - decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether 10U 86-73-7---------Fluorene 10 U 100-01-6--------4-Nitroaniline 20 U 534-52-1--------4,6-Dinitro-2-methylpheno _ 20 U 86-30-6---------N-Nitrosodiphenylamine (1) 10 U 101-55-3--------4-Bromophenyl-phenylether 10 U_ 118-74-1--------Hexachlorobenzene 10 U 87-86-5---------Pentachlorophenol 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------_Anthracene 10 U 86-74-8---------Carbazole 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene 10 U 129-00-0--------Pyrene 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3 ' -Dichlorobenzidine 10 U 56-55=3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis (2=Ethylhexyl)phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b)fluoranthene 10 U 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene 10 U 193-39-5--------Indeno(1,2,3-cd pyrene 10 U 53-70-3---------Dibenzo(a,h)anthracene 10 U 191-24-2--------Benzo(g,h,i)perylene 10 U (l. - Cannot be separated from Dipheny amine FORM I SV-2 OLM03:0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: _ Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID.- S2E3109 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated. Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N). N pH: CONCENTRATION UNITS:. CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol. 38 111-44-4--------bis(2-ChloroethyI)Ether 42 95-57-8---------2-.Chlorophenol 34 541-73-1--------1,3-Dichlorobenzene 35 106-46-7--------1,4-Dichlorobenzene 36 95-50-1---------1,2-Dichlorobenzene 37 95-48-7---------2-Methylphenol 45 108-60-1--------2,2'-oxybis(1-Chloropropane) 44 106-44-5--------4-Methylphenol 48 621-64-7--------N-Nitroso-di-n-propylamine_ 50 67-72-1---------Hexachloroethane 35 98-95-3---------Nitrobenzene 45 78-59-1---------Isophorone 47 88-75-5---------2-Nitrophenol 43 105-67-9--------2,4-Dimethylphenol _ 63 120-83-2--------2,4-Dichlorophenol 44 120-82-1--------1,2,4-Trichlorobenzene 41 91-20-3---------Naphthalene 43 106-47-8--------4-Chloroaniline _ 48 111-91-1--------bis (2-Chloroethoxy)met hane_ 46 87-68-3---------Hexachlorobutadiene 39 59-50-7---------4-Chloro-3-Methylphenol 48 91-57-6---------2-Methylnaphthalene 45 77-47-4---------Hexachlorocyclopentadiene 56 88-06-2---------2,4,6-Trichlorophenol 50 95-95-4---------2,4,5-Trichlorophenol 48 91-58-7---------2-Chloronaphthalene 48 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate 48 208-96-8--------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 50 99-09-2---------3-Nitroaniline 44 $3-32-9---------Acenaphthene 48 FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA- SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3109 Level: (low/med) LOW Date Received: 12/29/04 . Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCED]TRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 50 100-02-7--------4-Nitrophenol 49 132=64-9--------Dibenzofuran 47 121-14-2--------2,4-Dinitrotoluene 48 84-66-2---------Diethylphthalate 49 7005-72-3-------4-Chlorophenyl-phenylether 48 86-73-7---------Fluorene 49 100-01-6--------4-Nitroaniline 44 534-52-1--------4,6-Dinitro-2-methylphenol_ 50 86-30-6---------N-Nitrosodiphenylamine (1) 60 101-55-3--------4-Bromophenyl-phenylether 49 118-74-.1--------Hexachlorobenzene 50 87-86-5---------Pentachlorophenol 61 85-01-8---------Phenanthrene 49 120-12-7--------Anthracene 50 86-74-8---------Carbazole 54 84-74-2---------Di-n-butylphthalate 50 206-44-0--------Fluoranthene 50 129-00-0--------Pyrene 48 85-68-7---------Butylbenzylphthalate 48 91-94-1---------3,3' -Dichlorobenzidine 1 J 56-55-3---------Benzo(a)anthracene 52 218-01-9---------Chzysene 51 117-81-7--------bis(2-Ethylhexyl)phthalate_ 48 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b)fluoranthene 43 207-08-9--------Benzo(k)fluoranthene 54. 50-32-8---------Benzo(a)pyrene 48 193-39-5--------Indeno(1,2,3-cd)pyrene 46 53-70-3---------Dibenzo(a,h)anthracene 46 191-24=2--------Benzo(g,h;i)perylene 47 (1) Cannot be separated from Diphenylamine FORM I SV-2 OLM03:0 l.B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: - (low/med) LOW Date Received: 12/29/04 o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 36 111-44-4--------bis(2-Chloroethyl Ether 44 95-57-8---------2-Chlorophenol 31 541-73-1--------1,3-Dichlorobenzene 38 106-46-7--------1,4-Dichlorobenzene 39 95-50-1---------1,2-Dichlorobenzene 40 95-48-7---------2-Methylphenol 44 108-60-1--------2,2'-oxybis(1-Chloropropane) 45 106-44-5--------4-Methylphenol 47 621-64-7--------N-Nitroso-di-n-propylamine 49 67-72-1---------Hexachloroethane 38 98-95-3---------Nitrobenzene 46 78-59-1---------Isophorone 47 88-75-5---------2-Nitrophenol 39 105-67-9--------2,4-Dimethylpheno 63 120-83-2--------2,4-Dichlorophenol 39 120-82-1--------1,2,4-Trichlorobenzene 41 91-20-3---------Naphthalene 44 106-47-8--------4-Chloroani ine 48 111=91-1--------bis(2-Chloroethoxy .methane 47 87-68-3---------Hexachlorobutadiene 39 59-50-7---------4-Chloro-3-Methylphenol 47 91-57-6---------2=Methylnaphthalene 44 77-47-4---------Hexachlorocyclopentadi�� 54 88-06-2---------2,4,6-Trichlorophenol 46 95-95-4---------2,4,5-Trichlorophenoi 47 91-58-7---------2-Chloronaphthalene 48 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate 48 208-96-8---------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 50 99-09-2---------3-Nitroaniline 41 83-32-9---------Acenaphthene 48 FORM I SV-1 OLM03:0 j 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA 'SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: (low/med) IOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) -Date Analyzed: 01/06/0.5 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 48 100-02-7--------4-Nitrophenol 45 132-64-9--------Dibenzofuran 48 121-14-2--------2,4-Dinitrotoluene 49 84-66-2---------Diethylphthalate 50 7005-72-3-------4-Chlorophenyl-phenylether_ 47 86-73-7----------Fluorene 50 100-01-6--------4-Nitroaniline 44 534-52-1--------4,6-Dinitro-2-methylphenol 48 86-30-6---------N-Nitrosodiphenylamine (1)__ 59 101-55-3--------4-Bromophenyl-phenylether 49 118-74-1--------Hexachlorobenzene 50 87-86-5---------Pentachlorophenol 59. 85-01-8---------Phenanthrene J 49 120-12-7--------Anthracene 51 86-74-8---------Carbazole 54 84-74-2---------Di-n-butylphthalate 50 206-44-0--------Fluoranthene 49 129-00-0--------Pyrene 50 85-68-7---------Butylbenzylphthalate 49 91-94-1---------3,31 -Dichlorobenzidine 2 J . 56-55-3---------Benzo(a)anthracene 48 218-01-9--------Chrysene . 52 117-81-7--------bis(2-E ylhexyl)phthalate_ 48 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b)fluoranthene _ 44 207-08-9--------Benzo W fluoranthene 49 50-32-8---------Benzo(a)pyrene 46 193-39-5--------Indeno(1,2,3-cd)pyrene 46 53-70-3---------Dibenzo(a,h)anthracene 46 191-24-2------ ---Benzo(g,h,i)perylene_ 47 (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No SDG No. : MC1600 ) Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) IOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: . 1000 (UL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 10 U 111-44-4--------bis(2-Chloroethyl)Ether 10 U 95-57-8----------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108-60-1--------2,2' -oxybis(1-Chloropropane) 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol_ 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy)methane 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10. 0 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 10 U 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene - _ 10 U 606-20-2--------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 ' 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab' Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) IOW- Date Received: 12/25/04 o Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dini.trotoluene 10 U 84-66-2---------Diethylphthalate 10- U 7005-72-3-------4-Chlorophenyl-phenylether 10 'U 86-73-7------=--Fluorene. 10 U 100-01-6--------4-Nitroaniline _ 20 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 20 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 10 U 101-55-3------- 4-Bromophenyl-phenylether 10 U .118-74-1--------Hexachlorobenzene 1.0 U 87-86-5---------Pentachlorophenol^ 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene 10 U 129-00-0--------Pyrene . 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3 ' -Dichlorobenzidine 10 U 56-55-3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis (2-Ethylhexyl)phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b) fluoranthene 10 U 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene 10 U 193-39-5--------Indeno(1,2,3-cd pyrene 10 U 53-70-3---------Dibenzo(a,h)anthracene 10 U 191-24-2---------Benzo(g,h,i)perylene 10 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO: SEMIVOLATILE ORGANICS ANALYSIS DATA. SHEET S2QLCS Lab Name: MITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix:. (soil/water) WATEE2 Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3100 Level: (low/med) LOW Date Received: Moisture: decanted: (Y/N). Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date .Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 41 111-44-4--------bis(2-Chloroethyl)Ether 43 95-57-8---------2-Chlorophenol 37 541-73-1--------1,3-Dichlorobenzene 37 106-46-7--------1,4-Dichlorobenzene 37 95-50-1---------1,2-Dichlorobenzene 39 95-48-7---------2-Methylphenol 44 108-60-1--------2,2' -oxybis (1-Chloropropane 45 106-44-5--------4-Methylphenol 46 621-64-7--------N-Nitroso-di-n-propylamine . 49 67-72-1---------Hexachloroethane 36 98-95-3---------Nitrobenzene 45 78-59-1.---------Isophorone __ 47 88-15-5---------2-Nitrophenol 44 105-67-9--------2,4-Diinethylphenol 54 120-83-2--------2,4-Dichlorophenol 43 120=82-1--------1,2,4-Trichlorobenzene 40 T 91-20-3---------Naphthalene 43 106-47-8--------4-Chloroaniline 57 111-91-1--------bis(2-Chloroethoxy)methane_ 47 87-68-3---------Hexachlorobutadiene . 38 59-50-7---------4-Chloro-3-Methylphenol 46 91-57-6---------2-Methylnaphthalene 43 77-47-4---------Hexachlorocyclopentadiene 58 88-06-2---------2,4,6-Trichlorophenol 46 95-95-4---------2,4,5-Trichlorophenol 44 91-58-7---------2-Chloronaphthalene 47 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate_ 49 208-96-8--------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 49 99-09-2---------3-Nitroaniline 49 83-32-9---------Acenaphthene 48 FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2QLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL), ML Lab File ID: S2E3100 Level: (low/med) LOW Date Received: o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (UL) Date Analyzed: 01/05/05. Injection Volume: 1.0(uL) Dilution Factor: 1.0 _.. GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 29 100-02-7--------4-Nitrophenol 37 132-64-9--------Dibenzofuran 48 121-14-2--------2,4-Dinitroto uene 51 84-66-2---------Diethylphthalate 49 7005-72-3-------4-Ctilorophenyl-phenylether 48 86-73-7---------Fluorene 48 100-01-6--------4-Nitroaniline 47 534-52-1--------4,6-Dinitro-2-methylphenol 41 86-30-6---------N-Nitrosodiphenylamine (1)__ 60 101-55-3--------4-Bromophenyl-phenylether 48 118-74-1--------Hexachlorobenzene 49 87-86-5---------Pentachlorophenol 33 85-01-8---------Phenanthrene 47 120-12-7--------Anthracene 51 86-74-8---------Carbazole 49 84-74-2---------Di-n-butylphthalate 49 206-44-0--------Fluoranthene 49 129-00-0--------Pyrene 50 85-68-7---------Butylbenzylphthalate 51 91-94-1---------3,3' -Dichlorobenzidine 55 56-55-3---------Benzo(a)anthracene 49 218-01-9--------Chrysene 54 117-81-7--------bis(2-Ethylhexyl)phthalate_ 50 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b) fluoranthene 45 207-08-9--------Benzo(k)fluoranthene� 48 50-32-8---------Benzo(a)pyrene 47 193-39-5--------Indeno(1,2,3-cd pyrene_ 47 53-70-3---------Dibenzo(a,h)anthracene 47 191-24-2--------Benzo(g,h,i)perylene 49 (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03:0 DATA PACKAGE ADDENDUM SEMIVOLATILE ORGANICS C 1600 Data Summary Forms, followed by Full Data Package Pages. 1B EPA SAMPLE. NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: MW-5 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01D Sample wt/vol: 1000 (g/mL) ML Lab File ID: 82E3107 Level: (low/med) LOW Date Received: 12/28/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L. or ug/Kg) UG/L Q 62-53-3---------Aniline _ 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEH CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: ' (soil/water) WATER Lab Sample ID: C1600­02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3108 Level: (low/med) LOW Date Received: 12/29/04 . Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: .01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline ' 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 4 10 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEM VOLATILE ORGANICS 'ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab .Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: . (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3109 Level: (low/med) LOW Date Received: '12/29/04 ,. .Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000.(UL) Date Analyzed: 01/05/05 Injection Volume: 1.0(UL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 59 103-33-3--------Azobenzene 48 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03:0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: _ \ Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 1 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: (low/med) - LOW Date Received: 12/29/04- Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 60 103-33-3--------Azobenzene 49 98-86-2---------Acetophenone __ 10 U FORM I SV-1 OLM03.0 ) 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: MW-X Lab Code: MITKEM Case No. : SAS No. : SDG No.: MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) LOW Date Received: 12/29/04 Moisture: _ decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date-Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline ' 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U FORM I SV-1 0LM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2QLCS Lab Name: MITKEM CORPORATION Contract: l Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3100 Level: (low/med) LOW Date Received: Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 64 103=33-3--------Azobenzene 47 98-86-2---------Acetophenone 10 U i FORM I SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code-- MITKEM Case No. : SAS No. : SDG No. : 'MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE - --SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC #' REC. Aniline 50 0.0 59 118 40-140 Azobenzene 50 0.0 48 96 40-140 SPIKE MSD MSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------ ------ ---- Aniline 50 60 120 2 0'0-� 40-140 Azobenzene 50 49 98 2 8— 40-140 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out of 4 outside limits COV14ENTS: FORM III SV-1 OLM03.0 FORM 3 WATER SEt4IVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEMM CORPORATION Contract: Lab Code: MITKE24 Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC #. REC. Aniline 50 64 128 40-140 Azobenzene 50 47 94 40-140 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits COM ME TS: FORM III SV 4B. EPA SAMPLE NO. SEMIVOLATILE METHOD BLANK SUMMARY Lab Name: MITKEM CORPORATION Contract: SBLK2Q Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab. File ID: S2E3101 Lab Sample ID: MB-16345 .Instrument ID: S2 Date Extracted: 01/03/05 Matrix: (soil/water) WATER Date Analyzed: 01/05/05 Level: (low/med) LOW Time Analyzed: 1954 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: ` EPA LAB LAB DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED - -------------- -------------- ---------- 01 S2QLCS LCS-16345 S2E3100 01/05/05 02 MW-5 C1600-01D S2E3107 01/05/05 03 MW-6 C1600-02D S2E3108 01/05/05 04 MW-6MS C1600-02DMS S2E3109 ' 01/05/05 05 MW-6MSD C1600-02DMSD S2E3110 01/06/05 06 MW-X C1600-03D S2E3111 01/06/05 07 68 _ 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 _ 28 29 30 CONIIv=S: page 1 of I FORM IV SV OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SBLK2Q Lab Name: MITKEM CORPORATION Contract: _ Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16345 Sample wt/vol: 1000 . (g/mL) ML Lab File ID: S2E3101 Level: (low/med) LOW Date Received: Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U FORM I SV-1 01-M03:0 FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/yol: 1000 (g/ml) ML Lab File ID: E2E3242F o Moisture: decanted: (Y/N) Date Received: 12/29/04 Extraction: (SepF/Cont/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000 (uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L .or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 0.20 U 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor-1248 0.20 U 11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 0.20 U FORM I PCB FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET P2PLCS Lab Name: MITKE++I CORPORATION Contract: 1 Lab Code: MITKEM Case No.-: SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16376 Sample wt/vol: 1000 (g/ml) ML Lab File ID: E2E3240F Moisture: decanted: (Y/N) Date Received: Extraction: (SepF/Cont/Sonc) SEPF Date Extracted:01/0.5/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N J?H: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS-: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2-------Aroclor-1016 1.9 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor--1248 0.20 U 11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 2.0 FORM I PCB FORM 1 CLIENT SAMPLE No.. PCB ORGANICS ANALYSIS DATA SHEET P2PLCSD Lab Name: MITKEM CORPORATION Contract: Lab. Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16376 Sample wt/vol: 1000 "{g/ml) ML Lab File ID: E2E3241F o Moisture: decanted: (YIN) Date Received: Extraction: (SepF/font/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: '(YIN) N pH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 2.0 11104=28-2------Aroclor-1221 0.20 U 11141-16-5--=---Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor-1248 0.20 U "11097-69-1------Aroclor-1254 0.20 U 11096-82-5-------Aroclor-1260- 2.0 FORM I PCB U-S_ EPA - CLP } 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET - Mw-5 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITkEM Case No_ SAS No- : SDG No. : MC1600' Matrix (soil/water) : WATER Lab Sample ID: C1600-01 Level (low/med) : MED Date Received: 12/28/04 $ Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7440-36-0 Antimony 20 U _ P 7440-38-2 Arsenic 20 U P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium' -- 5 6 L3 - -- -P 7440-47-3 Chromium 25.6 P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U _ P 7440-22-4 silver 30 U P 7440-28-0 Thallium _ _ 20 U P 7440-62-2 Vanadium — SO U P } -t440-66-6 Zinc 50 U P 7439-97-6 Mercury _ 0_28 U CV Cyanide U N CA Comments: FORM I - IN SW846 0ObrA 1 _ IU_S_ EPA - CLP 1 EPA SAMPLE NO I INORGANIC ANALYSIS DATA SHEET MW-6 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No_ SAS No. : SDG No_: MC160G Matrix (soil/water) : WATER Lab Sample ID: C1600-02 Level (low/med) : MED Date Received: 12/29/04 $ Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/i, CAS No. Analyte Concentration C Q M 7440-36-0 Ajitimony_ 20 U p 7440-38-2 Arsenic _ 20 U_ P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium 5.0 U P 7440-47-3 Chromium 20 U P 7439-92-1 Lead --- 10 U ---- P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7.440-28-0 Thallium 20 U P 7440-62-2 anadium _ 50 U P 7440-66-6 Zinc __ _50 U P 7439-97-6 Mercury D.31 U Cv Cyanide D U N CA �7,11 r Comments: FORM I - IN SW846 0 0,9 6 U.S. EPA - CLP J 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET 3HnT—X Lab Name: Mitkem Corporation, Contract: 28367-005 Lab Code= MITKEM Case No_ SAS No. SDG No_: MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600-03 Level (low/med) : MED Date Received: 12/2.9/04 W Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7440-36-0 An tim-on y _ 20 U p 7440-38-2 Arsenic 20 u_ p 7440-39-3 Barium 200 U p 7440-41-7 Beryllium _ 5.0 U P 7440-43-9 Cadmium 5.0 U p 7440-47-3 Chromium 20 ul p 7439-92-1 Lead I0 U P 7440-02-0 Uickel 50 U p 7782-49-2 Selenium 30 U p 7440-22-4 Silver 30 U p 7440-28-0 Thallium _ 20 U p 7440-62-2 Vanadium _ 50 U p 7440-66-6 Zinc 50 U_ p 7439-97-6 _rcury 0.29 U - CV Cyanide i O U N CA No Comments: FORM I - IN Sw846 0087l, U.S. EPA - CLP 1 EPA SAMPLE NO' INORGANIC ANALYSIS DATA SHEET Mw�Lab Name: Mitkem Corporation Contract_ 28357-005 Lab Code: MITKEM Case No. SAS No_ : SDG No_ : MC16O0 Matrix (soil/water) : WATER Lab Sample ID: C1600-04 Level (low/med) : MED Date Received: 12/29/04 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No_ Analyte Concentration C Q M 7440-36-0 Antimony 20 U P 7440-38-2 Arsenic _ 20 U 7 p 7440-39-3 Barium _ 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium 5.0 U P 7440-47-3 Chromium _ 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U1 P 7440-22-4 Silver _ _30 U P I 7440-28-0 Thallium 20 U P 7440-62=2 Vanaditun 50 U P , 7440-66-6 Zinc 50 U P 7439-97-6 ercury 0_30 U CV i Cyanide U N CA s 5�LjiD�4� Comments: FORM I - IN SW846 0088 � U_S_ EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET — Mw-2 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No. SAS No_: SDG No- : MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600-05 Level (low/med) : MED Date Received: 12/29/04 $ Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No_ Analyte Concentration C Q M 7440-36-0 Antimony 20 U P 7440-38-2 Arsenic 20 U P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43_-9 Cadmium 5-0 U P 7440-47-3 Chromium -_ 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7440-28-0 Thallium 20 U P 7440-62-2 Vanadium _ 50 U �- P 7440-66-6 Zinc 50 U P 7439-97-6 Mercury 0.30 U CV Cyanide T_540,U N CA L,10104 Comments: FORM I - IN SW846 !• U-S_ EPA.- CLP 7 LABORATORY CONTROL SAMPLE Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No_ SAS No. : SDG No. : MC1600 Solid LCS Source: Aqueous LCS Source: LCS-16324 Aqueous (ug/L) Solid (mg/kg) 4 , Analyte True Found %R True Found C Limits %R Mercury 4.6 4.91 106.7 FORM VII - IN SW846 FORM 2 WATER PCB SURROGATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKE24 Case No. : SAS No. : SDG No. : C1600 ' GC Column(1) : RTXCLPPEST ID: 0.53 (mm) GC Column(2) : RTXCLPPEST 2 ID: 0.53 (mm) CLIENT TCX 1 TCX 2 DCB 1 DCB 2 OTHER OTHER TOT SAMPLE NO. .REC # .REC # %REC # .REC # (1) (2) . OUT 01 PBLK2P 80 84 102 99 _ 0 02 P2PLCS 89 88 108 106 0 03 P2PLCSD 90 89 97 102 0 04 MW-6 81 104 100 102 0 05 - 06 07 08 — -- — 09 -- — -- 10 11 12 13 14 15 16 _ 17 18- 19 __ ) 20 21 22 23 24 25 26 -- 27 28 29 30 ADVISORY QC LIMITS S1 (TCX) = Tetrachloro-m-xylene (29-158) S2 (DCB) = Decachlorobiphenyl (30-164) # Column to be used to flag recovery values * Values outside of QC limits D Surrogate diluted out page 1 of 1 FORM II PCB FORM 3 WATER VOLATILE MATRIX. SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample .No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------- --------- ------------- ------------- ------ ------ Dichlorodifluoromethane 50 0.0 48 96 48-135 Chloromethane 50 0.0 49 98 60-118 Vinyl Chloride 50 0.0 48 96 65-113 Bromomethane 50 0.0 55 110 73-122 Chloroethane 50 0.0 46 92 72-118 Trichlorofluoromethane 50 0.0 58 116 68-129 1,1-Dichloroethene 50 0.0 50 100 67-121 Acetone 50 0.0 30 60 38-161 Iodomethane 50 0.0 55 110 72-130 Carbon Disulfide 50 0.0 43 86 53-137 Methylene Chloride 50 0.0 51 102 59-132 trans-1,2-Dichloroethen 50 0:0 40 80 71-124 Methyl tert-butyl ether 100 0.0 78 78 75-123 1,1-Dichloroethane 50 0.0 39 78* 83-116 Vinyl acetate 50 0.0 66 132 44-160 2-Butanone 50 0.0 33 66 64-139 cis-1,2-Dichloroethene 50 0.0 42 84 83-120 2,2-Dichloropropane 50 0.0 37 74 70-129 Bromochloromethane 50 0.0 44 88 85-124 Chloroform 50 0.0 42 84* 89-118 Tetrahydrofuran 50 0.0 54 108 76-126 1,1,1-Trichloroethane 50 0.0 40 80* 81-122 1,1-Dichloropropene 50 0.0 43 86 76-122 Carbon Tetrachloride 50 0.0 39 78* 79-125 1,2-Dichloroethane 50 0.0 42 84 83-123 Benzene 50 0.0 43 86 81-120 Trichloroethene 50 0.0 43 86 77-121 1,2-Dichloropropane 50 0.0 42 84 81-116 rf Column to be used to flag recovery and RPD values .with an asterlT * Values outside of QC limits CONIMIIVTS: page 1 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: ) Lab Code: MITKEM - Case No. : - SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE SAMPLE MS MS QC.. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ -- Dibromomethane 50 0.0 45 90 86-124 Bromodichloromethane 50 0.0 39 78* 907114 cis-1,3-Dichloropropene 50 0.0 38 76* 78-119 4-Methyl-2-pentanone 50 0.0 37 74 57-138 Toluene 50 0.0 44 88 81=121 trans-1,3-Dichloroprope 50 0.0 37 74* 85-118 1,1,2-Trichloroethane 50 0..0 45 90 44-159 1;3-Dichloropropane 50 0.0 46 92 79-125 Tetrachloroethene 50 0.0 51 102 73-121 2-Hexanone 50 0.0 35 70 53-145 Dibromochloromethane 50 0.0 40 80 80-124 1,2-Dibromoethane 50 0.0 48 96 80-124 Chlorobenzene 50 0.0 49 98 82-118 1,1,1,2-Tetrachloroetha 50 0.0 44 88 84-121 Ethylbenzene 50 0.0 47 94 80-122 Xylene (Total) 150 0.0 140 93 81-121 Styrene 50 0.0 31 62* 77-128 Bromoform 50 0.0 35 70* 77-130 Isopropylbenzene 50 0.0 46 92 58-148 ) 1,1,2,2-Tetrachloroetha 50 0.0 52 104 76-125 Bromobenzene 50 0.0 50 100 76-124 1,2,3-Trichloropropane 50. 0.0 44 88 57-140 n-Propylbenzene 50 0.0 50 100 72-119 2-Chlorotoluene 50 0.0 50 100 75-120 1,3,5-Trimethylbenzene 50 01.0 44 88 76-116 4-Chlorotoluene 50 0.0 51 102 78-116 tert-Butylbenzene 50 0.0 50 100 71-115 1,2,4-Trimethylbenzene 50 0.0 . 44 88 77-117 Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MK-6 — SPIKE SAMPLE MS F MS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug./L) (ug/L) REC ## REC. -------- - ------------- --=---=------ ------ sec-Butylbenzene 50 0.0 50 100 67-117 4-Isopropyltoluene 50 0.0 50 100 68-118 1,3-Dichlorobenzene 50 0.0 51 102 80-116 1,4-Dichlorobenzene 50 0.0 52 104 80-114 n-Butylbenzene 50 0.0 52 104 58-121 1,2-Dichlorobenzene 50 0.0 52 104 81-116 1,2-Dibromo-3-chloropro 50 0.0 45 90 71-126 1,2,4-Trichlorobenzene 50 . 0.0 50 100 67-114 Hexachlorobutadiene 50 0.0 47 94 50-111 Naphthalene 50 0.0 52 104 58-133 1,2,3-Trichlorobenzene 50 0.0 50 100 64-118 Ether 50 0.0 49 98 70-130 Diisopropyl Ether 50 0.0 44 88 70-130 Ethyl tert-butyl ether 50 0.0 42 84 70-130 tert-Amyl methyl ether 50 0.0 46 92 70-130 1,4-Dioxane 1000 0.0 630 63* 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON]MENTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX- SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD .# RPD REC. ------------------------ --------- - -- Dichlorodifluoromethane 50 45 90 6 40 48-135 Chloromethane 50 48 96 2 40 60-118 Vinyl Chloride 50 45 90 6 40 65-113 Bromomethane 50 52 104 6 40 73--1-22 Chloroethane 50 46 92 0 40 72-118 Trichlorofluoromethane 50 56 112 4 40 68-129 1,1-Dichloroethene 50 49 98 2 40 67-121 Acetone 50 33 66 10 40 38-161 Iodomethane 50 53 106 4 40 72-130 Carbon Disulfide 50 53 106 21 40 53-137 Methylene Chloride 50 50 100 2 40 59-132 trans-1,2-Dichloroethen 50 40 80 0 40 71-124 Methyl tert-butyl ether 100 81 81 4 40 75-123 1, 1-Dichloroethane 50 38 76* 2 40 83-116 Vinyl acetate 50 41 82 47* 40 44-160 2-Butanone 50 35 70 6 40 64-139 cis-1,2-Dichloroethene 50 42 84 0 40 83-120 2,2-Dichloropropane 50 35 70 6 40 70-129 Bromochloromethane 5.0 44 88 0 40 85-124 Chloroform 50 42 84* 0 40 89-118 Tetrahydrofuran SO 59 118 9 40 76-126 1,1,1-Trichloroethane 50 39 78* 2 40 81-122 1, 1-Dichloropropene 50 42 84 2 40 76-122 Carbon Tetrachloride 50 37 74* 5 40 79-125 1,2-Dichloroethane 50 42 84 0 40 83-123 Benzene 50 43 86 0 40 81-120 Trichloroethene 50 43 86 0 40 77-121 1, 2-Dichloropropane 5.0 42 84 0 40 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON24ENTS: page 4 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION a % QC LIMITS COMPOUND (ug/L) (ug/L) REC ## RPD # RPD REC. --- - --- - - ------ ------ ------ Dibromomethane 50 45 90 0 40 86-124 Bromodichloromethane 50 38 76* 2 40 90-114 cis-1,3-Dichloropropene 50 38 76* 0 40 78-119 4-Methyl-2-pentanone 50 39 78 5 40 57-138 Toluene 50 43 86 2 40 81-121 trans-1,3-Dichloroprope 50 37 74* 0 40 85-118 1,1,2-Trichloroethane 50 46 92 2 40 44-159 1,3-Dichloropropane 50 48 96 4 40 79-125 Tetrachioroethene 50 50 100 2 40 73-121 2-Hexanone 50 40 80 13 40 53-145 Dibromochloromethane 50 40 80 0 40 80-124 1,2-Dibromoethane 50 50 100 4 40 80-124 Chlorobenzene 50 49 98 0 40 82-118 1,1,1,2-Tetrachloroetha 50 44 88 0 40 84-121 Ethylbenzene 50 46 92 2 40 , 80-122 Xylene (Total) 150 140 93 0 40 81-121 Styrene 50 30 60* 3 40 77-128 Bromoform 50 36 72* 3 40 77-130 Isopropylbenzene 50 46 92 0 40 58-148 1,1,2,2-Tetrachloroetha 50 54 108 4 40 76-125 Bromobenzene 50 50 100 0 40 76-124 1,2,3-Trichloropropane 50 42 84 5 40 57-140 n-Propylbenzene 50 48 96 4 40 72-119 2-Chlorotoluene 50 50 100 0 40 75-120 1,3,5-Trimethylbenzene 50 43 86 2 40 76-116 4-Chlorotoluene 50 51 102 0 40 7.8-116 tert-Butylbenzene 50 48 96 4 40 71-115 1,2,4-Trimethylbenzene 50 43 86 2 40 77-117 4 Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX. SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION o % QC LIMITS-_. COMPOUND (ug/L) (ug/L) REC # RPD ## RPD REC. ------------------------ --------- ------------- ------ ------ ------ -----= sec-Butylbenzene 50 49 98 2 40 67-117 4-Isopropyltoluene 50 48 96 4 40 68-118 1,3-Dichlorobenzene 50 51 102 0 40 80-116 1,4-Dichlorobenzene 50 52 104 0 40 80-114 n-Butylbenzene 50 49 98 6 40 58-121 1,2-Dichlorobenzene 50 52 104 0 40 81-116 1,2-Dibromo-3-.chlorcpro 50 47 94 4 40 71-126 1,2,4-Trichlorobenzene 50 50 100 0 40 67-114 Hexachlorobutadiene 50 45 90 4 40 50-111 Naphthalene 50 55 110 6 40 58-133 1,2,3-Trichlorobenzene 50 50 100 0 40 64-118 Ether 50 54 108 10 40 70-130 Diisopropyl Ether 50 44 88 0 40 70-130 Ethyl tert-butyl ether 50 44 88 5 40 70-130 tert-Amyl methyl ether 50 47 94 2 40 70-130 1,4-Dioxane 1000 830 83 27 40 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 72 outside limits Spike Recovery: 19 out of 144 outside limits COVR-1E TS: page 6 of 6 FORM III VOA ) FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix .Spike - Sample No. : V6WLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- ------------- ------------- ------ ------ Dichlorodifluoromethane 50 43 86 48-135 Chloromethane 50 44 88 60-118 Vinyl Chloride 50 45 90 65-113 Bromomethane 50 54 108 73-122 _ Chloroethane 50 47 94 72-118 Trichlorofluoromethane 50 51 102 68-129 1,1-Dichloroethene 50 47 94 67-121 Acetone 50 44 88 38-161 Iodomethane 50 51 102 72-130 Carbon Disulfide 50 46 92 53-137 Methylene Chloride 50 49 98 59-132 trans-1,2-Dichloroethen 50 45 90 71-124 Methyl tert-butyl ether 100 86 86. 75-123 1,1-Dichloroethane 50 44 88 83-116 Vinyl acetate 50 45 90, 44-160 2-Butanone ' 50 38 76 64-139 cis-1,2-Dichloroethene 50 46 92 83=120 2,2-Dichloropropane 50 44 88 70-129 Bromochloromethane 50 48 96 85-124 Chloroform 50 47 94 89-118 Tetrahydrofuran 50 48 96 76-126 1,1,1-Trichloroethene 50 45 90 81-122 1,1-Dichloropropene 50 48 96 76-122 Carbon Tetrachloride 50 45 90 79-125 1,2-Dichloroethane 50 45 90 83-123 Benzene 50 47 94 81-120 Trichloroethene 50 48 96 77-121 1,2-Dichloropropane 50 46 92 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COb1MENTS: page 1 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 } Matrix Spike - Sample No. : V6WLCS SPIKE SAMPLE LCS LCS QC. ADDED .CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. Dibromomethane 50 47 94 86-124 Bromodichloromethane 50 45 90 90-114 cis-1,3-Dichloropropene 50 45 90 78-119 4-Methyl-2-pentanone 50 38 76 57-.138 Toluene 50 48 96 81-121 trans-1,3-Dichloroprope 50 44 88 85-118 1,1,2-Trichloroethane 50 47 94 44-159 1,3-Dichloropropane 50 46 92 79-125 Tetrachloroethene 50 48 96 73-121 2-Hexanone 50 37 74 53-145 Dibromochloromethane 50 45 90 80-124 1,'2-Di.bromoethane 50 47 94 80-124 Chlorobenzene 50 48 96 82-118 1,1,1,2-Tetrachloroetha 50 46 92 84-121 Ethylbenzene 50 48 96 80-122 Xylene (Total) 150 140 93 81-121 Styrene 50 49 98 77-128 Bromoform 50 43 86 77-130 Isopropylbenzene 50 47 94 58-148 1,1,2,2-Tetrachloroetha 50 44 88 76-125 Bromobenzene 50 46 92 76-124 1,2,3-Trichloropropane 50 43 86 57-140. n-Propylbenzene 50 47 94 72-119 2-Chlorotoluene 50 47 94 75-120 1,3,5-Trimethylbenzene 50 47 94 76-116 4=Chlorotoluene 50 47 94 78-116 tert-Butylbenzene 50 46 92. 71-115 1,2,4-Trimethylbenzene 50 47 94 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: : page 2 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE SAMPLE - - - LCS LCS ADDED CONCENTRATION CONCENTRATION o LIMITS - COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. sec-Butylbenzene 50 47 94 67-117 4-Isopropyltoluene 50 48 96 68-118 1,3-Dichlorobenzene 50 47 94 80-116 1,4-Dichlorobenzene 50 47 94 80-114 n-Butylbenzene 50 47 94 58.-121 1,2-Dichlorobenzene 50 47 94 81-116 1,2--Dibromo-3-chloropro 50 38 76 71-126 1,2,4-Trichlorobenzene 50 46 92 67-114 Hexachlorobutadiene 50 44 88 50-111 Naphthalene 50 41 82 58-133 1;2,3-Trichlorobenzene 50 46 92 647118 Ether 50 49 98 70-130 Diisopropyl Ether 50 48 96 70-130 Ethyl tert-butyl ether 50 48 96 70-130 tert=Amyl methyl ether 50 50 100 70-130 1,4-Dioxane 1000 190 19* 70-130- # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COV24E VTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL- SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : VGWLCS SPIKE LCSD LCSD ADDED CONCENTRATION % a QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dichlorodifluoromethane 50 45 90 4 40 48-135 Chloromethane 50 46 92 4 40 60-118 Vinyl Chloride 50 46. 92 2 40 65-113 Bromomethane 50 55 110 2 40 73-122 Chloroethane 50 48 96 2 40 72-118 Trichlorofluoromethane 50 52 104 2 40 68-129 1,1-Dichloroethene 50 49 98 4 40 67-121 Acetone 50- 43 86 2 40 38-161 Iodomethane 50 52 104 2 40 72-130 Carbon Disulfide 50 47 94 2 40 53-137 Methylene Chloride 50 50 100 2 40 59-132 trans-1,2-Dichloroethen 50 46 92 2 40 71-124 Methyl tert-butyl ether 100 90 90 4 40 75-123 1,1-Dichloroetbane 50 45_ 90 2 40 83-116 Vinyl acetate 50 77 154 52* 40 44-160 2-Butanone 5-0 38 76 0 40 64-139 cis-1,2-Dichloroethene 50 48 96 4 40 83-120 2,2-Dichloropropane 50 43 86 2 40 70-129 Bromochloromethane 50 49 98 2 40 85-124 Chloroform 50 47 94 0 40 89-118 Tetrahydrofuran 50 47 94 2 40 76-126 1,1,1-Trichloroethane 50 45 90 0 40 81-122 1,1-Dichloropropene 50 48 96 0 40 76-122 Carbon Tetrachloride 50 44 88 2 40 79-125 1,2-Dichloroethane 50 46 92 2 40 83-123 Benzene 50 47 94 0 40 81-120 Trichloroethene 50 48 96 0 40 77-121 1,2-Dichloropropane 50 46 92 0 40 81-116 ## Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : M-C1600 Matrix Spike - Sample No. : V6WLCS SPIKE LCSD LCSD ADDED CONCENTRATION o a QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------ --------- ------------- ------ ------ ------ ------ Dibromomethane 50 48 96 2 40 86-124 Bromodichloromethane 50 46 92 2 40 90-114 cis-1,3-Dichloropropene 50 46 92 .2 40 78-119 4-Methyl-2-pentanone 50 40 80 5 40 57=13.8 - Toluene 50 48 96 0 40 81=121 trans-1,3-Dichloroprope 50 45 90 2 40 85-118 1,1,2-Trichloroethane 50 48 96 2 40 44-159 1,3-Dichloropropane 50 47 94 2 40 79=125 Tetrachloroethene 50 49 98 2 40 . 73-121 2-Hexanone 50 37 74 0 40 53-145 Dibromochloromethane 50 44 88 2 40 80-124 1,2-Dibromoethane 50 48 96 2 40 80-124 Chlorobenzene 50 48 96 0 40 82-118 1,1,1,2-Tetrachloroetha 50 45 90 2 40 84-121 Ethylbenzene 50 47 94 2 40 80-122 .Xylene (Total) 150 140 93 0 40 81-121 Styrene 5.0 48 96 2 40 77-128 Bromoform 50 43 86 0 40 77-130 Isopropylbenzene 50 47 94 0 40 58-148 1,1,2,2-Tetrachloroetha 50 45 90 2 40 76-125 Bromobenzene 50 46 92 0 40 76-124 1,2,3-Trichloropropane 50 43 86 0 40 57-140 n-Propylbenzene 50 46 92 2 40 72-119 2-Chlorotoluene 50 47 94 0 40 75-120 1,3,5-Trimethylbenzene 50 46 92 2 40 76-116 4-Chlorotoluene 50 46 92 2 40 78-116 tert-Butylbehzene 50 45 90 2 40 71-115 1,2,4-Trimethylbenzene 50 46 92 2 40 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 ) Matrix Spike - Sample No. : VGWLCS SPIKE LCSD LCSD ADDED CONCENTRATION o o QC LIMITS_- COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC.. ------------------------ --------- -- sec-Butylbenzene 50 46 92 2 40 67-117 4-Isopropyltoluene 50 46 92 4 40 68-118 1,3-Dichlorobenzene 50 47 94 0 40 80-116 1,4-Dichlorobenzene 50 47 94 0 40 80*114 n-Butylbenzene 50 46 92 2 40 58-121 1,2-Dichlorobenzene 50 47 94 0 40 81-116 1,2-Dibromo-3-chloropro 50 39 78 2 40 71-126 1,2,4-Trichlorobenzene 50 46 92 0 40 67-114 Hexachlorobutadiene 50 43 86 2 40 50-111 Naphthalene 50 46 92 11 40 58-133 1,2,3-Trichlorobenzene 50 46 92 0 40 64-118 Ether 50 53 106 8 40 70-130 Diisopropyl Ether 50 50 100 4 40 70-130 Ethyl tert-butyl ether 50 50 100 4 40 70-130 tert-Amyl methyl ether 50 52 104 4 40 70-130 1,4-Dioxane 1000 540 54* 96* 40 707130 ## Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 2 out of 72 outside limits Spike Recovery: 2 out of 144 outside limits COMMENTS: page 6 of 6 FORM III VOA J FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLFB - SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION a LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC #$ REC. Vinyl Chloride 1 0.8 80 60-120 1,1-Dichloroethene 1 1 100 60-120 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits COMMENTS: - FORM III VOA FORM 3 WATER VOLATILE LAB .CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No_ : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION It T. TS COMPOUND (ug/L) (ug/L) (ug/L)_ REC # REC. Dichlorodifluoromethane 50 48 96 48-135 Chloromethane 50 43 86 60-118 Vinyl Chloride 50 45 90 65-113 Bromomethane 50 58 116 73-122 .. Chloroethane 50 47 94 72-118 Trichlorofluoromethane 50 59 118 68-129 l,l-Dichloroethene 50 50 100 67-121 Acetone 50 46 92 38-161 Iodomethane 50 55 110 72-130 Carbon Disulfide 50 48 96 53-137 Methylene Chloride 50 51 102 59-132 trans-1,2-Dichloroethen 50 42 84 71-124 Methyl tert-butyl ether 100 79 79 75-123 1,1-Dichloroethane 50 40 80* 83-116 Vinyl acetate 50 69 138 44-160 2-Butanone 50 38 76 64-139 cis-1,2-Dichloroethene 50 42 84 83-120 2,2-Dichloropropane 50 38 76 70-129 Bromochloromethane 50 45 90 85-124 Chloroform 50 44 88* 89-118 Tetrahydrofuran 50 52 104 76-126 1,1,1-Trichloroethane 50 41 82 81-122 1,1-Dichloropropene 50 44 88 76-122 Carbon Tetrachloride 50 42 84 79-125 1,2-Dichloroethane 50 43 86 83-123 Benzene 50 44 88 81-120 Trichloroethene 50 44 88 77-121 1,2-Dichloropropane 50 43 86 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 1 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike Sample No. : V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. - ------------ --------- ------------- -----------__ ______ ______ Dibromomethane 50 45 90 - 86-124 Bromodichloromethane - 50 41 82* 90-114- cis-1,3-Dichloropropene 50 40 80 78-119 4-Methyl-2-pentanone 50 36 72 57-138 _ Toluene 50 45 90 . 81-121 trans-1,3-Dichloroprope .50 40 .80* 85-118 1,1,2-Trichloroethane 50 45 90 44-159 1,3-Dichloropropane 50 48 9.6 79-125 Tetrachloroethene 50 54 108 73-121 2-Hexanone 50 39 78 53-145 Dibromochloromethane 50 45 90 80-124 1,2-Dibromoethane 50 48 96 80-124 Chlorobenzene 50 50 100 82-118 1,1,1,2-Tetrachloroetha 50 46 92 84-121 Ethylbenzene 50 49 98 80-122 Xylene (Total) 150 150 100 81-121 Styrene 5.0 50 100 77-128 Bromoform 50 42 84 77-130 Isopropylbenzene 50 49 98 58-148 1,1,2,2-Tetrachloroetha 50 49 98 76-125 Bromobenzene 50 49 98 76-124 1,2,3-Trichloropropane 50 46 92 57-140 n-Propylbenzene 50 51 102 72-119 2-Chlorotoluene 50 50 100 75-120 1,3,5-Trimethylbenzene 50 50 100 76-116 4-Chlorotoluene 50 51 102 78-116 tert-Butylbenzene 50 49 98 71-115 .1,2,4-Trimethylbenzene 50 51 102 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL.SAMPLE .Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : -SAS No. : SDG No. : MC1600 v Matrix Spike - Sample No. : V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION It LIMITS _ COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- ------------- ------------- ------ ------ sec-Butylbenzene 50 51 102 67-117 4-Isopropyltoluene 50 52 104 . 68-118 1,3-Dichlorobenzene 50 52 104 80-116 1,4-Dichlorobenzene 50 52 104 80-114 n-Butylbenzene 50 52 104 58-121 1,2-Dichlorobenzene 50 52 104 81-116 1,2-Dibromo-3-chloropro 50 41 82 71-126 1,2,4-Trichlorobenzene 50 49 98 67-114 Hexachlorobutadiene 50 47 94 50-111 Naphthalene 50 46 92 58-133 1,2,3-Trichlorobenzene 50 50 100 64-118 Ether 50 51 102 10-130 Diisopropyl Ether 50 45 90 .70-130 Ethyl tert-butyl ether 50 44 88 70-130 ) tert-Amyl methyl ether 50 46 92 70-130 1,4-Dioxane 1000 650 65*. 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON24ENTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE LCSD LCSD - - - - ADDED CONCEN'iRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. - - ------- --------- ------ ------ ------ ------ ------ ------ Dichlorodifluoromethane 50 44 88 9 40 48-135 Chloromethane 50 44 88 2 40 60-118 Vinyl Chloride 50 47 94 4 40 65-113 Bromomethane 50 58 116 0 40 73-.122 Chloroethane 50 48 96 2 40 72-118 Trichlorofluoromethane 50 58 116 2 40 68-129 1,1-Dichloroethene 50 51 102 2 40 67-121 Acetone 50 41 82 11 40 38-161 Iodomethane -50 55 110 0 40 72-130 Carbon Disulfide 50 48 96 0 40 53-137 Methylene Chloride 50 51 102 0 40 59-132 trans-1,2-Dichloroethen 50 41 82 2 40 71-124 Methyl tert-butyl ether 100 79 79 0- 40 75-123 1,1-Dichloroethane 50 39 78* 2 40 83-116 Vinyl acetate 50 39 78 56* 40 44-160 2-Butanone 50 36 72 5 40 64-139 cis-1,2-Dichloroethene 50 42 84 0 40 83-120 2,2-Dichloropropane 50 38 76 0 40 707129 Bromochloromethane 50 45 90 0 40 85-124 Chloroform 50 43 86* 2 40 89-118 Tetrahydrofuran 50 52 104 0 40 76-126 1,1,1-Trichloroethane 50 41 82 0 40 81-122 1,1-Dichloropropene 50 44 88 0 40 76-122 Carbon Tetrachloride 50 40 80 5 40 79-125 1,2-Dichloroethane 50 42 84 2 40 83-123 Benzene 50 43 86 2 40 81-120 Trichloroethene 50 43 86 2 40 77-121 1,2-Dichloropropane 50 42 84 2 40 81-116 # ,Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CONIMENTS: page 4 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No.-: SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE LCSD LCSD ADDED CONCENTRATION 16 % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dibromomethane 50 44 88. 2 40 86-124 Bromodichloromethane 50 41 82* 0 40 90-114 cis-1,3-Dichloropropene 50 40 80 0 40 78-119 4-Methyl-2-pentanone 50 36 72 0 40 57-138 _ Toluene 50 44 88 2 40 81-.121 trans-1,3-Dichloroprope 50 39 78* 2 40 85-118 . 1,1,2-Trichloroethane 50 44 88 2 40 44-159 1,3-Dichloropropane 50 46 92 4 40 79-125 Tetrachloroethene 50 52 104 4 40 73-121 2-Hexanone 50 37 74 5 40 53-145 Dibromochloromethane 50 43 86 4 40 80-124 1,2-Dibromoethane 50 47 94 2 40 80-124 Chlorobenzene 50 48 96 4 40 82-118 1,1;1,2-Tetrachloroetha 50 44 88 4 40 84-121 Ethylbenzene 50 48 96 2 40 80-122 Xylene (Total) 150 140 93 7 40 81-121 Styrene 50 49 98 2 40 77-128 Bromoform 50 40 80 5 4.0 77-130 Isopropylbenzene 50 47 94 4 40 58-148 ) 1,1,2,2-Tetrachloroetha 50 50 100 2 40 76-125 Bromobenzene 50 50 100 2 40 76-124 1,2,3-Trichloropropane '50 46 92 0 40 57-140 n-Propylbenzene 50 50 100 2 40 72-119 2-Chlorotoluene 50 50 100 0 40 75-120' 1,3,5-Trimethylbenzene 50 51 102 2 40 76-116 4-Chlorotoluene 50 52 104 2 40 78-116 tert-Butylbenzene 50 49 98 0 40 71-115 1,2,4-Trimethylbenzene 50 50 100 2 40 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : VGXLCS SPIKE LCSD LCSD ADDED CONCENTRATION s o QC LIMITS COMPOUND (ug/L) (ug/L) ' REC # RPD ## RPD REC. sec-Butylbenzene 50 51 102 0 40 67-117 4-Isopropyltoluene 50 . 51 102 2 40 68-118 1,3-Dichlorobenzene 50 52 104 0 40 80-116. 1,4-Dichlorobenzene 50 51 102 2 40 80-114 n-Butylbenzene 50 52 104 0 40 58-121 -1,2-Dichlorobenzene 50 52 104 0 40 81-116 1,2-Dibromo-3-chloropro 50 42 84 2 40 71-126 1,2,4-Trichlorobenzene 50 49 98 0 40 67-114 Hexachlorobutadiene 50 47 .94 0 40 50-111 Naphthalene 50 50 100 8 40 58-133 1,2,3-Trichlorobenzene 50 49 98 2 40 64-118 Ether 50 53 106 4 40 70-130 Diisopropyl Ether 50 45 90 0 40 70-130 Ethyl tert-butyl ether 50 44 88 0 40 70-130 tert-Amyl methyl ether 50 47 94 2 40 70-130 1,4-Dioxane 1000 630 63* 3 40 70-130 # Column to-be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 72 outside limits Spike Recovery: 10 out of 144 outside limits COMMENTS: page 6 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6X9,FB SPIKE SAMPLE LCS LCS QC. ' ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- ------------- ------------- ------ ------ _ ------------------------ --------- ------------- ------------- ------ ------ - Vinyl Chloride 1 0.8 80 80-120 1,1-Dichl'oroethene 1 1 100 80-120 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits COMMENTS: FORM III VOA ) 3C.. WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Phenol 50 0.0 38 76 0-127 bis(2-Chloroethyl)Ether 50 0.0 42 84 46-109 2-Chlorophenol 50 0.0 34 68 22-117 1,3-Dichlorobenzene 50 0.0 35 70 28-103 1,4-Dichlorobenzene 50 0.0 36 72 28-104 1,2-Dichlorobenzene 50 0.0 37 74 29-107 2-Methylphenol 50 0.0 45 90 40-104 2,21-oxybis(1-Chloropro 50 0.0 44 88 10-134 4-Methylphenol 50 0.0 48 96 35-106 N-Nitroso-di-n-prop. (1) 50 0..0 50 100 44-122 Hexachloroethane 50 0.0 35 70 24-104 Nitrobenzene 50 0.0 45 90 47-112 Isophorone 50 0.0 47 94 48-118 2-Nitrophenol 50 0.0 43 86 29-122 2,4-Dimethylphenol 50 0.0 63 126* 14-109 2,4-Dichlorophenol 50 0.0 44 88 31-122 1;2,4-Trichlorobenzene 50 0.0 41 82 33-108 Naphthalene 50 0.0 43 86 38-117 4-Chloroaniline 50 0.0 48 96 0-152 bis(2-Chloroethoxy)meth 50 0.0 46 92 49-112 Hexachlorobutadiene 50 0.0 39 78 28-109 4-Chloro-3-Methylphenol 50 0.0 48 96 48-117 2-Methy1naphthalene 50 0.0 45 90 43-113 Hexachlorocyclopentadie 50 0.0 56 112* 34-103 2,4,6-Trichlorophenol 50 0.0 50 100 34-127 2,4,5-Trichlorophenol 50 0.0 48 96 32-131 2-Chloronaphthalene 50 0.0 48 96 47-116 2-Nitroaniline 50 0.0 48 96 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 1 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKE24 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- ------------- ------------- ------ ------ Dimethylphthalate 50 0.0 48 96 53-124 Acenaphthylene 50 0.0 49 98. 50-119 2,6-Dinitrotoluene 50 0.0 50 100 52-122 3-Ni.troaniline 50 0.0 44 88 47-115 Acenaphthene 50 0.0 48 96 50-121 2,4-Dinitrophenol 50 0.0 50 100 0-144 4-Nitrophenol 50 0.0 49 98 0-160 Dibenzofuran 50 0.0 47 94 51-122 2,4-Dinitrotoluene 50 0.0 48 96 52-126 Diethylphthalate 50 0.0 .49 98 53-126 4-Chlorophenyl-phenylet 50 0.0 48 96 .50-124 Fluorene 50 0.0 49 98 52-125 4-Nitroaniline 50 0.0 44 88 47-117 4,6-Dinitro-2-methylphe 50 0.0 50 .100 3-151 N-Nitrosodiphenylamine 50 0.0 60 120 48-121 4-Bromophenyl-phenyleth 50 0.0 49 98 51-124 Hexachlorobenzene 50 0.0 50 100 52-124 Pentachlorophenol 50 0.0 61 122 5-125 Phenanthrene 50 0.0 49 98 52-128 Anthracene 50 0.0 50 100 52-127 Carbazole 50 0.0 54 108 54-126 Di-n-butylphthalate 50 0.0 50 100 56.-132 Fluoranthene 50 �0.0 50 100 53-130 Pyrene 50 0.0 48 96 53-131 Butylbenzylphthalate 50 0.0 48 96 54-128 3,31 -Dichlorobenzidine 50 0.0 1 2* 41-117 Benzo(a)anthracene 50 0.0 52 104 56-124 Cbrysene 50 0.0 51 102 53-123 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III SV-1 OLM03.0 ! 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case- No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ---------------------- -- bis(2-Ethylhexyl)phthal 50 0.0 48 96 56-127 Di-n-octylphthalate 50 0.0 46 92 59-138 Benzo(b) fluoranthene 50 0.0 43 86 58-126 Benzo(k)fluoranthene 50 0.0 54 108 60-124 Benzo(a)pyrene 50 0.0 48 96 61-121 Indeno(1,2,3-cd)pyrene 50 0.0 46 92 23-152 Dibenzo(a,h)anthracene 50 0.0 46 92 60-122 Benzo(g,h,i)perylene 50 0.0 47 94 57-124 (1.) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CONIIMENTS: page 3 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY. Lab Name: MIT EM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 — Matrix Spike - EPA Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION % % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ -- Phenol 50 36 72 5 40 0-127 bis (2-Chloroethyl)Ether 50 44. 88 5 40 46-109 2-Chlorophenol 50 31 62 9 40 22-117 1,3-Dichlorobenzene 50 38 76 8 40 28-103 1,4-Dichlorobenzene 50 39 78 8 40 28-104 1,2-Dichlorobenzene 50 40 80 8 40 29-107 2-Methylphenol 50 44 88 2 40 40-104 2,21 -oxybis(1-Chloropro 50 .45 90 2 40 10-134 4-Methylphenol 50 47 94 2 40 35-106 H-Nitroso-di-n-prop. (1) 50 49 98 2 40 44-122 Hexachloroethane 50 38 76 8 40 24-104 Nitrobenzene 50 46 92 2 40 47-112 Isophorone 50 47 94 0 40 48-118 2-Nitrophenol 50 39 78 10 40 29-122 2,4-Dimethylphenol 50 63 126* . 0 40 14-109 2,4-Dichlorophenol 50 39 78 12 40 31-122 1,2-,4-Trichlorobenzene 50 41 82 0 . 40 33-108 Naphthalene 50 44 88 2 40 38-117 4-Chloroaniline 50 48 96 0 40 0-152 bis(2-Chloroethoxy)meth 50 47 94 2 40 49-112 Hexachlorobutadiene 50 39 78 0 40 28-109 4-Chloro-3-Methylphenol 50 4.7 94 2 40 48-117 2-Methy1naphthalene 50 44 88 2 40 43-113 Hexachlorocyclopentadie 50 54 108* 4 40 34-103 2;4,6-Trichlorophenol 50 46 92 8 40 34-127 2,4,5-Trichlorophenol 50 47 94 2 40 32-131 2-Chloronaphthalene 50 48 96 0 40 47-116 2-Nitroaniline 50 48 96 0 40 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD ## RPD REC. ------------------------ ------ ------ Dimethylphthalate 50 48 96 0 40 53-124 Acenaphthylene 50 49 98 0 40 50-119 2,6-Dinitrotoluene 50 50 100 0 40 52-122 3-Nitroaniline 50 41 82 7 40 47-115 - Acenaphthene 50 48 96 0 40 50-121 2,4-Dinitrophenol 50 48 96 4 40 0-144 4-Nitrophenol 50 45 90 8 40 0-160 Dibenzofuran 50 48 96 2 40 51-122 2,4-Dinitrotoluene 50 49 98 2 40 52-126 Diethylphthalate 50 50 100 2 40 53-126 4-Chlorophenyl-phenylet 50 47 94 2 40 50-124 Fluorene 50 50 100 2 40 52-125 4-Nitroaniline 50 44 88' 0 40 47-117 4,6-Dinitro-2-methylphe 50 48 96 4 40 3-151 N-Nitrosodiphenylamine 50 59 118 2 40 48-121 4-Bromophenyl-phenyleth 50 49 98 0 40 51-124 Hexachlorobenzene 50 50 100 0 40 52-124 Pentachlorophenol 50 59 118 3 40 5-125 Phenanthrene 50 49 98 0 40 52-128 Anthracene 50 51 102 2 40 52-127 Carbazole 50 54 108 0 40 54-126 Di-n-butylphthalate 50 50 100 0 40 56-132 Fluoranthene 50 49 98 2 40 53-130 Pyrene 50 50 100 4 40 53-131 Butylbenzylphthalate 50 49 98 2 40 54-128 3,31-Dichlorobenzidine 50 2 4* 67* 40 41-117 Benzo(a)anthracene 50 48 96 8 40 56-124 Chrysene 50 52 104 2 40 53-123 l) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON]ME TS: page 5 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE MSD -MSD - - — ADDED CONCENTRATION . % a QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ - bis(2-Ethyl4exyl)phthal 50 48 96 0 40 56-127 Di-n-octylphthalate 50 46 92 0 40 59-138 Benzo(b)fluoranthene 50 44 88 2 46 58-126 Benzo(k)fluorant_hene 50 49 98 10 40 60-124 Benzo(a)pyrene 50 46 92 4 40 61-121 Indeno(1,2,3-cd)pyrene 50 46 92 0 40 23-152 Dibenzo(a,h)anthracene 50 46 92 0 40 60-122 Benzo(g,h,i)perylene 50 47 94 0 40 57-124 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 64 outside limits Spike Recovery: 6 out of 128 outside limits COMMENTS: _-- page 6 of 6 FORM III SV-1 OLM03.0 FORM 3 WATER SENIIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No.- : MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. Phenol 50 41 82 0-127 bis(2-Chloroethyl)Ether 50 43 86 46-109 2-Chlorophenol ' 50 37 74 22-117 1,3-Dichlorobenzene 50 37 74 28-103 1,4-Dichlorobenzene 50 37 74 28-104 1,2-Dichlorobenzene 50 39 78 29-107 2-Methylphenol 50 44 88 40-104 2,21 -oxybis(1-Chloropro 50 45 90 10-134 4-Methylphenol 50 46 92 35-106 N-Nitroso-di-n-prop. (1) .50 49 98 44-122 Hexachloroethane 50 36 72 24-104 Nitrobenzene 50 45 90 47-112 Isophorone 50 47 94 48-118 2=Nitrophenol 50 44 88 29-122 2,4-Dimethylphenol 50 54 108 14-109 2,4-Dichlorophenol 50 43 86 31-122 1,2,4-Trichlorobenzene 50 40 80 33-108 Naphthalene 50 43 86 38-117 4-Chloroaniline 50 57 114 ' 0-152 bis(2-Chloroethoxy)meth 50 47 94 49-112 Hexachlorobutadiene 50 38 76 28-109 4-Chloro-3-Methylphenol 50 46 92 48-117 2-Methylnaphthalene, 50 43 86 43-113 Hexachlorocyclopentadie 50 58 116* 34-103 2,4,6-Trichlorophenol 50 46 92 34-127 2,4,5-Trichlorophenol 50 44 88 32-131 2-Chloronaphthalene 50 47 94 47-116 2-Nitroaniline 50 48 96 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMME TS: page 1 of 3 FORM III SV FORM 3 WATER SEMIVOLATILE- LAB CONTROL SAMPLE Lab Name: MITKE2I CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. i MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS - LCS QC. ADDED CONCENTRATION CONCENTRATION a LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. -------------- --------- - - Dimethylphthalate 50 49 98 53-124 Acenaphthylene 50 49 98 50-119 2,6-Dinitrotoluene 50 49 98 52-122 3-Nitroaniline 5-0 49 98 47--115 Acenaphthene 50 48 96 50-121 2,4-Dinitrophenol 50 29 58 0-144 4-Nitrophenol 50 37 74 0-160 Dibenzofuran 50 48 96 51-122 2,4-Dinitrotoluene 50 51 102 52-126 Diethylphthalate 50 49 98 53-126 4-Chlorophenyl-phenylet 50 48 96 50-124 Fluorene 50 48 96 52-125 4-Nitroaniline 50 47 94 47-117 4,6-Dinitro-2-methylphe 50 41 82 3-151 N-Nitrosodiphenylamine 50 .60 120 48-121 4-Bromophenyl-phenyleth 50 48 96 51-124 Hexachlorobenzene 50 49 98 52-124 Pentachlorophenol 50 33 66 5-125 Phenanthrene 50 47 94 52-128 . 1 Anthracene 50 51 102 52-127 Carbazole 50 49 98 54-126 Di-n-butylphthalate 50 49 98 56-132 Fluoranthene 50 49 98 53-130 Pyrene 50 50 100 53-131 Butylbenzylphthalate 50 51 102 54-128 3,31 -Dichlorobenzidine 50 55 110 41-117 Benzo(a)anthracene 50 49 98 56-124 Chrysene 50 54 108 53-123 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * values outside of QC limits C014ME VTS: page 2 of 3 FORM III SV FORM 3 WATER SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEm CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS LCS— QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. bis(2-Ethy1hexyl)phthal 50 50 100 56-127 Di-n-octylphthalate 50 46 92 59-138 Benzo(b)fluoranthene '50 45 90 58-126 Benzo(b)fluoranthene 50 48 96 60-124 Benzo(a)pyrene 50 47 94 61-121 Indeno(1,2,3-cd)pyrene 50 47 94 23-152 Dibenzo(a,h)anthracene 50 47 94 60-122 Benzo(g,h,i)perylene 50 49 98 57-124 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 1 out of 64 outside limits COMMENTS: page 3 of 3 FORM III SV FORM 3 WATER PCB LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix Spike - Sample No. : P2PLCS SPIKE SAMPLE LCS LCS QC- ADDED CONCENTRATION CONCENTRATION `s LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- --------- Aroclor-1016 2.0 1.9 95 45-162 Aroclor-1260 2.0 2.0 100 54-159 SPIKE LCSD LCSD ADDED CONCENTRATION o R. QC LIMITS COMPOi7ND (ug/L) (ug/L) REC # RPD ## RPD REC. 1 Aroclor-1016 2.0 2.0 100 5 40 45-162 .Aroclor-1260 2.0 2.0 100 0 40 54-159 ##. Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out of 4 outside limits CON24ENTS: FORM III PCB U.S. EPA - CLP 5A EPA SAMPLE NO SPIKE SAMPLE RECOVERY — Lab Name: Mitkem Corporation Contract: 28367-0050- Mw-6 Lab Code: MITKEM Case No_ SAS No:_ SDG No_ : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED 96 Solids for Sample: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Limit Spiked Sample Sample Spike Analyte %R. Result (SSR) C Result (SR) C Added (SA) %R Q M yanide 75-125 24-1760 _449-6_0 9- U 100.00 24.2 N CA dr,000) — Z� 10�0 Comments: FORM V (Part 1) - IN SW846 0 :?6 R U.S. EPA - CLP 5A EPA SAMPLE NO SPIKE SAMPLE RECOVERY MW-6 Lab Name: Mitkem Corporation Contract: 28367-0050- Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED % Solids for Sample: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Antimony 75-125 453.9091 20.0000 U 455.50 99.7 P Arsenic 75-125 461.3849 20.0000 U 455.50 101.3 P Barium 75-125 8715.4382 200.0000 U 9100.00 95.8 P Beryllium 75-125 219.6424 5.0000 U 227.00 96.8 P Cadmium 75-125 212.8834 5.0000 U 227.00 93.8 P Chromium 75-125 870.6539 20.0000 U 910.00 95.7 P Lead 75-125 431.1052 10:0000 U 455.00 94.7 P Nickel 75-125 2193.3999 50.0000 U 2270.00 96.6 P Selenium 75-125 435.1203 30.0000 U 455.00 95.6 P 1 Silver 75-125 1176.6854 30.0000 U 1130.00 104.1 P. Thallium 75-125 387.4990 20.0000 U 455.00 85.2 P Vanadium 75-125 2208.8549 50.0000 U 2270.00 97.3 P Zinc 75-125 2175.3672 50.0000 U 2270.00 95.8 P Mercury 75-125 4.8231 0.3100 U 4.55 106.0 CV Comments: FORM V (Part 1) - IN SW846 U-S_ EPA - CLP 5B EPA SAMPLE NO POST DIGEST- SPIKE SAMPLE RECOVERY f MVJ-6 Lab Name: Mitkem Corporation Contract: 28367-0050- ! Lab Code: MITKEM Case No_ SAS No_ : SDG No. : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED Concentration Units: ug/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Cyanide 50.42 9.10 U 40.0 126.0 . CA Comments: FORM V (Part 2) - IN SW846 FORM 4 CLIENT SAMPLE NO. PCB METHOD BLANK SUMMARY PBLK2P Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No'_ : SDG No. : C1600 Lab Sample ID: MB-16376 Lab File ID: E2E3239F Matrix (soil/water) WATER Extraction: (SepF/font/Sonc) SEPF- Sulfur Cleanup (Y/N) Y Date Extracted: 01/05/05 Date Analyzed (1) : 01/11/05 Date Analyzed (2) : 01/11/05 Time Analyzed (1) : 0145 Time Analyzed (2) : 0145 Instrument ID (1) : E2 Instrument ID (2) : E2 - GC Column (1) : RTXCLPPEST ID: 0.53 (mm) GC Column (2) : RTXCLPPEST 2 ID: 0.53 (mm) � THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: LAB DATE DATE f SAMPLE NO. SAMPLE ID ANALYZED 1 ANALYZED 2 ----------.--- -------------- ---------- ---------- 01 P2PLCS LCS-16376 01/11/05 01/11/05 02 P2PLCSD LCSD-16376 01/11/05 01/11/05 03 MW-6 C1600-02D 01/11/05 01/11/05 04 05 06 07 -- - — 08 09 10 11 _ 12 - 13 14 _ 15 16 17 -- 18 19 20 f 21 22 23 24 25 _ 26 COMMENTS: page 1 of 1 FORM IV PCB FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHCET PBLK2P Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : 'C1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16376- Sample wt/vol: 1000 (g/ml) ML Lab File ID: E2E3239F Moisture: decanted: (YIN) Date Received: Extraction: (SepF/font/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: -(Y/N) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 0.20 U 11104-28-2------Aroclor-1221 0:20 U 11141-16-5------Aroclor-1232 0.20- U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor-1248 _ 0.20 U 11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 0.20 U FORM I PCB U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM - Case No. SAS No. : SDG No. : MC1600 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration . Analyte (ug/L) C- 1 C 2 C 3 C Blank C M Mercury 0.0 U 0.0 U 0.0 UJ 0_2 B 0.047 U CV FORM III - IN SW846 U-S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 283 0-0050-0000 Lab Code: MITKEM Case No_ SAS No. : SDG No_: MC1600 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib_ Continuing Calibration, Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Mercury 0.1 B L — CVI FORM III - IN SW846 U.S_ EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No_ : SDG No_ :. MC1600 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) :j UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U I 9.1 I UL 9.1 U 9.1 1 U 1 9.100 U CA FORM III - IN SW846 U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No_: SDG No_ : MC1600 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg).: Initial Calib. Continuing Calibration [Blank repa- Blank Blank (ug/L) ation Analyte (ug/L) C 1 C 2 C 3 C C M Cyanide 9.1 U CA FORM III - IN SW846 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID . (Standard) . VGD5091 Date Analyzed: 01/04/05 Instrument ID: V6 Time Analyzed: 0946 GC Column: DB-624 ID: 0.25 (man) Heated Purge: (Y/N) N IS1 IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT ## ------------ ---------- ------- ------- 12 HOUR STD 1254041 5.69 979194 9.31 595531 12.28 --. UPPER LIMIT 2508082 6.19 1958388 9.81 1191062 12.78 LOWER LIMIT. 627021 5.19 489597 8.81 297166 11.78 ------------ ---------- ------- - EPA SAMPLE NO. ------------------ ---------- ------- ------ 01 VBLK6W 1082800 5.69 838062 9.31 459355 12.28 02 V6WLCS 1122075 5.69 867157 9.30 533632 12.28 03 V6WLCSD 1098175 5.70 870698 9.31 531242 12.28 04 V6WLFB 1139168 5.69 880198 9.31 493146 12.28 05 MW-5 1085406 5.69 835585 9.31 463660 12.28 06 MW-6 1111915 5.69 842493 9.31 467074 12.28 07 MW-X 1060318 5.70 822849 9.31 449003 12.28 08 MW-3 1191821 5.69 918968 9.30 574487 12.28 09 MW-2 1380904 5.70 1.063946 9.31 595842 12.28 10 11 12 z 13 14 15 16 17 18 19 20 21 g. 22 IS1 = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 Y IS3 (DCB) = 1,4-Dichlorobenzene-d4 t. AREA UPPER LIMIT = +1000 of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT ## Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 ,- FORM VIII VOA OLM03.0 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard).: V6p5131 Date Analyzed: 01/05/05 Instrument ID: V6 Time Analyzed: 0943 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (Y/N) N IS1 IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT # 12 HOUR STD 1277052 5.69 925287 9.31 542187 12..28 UPPER LIMIT 2554104 6.19 1850574 9.81 1084374 12.78 LOWER LIMIT 638526 5.19 462644 8.81 211094 11.78 - -- ------ ------- ---------- ------- EPA SAMPLE NO. ------ ------- ---------- ------- 01 VBLK6X 1186587 5.69 821619 9.31 391099 12.28 02 VGXLCS 1282813 5.69 913049 9.31 543721 12.28 03 V6XLCSD 1276723 5.69 910202 9.31 524488 12.28 04 VGXLFB 1230971 5.69 857081 9.31 423470 12.28 05 MW-2DL 1212495 5.69 851652 9.31 460303 12.28 06 MW-6MS 135600.2 5.69 961182 9.31 555419 12.28 07 MW-6MSD 1396537 5.69 978535 9.31 562504 12.28 08 MW-3DL 1376067 5.69 949794 9.31 506083 12.28 09 10 11 12 _ 13 14 15 --- 16 17 _ 18 - 19 20 -- 21 - - 22 - - IS1 = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 IS3 (DCB) = 1;4-Dichlorobenzene-d4 AREA UPPER LIMIT = +1000 of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal-standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03:0 8B SEMIVOLATILE INTERNAL STANDARD AREA.AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : S2E3096 Date Analyzed: 01/05/05 Instrument ID: S2 Time Analyzed: 1648 IS1(DCB} IS2 NPT IS3 ANT AREA # RT # AREA # RT # AREA # RT # ------------ ---------- ------- ---------- --- 12 HOUR STD 296671 6.39 1152334 8.33 628299 11.14 UPPER LIMIT 593342 6.89 2304668 8.83 1256598 11.64 LOWER LIMIT 148336 5.89 576167 7.83 314150 10.64 EPA SAMPLE NO. ------------ ---------- ------- ---------- ---- 01 S2QLCS 284576 6.38 1089611 8.33 607066 11.14 02 SBLK2Q 286951 6..38 1112165 8.32 620030 11.14 03 MW-5 292953 6.39 1111524 8.32 613208 11.14 04 MW-6 293093 6.38 1103577 8.33 608562 11.13 05 MW-6MS 305097 6.39 1164650 8.33 650294 11.14 06 MW-6MSD 293230 6.38 1115200 8.33 616463 11.14 07 MW-X 265165 6.38 1010076 8.33 565724 11.13 08 09 _ 10 11 12 - 13 14 _ 15 16 -- 17 18 19 20 21 22 - IS1 (DCB) = 1,4-Dichlorobenzene-d4 IS2 (NPT) = Naphthalene-d8 IS3 (ANT) = Acenaphthene-d10 AREA UPPER .LIMIT = +1000-. of internal standard area AREA LOWER. LIMIT = - 50 0 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT ## Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-1 0LM03.0 j 8C SEMIVOLATILF INTERNAL STANDARD AREA AND RT SUMMARY Lab Name-.: MITIEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : S2E3096 Date Analyzed: 01/05/05 Instrument ID: S2 Time Analyzed: 1648 IS4(PHN) IS5(CRY) IS6 PRY AREA # RT # AREA # RT # AREA # RT ## 12 HOUR STD 1114180 13.54 936462 17.03 763720 18.66 UPPER LIMIT 2228360 . 14.04 1872924 17.53 1527440 19.16 LOWER LIMIT 557090 13.04 468231 16.53 381860 18.16 ------ ------- EPA SAMPLE NO. 01 S2QLCS 1052731 13.53 861869 17.02 757179 18 66 0'2 SBLK2Q 1089198 13.54 944709 17.01 779784 18.66 03 MW-5 1056015 13.54 926658 17.02 748006 18.67 04 MW-6 1036880 13.53 892655 17.02 724690 18.66 05 MW-6MS 1108799 13.54 924647 17.03 769831 18.66 06 MW-6MSD 1058390 13.55 876722 17.03 744718 18.67 07 MW-X 984375 13.53 859066 17.02 701059 18.66 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 IS4 (PHN.) = Phenanthrene-d10 IS5 (CRY) = Chrysene-d12 IS6 (PRY) = Perylene-d12 AREA UPPER LIMIT = +100s of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT= + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to .flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-2 OLM03:0