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70-92 Boston Street - Phase 1 Initial Site Investigation and Tier Classification - Appendix B - January 2006 APPENDIX B EPA FILE REVIEW DOCUMENTS FLYNNTAN SITE (Identification Code - 015Y) REMOVAL ACTION ADMINISTRATIVE RECORD FILE AND INDEX Prepared For: U.S.'&Vironmental Protection Agency Region I Emergency Planning and Response Branch John F. Kennedy Federal Building Boston, Massachusetts 02203 CONTRACT NO. 68-W5-0009 TDD NO. 98-07-0015 PC$NO. 5402 rr Prepared by: Roy F. Weston, Inc. Region I Superfund Technical Assessment and Response`Team 217 Middlesex Turnpike Burlington, Massachusetts 01803 SEPTEMBER 199 INTRODUCTION This document is the Index to the Administrative Record File for the Flynntan Site Removal Action. The Index cites site-specific documents and guidance documents used by EPA staff in selecting a removal action at the site. The proposed actions will protect public health, welfare, and the environment by preventing people or animals from coming into contact with the contaminated areas of the site. The proposed actions are as follows: 1)Taking measures to prevent unauthorized access to the site, including repairing or installing additional security fencing and/or providing 24-hour security during removal activities; 2) conducting additional sampling of interior and.exterior floor surfaces,and of drums,pails,and settling pits; 3)sweeping up,consolidating,and staging hazardous waste contamination found on the floor surfaces; 4) categorizing, containerizing, and staging the contents of drums, vats, containers, and settling pits; and 5) collecting and staging exterior lead- contaminated soil. Also, all wastestreams will be manifested and shipped off site for appropriate reuse or disposal at EPA-approved disposal facilities. The Administrative Record File is available for public review, by appointment, at the EPA Records Center, 90 Canal Street,First Floor,Boston,Massachusetts,02114,and at the Salem Public Library, 370 Essex Street, Salem, Massachusetts, 01970. Questions concerning the Administrative Record File should be addressed to the EPA On-Scene Coordinator. The Administrative Record File is required by the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA), 42 U.S.C. § 9613 (k), and EPA's implementing regulations, 40 CRF § 300.800.-825. or PLEASE NOTE: TIC FOLLOWIN DOCUMENTS COMPILED IN THIS ADMINISTRATIVE RECORD HAVE BEEN MADE FROM THE BEST AVAILABLE COPIES SITE-SPECIFIC DOCUMENTS ADMINISTRATIVE RECORD FILE INDEX for the Flynntan Site REMOVAL Removal Reports (Site File 2.02) 1. "Removal Program Preliminary Assessment/Site Investigation Report for the Flynn Tan Site, Salem,Massachusetts, 14 April 1998",prepared by Roy F. Weston, Inc., Superfund Technical .Assessment and Response Team (START)for-EPA Region I, June 1998. 2. Site Investigation Closure Memorandum from Athanasios Hatzopoulos,EPA On-Scene Coordinator, through Steven Novick, Section Chief, Site Evaluation&Response Section II, EPA Region I,to the-Flynntan Site File, regarding the closure of the site investigation at the Flynntan Site, 70-92 Boston Street, Salem, MA, dated 28 April 1998. Pollution Reports (Site File 2.04) 3: Pollution Report No. 1, Flynntan Site, 70-92 Boston Street, Salem, Massachusetts, from U.S. EPA On-Scene Coordinator (OSC) A. Hatzopoulos, 20 July 1998. Action Memorandum (Site File 2.09) 4. Memorandum from Athanasios Hatzopoulos, On-Scene C(ordinator, EPA Region I,through Steven R.Novick,Chief,Site Evaluation and Response II, to Patricia L. Meaney,Director,Office of Site Remediation and Restoration, EPA Region I, concerning Request for a Removal Action at the Flynntan Site, Salem, Massachusetts, dated and signed 26 May 1998. (The Enforcement Section of the Memorandum is withheld as being CONFIDENTIAL).. POTENTIALLY RESPONSIBLE PARTY(PRP) PRP - Specific Correspondence(Site File 11.09) 5. Letter to Salem Realty; LLC, c/o Jan Exman, Manager, 66 Old Blue Hill Road, Durham, Connecticut 06422, from Dennisses Valdez, Acting Chief,. Emergency Planning and Response Branch, EPA Region I, concerning notice of potential liability and invitation to perform or finance proposed cleanup activities: Flynntan Site, dated 4 May 1998. COMMUNITY RELATIONS .News Clippings/Press Releases (Site File 13.03). 6. "Administrative Record File Available-for the Flynntan Site Removal Action,"text of the advertisement as it was requested to appear in the Salem Evening News, Salem, Massachusetts. w SELECTED KEY GUIDANCE DOCUMENTS EPA guidance documents may be reviewed at the EPA Superfund records room, Canal Street, Boston, Massachusetts. 1. Comprehensive Environmental Response, Compensation, and Liability Act of 1980, as amended,42 U.S.C. § 9601 et seq. 2.- "National Oil and Hazardous Substances Pollution Contingency Plan,"-Code of Federal Ret,,lations.(Title 40,Part 300) 1990. 3. "Action Memorandum Guidance", Superfund Removal Procedures, U.S. EPA, Office of Emergency and Remedial Response, OSWER Directive 9360.3-01, September 1990. 4. SWperfund Amendments and Reauthorization Act of 1986. a - REMOVAL,PROGRAM PRELIMINARY ASSESSMENT/ SITE INVESTIGATION REPORT FOR THE FLYNN TAN SITE SALEM, MASSACHUSETTS 14 APRIL 1998 Prepared For: U.S. Environmental Protection Agency Region I Emergency Planning and Response Branch John F. Kennedy Federal Building Boston, MA 02203 CONTRACT NO. 68-W5-0009 TDD NO. 98-05-0077 PCS NO. 5076 w DC NO. R-1523 Submitted By: Roy F. Weston, Inc. . Superfund Technical Assessment and Response Team 217 Middlesex Turnpike Burlington, MA 01803 June 1998 I TABLE OF CONTENTS I. Preliminary Assessment/Site Investigation Forms II. Narrative Chronology lII. Appendices Appendix A - Site Location Map (Figure 1) Appendix B - Site Diagram (Figure 2) - Appendix C - Sample Location Maps(Figures 3A and 3B) Appendix D - Chain-of-Custody Record Appendix E - Photodocumentation Log Appendix F - Volatile Organic Compound Analytical Data Appendix G - Semivolatile.Organic Compound Analytical Data Appendix H - pH Analytical Data Appendix.I - Polychlorinated Biphenyls Analytical Data Appendix.J - Metals Analytical Data w Appendix K - Flashpoint Analytical Data I. Preliminary Assessment/Site Investigation Forms r� C Aw EPA REGION I REMOVAL PRELIMINARY ASSESSMENT Site Name and Location Name:Flynn Tan Location: 70-92 Boston Street Town:Salem County.-Essex State: MA Site Status: ( )NPL ( )NON-NPL ' ( )RCRA ( )TSCA ( )ACTIVE (X)ABANDONED . ( )OTHER (X)Attached US.GS Map of Location (X)Site I.D. No,. :015Y Latitude: 427- 311 11.8" North Longitude: 700 54 ' 37. 9" West Referral ( )Citizen (X)City/Town ( )State ( )Preremedial ( )RCRA { )Other: Name of referring party: City of Salem, Planning Department Phone (978) 745-9595 Address: Planning Department, 1 Salem Green, Salem, I Massachusetts Contacts Identified 1)Ms. Jane Guy - Salem Planning Department Phone: (978) 745-9595 2)Mr. Charlie Latulippe - Town of Salem Fire Phone: (978) 745-7777 Chief fr Source of Information (X) Verbal: Conversations between Ms.' Jane Guy, Salem Planning Department, and Chief Charles Latulippe of the Salem Fire Department with START member Patricia Coppolino. ( ) Report ( ) Other: Potential Responsible Parties Owner: Mr. Jan Exman Phone: ( )Not Available Address: Operator: Mr. Jan Exman Phone: ( )Not Available Address : 70-92 Boston Street REMOVAL PRELIMINARY ASSESSMENT Site Access Authorizing Person: Mr. Jan Exman Date: 26 March 1998 (X)Obtained ( )Verbal Phone: Not Available ( )Not Obtained (X)Written Physical Site Characterization Background Information: There are four buildings located on the 1.89-acre Flynn Tan Site (the site) . Flynn Tan was an operational tannery from 1920 through 1988,- during which time the facility manufactured lamb skin products. In 19.88, the site was abandoned. There are drums located in the building suspected 'of containing chemicals commonly used in 'tanning manufacturing processes. - The current owner of the site is Mr. Jan- Exman. The City of Salem alleges that portions of the site are being rented by Mr. Exman to tenants illegally (without certificates of occupancy).. Description of Substances Possibly Present, Known or Alleged: Several types of heating oils are allegedly stored in underground storage tanks . (USTs) located on the site, and it is suspected that 1 numerous drums are located throughout the Flynn Tan facility, there may be solid debris contaminating the floors .of the site buildings. Existing Analytical Data ( ) Real-Time Monitoring Data: None Available ( ) Sampling Data: None. Available w Potential Threat Description ofpotential hazards to environment and/or population -identify any of the criteria for a Removal Action (from NCP) ' that may be met by the site under 40 CFR 300.415 (b] (2] . I . Actual or potential exposure to nearby human populations, animals, . or the food chain from hazardous substances, pollutants or contaminants. ii . Actual or potential contamination of drinking water supplies or sensitive ecosystems. 1 - - J 2 REMOVAL PRELIMINARY ASSESSMENT Potential Threat (Concluded) Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or other. bulk storage containers, that may pose a threat of release. IV. High levels of hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate. V. Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate or be released. vi . Threat of fire or explosion. vii . The availability of other appropriate federal or state response mechanisms to respond to the release. viii _ Other situations or factors that may pose threats to public health or welfare or. the environment. Prior Response Activities ( ) PRP ( ) STATE ( ) FEDERAL ( ) OTHER Brief Description: None Available. Priority for Site Investigation W High ( ) Medium ( ) Low ( ) None Comments: The site building has been abandoned since 1988 and is located in a heavily populated residential area. The presence of unknown tannery waste poses a threat to the nearby population as well as to the North River Canal, which is located approximately 0 . 5 miles north of the site. Report Generation Originator: Patricia Coppolino Date: 13 April 1998 Affiliation: Roy F. Weston, Inc. (START) Phone: (781)229-6430 TDD No. : 98-05-0077 PCS No. : 5076 3 A_ EPA REGION I REMOVAL SITE INVESTIGATION Inspection Information Site .Name: Flynn Tan Address: ' 70-92 Boston Street Town: Salem County: Essex State: MA Date of Inspection: 14,16 and 17 April 1998 Time of Inspection: 0900 hours Weather Conditions: Cloudy, 60OF Site Status at. Time of Inspection: ( ) ACTIVE W INACTIVE Comments: The Flynn Tan Site (the site) currently is an inactive k tannery facility. Agencies/Personnel Performing Inspection Names Program (x) EPA: Athanasios Hatzopoulos Site Evaluation and Response Section II . Michael R. Usovicz Criminal Investigation Div. (x) EPA Contractor: Patricia Coppolino Roy F. Weston, Superfund Technical Assessment and Response Team (START) - Todd Borci Roy F. Weston, START Stephen Amirault Roy F. Weston., START w } State: (x) Other: Chief Charles Latulippe Salem 'Fire Dept. Current Owner Based on Field Interview: Jan Exman Physical Site Characteristics karmeter quantities/Extent (. ) Cylinders: (x) Drums: Approximately 21 55-gallon steel and plastic drums were observed inside a site. building. Most were located on the first_ floor and had various labels including flammable, corrosive, formic acid, degreasing solvent, chrome complex in isopropanol, SYN FOG insecticide, and sodium acetate. REMOVAL SITE INVESTIGATION Physical Site Characteristics (Concluded) ( ) Lagoons: (x) Tanks: ( ) Above: (X.) Below: There are approximately six underground. storage .tanks (UST) possibly containing heating and fuel oil located at the site. In addition, two settling tanks were observed on the first floor of the site building and to contained two phases of materials, liquid and sludge. ( ) Asbestos: W Piles:' Animal hide piles were observed north of the .USTs along the exterior southern wall of the building. t (x) Stained Soil: Stained areas were observed under a capacitor located on the first floor, and on a .former transformer pad located outside of the building east of the loading. dock. In addition, soil located on the cut slope bank along the exterior southern wall of the tannery building was discolored. In many areas, the soil appeared -to contain scrap animal hides. { ) Sheens:. 1 (x). Stressed Vegetation: The cut slope bank along the exterior southern 'side of the tannery building contained areas of stressed vegetation, and in some areas bare soil. ( ) Landfill: (x) Population in Vicinity: The area ' surrounding the site is heavily populated with both residential and commercial structures. An estimated 1,000 -individuals reside/work within 0.25 miles of the site. The Endicott School, a day-care facility with an estimated enrollment of '200 children, is located 0.2 miles west of the site. In additio several other schools, including Salem High School, are located within 1-radial mile of the site. (X) Wells: ( ) Drinking: (x) Monitoring: One monitoring well' was observed .north of the USTs in the parking area outside the tannery building. (X) Other.: Located within the site building were approximately 15 electrical capacitors and approximately 40 miscellaneous jars. Physical Site Observations The tannery buildings consists of one four-story wood and metal frame building (building a) that has sustained .two fires, one two- story brick building (building b) , and three storage buildings constructed on. buildings A & B. Many of the windows and doors are broken, and there was graffiti throughout the site buildings. An 2- REMOVAL SITE INVESTIGATION Physical Site Observations (Concluded) open concrete pit (which was sealed on 16 April 1998 by the City of Salem) was observed in the parking' area. On 16 April 1988 signs were posted on every entrance to the site buildings by the City of Salem stating that the site buildings are structurally unsound for habitation. Most of the area outside the site buildings is paved except for one small area north of-the alleged USTs. This area had —stressed vegetation and piles of animal hides adjacent to the southern external wall of the site building. . The site is fenced with a locked gate. The site is bordered to the north by.Goodhue Street, 13eaver Street ` and a residential/commercial area; to the east by the intersection of Boston Road/Goodhue Street, and a residential/commercial area; to the south by Boston Street and a residential/commercial area; and to the west by a residential/commercial area. Field Sampling and Analysis Matrix Analytical Field Instrumentation Parameter CGI O RAD PID FID. Background Readings: 0.LEL/20.90;02 <15mrad <l unit <1 ppm Drums : D-001 600 ppm D-007 180 ppm No other readings above background were noted. Field Quality. Control Procedures . (X) SOP Followed ( ) Deviation From SOP Conmaents: Description of Sampling Conducted -Samples collected on 16 April 1998 consisted of 11 drum samples (D- 001 through D-011) which were analyzed for metals,. pH, . flashpoint, semivolatile organic compounds (SVOCs) , and volatile organic compounds (VOCs) ; two soil samples (C-01 and C-02) which were analyzed for polychlorinated biphenyls (PCBs) ; ten soil samples (S- 001 through S-010) which were analyzed for metals-; . and three tank samples, two liquid (T-001A and T-03) and one sludge (T-001B) , which were analyzed for metals.' Samples S-001 through S-010, T- 001A; T=00.1B, and . T-03 • were analyzed at RECRA Lab-Net Chicago located in University Park, IL. Samples D-001. through D7011, C-01 And C-02 were analyzed at the. EPA New England Regional Laboratory (NERL) located in Lexington, MA. 3 REMOVAL SITE INVESTIGATION ) Analyses Analytical Parameter Media Laboratory (x) VOC ( ) AIR (x) NERL (x) PCB ( ) WATER ( ) CLP ( ) PESTICIDE (x) SOIL (x) PRIVATE (x) METALS (x) 'SOURCE ( ) SAS ( ) CYANIDE ( ) SEDIMENT ( ) SOW (x) SVOC ( ) TOXICITY ( ) DIOXIN ( ) ASBESTOS (x) OTHER: pH, flashpoint t Analytical results: See attached Receptors Comments ( ) Drinking ( ) Private: Water ( ) - Municipal: j (X) Groundwater: Groundwater may be impacted by materials leaching from the site. ( ) Unrestricted Access: (x.) Population in- Proximity: The site is located in a, heavily populated residential and commercial area. A large day-care facility is located approximately 0.2 miles west of the site along Boston Street. (X) Sensitive Ecosystem: North River Canal is located approximately 0 .5 miles north of the site. ( ) Other: Additional Procedures for Site Determination ( } Biological Evaluation ( ) ATSDR To be determined by EPA personnel. Site Determination Depending on further information, criteria that may be met by the site include 40 CFR 300.415 (b] (2] .1 parts: i. Actual or. potential exposure to nearby human populations, animals, or the food chain from hazardous substances, pollutants. or contaminants. 4 REMOVAL SITE nmSTIGATION Site Determination (Concluded) ii. Hazardous substances or pollutants or contaminants .in drums, barrels, tanks, or other bulk storage containers, that may pose a -threat of. release. iii. High levels of hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate. iv. Threat of fire or explosion. V. The availability of other appropriate federal or state response mechanisms to respond to. the release. Report Generation Originator: Patricia Coppolino Date: 01 May 1998 Affiliation: Roy- F. Weston, Inc. (START) Phone: (781) 229-6430 TDD No. : 98-05-0077 PCS No. : 5076 w 5 II. Narrative Chronology f , rr Narrative Chronology On 14 April 1998, Roy F. Weston, Inc. Superfund Technical Assessment and Response Team (START)members Patricia Coppolino and Todd Borci mobilized to the Flynn Tan Property (the - site) located at 70 - 92 Boston Street, Essex County, Massachusetts (see Appendix A - Site Location Map). The site is an old tannery that manufactured lamb skin products.from the 1920s to 1988. After 1988 the site was abandoned. The site is approximately 1.89 acres, and is owned by Mr. Jan Exman. The City of'Salem alleges that portions of the site are being rented by Mr. Exman to tenants illegally (without certificate of occupancy). START personnel met with U.S. Environmental Protection Agency (EPA) On-Scene Coordinator (OSC) Tom Hatzopoulos to determine if there were any potential sources of contamination at the site to sample. Site activities were conducted in accordance with the site health and safety plan (HASP). The site HASP has been prepared as a separate document, entitled Removal Program Site Health and.Safety Plan for the Flynn Tan Site Preliminary Assessment/Site Investigation, Salem, Massachusetts. Prior to the initial walkthrough, START personnel calibrated a Radiation Meter,.a Combustible Gas/Oxygen meter(CG1102), an Organic Vapor Analyzer(OVA), and an Organic Vapor Monitor (OW. Following equipment calibration, START personnel donned level C personal protection equipment (PPE) and conducted a site walk-through. START observed approximately 15 electrical capacitors, 21 55-gallon drums, and approximately 40 miscellaneous jars were.located in the site building. The drums were labeled"sodium acetate", "chrome complex in isopropanol", "SYN FOG insecticide", "flammable", "corrosive", "formic acid", and "degreasing solvent". Many of the.jars contained what appeared to be different colored dyes, while others were labeled "pretan", "cirial G30", and "retan". - Following the site walk-through; EPA and 'START personnel departed the site. On 16 April 1998,. START members Coppolino, Borci, and Stephen Amirault mobilized to the site and met with OSC Hatzopoulos,to conduct site investigation and perform sagpling activities. Site activities were.conducted in accordance with the site HASP. Prior to the walk-through, START personnel calibrated the Radiation Meter, the CGI/02, the OVA, and the OVM. Following the calibration of the air monitoring instruments, START members Coppolino and Borci donned level C PPE and entered the building to select.drum sample locations. While in the building, Special Agent Michael R. Usovicz, from the EPA Criminal Investigation Division, Salem Fire Department Chief Charles Latulippe, and Deputy Chief Brophy met with OSC Hatzopoulos to discuss the fire hazards of the building and the current shipping and storing operations being conducted in the site building. Following drum sample location selection, START personnel donned Level B PPE and began collecting drum samples. Drum samples were collected from the following containers: sample D- 001 was collected from a blue 55-gallon plastic drum,.with a label that.read "corrosive, do not. freeze", located in the storage room on'the first floor of the facility and was analyzed for flashpoint, semivolatile organic compounds (SVOCs), and volatile organic compounds (VOCs); sample D-002 was collected from a blue 55-gallon plastic drum, with a label that read "coagulite", located in the storage room on the first floor of the facility and was analyzed for flashpoint, SVOCs, and VOCs; sample D-003 was collected from a 55-gallon drum located in the storage room on the first floor of the facility and was analyzed for flashpoint, pH, SVOCs, and VOCs; - sample D-004 was collected from a.55-gallon drum located in the storage room on the first floor of the'facility and was .analyzed for flashpoint, pH, SVOCs, and VOCs; sample D-005 was collected from a 55-gallon drum, with a label that read "formic acid", and was located in the back room across from the loading dock entrance on the first floor of the facility and was analyzed for pH; sample D-006 was collected from a 55-gallon drum, with a label that read "fuel oil additive", located in the room east of the tumble room and was analyzed for flashpoint, SVOCs, and VOCs.- sample D-007 was collected from a 55-gallon drum located-between the tumble room and the room to the east of the tumble room and was analyzed for pH, flashpoint, VOCs, and SVOCs; sample D-008 was collected from a 55-gallon drum located in the northeastern portion of the tumble room and was analyzed for flashpoint, pH, SVOCs, and VOCs; sample D-009 was collected from a 55- gallon drum, with a label that read "chrom complex in isopropanol", located in the southern portion of the room east of the tumble room and was analyzed for metals, flashpoint, pH, SVOCs, and VOCs; sample D-010 was collected from a white 55-gallon plastic drum located.in the back room across from the loading dock entrance on the first floor of the facility and was analyzed for flashpoint, pH, SVOCs, and VOCs; and sample D-011 was collected from a 55-gallon drum located in the southern portion of the room east of the tumble room and was analyzed for flashpoint, pH, SVOCs, and VOCs. In addition, sample T-001A (a liquid) was collected from a settling tank located south of tumbler one in the tumble room, and T-OO1B (sludge) was collected from the same tank. Both samples were analyzed for metals. Finally, sample T-003 was collected l from a settling tank located in the garage area of the northern portion of the building and was analyzed for metals. START personnel then exited the building and donned level C PPE to collect soil samples, which were all analyzed for metals. S-001 was collected from the northwestern vat tub located in the vat room on the second floor of the facility; S-002 from the southwestern vat tub located on the second floor of the facility; S-003 from the trench at the bottom of the stairs coming from the vat room on the first floor of the facility;.5-004 from a trench located north of sample station D-007; S-005_from a trench located between tumblers two and three in the tumble room on the first floor of the facility; 5-006 from a'separate room located west of the freight elevator d1i the first floor Of the facility; S-007 from a separate room that is south of the loading dock entrance on the first floor of the facility; S-008 from a trench north of sample station T-001 on the first floor of the facility; and S-009 and S-010 from.the southern exterior portion of the building. In addition, soil sample C-01 was collected from soil under a leaking capacitor located to the east of sample station D-007, and C-02 from stained soil on a transformer pad located to the west of the loading dock. Both samples were analyzed for polychlorinated biphenyls (PCBs) (see Appendix B and C -Site Location Map and Site Sample Location Map). Sample'activities were performed in accordance with the site sampling quality assurance/quality control (QA/QC)plan, Removal Program Quality Assurance/Quality Control Plan for Flynn Tan Site Preliminary Assessment/Site Investigation, Salem, Massachusetts. Descriptions of samples collected on site are summarized in Table 1. Following the completion of laboratory sample collection, START personnel completed chain of custody.(COC) paperwork (see Appendix D - Chain of Custody Record). On 17 April 1998, START members Coppolino and.Borci returned to the site, donned level C PPE, and photodocunnented sample areas (see Appendix E-Photodocumentation Log). Samples were then subsequently_delivered to the EPA New England Regional Laboratory (NERL) in Lexington, Massachusetts for pH, flashpoint, VOC;'SVOCs and PCB analyses by EPA Region I Method. In addition samples were also shipped via Federal Express to RECRA Lab-Net Chicago; located in University Park,_.Illinois for Resource Conservation and Recovery Act (RCRA) metals analyses. (See Appendices F-Volatile Organic Compound Analytical Data, G- Semivolatile Organic Compound Analytical Data, H -pH Analytical Data, I- Polychlorinated Biphenyls Analytical Data, ]=Metals Analytical Data, and K-Flashpoint Analytical Data). w TABLE 1 Sample Descriptions - _ _:: . __ -: : . /�gypp -- .�-.. - :: •` D-001 Drum Grab N/A Black Viscous Blue plastic drum Labeled "corrosive" D-002 Drum Grab N/A Brown Viscous Blue plastic drum Libeled " te" D-003 Drum Grab N/A Brown Viscous N/A 4 D-004 Drum. Grab N/A Clear Viscous NIA D-005 Drum Grab N/A Clear Viscous 55-gallon-drum labeled "formic acid" D-006 Drum Grab N/A Clear Viscous 55-gallon drum labeled "fuel oil additive" D-007 Drum Grab N/A Orange Thick N/A D-008 Drum Grab N/A Dark Viscous N/A D-009 Drum Grab N/A Clear Viscous Drum labeled "chrom complex in iso ol" D-010 Drum Grab N/A. Clear- Viscous N/A D-011 Drum Grab N/A Clear Viscous NIA T-001A Tank Grab N/A Clear Viscous Liquid from settling j iMgd I tank T-001B Tank Grab N/A Brown Muddy Sludge.from bottom of Sludge I seal ing tank T-003• Tank Grab N/A Clear Viscous Liquid from settling Liquid tank S-001 soil Grab N/A Brown Silty Solid from vat tub S-002 Soil Grab N/A Brown Silty Solid from vat tub S-003 Soil Grab N/A Reddish Sk Solid from trench S-004 Soil Grab N/A Reddish Silty Solid from trench -S-005 Soil Grab N/A Brown -Silty Solid from trench l S-006 Soil Grab NIA Reddish Silty -Solid from hole in the / ground . S-007 Soil Grab N/A Brown Silty Solid from trench S-008 i Soil Grab N/A Brown silty Solid from trench TABLE 1 Sample.Descriptions (Concluded) - - E � - vim•:>-= j-:;>_s.,�:_a::.__ � - _ - - - max: _- _- - «-x;-:. •`s��;;: S-009 Soil Grab 0-3 Light Silty Decomposing material Brown S-010 Soil Grab 0-3 Brown i Silty Soil underr-a pile of hides C-001 Soil Grab N/A Brown Oily Soil'-under a ca acitor F- C-002 Soil Grab N/A Brown Offy Soil on a transformer ad *-If applicable. NA-Not applicable. III. Appendices APPENDIX A Site Location Map (Figure l) 4 � w ~' tern - �r �6belstr _ �urse ` ''� m• _`` c- — awl'`_ �, �� _ �� {+� `_ �' h�. oint 2q�1 ". I(ek-ood Goff Course 3__vptF LDDster=F r5tJdaepha i Jr 'y+ A-'•' .�\ ._:`�' __ __ - = '- - - _ I�A R Mill _ Farxr.�or \�, � �" GreenlaN.n =�' �' y. • >z-;:. p. { �"�CSch - oaaea iti Ceme`tery`` �. \ � =� � � _ 1 � sir' . =�- _SE r tta_ •• :,;; -;=::.;.- f tR 9 FSire _ A^ !.gbw. f •< ~�:3'�' —__ ✓ice: _ c ,il'r. -. 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OUADRANGLE(S): Salem, Massachusetts. 1985 t 1/2 0 1.MILE 1000 0 1000 2000 3000 &000 sm 6000 7000 FEET ----- - -- — , OVAOftANGLE LOCATION ' SITE LOCATION MAP Flynn Tan Site 70 -- 9 2 Boston Street REGION I SUPERFUND TECHNICAL ASSESSMENT AND RESPONSE TEAM TOO p DRAWN BY: -)ATT_ Salem , M a s s a c h u s e t t s 98-05-0077 M. BUTTERWORTH 6/19/98 FILE NAME: R:\98040006\figt.dwg FIGURE 1 APPENDIX B Site Diagram(Figure 2) 4 i W o DUNKIN Q o W N N DONUTS cr W 2�2 in i U W Q cLn y U m Z cV cai Q W i 3 J x am WIX 111 �y/ W O \ i ~ \ < Z to / to La � O m y I U U Q o O) ` 00 _ O _Z m vo ,� 1 Z al 0 Q00W _J o t7) � W m Li Q to 0 Ix W N Z o N W F- W tZ (' - w F- < _ la. 0 vi Lit W Li m J O V Z Q _ _ o a ; Li Z Q W p + Z I.- Lij Z m O O Z Q cc OZ U7 Q CL Z a-p U. cn W N LL- W Qo0 c� 0 Z m CD o a I,- N (A a Z W Q C► cr W OF) 0 0 W J to LLJ W H � N Z W Q J O 0 < � � W [r C9 j Z U ►- 0O Z O Z W to W Q Z N D U t9 ® CE W p m ZJ� W O WWWQ Z U g 0 W Z t!1 O K d Xp _ WY 20 CZ-3 O aJ O WQ O L Vl =) h- W U a O j n to j Q O o = b O zX X - J APPENDIX C Sample Location Maps (Figures 3A and 3B) 4 ' - i w ' J 2 00 0 La i M W p W t0 p Z 1W- cY O z 00 O p Cw7 M 1 O mm X % <O Z m (Wa (¢� ~ c H LL �, W �� W VC: m O o D Q N BOILER ^ m m w o ` ROOM op i z p ! C W C7 1 En W ` li ZY o a �� o a z 14:D wo Q o ® p to �U)Q o W ® ® o oz� c�� ®® 1 a o 0 L, Q m O0 ®O y I � Qo - cv p z in pip pl q to I -C ` O V 0 ccI10 W/ Q 1 N G cr O T 1 W Y J V) Q O. W U: O < in i _ U O p w m © Q M 045 [L I- acn o ch Y '� .a Q W F— O U N = LLJ I� ®/ Q p I- 4J — N ai m Z F- t- p (n 0 8 �0 0 Ef) N J = o© 4 Q Z .oM < L a ~ '�" ©© oCED o ~ � � Q 0 p '� \o Z m o : $ ©© cn Z w o cr LL. LL- N _o Go 0 o 1 1 ir N W J m Cl)Q (jj FO- W F O p O Z W O Z W © [7 0O0O OF O0 W U 0m� 2 m I-- QW Q J N �. <<O w F- aZ CL p > > Z mJm rr W Qp Q v, cr W a D.,r) cn Uv Uv U O- ©. 0f El 0 8 ® gym Am 5-001 VATS VAT ROOM STAIRS. . LEAD TO • 5-002 TUMBLER ROOM TOOL STAIRS. LEAD TO ROOM LOADING DOCK ENTRANCE 3 w � NOT TO SCALE SAMPLE LOCATION MAP FLYNN TAN SITE REGION 1 SUPERFUND TECHNICAL ASSESSMENT AND RESPONSE TEAM 70-90 BOSTON STREET MD NO. I DRAYM BY: DATE SECOND FLOOR 98-05-0077 BLANCHARD 4/20/98 SALEM, MASSACHUSETTS FILE NAME: FIGURE 3B r:\98040006\FIGURE38 APPENDIX D Chain-of-Custody R,ecoid 4 ' w - — o /15 � .PC TL QL - - - ��.o N Y L � - > c 4 O � Y. � H (1, v lu 75 cro oa -90 k 92 r 4� v Z o IL o z �1- o o 0 0 J IA 4 .4 0 0 U r +� 'O ? C) cJ U o� a > c 1 I oC r q 0 1 � Ob a o + E cc r 1 E Q s O WLU 8Vtl9 ccCL c 0 Z drM F- a pp O 1 1 r ttJ 6. Cul Z h liJ O t/i 1 4� is v v z r o 0 TAM ` � CL. Q. �L7 O O Q d �Q Cam - - Q -O C`p\\ C C - r . •'YAAI � '1 0000 � i i _i y O A lv V 11 N � � 1 1 ) J2 d Q d' o o p t] cd i k^ cc LP t°'� 6 09 � � � N P �� I \ns 00 - O N Y g w 0 q) "'c >�j cl /fir o M � 4 7� x o o z o Q 0 C 1Nt Q .. z O w 'o .- > > :% J o 0 o E V H o � o .�• o � s z E r1 E E W E M M V YYY g a Q � O Z �Z* US _M W Q Q z. C a N N tJ N K fu n' io ---- Z Q LU 0 0 �- y r z �p _Vo .. y . J O �r !�l pp O � 7 �7 •'� U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I N9 65644 - LAB CODE SOURCE �Vsl�f1 T�h PERMIT NO PROJECT# = ,} CITY ,`��GA'1/. /�� COLLECTOR STATION # 'WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) T'444 S SAMPLE TYPE:GRAB'^ T V, AIR TEMP (-C):< 00, 0'10 114-20-,> 21- COLLECTION DATE SAMPLE_LOCATION: SUPPLY WATER, WASTEWATER: RAW, TREATED Y Y M M D D Y Y M M D D (Circle One) Other 11,plalff I I b RpTolgli START. END PARAMETERS (CHECK APPROPRIATE) METALS _ a COLLECTION TIME BactI NH3 Phenol Tot_ Diss. ®. BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP (-C) _* Turb T P X-Ray Cr (T) Organics O&G Other S—M—be- -Cr(+6) pH(SU) , VOA's CN Fe TOT C12(mg/1) Hg ' FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (mi/1) 4 None NI Magmeter SIZE Pb Venturi m Sri FLOW METER EPA. SOURCE Parshall Zn TOTALIZER .V-Notch Inches/Degrees Other START :Rectangular END .Other EPA RIa-900-31 'Unpreserved sample MULTIPLIER . � U.S. ENVIRONMENTAL PROTECTION.AGENCY REGION I NO 65645 SOURCE—Flynn --rqn PERMIT NO.—_ LAB CODE PROJECT# CITY _L AlEnl, 1►l17 COLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) Z'ndo4M SAMPLE TYP B T V AIR TEMP (-C): < 0-, 0--10-, 11 --20 > 21 - COLLECTION DATE SAMPLE LOCATION:SUPPLY WATER, WASTEWATER: RAW, TREATED Y Y M M D D Y Y M M D O (Circle One) Other PARAMETERS (CHECK APPROPRIATE) METALS START END COLLECTION TIME Bacti NH3 Phenol Tot. Diss. SOD. NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP (-C) m Turb T P X-Ray Cr (T) Organics O&G Other W 'Cr (+6) pH(SU) m - VOA's CN Fe Hg TOT C12 (mg/l) [� _ - FLOW MEASUREMENT Mn SETTLEABLE SOLIDS(m1/1) None Ni Magmeter SIZE Pb Venturi. Sri FLOW METER EPA SOURCE Parshall Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END coe o�?wei, 'Unpreserved sample MULTIPLIER. . ' U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I LAB CODE NO _ 65646 SOURCE PERMIT NO PROJECT#1 11 CITY COLLECTOR STATION #ILI— ,0 Q 3 / WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) :F 'oon SAMPLE TYPE:GRAB, T V AIR TEMP (°C): < 00, 00A00, 11'-20°,> 210 COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED YYMMDD Y Y M M D �= (Circle One) Other d 1 '. PARAMETERS (CHECK APPROPRIATE) METALS START END COLLECTION TIME Bacti NH3 Phenol Tot. Diss. UTAI� BOD NO2+3 COD Cd START END TSS TKN PCB ' Cu SAMPLE TEMP (°C) El T P X-Ray Cr(T) Organics O&G .Other F 'Cr(+6) pH(SU) m .[ .. VOA's CN SVnL Fe TOT C12(mg/1) FLOW MEASUREMENT Hg Mn SETTLEABLE SOLIDS (ml/1) None - Ni � Magmeter SIZE Pb .Venturi m Sn FLOW METER EPA SOURC Parshall Zn TOTALIZER r --V-Notch Inches/Degrees Other START 'Rectangular - END Other _ °Unpreserved sample MULTIPLIER EPA RI-7500.31 j - U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I rj. 65647 LAB CODE SOURCE --fin PERMIT NO PROJECT # CITY �j �p, COLLECTOR STATION # El WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) L dOPC50 SAMPLE TYPE:GRABT V_ AIR TEMP (°C): < 0%0'-10 11 °=20%> 21° COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED YYMMDD YYMMDD (Circle One) Other 191 Sidel O START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. BOD NO2+3 COD Cd . START END TSS TKN PCB Cu SAMPLE TEMP (°C) Turb T P X-Ray Cr(T) Organics O&G Other_(�'lel�Py. Cr.(+6) pH(SU) VOA's . CN Fe TOT C 12(mg/1) [�[ FLOW MEASUREMENT H Mn SETTLEABLE SOLIDS (m111) None NI FT Magmeter SIZE Pb Venturi m Sn FLOW METER EPA- SOUR"rc Parshall. Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END flfhnr - U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 1 NO 65648 SOURCE l �n PERMIT NO LAB CODE PROJECT# CITY 'endCOLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) Tpkj/Oof s SAMPLE TYPE: AB T V_ AIR TEMP ("C): < 0 0°-i0°, 11°-20%>21 ° COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER,WASTEWATER: RAW,TREATED Y Y.M M D D. Y Y M M D D _ (Circle One) Other START END PARAMETERS (CHECK APPROPRIATE) METALS COrLLT_ECT�IOiN. TIME Bacti NH3 Phenol Tot. Diss. BOD NO2+3 COD Cd .START END TSS TKN PCB Cu SAMPLE TEMP (°C) ED Turb T P X-Ray. Cr(n Organics O&G Other x7h 'Cr (+6) pH(SU) m .� VOA's CN - Fe TOT C12(mg/1) � FLOW MEASUREMENT- Hg "Mn SETTLEABLE SOLIDS (mill) = None Ni. . Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshal l Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular _ END EPA AOt�her 'Unpreserved sample MULTIPLIER ' U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 1 LAB CODE 65649 SOURCE PERMIT NO PROJECT# CITY COLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) 11';�00f-s SAMPLE TYPE:GRAB,_T V_ AIR TEMP (°C): < 0 0440 11 0-200,> 21° COLLECT40N DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW, TREATED Y Y M M D D Y Y M M D D (Circle One) Other START END PARAMETERS (CHECK APPROPRIATE) METALS. COLLECTION TIME Bactl NHa Phenol Tot. Diss. BOD NO2.+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP (°C) [Q Turb T-P . X-Ray Cr.( ) Organics O&G Other Fl&%,&at- *Cr (+6) pH.(SU) Q VOA's- CN Fe, TOT C 12(mg/1) FLOW MEASUREMENT Hg Mn SETTLEABLE SOLIDS (mill) None NI 1 Magmeter SIZE Pb Venturi- m Sn FLOW METER EPA SOURCE Parshali Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END Other `Unpreserved sample MULTIPLIER U.S. ENVIRONMENTAL PROTECTION AGENCY'REGION I LAB CODE r0 65650 SOURCE PERMIT NO PROJECT# CITY 4qA COLLECTOR STATION # - r ) WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) SAMPLE TYPE:GRAB. T k AIR TEMP("C), < 00, 01%10, 11'-20',> 21 COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER,WASTEWATER: RAW,TREATED Y Y M M D D Y Y M M D D (Circle One) Other - START END sCi PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME rT ra. Bacti NH3 Phenol Tot. Diss. C�LuL21 BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP ("C) Turb T P X-Ray Cr(i) Organics O&G Other. 1 'Cr(+6) pH(SU) .❑ VOA's CN- Svet_ Fe TOT C12(mgt1) FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (m1/1) None Ni Magmeter SIZE Pb Venturi m SriFLOW METER EPA SOURCE Parshall Zn TOTALIZER —,V-NotchH Inches/Degrees Other START r =Rectangular END EPARtO-t7her 'Unpreserved sample MULTIPLIER a U.S. ENVIRONMENTAL.PROTECTION AGENCY REGION C 1. 0 65651 �J LAB CODE SOURCE f- n i n PERMIT NO PROJECT# CITY COLLECTOR STATION # D WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) DO fs SAMPLE TYPE:GRAB, -T—V- A AIR.TEM P ("C): < 0", 0'-10", 11'-20,> 21' COLLECON DATE SAMPLE LOCATION: SUPPLY WATER,WASTEWATER: RAW, TREATED Y Y M M D D Y Y M M D D (Circle One) Other START END _PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION-TIME Bacti NH3 Phenol. Tot. Diss. B.OD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP('C) m Turb T P- X-Ray Cr( ) Organics O&G Other H 'Cr(+6) pH(SU) [�] .❑ VOA's _CN ��G Fe TOT C12(mgt1) FLOW MEASUREMENT Hg Mn SETTLEABLE SOLIDS (mlll) l None Ni - Magmeter- SIZE Pb- Venturi m Sri FLOW METER EPA SOUR"- Parshall Zn TOTALIZER V-Notch HInches/Degrees Other START Rectangular END U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I LAB CODE N9 65652 = ' SOURCE Fwrnlail PERMIT NO PROJECT# CITY brn . AAA- COLLECTOR STATION # - WEATHER: CLEAR, RAIN,-SNOW(CIRCLE ONE) 1hd 400r.S SAMPLE TYPE- RA T V_ AIR TEMP ("C): < 0 0, 0 440. 114-20-,>210 COLLECTION DATE ,SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED ' Y Y M M D D Y Y M M D D (Circle One) Other .': PARAMETERS (CHECK APPROPRIATE) METALS START ENO COLLECTION TIME Bacti NH3 Phenol Tot Diss. t BOD N.02+3 COD START END TSS TKN PCB Cu SAMPLE TEMP (°C) m Turd . T P X-Ray' Cr M Organics O&G Other -Cr(_+6) pH(SU) M .E] 1(OA's CN Fe - TOT C12(mg/1) FLOW MEASUREMENT Hg 4 Mn SET Ni TLEABLE SOLIDS(mt/1) None �-T-� Magmeter SIZE L--�-i-1 Pb Venturi MSri FLOW METER EPA SOURCE Parshai l Zn TOTALIZER V-Notch Inches/Degrees Other A START ,Rectangular i Other END EPA RI-7500-31 -Unpreserved sample MULTIPLIER } �lv U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I jvQ 67261 SOURCE 4tfhn PERMIT NO LAB CODE PROJECT# CITY, tm- AL4 COLLECTOR- �• STATION # - ! WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE �- IGt'GbTs SAMPLE TYPE:GRAB,-T V_ w AIR TEMP (°C): < 00, 0°-10 0, 11°-20 >21- COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW, TREATED YYMMDD Y Y M M D D (Circle One) Other 4 ¢ PARAMETERS. - (CHECK APPROPRIATE) METALS START END COLLECTION TIME 6acti NH3 Phenol 71 Tot. Diss_ BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP('C) .Turb T P X-Ray Cr (T) Organics O&G Other J*1f -Cr(+6) pH(SU) . VOA's CN - - ► 4 Fe TOT C12(mg/1) H FLOW MEASUREMENT Mn SETTLEABLE SOLIDS ml/1) j None Mag meter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshal l Zn TOTALIZER V-Notch. Inches/Degrees Other START Rectangular END Mhnr U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 1 Np 67260 n PERMIT NO LAB CODE ' SOURCE T PROJECT# `! CITY COLLECTOR STATION #101 Azql 1)FT SAMPLE TYPE GRAB, T RAIN, �V WEATHER: CLEAR. SNOW(CIRCLE ONE) TryotdOTS AIR TEMP (°C): < 00, 0'-10', 11"-20 0,> 21' COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED Y Y M M D D Y Y M M Or D (Circle One) Other START END `-! PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME -Bacti NH3 Phenol Tot. Diss. tS�� BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE-TEMP (°C) Turb. T P X-Ray Cr M Organics O&G - Other 'Cr-(+6) pH (SU) [ .❑ VOA's CN Fe TOT C 12(mg/l) Hg FLOW MEASUREMENT Mn SETTLEABLE SOLIDS(mI/I) None Ni Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshall TOTALIZER V-Notch Inches/Degrees Other START Rectangular END EPA OOther 'Unpreserved sample MULTIPLIER I-7500-3Zvi U.S. ENVIRONMENTALPROTECTION AGENCY REGION 1 No -67265 rr LAB CODE t SOURCE Tlaan� PERMIT NO PROJECT# r CITY COLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE):rdPLpalS SAMPLE TYPE GRAB,_T - V_ AIR TEMP ('C): < 0 00-100, 11°-200,> 21° COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED Y Y M MriD D Y Y M M - D 01 (Circle One) Other. c START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. BOD NO2+3 COD Cd START END - TSS TKN PCB Cu SAMPLE TEMP("C) EE Turb T P X-Ray Cr M Organics O&G Other 'Cr (+6) pH (SU) m •❑ VOA's CN Fe TOT C 12(mg/1) Hg FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (m111) Npne Ni E Magmeter SIZE Pb1. Venturi Sn FLOW METER EPA SOl Parshall m Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END: EPA ROther 'Unpreserved sample MULTIPLIER - , •_ _ ... _ � -mot- ..._. _ .. .. 1• _ _ - - _ _ - •_• '• _ _ U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I t1i0 6i264 LAB CODE 1 SOURCE Jaqn PERMIT NO PROJECT# CITY COLLECTOR STATION # O l WEATHER: CLEAR. RAIN, SNOW(CIRCLE ONE)-2+?D� Q SAMPLE TYPE:GRABXT V_ AIR TEMP (*Q: < 0', 04100 11--20',> 21' COLLECTION DATE SAMPLE LOCATION:SUPPLY WATER,WASTEWATER: RAW,TREATED Y Y:M M D D YYMMDD (Circle One) Other I Of 91 r G Y 1 START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. EJEE15- � ` BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEM P(-C) m Turb T P X-Ray Cr( ) Organics O&G Other 'Cr(+6) pH(SU) M .E] VOA's CN Fe TOT C 12 09/1) [[[] Hg FLOW MEASUREMENT 4 Mn SETTLEABLE SOLIDS (ml/l) None Ni Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshall Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END M Other EPA RI-7-AM31 'UnpreserGed sample MULTIPLIER APPENDIX E Photodocumentation Log ; a 5 PHOTOGRAPHY LOG. SHEET Flynn Tan Property Site, Salem, Massachusetts D - 0 © 1 -�� 2. D_-001 D -00 r 1 - SCENE-."View of sample locations D-001, D-002,D-003,and.D-004 located in storage room on the first floor. FRAME NUMBER: 1 DATE:4/17/98 TIME:. 1000 SKY CONDPTION: Inside PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic M M TYPE:35 mm FILM ROLL: 95484 5 C - 02 1. _ . _ y t• . SCENE: View facing west of former exterior transformer pad and sample location C-02. `AME NUMBER:2 DATE:4/17/98 TIME: 1010 _Y CONWTION:Cloudy PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci 'CAMERA: Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL: 95484 , TDD No. 98-04-0016 Pagel o!6 PCS Nn_ S!Y!S PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts Mftm C . 02 SCENE: View facing west of former transformer pad and sample location C-02_ FRAME NUMEBER:3 DATE:4/17/99 TIME: 1010 SKY CONDITION:Cloudy PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic / FILM TYPE:35 mm FILM ROLL: 95484 t> - CAPACITOR w SCENE: Interior:view facing toward laboratory.room in basement. A capacitor,still connected,can be seen at upper:left. FRAME NUMBER:4 DATE:4/17/99 TIME: 1020 J SKY CONDITION: Inside PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL: 77270 PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts CAPACITORS SCENE:Interior view of basement Engine Room. Two connected capacitors can be seen at center. Two identical connected capacitors are out of view io the right. FRAME NUMBER 5 DATE:4/17/98 TIM: 1030 `KY_CONDMON:Inside PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci ;AMERA: .Olympus SETTING: Automatic -UM TYPE:35 mm FILM ROLL: 77270 w i i i:ENE:: View facing east of southwestern portion of Flynn Tan building. - iTtAME NUMER:6 DATE:4/17/98 TIME: 1040 SKY CONDITION:Cloudy PHOTO BY: Patricia Coppolino WTTNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL: 77270 PHOTOGRAPHY LOG SHEET Flynn Tan Property.Site, Salem, Massachusetts CAPACITORS ` r O- 01 1, J SCENE:Interior view of center basement area and sample location C-01. Three capacitors(one leaking oil)can be seen at center: FRAME NUMBER:7 DATE:4/17/98 TIME: 1100 SKY CONDMON:Inside PHOTO.BY: Patricia Coppolino WITNESS(ES):Todd Borci 1 CAMERA:.Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL:77270 - 006 SCENE:Interior view of sample location S-006. FRAME NUMBER:8 DATE:4/17/98 TIME: 1110 SKY CONDITION.-Inside PHOTO BY: Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 turn FILM ROLL: 77270 PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts S- 010 S • 0v � f t SCENE: View.facing northeast of southern exterior portion of building, and sample locations S-009 and S-010_ FRAME NUMBER:9 DATE:4/17/98 TIME: 1120 SKY CONDITION:Cloudy PHOTO BY: Patricia Coppolino WITNESS(ES): Todd Borci CAMERA: Olympus SETTING: Automatic 'LM TYPE:35 mm FILM ROLL:77270 SCENE: View of southern entrance to Flynn Tan building and sign posted by City of Salem building inspectors on 16 April 1998,stating 'lding is condemned: --CAME NUMBER: 10 DATE: 4/17/98 TIME: 1200 "CONDITION: Cloudy PHOTO BY:Patricia Coppolino WITNESS(ES): Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL: 77270 TDD No.98-04-0016 Paee 5 of6 PCSNo.5076 PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Nfanwhusetts _.,. ` -010. Q'11005- SCENE:Interior view facing sample locations D-005 and D-010. Broken bags of pumice can be seen_ at lower right. FRAME NUMBER: 11 DATE:4/17/98 TIME: 1210 SKY CONDITION:Inside PHOTO BY:Patricia Coppolino WITNESS(ES):.Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 mm FILM ROLL:77270 Roy F.Weston,lea.- 217 Middlesex Tunpiae eurkvk n,Nassadwsoft 01803.33M m MWANAGUERS p lNSLXTAWS SUPERFUND TECHNICAL ASSESSMENT AND RESPONSE TEAM EPA CONTRACT 68-WS-0009 NEGATIVES. APPENDIX F Volatile Organic Compound Analytical Data w US ENVIRONMENTAL PROTECTION AGENCY 60 Westview Street Lexington, MA. 02173 DATE:May 1, 1998 SUBJECT:Flynntan Building,Salem,.MA Drums—Volatile Organic Analysis by GC/MS Samples Received: 65644, 65645, 65646, 65647, 65649,65650,65651, 65652, 67261, 67260 FROM:Joseph MontanaYo -E�IA- TO:Tom Hatzopoulos, HBR THRU:William Andrade, Ph.D.,Analytical Specialist PROJECT NUMBER: 98267 DATE(S) SAMPLES RECEIVED BY THE LABORATORY: 4/1.7/98 ANALYTICAL PROCEDURE.- Drum:- The samples were processed by Method 5035,High Concentration for Solid Waste and NonaQueous Liquid Waste. .The extracts were analyzed by SW-846, Method 8260B, Rev 0, January 1995, (VOAGCMS. SOP 8/97). Data file reference. VOADRML.SOP QUALITY CONTROL: 1.. A method blank was analyzed prior to sample analysis. --2. Each sample was spiked with three surrogate compounds at 25 ppb concentration. The results for the surrogate recoveries are reported for.each sample. 3. Sample 65645 was spiked in duplicate and analyzed to determine laboratory precision and accuracy. DATA FILE: J:ICHEMSTRYIREPORTS\VOA198267DR.WK4 p. 1 of 28 ANALYTICAL PARAMETERS { PURGEABLE ORGANIC ANALYSIS l INSTRUMENTS: Variion Archon Purge and Trap Autos_ampler l . Tekmar LSC-2000 Finnigan INCOS-50 XL PURGE CONDITIONS: Gas: Helium Purge Time and Flow: 11 min.,40 ml/min Dry Purge: 4 min.,40 ml/min Trap: 25 cm stainless steel (1/8 in.OD)packed with Carbopack B(10 cm) Carboxen 1000(6.cm), and Carboxen 1001 (1 cm) Desorption Time,Flow,Temperature: 4 min, 15 mVmin., 250 C Bake out cycle: 8 min @ 260 C CHROMATOGRAPHIC CONDITIONS: ) r Column: Restek MXT 105M length,0.28 mm id, 1.6.df(um) Program, Initial 50 C programmed;at 8 C/min to 220 C and held 220 C for 7 minutes. w Injector and 200 C Transfer Temperatures: Carrier Gas and Flow. Helium;15-ml/min MASS SPECTROMETER CONDITIONS: Electron Energy: 70 V Mass Range: 35 to 300 Scan Rate: 1.5-seconds \ % _s no US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY PROJECT AND REPORT FORM a Chemist Reviewing Data: William J.Andrade, Ph-.D. Method Modifications: None Limitations of Data: None Laboratory Blank Problems: None instrument Performance Problems: None Surrogate or Spike Recovery Problems: None Additional Comments: w There was no field trip blank sample for this analysis. A few target compounds did not meet the continuous calibration criteria for the analysis. These compounds were not observed in the samples analyzed. p. 3 of 28 MATRIX SPIKE DUPLICATE ANALYSIS - , FACILITY SAMPLED: FLYNN TAN SAMPLE NUMBER: 65645 FILE NAME(S): 04228E15.&04228E16 1 DATE OF ANALYSIS: 04/22/98 / ACCURACY COMPOUND AVERAGE% RECOVERY ACCEPTABLE RANGE2 1,1 Dichloroethylene 94_ 39-151 Chloroform 102 44-143 1,2 Dichlofoethane 86 45-143 1,1,1 Trichloroethane 96 49-158 Carbon Tetrachloride 85 62-139 Bromodichloromethane 84 49-130 Trichloroethylene 84. 41-139 Benzene 96 51-144 dibromochloromethane 82 32-141 Bromoform 71 28-132 1,4 Dichlorobenzene 90 68-121 .Vinyl chloride 83 D-181 PRECISION 1 #1 #2 ACCEPTABLE l Compound RECOVERY RECOVERY RPD RANGE2 1,1 Dichloroethylene 95 93 2 0-29 Chloroform 103 101 2 0-12 1,2 Dichloroethane 84 88 5 0-30 1,1,1 Trichloroethane 92 101 9 0-32 .. Carbon Tetrachloride 84 -B6 2 0-28 Bromodichloromethane 83 85 2 0-32 Trichloroethylene 80 88 9 or 0-28 Benzene 93 99 6 0-26 Dibromochloromethane 83 82 1 ' 0-42 Bromoform 68 .74 8 0-44 1,4 Dichorobenzene 94 87 5 0-19 Vinyl chloride 82 84 2 0-30 i=out of range J z=quality control acceptance criteria as per.laboratory p.4 of 28. FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION 1 LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID.: Lab Blank DILUTION FACTOR(S): 1 FILE NAME(S): 04228E3 DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppb Reporting CAS STORET Compound Conc. Limits Comments - NO. NO. (ug/L) (ug/L) TARGET COMPOUNDS 74787-3 34418 Chloromethane ND 5 74-83-9 34413 Bromomethane ND 5 75-01-4 39175 Vinyl Chloride ND 5 75-M3 34311 Chloroethane ND 5 15-09-2 34423 Methylene Chloride ND 5 75-69-4 34488 Trichlorofluoromethane ND 5 75-35-4 34501 1,1-Dichloroethylene ND 5 75-34-3 34496 1,1-Dichloroethane ND 5 . 156-60-5 34546 1,2-Dichloroethylene isomers . ND 5 67=66-3 32106 Chloroform ND 5 07-06-2 34531 1,2-Dichloroethane ND 5 11-55-6 34506. 1,1,1-Trichloroethane ND 5 56-23-5 32102 Carbon Tetrachloride ND 5 75-27-4 32101 Bromodichloromethane ND - 5 78-87-5 34541 1,2-Dichloropropane ND 5 10061-02-6 34699 t=1,3-Dichloropropene ND. 5 79-01-6 39180 Trichloroethylene ND 5 124-48-1. 32105 Dibromochloromethane ND 5 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 5 1,1-Dichloropropene 79-00-5 34511 1,1,2-Trichloroethane ND w 5 71-43-2 34030 Benzene, ND 5 75-25-2 32104 Bromoform ND 5 127-18-4 34475 Tetrachloroethylene ND 5 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 5 108-88-3 34010 Toluene ND 5 108-90-7 34301 Chlorobenzene ND 5 100-41-4 34371 Ethylbenzene ND 5 Dichlorobenzene isomers ND 5 1,1,2-Trichloro-1,2,2 h fluoroethane ND 5 67-64-1 8.1662 Acetone 5 10, L 75-15-0 77041 Carbon-Disulfide ND is (con't) p. 5 of 28 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY - GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM-- SAMPLE ID.: Lab Blank ) Sample Results Continued: pp CAS STORET Compound Conc. Reporting g Comments y NO. NO. (ug/L) (u9/W 78-93-3 81595 2-Butanone(MEK) ND 20 591-10-6 77103 2-Hexanone ND 3 108-10-1 81596- 4-Methyl-2-1?entanone(MIBK) ND 3 100-42=5 81708 Styrene ND 5 133-02-7 81551 Xylenes(total) ND 5 1;2-Dibromoethane (EDB) ND 5 Tetrahydrofuran ND 35 Ethyl ether ND 15 Isopropylbenzene ND 5 n-Propylbenzene ND 5 1,3,5-Trimethylbenzene ND 5 1,2,4-Trimethylbenzene ND 5 sec-Butylbenzene ND 5 para-Isopropyltoluene ND 5 n-Butylbenzene NO 5 Naphthalene ND 5 OtheFCompounds ) Tentatively Identified Other Compounds Quantitated w Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Ranger 1,2-Dichloroethane,d4 97 56-156 Toluene,d8 99 70-121 1,4-Bromofluorobenzene 93 76-125 Notes: ND-none detected above the detection level RL=Reporting Limit J=approximate 1 NA=not available due to dilution or interference J E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank i=out of range FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY . REGION I LABORATORY GC/MS PURGEABLE ORGANIC.ANALYSIS-DRUM SAMPLE_ID.: Method Blank SAMPLE WEIGHT: 0.097 g FILE NAME(S): 04228E4 DILUTION FACTOR(S): 50 DATE OF ANALYSIS: 04/22198 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO.. NO. (ug/g) (ug%g) TARGET COMPOUNDS 748.7-3 34418 Chloromethane ND 26 74-83-9 34413 Bromomethane ND 26 75=01-4 39175 Vinyl Chloride ND 26 75-00-3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488 Trichlorofluoromethane ND 26 75-35-4 34501 1,1-Dichloroethylene ND 26 75-34-3 34496 1,1-Dichloroethane ND 26 156-60-5 34546 1,2-Dichloroethylene isomers ND 26- 67-66-3 32106 Chloroform ND 26 07-06-2 34531 1,2-Dichloroethane ND 26 '1-55-6 34506 1 J,1-Trichioroethane ND 26 56-23-5 32102 Carbon Tetrachloride ND 26 75-27-4 32101 Bromodichloromethane -ND 26 78-87-5 34541 1,2-Dichloropropene ND 26 10061-02-6 34699 t-1,3-Dichloropropene ND 26 79-01-6 39180 Trichloroethylene ND 26 124-48-1 32105 Dibromochloromethane ND 26 10061-01-5 34704 c 1,3-Dichloropropene and/or ND 26 1,1-Dichloropropene 79-M5 34511 1,1,2-Trichloroethane ND 026 71-43-2 34030 Benzene ND 26 75-25-2 32104 Bromoform ND 26 127-18-4 34475 Tetrachloroethylene ND' 26 79-34-5 34516 1,1,2,2-Tetrach[oroethane ND 26 108-88-3 34010 Toluene ND 26 108-90-7 34301 Chlorobenzene ND 26 100-41-4 34371 Ethylbenzene ND 26 Dichlorobenzene isomers ND 26 1,1,2 Trichloro-1,2,2 trifluoroethane ND 26 67-64-1 81552 Acetone ND _ 52 75-15-0 77041 Carbon Disulfide ND 78 (con't) p.7 of 28 US ENVIRONMENTAL PROTECTION-AGENCY ` REGION I LABORATORY } GC/MS PURGEABLE ORGANIC.ANALYSIS--DRUM SAMPLE ID.: Method Blank ) Sample Results Continued: ppm Reporting . CAS STORET Compound Conc. Limits Comments . NO. NO. (4919) (uglg) 78-93-3 81595 2-Butanone(MEI) ND 104 591-10-6 77103 2-Hexanone ND 16 108-10-1 81596. .4-Methyl-2-Pentanone(MIBK). ND 16 100-42-5 81708 Styrene ND 26- 133-02-7 81551 Xylenes(total) ND 26 1,2-Dibromoethane (EDB) ND 26 Tetrahydrofuran ND 182 Ethyl ether ND 78 Isopropylbenzene ND 26 n-Propylbenzene ND 26 1,3,5-Trimethylbenzene ND 26 1,2,4-Trimethylbenzene ND 26 sec-Butylbenzene ND . 26 para-Isopropyftoluene ND 26 n-Butylbenzene ND 26 Naphthalene ND 26 Other Compounds . Tentatively Identified i Other Compounds Quantitated Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Rangei 1,2-Dichloroethane,d4 90. 56-156 Toluene,d8 101 70-121 1,4-Bromofluorobenzene 96 76-125 Notes: ND--none detected.above the detection level RL=Reporting Limit J=approximate NA=not.available due to dilution or interference . E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank i=out of range p. 8 of 28 FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY. GC/MS PURGEA13LE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65644 SAMPLE VV/EIGHT: 0.079 g FILE NAME(S): 04228E13 DILUTION FACTOR(S): 5000 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74-87-3 34418- Chloromethane ND 3200 74,83-9 34413 Broniomethane ND • 3200 75701-4 39175 Vinyl Chloride. ND 3200 75-00-3 34311 Chloroethane ND 3200 75-09-2 34423 Methylene Chloride ND 3200 75-69-4 34488 Trichlorotluoromethane ND 3200 75-35-4 34601 1,1-Dichloroethylen_e ND 3200 75-34-3 34496 1,1-Dichloroethane ND 3200 156-60-5 34546 1,2-Dichloroethylene isomers NO 3200 7-66-3 . 32106 Chloroform . ND 3200 ,07-06-2 34531 1,2-Dichloroethane ND 3200 71-55-6 34506 1,1,1-Trichloroethane ND 3200 56-23-5 32102 Carbon Tetrachloride NO, 3200 75-27-4 32101 Bromodichloromettiane ND 3200 78-87-5 34541 1,2-Dichloropropane ND 3200 10061-02-6 34699 t 1,3-Dichloropropene NO 3200 79-01-6 39180 Trichloroethylene ND- ' 3200 12448-1 32105 Dibromochloromethane ND 3200 10061-01-5 34704 c-1,3-Dichloropropene and/or ND' 3200 1,1-Dichloropropene Of 79-00-5 34511 1,1,2-Trichloroethane NO 3200 71-43-2 -34030 Benzene NO 3200 75-25-2 32104 Bromoform NO 3200 127-18-4. 34475 Tetrachloroethylene ND 3200 79-34-5 34516 1,1,2,2-Tetrachloroethane NO 3200 108-88-3 34010. Toluene NO 3200 108-90-7 3430-1 Chlorobenzene ND 3200 100-41-4: 34371 Ethylbenzene ND 3200 Dichlorobenzene isomers NO 3200 1,1,2-Trichloro-1,2,2- tritluoroethane NO 3200 67-64-1 81552 Acetone ND 6400 75-15-0 77041 Carbon Disulfide . ND' 9600-- (con't) n A of 28 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS—DRUM SAMPLE ID.: 65644 i Sample Results Continued: ppm Reporting - CAS STORET Compound Conc. Limas Comments NO. NO. (ug/gm) 0919m) 78-93-3 81595 2-Butanone(MEIn ND .12800 591-10-6 77103 2-Hexanone ND 1920 108-10-1 81596 4-Meth*2-Pentanone(MIBIq ND 1920 100-42-5 81708 Styrene ND 3200 133-02-7 81551 Xylenes(total) ND 3200 1,2-Dibromoethane ND 3200 Tetrahydrofuran ND 22400 Ethyl ether ND 9600 Isopropylbenzene ND 3200 n-Propylbenzene ND 3200 1,3,5-Trimethylbenzene 1100 3200 L 1,2,4-Trimethylbenzene 3800 3200 sec-Butylbenzene ND 3200 para-Isopropyltoluene ND 3200 n-Butylbenzene ND 3200 Naphthalene ND 3200 Other Compounds Tentatively Identified t Decane 4-Methyl Decane Undecane Other Compounds Quantitated w Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Ranges 1,2-Dichloroethane,d4 . 93 56-156 TolueneA8 106 70-121 1,4-Bromofluorobenzene 103 7.6-125 Notes: ND=none detected above the detection level RL=Reporting Limit J=approximate l NA=not available due to dilution or interference 1 E=estimated value exceeds the calibration range L=estimated value is below the calibration range -- B=analyte is associated with lab blank =out of range a n —s etc FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY - GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65645 SAMPLE WEIGHT: 0.139 g FILE NAME(S): 04228E5 DILUTION FACTOR(S): 50 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C . DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting: CAS- STORET Compound Conc. Limits. Comments NO. NO. (uglgm) (ug/grh) TARGET COMPOUNDS 74-87-3. 34418 Chloromethane ND 18 74-83-9 34413 Bromomethane ND 18 q 75-01-4 39175 Vinyl Chloride ND 18 75-00-3 34311 Chloroethane ND 18 75-09-2 34423 Methylene Chloride ND 18 75-69-4 34488 Trichlorofluoromethane ND 18 75-35-4 34501 1,1-Dichloroethylene ND 18 75-34-3 34496 1,1-Dichloroethane ND 18 156-60-5 34546 1,2-Dichloroethylene isomers ND 18 17-66-.3 .3210fi Chloroform ND 18 107-06-2 .34531 1,2-Dichloroethane ND 18 71-55-6 34506. 1,1,1-Trichloroethane -ND 18 56-23-5 32102 Carbon Tetrachloride ND 18 75-27-4 32101 Bromodichloromethane ND 18 78-87-5 34541 1,2-Dichloropropane ND 18 10061-02-6 -34699 t 1,3-Dichloropropene ND 18 79-01-6 39180 Trichloroethylene ND 18 124-48-1 32105 Dibromochloromethane ND 18 10061-01-5 34704. c-1,3-Dichloropropene and/or ND 18 1,1-Dichioropropene ff 79-00-5 34511 1,1,2-Trichloroethane ND 18 71-43-2 34030 Benzene ND 18 75-25-2 32104 Bromoform ND 18 127-18-4 34475 Tetrachioroethylene ' ND 18 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 18 108-88-3 34010 Toluene ND 18 108-90-7 34301 Chioroberizene ND 1.8 100-41-4 34371 Ethylbenaene ND 18 Dichlorobenzene isomers ND 18 1,2,2-Trichioro-1,2,2 b ifluoroethane ND 18 67-64-1 81552 Acetone ND 36 75-15-0 17041 Carbon Disulfide ND 54 (con't) p. 11 of 28 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/M$PURGEABLE'ORGANIC ANALYSIS-DRUM 1 SAMPLE 1D.: 65645 Sample Results Continued: ppm Reporting CAS STORET Compound Conc. Limits' Comments NO. NO. (ug/gm) (ug/gm) 78-93-3 81595 2-Butanone(MEK) ND 72 591-10-6 77103 2-Hexanone ND 11 108-10-1 81596 4-MethyP2-Pentanone(MIBK) ND 11 100-42-5 81708 Styrene . ND 18 133-02-7 81551 Xylenes(total) ND 18 1,2-Dibromoethane(EDB) ND .18 Tetrahydrofuran ND 126 Ethyl ether ND 54 Isopropylbenzene ND 18 - n-Propylberizene ND 18 1,3,5-Trimethylbenzene ND 18 1,2,4-Trimethylbenzene ND 18 sec-Butylbenzene ND 18 para-Isopropyltoluene ND 18 n-Butylbenzene ND 18 Naphthalene ND 18 Other Compounds ) Tentatively Identified Other Compounds Quantitated Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Range, 1,27Dichloroethane,d4 90 56-156 Toluene,d8 97 70-121 1,4-Bromofluorobenzene 90 76-.125 Notes: ND--- none detected above the detection level RL=Reporting Limit J=approximate l NA=not available due to dilution or interference - E=estimated value exceeds the calibration range t_=estimated value is below the calibration range B=analyte.is associated with lab blank i=out of range FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: . 65646 SAMPLE WEIGHT: 0.106 g FILE NAME(S): 04228E6 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C. DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Cont. Limits Comments NO. NO. (ug/gm) (uglgm) TARGET COMPOUNDS 74187-3 34418 Chloromethane ND - 24 74-83-9 34413 Bromomethane ND - 24 .75-01-4 39175 Vinyl Chloride ND 24 75-00-3 34311 Chloroethane ND 24 75-09-2 34423 Methylene Chloride ND 24 75-69-4 34488- Trichlorofluoromethane ND 24 75-35-4 34501 1,1-Dichloroethylene ND 24 75-34-3 34496 1,1-Dichloroethane ND 24 156-60-5 34546 1.2-Dichloroethylene isomers ND 24 7-66-3 32106 Chloroform ND 24 ,07-06-2 34531 1,2-Dichloroethane ND 24 71-55-6 34506 1j,1-Trichloroethane ND 24 56-23-5 32102 Carbon Tetrachloride. ND 24 75-27-4 32101 Bromod'rchloromethane ND 24 78-87-5 34541 1,2-Dichloropropane ND 24 10061-02-6 34699 t-1,3-Dichloropropene ND 24 79-01-6 39180 Trichloroethylene ND 24 124-48-1 32105 Dibrom' ochloromethane ND 24 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 24 1,1-Dichloropropene w 79-00-5 34511 1,1,2-Tiichloroethane ND 24 71-43-2 34030 Benzene - ND 24 75-25-2 '32104 Bromoform ND 24 127-18-4 34475 Tetrachloroethylene ND 24 79-34-5 34516 1,1;2,2-Tetrachloroethane ND 24 108-88-3 34010 Toluene ND 24 108-90-7 34301 Chlorobenzene NU 24 100-41.4 34371 Ethylbenzene ND 24 Dichlorobenzene isomers ND 24 .1,2,2-Trichloro-1,2,2 - trifluoroethane ND 24 67-64-1 81552 Acetone NO 48 75-15-0 77041 Carbon Disulfide ND 72 (con,t) n IAnf9R US ENVIRONMENTAL PROTECTION AGENCY REGION 1 LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID.: 65646 Sample Results Continued: pprn Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (uglgm) 78-93-3 81595 2-Butanone(MEK) ND 96 591-10-6 77103 2-Hexanone ND 14 108-10-1 81596 44Methyl-2-Pentanone(MIBK) ND 14 100-42-5 81708 Styrene ND 24 133-02-7 81551 Xylenes (total) ND 24 1,2-Dibromoethane(EDB) ND 24 Tetrahydrofuran ND 1.68 Ethyl ether ND 72 Isopropylbenzene ND 24 n-Propylbenzene ND 24- 1,3,5-Trimethylbenzene ND 24 1,2,4-Trimethyibenzene . ND 24 sec-Butylbenzene ND 24 para-Isopropykduene ND 24 n-Butylbenzene ND 24 Naphthalene ND 24 Other Compounds Tentatively Identified r. Other Compounds Quantitated rr Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Ranges 1,2-Dichloroethane,d4 98 56-156 Toluene,d8 97 70-121 1.4-Bromofluorobenzene 90 76-125 Notes: ND=none detected above the detection level RL=Reporting Limit J=approximate 1 NA--not available due to dilution or interference l E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank i=out of range FACILITY SAMPLED: FLYNNTAN BUILDING US.ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65647 SAMPLE WEIGHT: 0.119 g FILE NAME(S)4- 04228E7 DILUTION FACTOR(S): 50 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4-C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74-87-3 34418 Chloromethane NO 21 74-83-9 34413 Bromomethane ND 21 75-01-4 39175 Vinyl Chloride NO 21 75-00-3�- 34311 Chloroethane ND 21 75-09-2 34423 Methylene Chloride ND 21 75-69-4 34488 Trichlorofluoromethane ND 21 75-35-4 34501 1,1-Dichloroethylene NO 21 75-34-3 34496 1,1-Dichloroethane ND 21 156-60-5 34546 1,2-Dichloroethylene isomers ND 2.1 7-66-3 32106 Chloroform ND 21 :07-06-2 34531 1,2-Dichloroethane ND 21 - 71-55-6 34506 1,1,1-Trichloroethane ND 21 56-23-5 32102. Carbon Tetrachloride ND 21 75-27-4 32101 Bromodichloromethane ND 21 78-87-5 34541 1,2-Dichloroprnpane ND 21 10061-02-6 34699 tAi3-Dichloropropene ND 21 79-01-6 39180 Trichloroethylene NO 21 124-48-1 32105 Dibromochloromethane ND 21 . 10061-01-5 34704 c-1,3-Dichloropropene andlor ND 21 1,1-Dichloropropene hr 79-00-5 34511 1,1,2-Trichloroethane NO 21 71-43-2 34030 Benzene -ND 21 75-25-2 32104 Bromoform NO 21 127-184 34475 Tetrachloroethylene ND 21 79-34-5 34516 1,1,2,2-Tetr_achloroethane ND 21 108-88-3 34010 Toluene ND 21 108-90-7 34301 Chlorobenzene ND 21 100-41-4 34371 Ethylbenzene ND 21 Dichlorobenzerie isomers NO 21 1,22-Trichloro-1,22 trifluoroethane ND 21 67-64-1 81552 Acetone NO 42 75-15-0 77041 Carbon Disulfide ND 63 (con't) US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS=DRUM l SAMPLE ID.: 65647 / Sample Results Continued: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ugf9m) 0919m) 78-93-3 81596 2-Butanone(MEK) ND .84 591-10-6 77103 24Hexanone ND 13 108-10-1 81596 4-Meffrk2-0"none(MIBK) ND 13 100-42-5 81708 Styrene NO 21 133-02-7 81551 Xylenes(total) ND 21 1,2-Dibromoethane(EDB) ND 21 Tetrahydrofuran ND. 147 Ethyl ether ND 63. Isopropylbenzene ND 21' t n-Propylbenzene NO 21 1,3,5-Trimethylbenzene ND - 21 1,2,4-Trimethylbenzene ND 21 sec-Butyibenzene ND 21 pars-Isopropyltoluene ND 21 n-Butylbenzene ND 21 Naphthalene ND 21 Other Compounds Tentatively Identified Other Compounds Quantitated w Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Range, 1.2-Dichloroethane,d4 90 66-156 Toluene,d8 87. 70-121 1,4-Bromofluorobenzene 94 76-125 Notes: ND=none detected above the detection level RL=Reporting Limit J=approximate 1 NA=not available due to dilution or interference - E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab.blank c=out of range FACILITY SAMPLED: FLYNNTAN-BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65649 SAMPLE WEIGHT: 0.160 g FILE NAME(8): 04228E11 - DILUTION FACTOR(S): 1000 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22198 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Cone. Limits Comments NO. NO. (ug/gm) (ug/9m) TARGET COMPOUNDS 74=87-3, 34418 Chloromethane ND 310 7", 3-9 34413 Bromomethane ND 310 75-01-4 39175 Vinyl Chloride ND 310 75-00-3 -34311 Chloroethane ND 310 75-09-2 34423 Methylene Chloride ND 310 75-69-4 34488 Trichlorolluoromethane ND 310 75-35-4 34501 1,1-Dichloroethylene ND 310 75-34-3 34496 1,1-Dichloroethane ND" 310 156-60-5 34546. 1,2-Dichloroethylene isomers- ND 310 7-66-3 32106 Chloroform ND _ 310 07-06-2 34531 1,2-Dichloroethane ND 310 71-5.5=6 34.506 1,1,1-Trichloroethane ND 310 .56-23-5 32102 - Carbon Tetrachloride ND 310 75-27-4 32101 Bromodichloromethane ND 310 78-87-5 34541 1,2-Dichloropropane ND 310 10061-02-6 34699 t 1,3-Dichloropropene ND 310 79-01-6 39180 Tiichloroethylene ND 310 124-48-1 32105 Dibromochloromethane ND 310 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 310 1.1-Dichloropropene fr 79-00-5 34511 1,1,2-Trichloroethane ND 310 71-43-2 . - 34030 Ben'zene ND 310 75-25-2 32104 Bromoform -ND- 310 127-18-4. 34475 Tetrachloroethylene ND 310 79-34-5 34616 1,1,2,2-Tetrachloroethane 190 310 L 108-88-3 .34010 Toluene ND 310 108-90-7_ 34301 Chlorobenzene ND 310 100-41-4 34371 Ethylbenzene ND -310 Dichlorobenzene isomers ND 310 1,2,2-Tri6htoro-1,2,2 bffluoroethane ND 310 -67-64-1 81552 Acetone ND 620 75-15-0 77041 Carbon Disulfide ND 930 (con't) n_ 17 of 28 US ENVIRONMENTAL PROTECTION AGENCY REGION 1 LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM 1 SAMPLE ID.: 65649. Sample Results Continued: ppm Reporting CAS STORET Compound .Conc. Limits Comments NO. NO: (ugf9m) (ug/gm) 78-93-3 81595 2-Butanone(MEK) ND 1240 591-10-6 77103 . 2-Hexanone ND 186 108-10-1 81596. 4-Methyl-2-Pentanone(MIBI) ND 186 100-42-5 81708 Styrene ND 310 133-02-7 81551 Xylenes(total) 170 310 L 1,2-Dibromoethane(EDB) ND 310 Tetrahydrofuran ND 2170 Ethyl ether ND _930 Isopropylbenzene ND 310 n-Propyibenzene 120 310. L 1;3,5-Trimethylbenzene 420 310 15,4-Trimethylbenzene 1300 310 sec-Butylbenzene 140 310 L pare-lsopropyltotuene 200 310 L Naphthalene 70 310 L Other Compounds Tentatively Identified \ Nonane 44methyl Nonane 3-methyl Nonane Decane 4-methyl Decane butyl Cyclohexane Undecane 1-methyl-3-propyl Benzene Other Compounds Quantitated _ w Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Rangei 1,2-Dichloroethane,d4 91 56-156 Toluene;d8 107 - 70-121. 1,4-Bromofluorobenzene . 92 76-125 Notes: ND--none detected above the detection level RL=Reporting Limit J=approximate 1 NA=not available due to dilution or interference - E=estimated value exceeds the calibration range L--estimated value is below the calibration range -' B=analyte is associated with tab blank ]=out-of.range . FACILITY SAMPLED: -FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65650 SAMPLE WEIGHT: 0.083 9- FILE NAME(S): 04228E8 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04122/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Cont. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS- 7, 7-3 34418 Chloromethane ND 30 74-83-9 34413 Bromomethane ND 30 75-01-4 39175 Vinyl Chloride ND 30 75-00-3 34311 Chloroethane ND 30 75-09-2- 34423 Methylene Chloride NO 30 75-69-4 34488 Trichlorofluoromethane ND 30 75-35-4 34501 1,1-Dichloroethylene ND 30 75-34-3 34496 1,1-Dichloroethane ND 30 156-60-5 34546. 1,2-Dichloroethylene isomers ND 30 37-66-3 32106 Chloroform ND 30 107-06-2 34531 1,2-Dichloroethane ND 30 71-55-6 34506 1,1,1-Trichloroethane ND 30 56-23-5 32102 Carbon Tetrachloride ND 30 75-27-4 32101 Bromodichloromethane ND 30 78-87-5 34641 1,2-Dichloropropane ND 30, 10061-02=6 34699 t 1,3-Dichloropropene ND 30 79-01-6 39180 Tdchloroethylene ND 30 124-48-1 32105 Dibromochloromethane ND 30 10061-0.1-5 34704 a1,3-Dichloropropene and/or ND 30 1,1-Dichloropropene +f _79-00-5 34511 1,1,2-Trichloroethane ND 30 71-43-2 34030 Benzene ND 30 75-25-2 32104 Bromoform ND 30 127-18-4 34475 Tetrachloroethylene7 ND 30 79-34-5 34516 1,1,2,2-Tetrachloroethane ND- 30 108-88-3 34010 Toluene ND 30 108-90-7 34301 .Chlorobenzene ND 30 100-41-4 34371 Ethylbenzene ND 30 Dichlorobenzene isomers ND 30 1,2,2-Trichloro-1,22 trifluoroeth.ane ND 30 67-64-1 81552 Acetone ND 60 75-15-0 77041 Carbon Disulfide ND 90 (con't) - AA ..�74 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM _ SAMPLE ID.: 6565.0 Sample Results Continued: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ugfgm) (ugfgm) 78-93-3 81595 2-Butanone(MEK) ND 120 591-10-6 77103 2-Hexanone ND 18 108-10-1 81596 4-Methyl-2-Pentanone(MIBK) ND 18 100-42-5 81708 Styrene ND 30 133-02-7 81551 Xylenes(total) ND 30 12-Dibromoethane(EDB) ND 30 Tetrahydrofuran ND 210.. Ethyl ether ND 90 Isopropylbenzene ND 30 ` n-Propylbenzene ND 30 1,3,5-Trimethylbenzene ND 30 1,2,4-Trimethylbenzene ND 30 sec-Butylbenzene ND - 30 para-Isopropyltoluene ND 30 n-Butylbenzene ND 30 Naphthalene 'ND 30 Other Compounds Tentatively Identified Other Compounds Quantitated Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Rangei 1,2-Dichloroethane,d4 . 88 56-156 Toluene,d8 88 70-121 1,4-Bromofluorobenzene 101 76-125 Notes: ND,--none detected above the detection level RL=Reporting Limit J=approximate. NA--not available due to dilution or interference: - E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank i=out of range FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I-LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65651 SAMPLE WEIGHT: 0.075 g FILE NAME(S): 04228E12 DILUTION FACTOR(S): 10000 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET - Compound Conc. urnifis Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74-8-7-3 34418 Chloromethane ND 6700 74-83-9 34413 Bromomethane NO , 6700 75=01-4 39175 Vinyl Chloride NO 6700 75-00-3 34311 Chloroethane NO 6700 75-09-2 34423 Methylene Chloride NO 6700 75-69-4 34488 Trichlorofluoromethane NO 6700 75-35-4 34501 1,1-Dichloroethylene NO 6700 75-34-3. 34496 1,1-Dichloroethane NO 6700 156-60-5 34546 1,2-Dichloroethylene isomers ND 6700 17-66-3 32106 Chloroform NO 6700 .i 07-06-2 34531 1,2-Dichloroethane NO 6700 71-55-6 34506 1,1,1-Trichloroethane ND 6700 56-23-5 32102 Carbon Tetrachloride NO 6700 75-27-4 32101 Bromodichloromettiane NO 6700 78-87-5 34541 1,2-Dichloropropane NO 6700 10061-02-6 34699 t 1,3-Dichloropropene ND 6700 79-01-6 39180 Trichloroethylene NO 6700 124-48-1 32105 Dibromochloromethane ND 6700 10061-01-5 34704 c 1,3-Dichloropropene and/or NO 6700 1,1-Dichloropropene 79-00-5 .34511 1,1,2-Trichloroethane ND- 6706 71-43-2 34030 Benzene NO 6700 75-25-2 32104 Bromoform NO 6706 127-18-4 34475 Tetrachloroethylene NO 6700 79-34-5 .34516 1,1,2,2-Tetrachloroethane ND: 6700 108-88-3 34010 Toluene NO 6700 108-90-7 34301 Chlorobenzene ND 67.00 100-41-4 34371 Ethylbenzene NO 6700 Dichlorobenzene isomers NO -6700 1,2,2-Trichloro-1,2,2 tfifluoroethane NO 6700 67-6.4. 1 81552 Acetone ND 13400 75-15-0 77041 Carbon Disulfide NO 20100 (con't) p. 21 of 28 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM- 1 . SAMPLE ID.: 65651 J Sample Results Continued: _ ppm Reporting CAS STORET Compound . Conc. Limits Comments_ NO. NO. (ug/gm) (ug/gm) 78-93-3 81595 2-Butanone(MEK) ND 26800 591-10-6 77103 2-Hexanone ND 4020 108-106_1- 81596 4-Methyl-2-Pentanone(MI13I) ND . 4020 100-42-5. 81708 Styrene ND 6700 133-02-7 81551 Xylenes(total) ND 6700 1,2-Dibromoethane(EDB) ND 6700 Tetrahydrofuran ND 46900 Ethyl ether ND 20100 Isopropylbenzene ND 6700 .n-Propylbenzene ND 6700 1,3,5-Trimethylbenzene ND 6700 1,2,4-Trimethylbenzene 2400 6700 L sec-Butylbenzene NO 6700 para-Isopropyltoluene ND 6700 n-Butylbenzene ND 6700 Naphthalene ND 6.700 Other Compounds Tentatively Identified Decane Other Compounds Quantitated Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Ranger 12-Dichloroethane,d4 94 58-156 Toluene,d8 97 70-121 1,4-Bromofluombenzene 97 76-125 Notes: ND=none detected above the detection level RL=Reperting Limit J=approximate l NA:--not available due to dilution or interference. E=estimated value exceeds the calibration range L=estimated value is below the calibration.range ` } B=analyte is associated with lab blank 1=out of range FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65652 SAMPLE WEIGHT. 0.095 g FILE NAME($): 04228E9 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET' Compound Cone Limits Comments NO. NO. (ug/gm) (ug/gm). TARGET COMPOUNDS 7, =87-3 .34418 Chloromethane ND' 26 74=83-9 34413 Bromomethane ND 26 75-01-4 39175 Vinyl Chloride ND 26 75-00.3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488 Trichlorofluoromethane ND 26 75-35-4' 34501 1,1-Dichioroethyiene ND 26 75-34-3 34496 1,1-Dichloroethane ND 26. 156-60-5 34546 1,2-Dichloroethylene isomers ND 26 7-W3 32106 Chloroform ND 26 07-06-2 34531 1,2-Dichloroethane . ND 26 71-55-6 34506 1,1,1-Trichloroethane ND 26 56-23-5 32102 Carbon Tetrachloride ND 26 . 75-27-4 32101 13romodichloromethane ND 26 78-87-5 34541 1,2-Dichloropropane_ ND 26 10061=02-6 34699 t 1,3-Dichloropropene ND 26 79-01-6 39180 Trichloroethylene ND 26 124-48-1 32105 Dibromochloromethane- ND 26 10061-01-5 34704 c-1.3-Dichloropropene and/or ND 26 1,1-Dichloropropene rr 79-00-5 34511 1,1,2-Trichloroethane ND 26 71-43-2 34030 Benzene NO 26 75-25-2 32104 Bromoform ND 26 127-18-4 34475 Tetrachloroethylene ND 26 79-34-5 34516 1,1,2,2-Tetmchioroethane ND 26 108-88-3 34010 Toluene .ND; 26 108-90-7 34301 Chlorobenzene ND 26 100-41-4 34371 Ethylbenzene ND 26 Dichlorobenzene isomers ND 26 - 1,2,2-Trichloro-1,2,2 trifluoroethane ND 26 67.-64-1 . 81552 Acetone ND 52 75-15-0 77041 Carbon Disulfide . ND 78 (con't) US ENVIRONMENTAL PROTECTION AGENCY_ REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID.: 65652 Sample Results Continued: r ppm Reporting ` CAS - STORET Compound Cone Limits Comments NO. NO. (ug/gm) (uglgm) 78-93-3 81595 2-Butanone(MEK) ND 104 591-10-6 77103 2-Hexanone ND 16 108-10-1- 81596 4-Methyl•2-Pentanone(MIBI) ND 16 100-42-5 81708 Styrene ND 26 133-02-7 81551 Xylenes(total) ND 26 1,2-Dibromoethane(EDB) ND 26 Tetrahydrofuran ND 182 Ethyl ether ND 78 Isopropyibenzene ND 26 n-Propylbenzene ND 26 1,3,5-Tdmethylbenzene ND 26 1,2,4-Trimethyibenzene ND 26 sec-Butylbenzene ND 26 Para-Isopropyltoluene ND 26 n-Butylbenzene ND 26 Naphthalene NO 26 Other Compounds Tentatively Identified Other Compounds Quantitated Sample Recoveries fdr Observed . Acceptable Surrogate Compounds: Recoveries Ranget 1,2-Dichloroethane,d4 94 56-156 Toluene,d8 103 70-1.21 1,4-Bromofluorobenzene 100 76-125 Notes: ND--none detected above the detection level RL=Reporting.Limit J=approximate l NA--not available due to dilution or interference _ J E=estimated value exceeds the calibration range L=estimated value is below the calibration range - B=analyte is associated with lab blank t=out of range FACILITY'SAMPLED:-FFLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY - GC/MS PURGEABLE ORGANIC ANALYSIS - DRUM SAMPLE ID: 67261 SAMPLE WEIGHT: 0.080 g FILE NAME(S): 04228E14 DILUTION FACTOR(S): 5000 DATE OF COLLECTION:04/16198 PRESERVATIVE. Cool to 4 C DATE OF ANALYSIS: 04122/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (uglgm) TARGET COMPOUNDS 7"7-3 34418 Chloromethane ND 3100 74,83-9 34413 Bromometharie ND 3100 75-01-4 39175 Vinyl Chloride ND 3100 75-00-3. 34311 Chloroethane ND 3100 75-09-2 34423 Methylene Chloride ND 3100 75-69-4 3448.8 Trichlorofluoromethane ND 3100 75-35-4 34501 1,1-Dichloroethylene ND 3100 75-34-3 34496 1,1-Dichloroethane ND 3100 156-60-5 34546 1,2-Dichloroethylene isomers ND 3100 37-66-3 32106 Chloroform ND 3100 107-06-2 34531 1,2-Dichloroethane ND 3100 71-55-6 34506 1,1,1-Tr chloroethane ND 3100 56-23-5 32102 Carbon Tetrachloride ND 31'00 75-27-4 32101 Bromodichloromethane ND 3100 78-87-5 34541 1,2-Dichloropropane ND '3100 10061-02-6 34699 t 1,3-Dichloropropene ND 3100 79-01-6 39180 Trichloroethylene ND 3100 - 124-48-1 32105 Dibromochloromethane ND 3100 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 3100 1,1-Dichloropropene w 79-00-5 34511 1,1,2=Trichloroethane ND 3100 71-43-2 34030 Benzene ND 3100 . 75-25-2 32104 Bromoform ND 3100 127-18-4 3.4475 Tetrachloroethylene ND 3100 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 3100 .108-88-3 34010 Toluene ND 3100 108-90-7 34301 Chlorobenzene ND 3100 100-41-4 34371 Ethylbenzene ND 3100. Dichlorobenzene isomers ND 3100- 1,2,2-Trichloro-1,2,2 trifluoroethane ND 3100 67-64-1 81552 Acetone ND 6200 75-15-0 77041 Carbon Disulfide ND 9300' (con't) US ENVIRONMENTAL PROTECTION AGENCY. . = REGION I LABORATORY GC/MS PURGE4BLE ORGANIC ANALYSIS- DRUM 1 SAMPLE ID.: 67261 l Sample Results Continued: _. ppm Reporting CAS STORET Compound Conc. . Limits Comments 'NO. NO. NOW (ug/gm) 78-93-3 81595 2-Butanone(MEI) ND 12400 591-10-6 71103 2-Hexanone ND 1860 108-10-1 81596 4-Methyl-2-15entanone(MIBI) ND 1860- 100-42-5 81708 Styrene ND 3100 133-02-7 81551 Xylenes (total) ND 3100 1,2-Dibromoethane(EDB) ND 3100 Tetrahydrofuran ND 21700 Ethyl ether ND 9300 Isopropylbenzene ND 3100 n-Propylbenzene 1000 3100 L 1,3,5-Trimethylbenzene 3500- 3100" 1,2,4-Trimethylbenzene 13,000 3100 sec-Buty[benzene 1600 3100 L para-lsopropyltoluene 1800 3100 L n-Butylberizene ND 3100 Naphthalene 900 3100 L Other Compounds Tentativ__ely Identified Nonane � - 4-methyl Nonane 3-methyl Nonane Decane 4-methyl Decane 2-methyl Decane Undecane 1-methyl-2-propyl Benzene Other Compounds Quantitated If Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Range 1,2-Dichloroethane,d4 96. 56-156 Toluene,d8 94 70-121 1.4-Bromofluorobenzene 88 76-125 Notes: ND=none detected above the detection level RL=Reporting Limit J=approximate NA=not available due to dilution or interference ` E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank i=out of range FACILITY SAMPLED: -FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 67260 SAMPLE WEIGHT: 0.095 g FILE NAME(S): 04228E10 DILUTION FACTOR(S): 50 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Cons Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74-b7-3 34418 Chloromethane- ND 26 74-83-9 34413 Bromomethane ND 2-6 75-01-4 39175 Vinyl Chloride ND 26 75-00-3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488. Trichlorofluoromethane ND 26 75-35-4 34501 1,1-Dichloroethylene ND 26 75-34-3 34496 1,1-Dichloroethane ND 26 156-60-5 34546 1,2-Dichloroethylene isomers ND 26 7-66-3 32106 Chloroform ND 26 ;07-06-2- 34531 1,2-Dichloroethane ND 26 71-55-6 34506 1,1,1-Trichloroethane ND 26 56-23.5 32102 Carbon Tetrachloride ND 26 75-27-4 32101 Bromodichloromethane ND 26 78-87-5 34541 1,2-Dichloropropane ND 26 10061-02-6 34699 t 1,3-bichloropropene ND 26 79-01-6 39180 Trichloroethylene ND .26 124-48-1 32105 Dibromochloromethane ND 26 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 26 1,1-Dichloropropene w 79-00-5 34511 1,1,2-Trichloroethane ND 26 71-43-2 34030 Benzene ND 26 75-25-2 32104 Bromofonn ND 26 127-18-4 34475 Tetrachloroethylene ND 26 79-34-5 '34516 1,1,2,2-Tetrachidroethane ND 26 108-88-3, 34010 Toluene ND 26 108-90-7 34301 Chlorobenzene ND 26 100-41-4 34371 Ethylbenzene ND 26 Dichlorobenzene isomers ND 26 1,2,2-Trichloro-1,2,2 triAuoroethane ND 26 67-64-1 81552 Acetone ND 52 75-15-0 77041 Carbon Disulfide ND 78_ (con't) US ENVIRONMENTAL PROTECTION AGENCY • REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-.DRUM SAMPLE ID.: 67260 ' 1 Sample Results Continued: _. ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (uglgm) (ug/gm) 78-93-3 81595 2-Butanone(MEK) ND 104 591-10-6 77103 2-Hexanone ND 16 108-10-1 81596 4-Methyl 2-Pentanone(MIBK) ND 16 100-42-5 81708 Styrene ND 26 133-02-7 81551 Xylenes(total) ND 26. 1,2-Dibromoethane(EDS) ND 26 Tetrahydrofuran ND 182 Ethyl ether ND 78 Isopropylbenzene ND 26 ` n-Propylbenzene ND 26 1,3,5-Trimethylbenzene ND 26 1,2,4-Trimethylbenzene ND 26 sec-Butylbenzene ND 26 para-Isopropyltoluene ND 26 n-Butylbenzene ND 26 Naphthalene ND 26 Other Compounds Tentatively Identified ' Other Compounds Quantitated w Sample Recoveries for Observed Acceptable Surrogate Compounds: Recoveries Rangei 1,2-Dichloroethane;d4 90 56-156 Toluene,d8. 99 70-121 1,4-Bromofluorobenzene 92 76-125 Notes: ND--none detected above the detection level RL=Reporting Limit. J=approximate NA.-mot available due to dilution or interference. E=estimated value exceeds the calibration range L=estimated value is below the calibration range B=analyte is associated with lab blank_ t=out of range APPENDIX G Semivolatile Organic Compound Analytical.Data { .Of ) - w l �.� UNITED STATES ENVIRONMENTAL PROTECTION AGENCY A W . REGION 1 ENVIRONMENTAL SERVICES DIVISION ;F 60 WESTVIEW STREET 44 LEXINGTON,MASSACHUSETTS02173-3185 )ATE: May 20, 1998 ;UBJ: Gas Chromatography Analysis of Extractable Organics in a Aqueous Sample _ FLYNN TANNERY FROM: Dick SiscAtaw, Chemistry Section CHRU� Dr. William J. Andrade; Advance4 Analytical Chemistry Specialist TO: .Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received and logged in by the laboratory according to - the SOP for Sample Log-in (EIA-ADMLOGNI .SOP, 7/97) . EPA Region 1 Procedure: Base Neutral Acids. Extractables in Aqueous Samples, BNAWAHLI.SOP, 12/4/91. The samples are extracted using methylene chloride as the solvent. The, extracts are analyzed on a gas. chromatograph equipped with a FID detector. - w The analytical support for this report was performed by ESAT contractors . Dates) Samples Received by the Laboratory: 4/17/98- Date Analysis Started: 04/22/98 cc: - .File: J: \CHEMSTRY\REPORTS\BNA\98267WB.WPD AsoydodMocydabW•Printed wdh Vegetable Oti.Based kft on IOU%Rec cMd Paper(40%Postconsumed US ENVIRONMENTAL PROTECTION AGENCY 60 Westview Street Lexington, MA 02173 Chemist who reviewed data: Dick Siscanaw Holding times meet (YIN) : Yes Extraction (Water - 7 days, Soils - 14 days) ` Analytical (40 days after extraction) Method modifications: None .Limitations of data: None * Laboratory blank problems:. None w Instrument performance problems: None Surrogate and spike recovery problems: The acid surrogatet recoveries for sample 65652 are -low. This could be due to- the sample matrix or a laboratory preparation error. , Sample 67260 has low recovery for 2-fluorophenol. Additional comments: Sample 65646 formed a gelatinous emulsion during the aqueous L 2 US ENVIRONMENTAL PROTECTION AGENCY 60 Westview Street . Lexington, MA 02173 ANALYTICAL PARAMETERS INSTRUMENTS:' Hewlett Packard 5890 Gas Chromatograph Hewlett Packard 5987" Gas Chromatograph-Mass Spectrometer . GC/FID Screening Conditions: Gas: Hydrogen Capillary Column: DB-1, 30m, 25mm ID-, 0.25 micron film thickness Injection-Mode: Splitless Temperature Program: Isothermal for 3 min at 40°C, programmed at 150C/min to 3200C for 3 min a GC-MS Conditions: Gas: Helium . Capillary Column: DB-5, 60m, 25mm .ID, 0.25. micron film thickness w Injection Mode: Splitless Temperature Program: Isothermal for 4 min at 40°C, programmed at 70C/min to . 300°C Injector, Transfer Temperatures: 290°C, 3000C Electron Energy:- 70 V Mass Range: 35-550 Scan Rate: 6.9 seconds 3 US ENVIRONMENTAL PROTECTION AGENCY 60 Aestview Street Lexington, MA 02173 1 : A laboratory blank was processed with the samples. 2. Each sample was .spiked with 106 ug of base/neutral compounds and 200 ug of acid surrogate compounds. The results for the surrogate recoveries are reported out for each sample. 3. One sample, LCS Aqueous, was spiked with 100 ug of base/neutral- and 200 ug of -acid matrix spike compounds::, The results for the analyses are listed below. Compound Rec. QC Range . Comments M ($) Acenaphthene 84 46-118 4-Chloro-3-methylphenol 88 23-97 2-Chlorophenol 76 27-123 1, 4-Dichlorobenzene 68 36-97 1 2, 4-Dinitrotolueno 84 24-96 4-Nitrophenol 80 10-80 N-Nitrosodi-n-propylamine 76 41-116 Pentachlorophenol 98 9-103 Phenol 78 12-110 Pyrene 80 26-127 1,2, 4-Trichlorobenzene 80 39-98 - w SAMPLE (S) ANALYZED: BLANK, LCS, 65646, 65652, 67260 FACILITY SAMPLED: FLYNN TANK US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Matrix: Water DATE OF COLLECTION: NA Sample pH: N/A DATE OF EXTRACTION: 04/22/98 Conc. Final .Vol. 1 mL DATE OF ANALYSIS : 04/24/98 Dilution. Factor: None VOLUME EXTRACTED: 40 .mL Report Factor: 25 SAMPLE RESULTS: CAS ' Compound Conc. RL Qualifier NO. (ug/L) (rug/L) or Comment ------------------------------------------------------------------------ Priority Pollutants. 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND 160 309-00-2 Aldrin ND 160 56-55-3 Benzo (a) anthracene. ND 160 205-99-2 Benzo (b) fluoranthene ND 160' 207-08-9 Benzo(k) fluoranthene ND 160 50-32-8 -Benzo (a)pyrene' ND 160 191-.24-2 Benzo(ghi)perylene ND 160 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 319-86-8 delta-BHC ND- 160 111-44-4 Bis (2-chloroethyl) ether ND 160 111-91-1 Bis (2-chloroethoky)methane ND 160 117-81-7 Bis (2- ethylhexyl)phthalate ND 190 108-60-1 Bis'(2-chloroisopropyl-) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND . 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene- ND .160 95-57-8 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyl ether ND 160 218-01-9 Chrysene ND 1.60 72-54-8 4, 4'-DDD ND 160. 72-55-9 4, 4 ' -DDE ND 16.0 50-29-3 4, 4 '- DDT ND 160 53-70-3 Dibenzo(a,.h) anthracene ND 160 84-74-2 Di-n-butylphthalate ND 160 541-73=1 1, 3-Dichlorobenzene ND _ 160 (cont. ) 5 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : ' BLANK Sample Results Continued: CAS Compound Conc. RL Qualifier -NO. (ug/L) (ug/L) or Comment ----------------------------------------------------------------------- 95-50-1 1, 2-Dichlorobenzene ND 160 106-46-7 1, 4-Dichlorobenzene ND 160 91-94-1 3, 3 '-Dichlorobenzidine ND 160 120-83-2 2, 4-Dichlorophenol ND 310 60-57-1 Dieldrin ND 160 84-66-2 Diethylphthalate ND 160 105-67-9 2, 4-Dimethylphenol ND 310 131-11-3 Dimethylphthalate ND 160 534-52-1 4, 6-Dinitro-2-methyl phenol ND 310 51-28-5 2, 4-Dinitrophenol ND. 310 121-14-2 2, 4-Dinitrotoluene ND 160 606-20-2 2, 6-Dinitrotoluene ND 160 117=84-0 Di-n-octylphthalate ND 160 206-44=0 Fluoranthene ND 160 86-73-7 Fluorene ND 160 76-44-8 Heptachlor ND 160 1024-57-3 Heptachlor epoxide :ND 160 118-74-1 Hexachlorobenzene ND 160 87-68-3 Hexachiorobutadiene ND 160 77-47-4 Hexachlorocyclopentadiene ND 160 67-72-1 Hexachloroethane ND 160 193-39-5 Indeno(1,2,3-cd)pyrene ND 160 78-59-1 Isophorone ND: 160 91-20-3 Naphthalene ND 160 98-95-3 Nitrobenzene ND 160 88=3 5-5 2-Nitrophenol ND 310 100-02-7 4-Nitrophenol ND 310 86-30-3 N-Nitrosodiphenylamine ND 160 621-64-7 N-Nitrosodi-n-propylamine ND 160 87-86-5 Pentachlorophenol ND 310 85-01-8 Phenanthrene ND 160 108-95-2 Phenol ND- 310 l 129-00-0 Pyrene ND _ 160 (cont. ) US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : -BLANK Sample Results Continued: . CAS Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment ------------------------------------------------------------------------ 1-20-82-1 1,2, 4-Trichlorobenzene ND 160 86-06-2 2, 4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51-6 Benzyl Alcohol ND 160 106-47-8 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND . 160 95-48--7 2-Methylphenol ND. 160 106-44-5 4-Methylphen6l ND 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND 160 100-01-6 4-Nitroaniline ND 160. 95-95-4 2,4,5-Trichlorophenol ND 160 Other Compounds Quantitated tr Diphenylhydrazine ND 160 (azobenzene). Est. Tentatively Identified Conc. Compounds (.ug/L) None detected ND 7 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS. EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Sample Results Continued: -------=-----------------------------------------------=---------------- Sample Recoveries For Recoveries QC Range Surrogate Compounds: M M ------------------------------------------------------------------------ '2-Fluorophenol 102 21-110 Phenol,d5 99 10-110 Nitrobenzene,d5 88 35-114 Fluorobiphenyl 73 43-116 2, 4, 6-Tribromophenol 80 10-123 p-Terphenyl,d14 78 33-141 2-Chlorophenol-d4 .101 33-110 1, 2-Dichlorobenzene-d4 66 16-110. -------------------------=--------------------- �. Notes : RL Reporting limit ND None detected = Approximate < = Less than > = Greater than - NA = Not available, due to sample dilution or interference E = Estimated value exceeds the calibration range L = Estimated value is below the calibration range B = Analyte is associated with lab blank or -trip- blank contamination. Values are qualified when the observed concentration of the contaminant' in the sample extract is less than ten times the concentration in the blank extract for the common contaminants (phthalates and adipates) , or less than five times for the remaining contaminants. C = This. compound is confirmation for the pesticide analyses. See the pesticide report for the quantitation. A = Suspected aldolcondensation product J = Estimated value 1 R FACILITY SAMPLED: FLYNN TANN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65646 Matrix: Water DATE OF COLLECTION: 04/16/98 Sample pH: N/A DATE OF EXTRACTION: 04/22/98 Conc.' Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene , ND 1.60 '309-00-2 Aldrin ND 160 56-55-3 Benzo(a) anthracene ND 160 205-99-2 Benzo(b) fluoranthene ND 160 207-08-9 - Benzo (k) fluoranthene ND 160 50-32=8 Benzo (a)pyrene. - ND 160 191-24-2 Benzo(ghi)perylene ND 160 85=68-7 Butyl. Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 319-8 6-8 delta-BHC ND 160 1,11-44-4 Bis (2-chloroethyl) ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND 169, 117-81-7 Bis (2-ethylhexyl)phthalate 40 160 L 108-60-1 Bis (2-chloroisopropyl).ether ND 160- 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene ND 160 95-57-8 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyl ether ND 160 218-01-9 Chrysene ND 160 72-54-8 4, 4 '-DOD ND 160 72-55-9 4, 4 '-DDE ND 160 50-29-3 4,_4 '-DDT ND 160 53-70-3 Dibenzo (a,h) ahthracene ND 160 A-74-2 Di-n-butylphthalate ND _ 160 j41-73-1 1, 3-Dichlorobenzene ND 160 (cont. ) 9 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC- ANALYSIS-SAMPLE NO. : 65646 Sample Results Continued: CAS Compound Conc. RL Qualifier. NO. (ug/L) (ug/L) or Comment 95-50-1 1, 2-Dichlor6benzene ND 160 106-46-7 1, 4-Dichlorobenzene ND 160 91-94-1 3, 3'-Dichlorobenzidine ND 160 120-83-2 2, 4-Dichlorophenol ND 310 60-57-1 Dieldrin ND: 160 84-66-2 Diethylphthalate ND 160 105-67-9 2, 4-Di.methylphenol: ND 310 131-11-3 Dimethylphthalate ND 160 534-52-1 4, 6-Dinitro-2-methyl phenol ND 310 51-28-5 2, 4-Di.nitrophenol ND 310 121-14-2 2, 4-Dinitrotoluene ND i 160 606-20-2 2, 6-Dinitrotoluene ND 160 117-84-0 Di-n-octylphthalate ND 160 206-44-0 Fluoranthene ND 160 86-73-7 Fluorene ND 160 76-44-8 Heptachlor ND 160 1024-57-3 Heptachlor epoxide ND 16Qr 118-74-1 Hexachlotobenzene ND 160 87-68-3 Hexachlorobutadiene ND 160 77-47-4 Hexachlorocyclopentadiene ND 160 67-72-1 Hexachloroethane- ND 160 193-39-5 Indenc,(1,2, 3-cd)pyrene ND 160 78-59-1 Isophorone ND 160 91-20=3 Naphthalene ND 160 98=95=3 Nit.robenzene ND- 160 88-75-5 2-Nitrophenol ND 310 100--02-7 4-Nitrophenol ND 310 -86-30-3. N-Nitrosodiphenylamine ND 160 621-64-7 N-Nitrosodi-n-propylamine ND 160 87-86-5 - Pentachlorophenol ND Y 310 85-01-8 .Phenanthrene ND. 160 108-95-2 Phenol ND 310 j 129-00-0 Pyrene ND 160 (cont..) in US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65646 Sample Results Continued: } CAS Compound Conc. RL- Qualifier <. NO. (ug/L) .(ug/L) or Comment 12:0-82-1 1,2, 4-Trichlorobenzene ND 160 88-06-2 2, 4, 6-Trichlorophenol ND 310 Hazardous Substances -5-53=3 Aniline ND 160 -85-0 Benzoic Acid ND 310 s00-51-6 Benzyl Alcohol ND 160- 106-47-8 . 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND 160 95-48-7 2-Methylphenol ND 160 106-44-5 4-Methylphenol ND 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND 160 100-01-6 4-Nitroaniline ND 160W 95-95-4 2, 4, 5-Trichlorophenol ND 160 Other Compounds Quantitated Diphenylhydrazine ND 160 (azobenzene) Est. Tentatively -Identified Conc. Compounds (ug/L) C12 Hydrocarbon 200, 000 J Organic Acid 100, 000 J Organic Acid C18 Hydrocarbon 100, 000 J Organic Acid (poss. C18) 30, 000 J 11 US ENVIRONMENTAL PROTECTION AGENCY - REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65646 Sample Results Continued: Sample Recoveries For Recoveries QC Range Surrogate Compounds: M M ------------------------------------------------------------------------- 2-Fluorophenol 64 21-110 4 Phenol,d5 74 10-110 Nitrobenzene,d5 70 35-114 Fluorobiphenyl 72 43-116 2, 4, 6-Tribromophenol 11 10-123 p-Terphenyl,d14 100 33-141 2-Chlorophenol-d4 71 33-110 1,2-Dichlorobenzene-d4 72 16-110. -----------.--.---------------------------------------------------------- �- r a if FACILITY SAMPLED: FLYNN TANN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652, Matrix: Water DATE OF COLLECTION: 04/16/98 Sample pH: -N/A DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: . 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound Conc. RL Qualifier NO. (ug/L) ' (ug/L) or Comment Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthr.acene ND 160 309-00-2 Aldrin ND 160 56-55-3 Benzo (a) anthracene ND 160 205-99-2' Benzo (b) fluoranthene ND 160 207-68-9 Benzo (k) f luoranthene ND 160 50-32-8 Benzo (a)pyrene ND 160 191-24-2 Benzo (ghi)perylene - ND 160 85-68-7 Butyl Benzyl Phthalate ' ND 160 319-85-7 beta-BHC ND 160 319-86-8 delta-BHC ND 160 111-44-4 Bis (2-chloroethyl) ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND 160 117-81-7 Bis (2-ethylhexyl)phthalate ND 16t 108-60-1 Bis (2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole -ND. 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58=7 2-Chloronaphthalene ND 160 95-57-8 2-Chlorophenol ND .310 7005-72-3 4-Chlorophenylphenyl ether ND 160 218-01=9 Chrysene ND 160 72-54-8 4, 4 '-DDD ND 160 72-55-9 4, 4 '-DDE ND 160 50-29-3 4, 4'-DDT ND 160 53-70-3 Dibenzo(a,h) anthracene ND 160 94-74-2 Di-n-butyl.phthal:ate ND 160 j41-73-1 1, 3-Dichlorobenzene ND - 1.60 (cont. ) 13 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652 Sample Results Continued: CAS Compound Conc. RL Qualifier' NO. (ug/L) (ug/L) or Comment '_95-50-1 1, 2-Dichlorobenzene ND 160 '4106"-46-7 1, 4-Dichlorobenzene ND 160 91-94-1 3, 31-Dichlorobenzidine ND 160 120-83-2 2, 4-Dichlorophenol ND 310 60-57-1 Dieldrin ND 160 84-66-2 Diethylphthalate ND 160 105-67-9 2, 4-Dimethylphenol ND 310 131-11-3 Dimethylphthalate ND 160 534-52-1 4, 6-Dinitro-2-methyl phenol ND 310 51-28-5 2,4-Dinitrophenol ND 310 121-14-2 2, 4-Dinitrotoluene ND 160 606-20-2 2, 6-Dinitr6toluene. ND 160 117-84-0 Di-n-octylphthalate NO 160 206-44-0 Fluoranthene ND 160 86-73-7 Fluorene ND 160 76-44-8 Heptachlor ND 160 1024-57-3 Heptachlor epoxide ND 160 118-74-1 Hexachlorobenzene ND 160 87-68-3 Hexachlorobutadiene ND 10 77-47-4 Hexachlorocyclopentadiene ND 160 67-72-1 Hexachloroethane ND 160 193-39-5 Indeno(1,2, 3-cd)pyrene ND 160 78-59-1 Isophorone ND : 160 91-20-3 Naphthalene ND 160 98-95-3 Nitrobenzene ND 160 88-75-5 2-Nitrophenol ND 310 100-02-7 4-Nitrophenol ND 310 86-30-3 N-Nitrosodiphenylamine ND 160 621 : 64-7 N=Nitrosodi-n-propylamine ND 160 87-86-5 Pentachlorophenol ND 310 85-01-8 - Phenanthrene ND 160 108-.95-2 Phenol ND 310 129-00.-0 Pyrene ND 160 1 (cont. ) - l 14 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652 Sample Results Continued: CAS . Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment i20-82-1- 1, 2, 4-Trichlorobenzene ND 160 6L8-06-2 2, 4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51=6 Benzyl Alcohol ND 16.0 106-47-8 4-Chloroaniline ND 160 132-64-9 Dibenzofurari ND 160 91-57-6 2-Methylnaphthalene ND- 16.0 95-48-1 2-Methylphenol ND 160 106-44-5 4-Methylphenol ND. 160 88-74-4 2-Nitroaniline ND 1.60 99-09-2 3-Nitroaniline ND i60 100-01-6 4-Nitroaniline ND 160- 95-95-4 2, 4, 5-Trichlorophenol ND 160 Other Compounds Quantitated rr Diphenylhydraz.ine ND 160 (azobenzene) Est. Tentatively Identified Conc. Compounds (ug/L) Unknown 100 J C12 Hydrocarbon 200 J Methylene bis(dimethyl diethyl) methy-1 phenol 200 - J 15 US ENVIRONMENTAL PROTECTION AGENCY REGION I - LABORATORY GC/MS- EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652 Sample Results Continued: ------------------------------------------------------------------------ Sample Recoveries For . Recoveries QC Range Surrogate Compounds: M M ---------------------- - - 2-Fluorophenol 0* 21-110 Phenol,d5 2* 10-110 Nitrobenzene,d5 84 35-114 Fluorobiphenyl 78 43-116 2,4, 6-Tribromophenol 0* 10-123 p-Terphenyl,d14 80 33-14I 2-Chlorophenol-d4 1* 33-110 1, 2-Dichl.orobenzene-d4 78 16-110 ------------------------------------------------------------------------ l * Out of range rr 16 - FACILITY SAMPLED: FLYNN TANN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS- EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. :. 67260 Matrix: Water DATE OF COLLECTION: 04/16/98 Sample pH: N/A DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound Conc.. RL Qualifier NO. (ug/L) (ug/L) or -comment ------------------------------------------------------------------------ Priority Pollutants 63-32-9 Acenaphthene _ ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND 160 309-00-2 Aldrin ND 160 56-55-3 Benzo (a) anthracene ND 160 205-99-2 Benzo (b) fluoranthene ND 160 207-08-9 Benzo (k) fluoranthene. ND 160 50-32-8' Benzo (a)pyrene, ND 160 191-24-2 Benzo (ghi)perylene ND 160 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 .319-8.6-8 delta-BHC ND 160 111-44-4 Bis (2-chloroethyl) ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND. 16% 117-81-7 Bis (2-ethylhexyl)phthalate ND 160 108-60-1 Bis (2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyi ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol : ND 310 91-58-7 2-Chloronaphthalene ND 160 95-57-8 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyi ether ND 160 218-01-9 Chrysene ND 1.60 72-54-8 4, 4 '-DDD ND 160 72-5.5-9 4, 4'-DDE ND 160- 50-29-3 4, 4 '-DDT ND 160 - 53-10-3 Dibenzo (a;h)anthracene ND 160- 84.-74-2 Di-n-butylphthalate ND _ 160 541-73-1 • 1, 3-Dichlorobenzene ND 160 (cont.) l US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67260 Sample Results Continued: CAS Compound Conc. RL Qualifier NO.. (ug/L) (ug/L) or Comment ------------------------------- ---------------------- -------------- 95-50-i 1,2-Dichlorobenzene ND 160 106-4'6-7 1,4-Dichlorobenzene ND 160 91-94-1 3,3'-Dichlorobenzidine ND 160 120-83-2 2, 4-Dichlorophenol ND 310 60-57-1 Dieldrin ND 160 84-66-2 . Diethylphthalate ND 160 105-67-9 2,4-Dimethylphenol ND 310 ' 131-11-3 Dimethylphthalate ND 160 1 534-52-1 4,6-Dinitro-2-methyl phenol ND 310 / 51-28-5 2,4-Dinitrophenol ND 310 121-14-2 -2,4-Dinitrotoluene ND 160 606-20-2 2, 6-Dinitrotoluene ND 160 117-§4-0 Di-n-octylphtha-late ND 160 206-44-0 Fluoranthene ND 160 86-73-7 Fluorene ND 160 76-44-8 Heptachlor ND 160 1024-57-3 Heptachlor epoxide ND" 160 118-74-1 Hexachlorobenzene ND 160 . 87-68-3 Hexachlorobutadiene ND 16Q, 77-47-4 Hexachlorocyclopentadiene ND 160 67-72-1 Hexachloroethane ND 160 193-39-5 Indeno (1,2, 3-cd)pyrene ND 160 78-59-1 Isophorone ND 160 91-20-3 Naphthalene ND 160 98-95-3 Nitrobenzene ND 160 88-75-5 2-Nitrophenol ND 310 100-02-7 4-Nitrophenol ND' 310 86-30-3 N-Nitrosodiphenylamine ND 160 621-64-7 N-Nitrosodi-n-propylamine ND 160 - 87-86-5 Pentachlorophenol ND 310 85-01-8 Phenanthrene ND 160 108-95-2 Phenol ND 310 1 129-00-0 Pyrene ND 160 (cont. ) r US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE No. : 672 60 Sample Results Continued: CAS Compound Conc.. RL.: Qualifier NO. (ug/L) (ug/L) or Comment -j---------------------------------------------------------------------- 120-82-1 1,2, 4-Trichlorobenzene ND 160 86-06-2 2,4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 -Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51-6 Benzyl Alcohol ND 160 106-47-8- 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND 160 - 95-48-7 2-Methylphenol ND 160 106-44-5 4-Methylphenol ND j 160 88-74-4 2-Nitroani.line ND 160 99-09-2 3-Nitroaniline ND 1.60 100-01-6 4-Nitroaniline ND 160 95-95-4 2, 4, 5-Trichlorophenol ND - 160 Other Compounds Quantitated w Diphenylhydrazine ND 160 (azobenzene) Est. Tentatively Identified Conc: Compounds (ug/L) None detected ND 19 US ENVIRONMENTAL PROTECTION AGENCY / REGION I LABORATORY - GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67260 Sample Results Continued: ---------------------- ---------------------------------- ---------------- Sample Recoveries For- Recoveries QC Range Surrogate- Compounds (%) _ M. 2-Fluorophenol 15* 21-110 Phenol.,d5 59 10-110 Nitrobenzene,05 81 35-114 Fluorobiphenyl 68 43-116 2,4, 6-Tribromophenol 17 10-123 p-Terphenyl,dl4 76 33-141 2-Chlorophenol-d4 40 33-110 1,2-Dichlorobenzene-d4 61 16-110 ---------------=-------------------------- ) * = out of QC range A UNITED STATES ENVIRONMENTAL PROTECTION AGENCY s REGION t ENVIRONMENTAL SERVICES DIVISION. 60 WESTVIEW STREET . �� sE LEXINGTON,MASSACHUSETTS=73-31s5 DATE: May 21, 1998 SUBJ: Gas Chromatography-Mass Spectrometry Analysis of Extractable Organics in Soils and Sediments - FLYNN TAN 'FROM: Dick Siscanaw, Chemistry Section - ; - - THRU: Dr. William J. Andrade, Adv ced. Analytical Chemistry Specialist TO: Tom Hatzopoulos. PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All. samples were received and logged in by the laboratory according to the SOP for Sample Log-in (EIA-ADMLOGNI.SOP, 7/97)- . EPA Region I Procedure: High Level BNA Analyses for. Drum and or Pure Product Samples, BNADRML2-.SOP. The modules used for this procedure were: GC/FID Screening of BNA Extracts, BNASCRE4.BNA, Gas Chromato ra by Mass Spectrometry Analysis of Semivolatile Organics, BNAENVII.MOD, Quality Control Module, QC3.MOD. All Values are reported out on a dry- weight basis. w The analytical support for this report was performed by ESAT contractors. Date (s) Samples Received by the Laboratory: 04/17/98 Date Analysis Started: 04/22/98 cc: File: J: \CHEMSTRY\REPORTS\BNA\98267DB.WPD R.�vdad/R�tvda6b.PriMad u-M Vaiw vi"M R%e A IM"—1MY a--]-I P—unw-o.,dmn wmA US ENVIRONMENTAL PROTECTION AGENCY 60 Aestview- Street Lexington, MA 02173 QUALITY CONTROL: 1. A laboratory blank was analyzed before the sample analysis. 2. Each sample' was spiked. with 100 ug of base/neutral and 200 ug of acid surrogate compounds. The results for the surrogate recoveries are reported_ out, for each sjanple. - 3. One sample, 65645, was spiked with 100 ug of ba-se/neutral and 200 ug of acid matrix spike compounds. The results for the analyses are reported on the following page. - l w U.S. EPA REGION I LABORATORY Semivolatile Organic Analyses WATER MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Sample No. : Date (s) Analyzed: Spike Sample MS QC Added Conc. Coac. MS % Limits Compound (ug/L) (ug/L) (ug/L) Rec Aec Phenol 1562 0 1400 -90 12-110 2-Chlorophenol 1562 0 1500 96 27-123 s1, 4-Dichlorobenzene 781 0 760 97 .36-97 N-Nitroso-di-n-prop. (1) 781 0 710 91 41-116 °1, 2, 4-Trichlorobenzene 781 0 670 86 39-98 4-Chloro-3-methylphenol 1562 0 1200 77 23-97 Acenaphthene 781 0 660 85 46-1.18 4-Nitrophenol 1562. 0 1200 77 10-80 2, 4-Dirlitrotoluene 781 0 496 63 24-96 Pentachlorophenol 1562 0 1300 83 9-103 Pyrene 781 0 690 88 26-127 Spike MSD Added Conc. MSD % % QC LIMITS Compound (ug/L) (ug/L) Rec RPD RPD Rec Phenol 1562 1600 102 13 42 12-110 2-Chlorophenol 1562 1600 102 6 40 -27-123 1, 4-Dichlorobenzene 781 780 100 3 28 36-97 N-Nitroso-di-n-prop. (I) 781 770 99 8 38' 41-116 1, 2, 4-Trichlorobenzene 781 730 93 8 28w 39-98 4-Chloro-3-methylphenol 1562 1300 83 8 42 23-97 'Acenaphthene 781 710 91 7 31 46-118 4-Nitrophenol 1562 1300 83 8 50 - 10-80 2, 4-Dini tro toluene 781 490 63 0 38 24-96 Pentachlorophenol 1562 13.00 83 0 50 9-103 Pyrene 781 730 93 5 31 26-127 (1) N-Nitroso-di-n-propylamine * Values outside of QC limits RPD: 0 out of 11- outside limits Spike Recovery: - 0 out of 22 outside limits US ENVIRONMENTAL PROTECTION AGENCY 60 Aestvi.ew Street Lexington, MA 02173 NOTE: Phthalates (1,2-Benzenedicarboxylic esters) and adipates (hexanedioic esters) are common method contaminants. Values at the detection levels are most likely due to method contamination. i. w Samples Analyzed: BLANK; 65644, 65645, 65645 MS,_ 65645 MSD, 65647, 65649, 65650, 65651, 67261 Q - ' e US ENVIRONMENTAL PROTECTION AGENCY 60 Aestview Street. Lexington, MA 02173 ANALYT I CAL PARAMETERS - INSTRUMENTS: Hewlett Packard. 5890 Gas Chromatograph ; y Hewlett Packard 5987 Gas Chromatograph-Mass Spectrometer: ' GC/FID Screening Conditions: Gas : Hydrogen Capillary Column: DB-1, 30m, 25mm ID, 0'.25 micron film thickness Injection Mode.: Splitless Temperature Program! Isothermal for 3 min at 40°C, programmed at 15°C/min to 320°C. for 3 min GC-MS. Conditions: ' Gas: Helium Capillary Column: DB-5, 60m, 25mm PD, 0.25 micron film thickness Injection Mode: Splitless Temperature Program: Isothermal for 4 min at 40°C, programmed at 7°C/min- to 300°C Inj ector;._. Transfer Temperatures: 290°C, 300°C .Electron Energy: 70 V- Mass Range: 35-550 _ Scan Rate: 0.9 seconds 5 US ENVIRONMENTAL PROTECTION AGENCY / 60 Westview Street Lexington, MA 02173 Chemist who reviewed data: Dick Siscanaw Holding times meet (YIN) : Yes } Extraction (Water - 7 days,. Soils - 14 days) Analytical (40 days after extraction) Method modifications: None Limitations of data: None Laboratory blank problems: None Instrument. performance problems: None w Surrogate and spike recovery problems: There appears to be a matrix effect on the acidic surrogates. in ' sample 65647. Sample 65651 has a low recovery for Nitrobenze,d5. Additional comments: None 6 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY. REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Matrix: Drum DATE OF COLLECTION: Not Applicable Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF- ANALYSIS: 04/24/98 Dilution Factor None WET WEIGHT. EXTRACTED.: 0.200 g Report Factor 1 RESULTS: CAS Compound . Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment Priority Pollutants 83-32-9 Acenaphthene ND 300 208=96-8 Acenaphthylene ND 300 120-12-7 Anthracene ND 300 309-00-2 Aldrin ND 300 56-55-3 Benzo (a)-anthracene ND 300 205-99-2 Benz.o (b) fluoranthene ND 300 207-08-9 Benzo (k) fluoranthene ND 300 50-32-8 Benzo (a)pyrene ND 300 191-24-2 Benzo (ghi)perylene ND 300 85-68-7 Butyl Benzyl Phthalate ND 300 319-85-7 beta-BHC ND 300 319-86-8 delta-BHC ND 300 111-44-4 Bis (2-chl.oroethyl) ether ND 30g. 111-91-1 Bis (2-chloroethoxy)methane ND 300 117-81-7 Bis (2-ethylhexyl)phthalate ND 300 108-60-1 Bis (2-chloroisopropyl) ether ND 300. 101-55-3 . 4-Broinophenylphenyl ether ND 300 86-74-8 Carba.zole ND 300 59-50-7 4-Chloro-3-methylphenol - ND 600 91-58-7 2-Chloronaphthalene ND 300 95-57-8 2-Chlorophenol ND 600 7005-72-3 4-Chlorophenylphenyl ether ND 300 218-01-9 Chrysene ND 300 72-54-8 4, 4'-DDD ND .300 72-55=9 4,-4 '-DDE ND 300 50-29-3 4, 4 '-DDT ND 300 53-70-3 Dibenzo(a,h) anthracene ND 300 (con't) 7 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE .NO. : BLANK Results Continued: CAS Compound Conc. RL Qualifier NO. (Mg/Kg) (mg/Kg) or Comment 84-74-2 Di-n-butylphthalate ND 300 117-84-0 Di-n-octylphthalate ND 300 541-73=1 1, 3-Dichlorobenzene ND 300 95-50-1 1,2-Dichlorobenzene ND 300 106-46-7 1, 4-Dichlorobenzene ND 300 91-94-1 3, 31-Dichlorobenzidine ND 300 120-8.3-2 2, 4-Dichlorophenol ND 600 60-57-1 Dieldrin ND 300 84-66-2 Diethylphthalate ND . 300 -105-67-9 2-4-Dimethylphenol ND 600 131-11-3 Dimethylphthalate ND 300 51-28-5 2, 4-Dinitrophenol ND 600 121-14-2 2,4-Dinitrotoluene ND 300 606-20-2 2, 6-Dinittotoluene ND 300 86-73-7 Fluorene ND 300 76-44-8 'Heptachlor ND . 300 1024-57-3 Heptachlor epoxide ND 300 118-74-1 Hexachlorobenzene ND 300• 87-68-3 Hexachlorobutadiene "- ND 309- 77-47-4 . Hexachlorocyclopentadiene ND 300 67-72-1 Hexachloroethane . ND 300 193-39-5 Indeno (1,2, 3-cd)pyrene ND 300 78=59-1 Isophorone . ND 300 534-52-1 2-methyl-4, 6-dinitrophenol ND 600 91-20-3 Naphthalene ND 300 98-95-3 Nitrobenzene ND 300 88-75-5 2-Nitrophenol ND 600 100-02-7 4-Nitrophenol ND 600 86-30-3 N-nitrosodiphenylamine ND 300 621-64-7- N-Nitrosodi-n-propylamine ND 300 87-86=5 Pentachlorophenol ND 600 85-01-8 Phenanthrene ND 3.00 108-95-2 Phenol ND 600 129-00-0 Pyrene ND 300 (con't) o US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE .ORGANIC ANALYSIS SAMPLE NO. : BLANK Results Continued: : a CAS Compound Conc. RL Qualifier . -NO (mg/Kg) (mg/Kg) or Comment ------- ------------------=- 120-82-1 1,2, 4-Trichlorobenzene ND 300 88-06-2 2,4, 6-Trichlorophenol ND 600 Hazardous Substances 65-53-3 Aniline ND _ 300 65-85-0 Benzoic Acid ND 600 100-51-6 Benzyl Alcohol ND 300 106-47-8 4-Chloroaniline ' ND 300 132-64-9 , Dibenzofuran ND 300 91-57-6 2'-Methylnaphthalene ND 300 95-48-7 2-Methylphenol ND 300 106-44-5 4-Methylphenol ND 300 8.8-74-4 .2-Nitroaniline ND 300 99-09-2 3-Nitroaniline ND 300 100-01-6 4-Nitroaniline ND 300 95-95-4 2,4,5-Trichlorophenol ND 30W Other Compounds Quantitated None detected ND 300 Est. Tentatively Identified Conc. Compounds (mg/Kg) None detected ND 9 4 1/ US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Results Continued: Sample Recoveries For Recoveries QC Range Surrogate Compounds-: M M -------------------------------------------------_------------------------ 2=Fluorophenol 87 25-121 Phenol,d5 84 24-113 Nitrobenzene,d5 85 23-120 Fluorobiphenyl 88 30-115 2, 4, 6-Tribromophenol 75 19-122 p-Terphenyl,d14 91 18-137. 2-Chlorophenol-d4 90 20-130 1 2-Dichlorobenze-d4 91 20-130 ------------------------------------------------------------------------- Notes: RL = Reporting Limit .(6E+00 = 6, 1E+01. = 10, 4E-01 = 0.4) ND = None detected ' - = Approximates < = Less- than > = Greater than NA '= Not available, due to sample dilution or interference E = Estimated value exceeds the calibration .range L = Estimated value is below the calibration range B. = Analyte is associated 'with lab blank or trip blank' contamination. Values are qualified when the observed concentration of the contaminant in the sample extract is less than_ ten times the concentration in the blank extract. for the common contaminants (phthalates and adipates) , or less than five times for the remaining contaminants. C = This compound is confirmation for the pesticide J = Estimated value FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Matrix: Drum DATE OF'COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS:. 04/24/98 Dilution Factor None WET WEIGRT EXTRACTED: 0.256 g Report Factor 0.78 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acehaphthene ND 230 208-96-8 Acenaphthylene ND 230 '.20-12-7 Anthracene ND 230 309-00-2 Aldrin ND 230 56-55-3 Benzo (a) anthracene ND 230 205-99-2 Benzo (b) fluoranthene ND 230 207-08-9 Benzo (k)-fluoranthene ND 23.0 50-32-8 Benzo (a)pyrene ND 230 191-24-2 Benzo (ghi)perylene ND 230 85-68-7 Butyl Benzyl Phthalate ND 230 319-85-7 beta-BHC ND 230 319-86-8 delta-BHC ND 230 111-44-4 Bis (2-chloroethyl) ether ND 23W 111-91-1 Bis (2-chloroethoxy)methane ND 230 117-81-7 Bis (2-ethylhexyl)phthalate ND 230 108-60-1. Bis (2-chloroisopropyl) ether ND 230 101-55-3 4-Bromophenylphenyl ether ND 230 86-74-8 Carbazole ' ND 230 59-50-7 4-Chloro-3-methylphenol ND 470 91-58-7 2=Chloronaphthalene ND 230 .95-57-8- 2-Chlorophenol ND 470 7005-72-3 4-Chlorophenylphenyl ether ND 230 218-01-9 Chrysene ND 230 72-54-8 4, 4 '-DDD ND 230 72-55-9 4, 4 '-DDE ND 230 50-29-3 4, 4'-DDT ND 230 3-70-3 Dibenzo (a,h) anthracene ND 230 . (con't) 11 US ENVIRONMENTAL PROTECTION AGENCY / REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Results Continued: CAS.' Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment - ------------------------------------------------------------------------ 84-74-2 Di-n-butylphthalate ND 230 117-84-0 Di-n-octylphthalate ND 230 541-73-1 1, 3-Dichlorobenzene- . ND 230 95-50-1 1, 2-Dichlorobenzene ND 230 106-46-7 1, 4-Dichlorobenzene ND 230 91-94-1 3, 3 '-Dichlorobenzidine ND 230 120-83-2 2, 4-Dichlorophenol ND 470 60-57-1 Dieldrin ND 230 84-66-2 Diethylphthalate ND 230 105--67-9 2-4=Dimethylphenol ND 4.70 131-11-3 Dimethylphthalate ND 230 51-28-5 2, 4-Dinitrophenol ND 470 121-14-2 2, 4-Dinitrotbluene ND 230 606-20-2 2, 6-Dinitrotoluene ND 230 86-73-7 Fluorene ND 230 76-44-8 Heptachlor ND 230 1024-57-3 Heptachlor epoxide ND 230 118-74-1 Hexachlorobenzene ND 230 87-68-3 Hexachlorobutadiene ND 239E 17-4.7-4 Hexachlorocyclopentadiene ND 230 67-72-1 Hexachloroethane. ND 230 1.93-39-5 Indeno (1,2,.3-cd)pyrene ND 230 78-59-1 Isophorone ND 230 534-52-1 2-methyl-4, 6-dinitrophenol ND 470 91-20-3 Naphthalene ND 230 98-95-3 Nitrobenzene -.ND 230 88-75-5 2-Nitrophenol -ND 470 100-02-7 4-Nitrophenol ND 470 86-30-3 N-nitrosodiphenylamine ND 230 621-64-7 N-Nitrosodi-n-propylamine ND 230 87-86-5 Pentachlorophenol ND 470 85-01-8 Rhenanthrene ND 230 1 108-95-2 Phenol ND 470, J 129-00-0 Pyrene ND 230 (con't) US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mq/Kg) or Comment 120-82-1 1,2,4-Trichlorobenzene ND 230 88-06-2 2, 4, 6-Trichlorophenol ND 470 Hazardous Substances ---------------------------- 65-53-3 Aniline ND 230 65-85-0 Benzoic Acid . ND 470 100-51-6 Benzyl Alcohol ND 230 ',06-47-8 4-Chloroaniline ND 230 .32-64-9 Dibenzofuran ND 230 91-57-6 2-Methy1naphthalene ND 230 95-48-7 2-Methylphenol i ND 230 106-44-5 4-Methylphenol ND 230 88-74-4 2-Nitroaniline ND 230 99-09-2 3-Nitroaniline ND 230 100-01-6 4-Nitroaniline ND 230 95-95-4 2, 4,5-Trichlorophenol ND 230 ---------------------------- Other Compounds Quantitated w None detected ND 230 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- None detected ND 13 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Results- Continued: ---------------------------------------- ------------------------------- S-ample Recoveries For Recoveries QC Range Surrogate Compounds: M M ------------ ----------------- ------------------------------------ 2-Fluorophenol 96 25-121 Phenol,-d5 94 24-113 Ritrobenzene,d5 83 23-120 Fluorobiphenyl 88 30-115 2.,4, 6-Tribromophenol- 83 19-122 p-Terphenyl,dl4 . 88 18-137 2-Chlorophenol-d4 99 20-130 1,2-Dichlorobenze-d4 102 20-130 - ---------- -------------------------------------------------------------- FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65647 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.87 g Report Factor 0.87 _RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------- Priority Pollutants 83-32-9 Acenaphthene ND 260 208-96-8 Acenaphthylene ND 260 120-12-7 Anthracene ND 260 309-00-2 Aldrin . . ND 260 56-55-3 Benzo (a)anthracene ND .260. 205-99-2 Benzo (b) f luoranthene ND 260 207-08-9 Benzo (k) fluoranthene ND 260 50-32-8 - Benzo (a)pyrene ND: 260 191-24-2 Benzo (ghi)perylene . ND 260- 85-68-7 Butyl Benzyl Phthalate ND 260 319785-7 beta-BHC ND 260 319-86-8 delta-BHC ND 260r 111-44-4 Bis (2.-chloroethyl)ether ND 260 111-91=1 Bis (2-chloroe-thoxy)methane ND 260 117-81-7 Bis (2-ethylhexyl)phthalate ND 260 108-60-1 Bis (2-chloroisopropyl) ether ND 260 101-55-3 4-Bromophenylphenyl ether ND 260 86-74-8 Carbazole ND 260 59-50-7 4-Chloro-3-methylphenol ND 520 91-58-7 2-Chloronaphthalene ND 260- 95-57-8 2-Chlorophenol ND 520 7005-72-3 4-Chlorophenylphenyl ether ND 260 21.8-01-9 Chrysene ND 260 72-54-8 4, 4 '-DDD ND 260 72-55-9 - 4, 4 '-DDE ND 266 i0-29-3 4, 41-DDT ND _ 260 53-70-3 Dibenzo(a.h) anthracene ND 260 (con't) 15 US ENVIRONMENTAL PROTECTION AGENCY � .. REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS ` SAMPLE NO. : 65647 Results Continued: CAS. Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kcj.) or Comment ------------------------------------------------------------------------ 8.4-74-2 Di-n-butylphthaiate ND 260 117-84-0 Di-n-octylphthalate ND 260 541-73-1 1, 3-Dichlorobenzene, ND 260 95-50-1 1,2-Dichlorobenzene ND 260 10F6-46-7 1, 4-Dichlorobenzene ND 260 91-94-1 3, 31-Dichlorobenzidine ND 260 120-83-2 2,4-Dichlorophenol ND 520 60.-57-1 Dieldrin ND 260 84-66-2 Diethylphthalate ND 260 105-67-9 2-4-Dimethylphenol ND 52.0 .131-11-3 Dimethylphthalate ND 260 51-28-5 2, 4-Dinitrophenol ND 520 121-14-2 2,4-Di'nitrotoluene ND 260 606-20-2 2, 6-Dinitrotoluene ND 260 86-73-7 Fluorene ND 260 76-44-8 heptachlor ND 260 1024-57-3 Heptachlor epoxide ND 260 118-74-1 Hexachlorobenzene ND 260 87-68-3 Hexachlorobutadiene ND 2 77-47-4 Hexachlorocyclopentadiene ND 25 67-72-1 Hexachloroethane ND 260 193-39-5 Indeno(1,2, 3-cd)pyrene-. . ND 260 78-59-1 Isophorone ND 260 534-52-1 2=methyl-4, 6-dinitrophenol ND' 520 91-20-3 Naphthalene ND 260 98-95-3 Nitrobenzene ND '260 88-75-5 2-Nitrophenol ND 520 160=-02-1 4-Nitrophenol ND 520 86-30-3 N.-nitrosodiphenylamine ND 260 621-64-7 N-Nitrosodi-n-propylamine. ND 260 87-86-5 Pentachl.orophenol ND 520 -85-01-8 Phenanthrene ND 260 108=95-2 Phenol ND _ 520 129-00-0 Pyrene ND 260 (con't) ; US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS - SAMPLE NO. : 65647 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ---------------------------------------------------------------- ----- 120-82-1 1, 2, 4-Trichlorobenzene ND .260 88-06-2 2, 4, 6-Trichlorophenol ND 520 ---------------------------- Hazardous Substances 65-53-3 Aniline ND 260 65-85-0 Benzoic Acid ND 520 100751-6 Benzyl Alcohol ND 260 106-47-8 4-Chloroaniline ND 260 132-64-9 Dibenzofuran ND 260 91=57-6 2-Methylnaphthalene ND 260 95-48-7 2-Methylphenol ND 260 106-44-5 4-Methylphenol ND 260 88-74-4 2-Nitroaniline ND 260 99=09-2 3-Nitroaniline ND 260 100-01-6 4-Nitroaniline. ND 260 95-95-4 2, 4,5-Trichlorophenol ND 2 60- ---------------------- Other Compounds Quantitated rr ---------------------------- None detected ND 260 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ----------------------- Cyclotetra siloxane, octa methyl 2800 J Cyclopenta siloxane, deca methyl 2000 J Cyclohexa siloxane, dodeca methyl 5000 _ J Siloxane product 3600 J Siloxane product 810 J 17 US ENVIRONMENTAL PROTECTION AGENCY / REGION I LABORATORY _. GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE .NO. : 65647 Results Continued: Sample Recoveries For Recoveries 'QC Range Surrogate Compounds:- (%) M ------------------------------------------------------------------------ 2-Fluorophenol . 0* 25-121 4 Phenol,d5 21 24-113 Nitrobenzene,d5 60 23-120 Fluorobiphenyl 94 30-115 2, 4, 6-Tribromophenol 0* 19-122 . p-Terphenyl,dl4 96 18=137 2-Chlorophenol-d4 4* 20-130 1,2-Dichlorobenze-d4 103 20-130 l -----------------------------------------------------------------------• J * Out of range w 18 FACILITY SAMPLED: FLYNN 'TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.172 g Report Factor 1 .16 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments Priority Pollutants 83-32-9 Acenaphthene ND 350 ?08-96-8 Acenaphthylene ND 350 - -120-12-7 Anthracene ND 350 309-00-2 Aldrin ND 350 56-55-3 Benzo (a) anthracene ND 350 20$-99-2 Benzo (b) fluoranthene ND 350 207-08-9 Benzo (k) fluoranthene ND 350 50-32-8 Benzo (a)pyrene ND 350 191-24-2 Benzo (ghi)perylene ND 350 85-68-7 Butyl Benzyl Phthalate ND 350 319-85-7 beta-BHC ND 350 319-86-8 delta-BHC ND 35% 111-44-4 Bis (2-chloroethyl) ether ND 350 111-91-1 Bis (2-chloroethoxy)methane ND 350 117-81-7 Bis (2-ethylhexyl)phthalate ND 350 108-60-1 Bs (2-chloroisopropyl) ether ND 350 101-55-3 4-Bromophenylphenyl ether ND 350 86-74-8 Carbazole ND 350 59-50-7. -4-Chloro-3-methylphenol ND 700 91-58--7 2-Chloronaphthalene ND 350 95-57-8 2-Chlorophenol ND 700 7005-72-3 4-Chlorophenylphenyl ether ND 350 218-01-9 Chrysene. ND 350 72-54-8- 4, 4 '-DDD. ND 350 72-55--9 4,4--DDE ND 350 0-29-3 4,V-DDT ND. 350 -:)3-70-3 Dibenzo (a,h) anthracene ND 350 (con*t) 19 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY. .GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Results Continued: C.A.S. Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment 84-74-2 Di-n-butylphthalate ND 350 117-84--0 Di-n-octylphthalate ND 350 541-73-1 1, 3-Dichlorobenzene ND 350 95-50-1 1,2-Dichlorobenzene ND 350 106-46-7 1, 4-Dichlorobenzene ND 350 91-94-1 3,31-Dichlorobenzidine ND 350 120-83-2 2, 4-Dichlorophenol ND 700' 60-57-1 Dieldrin ND 350 84--66-2 Diethylphthalate ND 350 105-67-9- 2-4-Dimethylphenol ND 700 131-11-3 Dimethylphthalate ND 350 51-28-5 2, 4-Dinitrophenol '- ND 700 121-14-2 2,4-Dinitrotoluene ND 350 606-20-2 2, 6-Dinitrotoluene 'ND 350 86-73-7 Fluorene ND. 350 76-44-8 Heptachlor ND 350 1024-57-3 Heptachlor epoxide ND 350 118-74-1 Hexachlorobenzene ND 350 87-68-3 Hexachlorobutadiene ND 35(W 77-47-4 Hexachlorocyclopentadiene ND .- .350 67-72-1 Hexachloroethane ND 350 193-39-5 Indeno'(1, 2, 3-cd)pyrene ND 350 78-59-1 Isophorone ND 350 534-52=1 2-methyl-4, 6=dinitrophenol - ND 700 91-20-3 Naphthalene 200 350 L 98-95-3 Nitrobenzene ND 350 88-75-5 2-Nitrophenol ND 700 100-02-7 4-Nitrophenol ND 700 86-30-3 N-nitrosodiphenylamine ND - 350 621-64-7 N-Nitrosodi-n-propylamine ND 350 87-86-5 Pentachlorophenol ND 700 .85-01-8 Phenanthrene ND 350 108-95-2 Phenol ND _ 700 129-00-0 Pyrene ND- 350 (con't) US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment --- --------- - ----------------------------------------------------------- 120-82-1 1, 2, 4-Trichlorobenzene ND 350 88-06-2 2, 4, 6-.Trichlorophenol. ND 700 ---------------------------- Hazardous Substances ---------------------------- 65-53-3 Aniline ND 350 5-85-0 Benzoic Acid ND 700 100-51-6 Benzyl Alcohol ND 350 106-41-8 4-Chloroaniline ND 350 132-64-9 Dibenzofuran ND 350 91-57-6 2-Methylnaphthalene ND 350 95-48-7 2-Methylphenol ND 350 106-44-5 4-Methylphenol ND .350 88-74-4- ' 2-Nitroaniline ND 350 99-09-2 3-Nitroaniline ND 350 100-01-6 4'-Nitroaniline ND 350 9.5-95-4 2, 4,5-Trichlorophenol ND 350w ---------------------------- Other Compounds Quantitated. ---------------------------- None detected ND 350 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Hydrocarbon 2000 J C12 Hydrocarbon 5000 J Hydrocarbon 2000. J C12 Hydrocarbon 2000 C12 Hydrocarbon 3000 J note: light petroleum product 21 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Results Continued: -=---------------------------------------------------------------------- Sample Recoveries For. Recoveries QC Range Surrogate Compounds:. M ( ) ------------------------------------------------------------------------ 2-Fluorophenol 60 25-121 Phenol;d5 78 24-113 Nitrobenzene,d5 89 23-120 Fluorobiphenyl 89 30-115 2,4, 6-Tribromophenol 15* 19-122 p-Terphenyl,dl4 89 .18-137 2-Chlorophenol-d4 72 20-130 1, 2-Dichlorobenze-d4 100 20-130 ------------------------------------------------------------------------ * Out of range i 22 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY . GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65651 Matrix: Drum DATE OF COLLECTION: - 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL .DATE OF. ANALYSIS: 04/30/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.151 g Report Factor 1 .3 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) . (mg/Kg) or Comments ----------------------------------------------=------------------------- Priority Pollutants 83-32-9 Acenaphthene ND 390 208-96-8 Acenaphthylene ND 390 120-12-7 Anthracene ND 390 309-00-2 Aldrin ND 390 56-55-3 Benzo(a)anthracene ND 390 205-99-2 Benzo (b) fluoranthene ND 390 207-08-9 Benzo(k) £luoranthene ND 390 50-32-8 Benzo (a)pyrene ND 390 191-24.-2 Benzo(ghi)perylene . ND 390 85-68-7 Butyl Benzyl Phthalate ND 390 319-85-7 beta-BHC ND 390 319-86-8 delta-BHC ND 39% 111-44-4 Bis (2-chloroethyl) ether. ND 390 111-91-1 Bis (2-chloroethoxy)methane ND 390 117-81-7 Bis (2-ethylhexyl)phthalate ND 390 108-60-1 Bis (2-chloroisopropyl) ether ND 390 101-55-3 4-Bromophenylphenyl ether ND 390 86-74-8 Carbazole ND 390 59-50-7 4-Chloro-3-methylphenol ND 780 91-58-7 2-Chloronaphthalene ND. 390 95-57-8 2-Chlorophenol ND 780 7005-72-3 4-Chlorophenylphenyl ether ND 390 218-01-9 ' Chrysene . ND 390 72-54-8 4, 4 '-DDD ND -390 72-55-9 4, 4 '-DDE ND 390 i0-29-3 4, 4 '-DDT ND 350 :53-70-3 Dibenzo(a,h)anthracene ND 390 (con't) 23 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65651 Results Continued: CAS. Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or, Comment 84-74-2 Di-n-butylphthalate ND 390 T17-84-0 Di-n-octylphthalate ND 390 541-73=1 1, 3-Dichlorobenzene ND 390 95-50-1 1,2-Dichlorobenzene ND 390 106-46-7 1, 4-Dichlorobenzene ND 390 91-94-1 3, 31-Dichlorobenzidine ND 39.0 120-83-2 2, 4-Dichlorophenol ND 780 60-57-1 Dieldrin ND ' 390 84-66-2 Diethylphthalate ND 390 105-67-9 2-4-Dimethylphenol ND 780 131-11-3 Dimethylphthalate ND 390 51-28-5 2, 4-Dinitrophenol ND 780 121-14-2 2, 4-Dinitrotoluene ND 390 606-20--2 2, 6-Dinitrotoluene ND 390 86-73-7 Fluorene ND 390 76-44-8 Heptachlor ND 390 1024-57-3 Heptachlor epoxide ND 39-0 118-74-1 Hexachlorobenzene ND 390 87-68-3 Hexachlorobutadiene ND 39% 77-47-4 'Hexachlorocyclopentadene ND 390 67-72-1 Hexachloroethane ND 390 193-39-5 Indeno(1,2, 3-cd).pyrene ND 390 78-59-1 Isophorone ND 390 534-52-1 2-methyl-4, 6-dinitropheriol ND 780 91-20-3 Naphthalene 950 390 98-95-3 Nitrobenzene ND 390 88=75-5 2-Nitrophenol " ND 780 100-02-7 4-Nitrophenol ND 780 86-30-3 N-nitrosodiphenylamine. ND . 390 621-64-7 N-Nitrosodi-n-propylamine ND 390 . 87-86-5 Pentachlorophenol ND 780 85-01-8 Phenanthrene ND 390 \ 108-95-2 Phenol ND _ 780 J 129-00-0 Pyrene ND 390 (con't) n w US ENVIRONMENTAL-PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS- SAMPLE NO. : 65651 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ---------------------- 120-82-1 1, 2, 4-Trichlorobenzene ND 390 88-06-2 .2, 4, 6-Trichlorophenol ND 780 ---------------------------- Hazardous Substances ---------------------------- 65-53-3 Aniline ND 390 65-85.-0 Benzoic Acid ND 780 100-51-6 Benzyl Alcohol ND 390 106-47-8 4-Chloroaniline ND 390 132-64-9 Dibenzofuran ND 390 91-57-6" 2-Methylnaphthalene 90 390 L: 95-48-7 2-Meth ND 390 106-44-5 4-Methylphenol ND -390 88-74-4 2-Nitioaniline ND 390 99-09-2 3-Nitroaniline ND 390 100-01-6 4-Nitroaniline - ND 390 95-95-4 2,4, 5-Trichlorophenol. ND 390 ---------------------------- Other Compounds Quantitated ------------------- None detected ND 390 ---------------------------- Est. Tentatively Identified ' Conc. Compounds (mg/Kg) ---------------------------- Nonane 3000 J Hydrocarbon (C10) 3000 J Benzene Alkyl (C3) 3000 J C12 Hydrocarbon 9000 J C12 Hydrocarbon 50.00 J note: light petroleum product 25 l US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS . SAMPLE NO. : 65651 Results Continued: ------------------------------------------------------------------------ Sample Recoveries For Recoveries QC Range Surrogate Compounds: (0 M . 2-Fluorophenol 119 25-121 Phenol,d5 105 - 24-113- Nitrobenzene,d5 1* 23-120 Fluorobiphenyl . 88 30-115 2, 4, 6-Tribromophenol 70 19-122 p-Terphenyl,dl4 86 18-137 2-Chlorophenol-d4 106 20-130 1,2-Dichlorobenze-d4 9.8 20-130 ------------------------------------------------------------------------- * Out of range - w ro 26 FACILITY SAMPLED: FLYNN TAN US- ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE. NO: : 65644 Matrix: Drum DATE. OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/30/98 Dilution Factor 1: 10 WET .WEIGHT EXTRACTED: 0..178 g Report Factor 11 RESULTS: - CAS Compound Conc. kL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------ Priority Pollutants. 83=32-9 Acenaphthene ND 3300 208-96-8 Acenaphthylene ND 3300 120-12-7 Anthracene ND 3300 309-00-2 Aldrin ND 3300 56-55-3 Benzo (a) anthracene ND 3300. 205-99-2 Benzo (b) fluorantliene ND 3300 207-08-9 Benzo (k) fluoranthene ND 3300 50-32-8 Benzo (a)pyrene ND 3300 191-24-2 Benzo (ghi)perylene ND 3300 85-68-7 Butyl Benzyl Phthalate ND 3300 319-85-7 beta-BHC ND 3300 319-86-8 delta-BHC ND 330% 111-44=4 Bis (2-chloroethyl)ether ND 3300 I11-91-1 Bis (2-chloroethoxy)methane ND 3300 117-81-7 Bis (2-ethylhexyl)phthalate ND 3300 108-60-1 Bis (2-chloroisopropyl) ether ND 3300 101-55=3 .4-Bromophenylphenyl ether- ND 3300 86-74-8 Carbazole ND 3300 59-50-7 4-Chloro-3-methylphenol ND 6600 91-58-7 27Chloronaphthalene ND 3300 95-57-8 2-Chlorophenol ND 6600 7005-72-3 4-Chlorophenylphenyl ether ND 3300 218-01-9 Chrysene ND 3300 72-54-8. 4, 4 '-DDD ND 3300 72-55-9 4, 4 '-DDE ND 3300 0-29-3 4,.4 -DDT ND _ 3300 53-7-0-3 Dibenzo(a,h) anthracene ND 3300 (con' t) 27 US ENVIRONMENTAL PROTECTION AGENCY - REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65644 Results Continued: CAS. Compound Conc. RL Qualifier. NO. (mg/Kg) (mg/Kg) or Comment ;�--------------------- ------------------------ -------------------- 84-74-2 Di-n-butylphthalate ND 3300 i17-84-0 Di-n-octylphthalate ND �3300 . 541-73-1 1,3-Dichlorobenzene ND 3300 95-50-1 1,2-Dichlorobenzene ND 3300 106-4 6=7 1, 4-Dichlorobenzene ND 3300 91-94-1 3,31-Dichlorobenzidine ND 3300 120-83=2 2,4-Dichlorophenol ND 6600 60-57-1 Dieldrin. ND 3300 \ 84-66-2 Diethylphthalate ND 3300 105-67-9 2-4-Dimethylpheno.1 ND 6600. 131-11-3 Dimethylphthalate ND 33.00 51-28-5 2,4-Dinitrophenol ND 6600 121-14-2 2,4-Dinitrot6luene ND 3300 606-20-2 2, 6-Dinitrotoluene ND 33.00 86-73-7 Fluorene ND 3300 76-44-8 Heptachlor ND 3300 1024-57-3 Heptachlor. epoxide ND 3300 118-74-1 Hexachlorobenzene ND 3300 87-68-3 Hexachlorobutadiene ND 330% 7.7-47-4 Hexachlorocyclopentadiene ND 3300 67-72-1 Hexachloroethane ND 3300 .193-39-5 Indeno.(1,2,3-cd)pyrene. ND 3300 78-59-1 Isophorone ND 3300 534-52-1 2-methyl-4,-6-dinitrophenol ND 6600 91-20-3 Naphthalene .800 3300 L 98-95-3 Nitrobenzene ND- 3300 .88-75-5 2-Nitrophenol ND 6600 100-02-7 4-Nitrophenol ND 6600 86-30-3 N-nitrosodiphenylamine ND 3300 621-64-7 N-Nitrosodi-n-propylamine ND 3300 87-86-5 Pentachlorophenol ND 6600 85-01-8 Phenanthrene ND 3300 ) 108-95-2 -Phenol ND _ 6600 129-00-0 Pyrene ND 3300 (con't) US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY - GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65644 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ 120-82-1 1,214-Trichlorobenzene ND 3300 88-06-2 2,4, 6-Trichlorophenol ND 6600 ---------------------------- Hazardous Substances ---------------------------- 65-53-3 Aniline ND 3300 65-85-0 Benzoic Acid ND 6600 100-51-6 Benzyl Alcohol WD 3300- 106-47-8 4-Chloroaniline ND 3300 132-64-9 -Dibenzofuran ND 3300 91-57-6 2-Methylnaphthalene 2000 3300 L 95-48-7 2-Methylphenol ND 3300 106-44-5 4-Methylphenol ND 3300 88-74-4 2-Nitroaniline . ND 3300 99-09-2 3-Nitroaniline ND 3300 100-01-6 4-Nitroaniline ND 3300 95-95-4 2,4, 5-Trichlorophenol ND 3.300 ---------------------------- Other Compounds. Quantitated rr ---------------------------- None detected ND 3300 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) -------------------------- Hydrocarbon (C8) 600.0 J C14- Hydrocarbon 6000- J C16 Hydrocarbon 6000 J C16 Hydrocarbon 6000 J C18 Hydrocarbon 10000 J note: Petroleum Product. Possible mix of light petroleum and fuel no. 2. 29 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS. EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65 64 4 Results Continued: ------------------------------------------------------------------------- Sample Recoveries For Recoveries QC Range Surrogate Compounds M ($) ----------------------------------------------------------------------- 2-Fluorophenol NA 25-121 Phenol,d5 NA 24-113 Nitrobenzene,d5 NA 23-120 Fluorobiphenyl NA 30-115 2,4, 6-Tribromophenol NA 19-122 p-Terphenyl,d14. - NA 18=137 2-Chlorophenol-d4 NA 20-130 1 2-Dichlorobenze-d4 NA 20-130 ------------------------------------------------------------------------ rr - 1 \ �n FACILITY SAMPLED: FLYNN TAN US -ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY _ GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : ' 67261 - Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04122/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/30/98 Dilution Factor 1: 10 WET WEIGHT EXTRACTED: 0.164 g Report. Facto.r 12 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 3600 208-96-8 Acenaphthylene ND 3.60.0. 120-12-7 Anthracene. ND 3600 309-00-2 Aldrin ND 3600 56-55-3 - Benzo (a) anthracene- ND 3-600 205-99-2, Be'nzo (b) fluoranthene ND 3600 ' 207-08-9 Benzo (k) fluoranthene ND 3600 50-32-8 Benzo (a)pyrene ND 3600 191-24-2 Benzo (ghi)perylene ND 3600 85-68-7 Butyl Benzyl Phthalate ND 3600 319-85-7 beta-BHC ND 3600 319-86-8 delta-BHC ND 3600r 111-44-4 Bis (2-chloroethyl)e.ther ND 3600 111-91-1 Bis (2-chloroethoxy)methane - ND 3600 117-81-7 Bis (2-ethylhexyl)phthalate ND. 3600 108-60-1 Bis (2-chloroisopropyl)ether ND 3600 101-55.-3 4-Bromophenylpheny-1 ether ND 3600 86-74-8 Carbazole ND 3600 59-50-7 4-Chloro-3-methylphenol ND 7200 91-58-7 2-Chloronaphthalene ND 3600 95-57=8 2-Chlorophenol ND 7200 7005-72-3 4-Chlorophenylphenyl ether ND 3600 218-01-9 Chrysene ND 3600 72-54-8. 4, 4'-DDD ND 3600 72-55-9 a 4,4 '-DDE ND 3600 )0-29-3 414'-DDT ND 3:6.00 63-70-3 Dibenzo (a,h)anthracene ND- 3600 (con't) 31 Y ' US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67261 Results Continued: CAS. Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ---------------------------------------------------------------------- 84-74-2 Di-n-butylphthalate ND �600 117-84-0 Di-n-octylphthalate ND 3600 541-73-1 113-Dichlorobenzene ND 3600 95-50-1 1, 2-Dichlorobenzene . ND 3600 106-46-7 1, 4-Dichlorobenzene ND 3600 91-94-1 3.131-Dichlorobenzidine ND 3600 120-83-2 2, 4-Dichlorophenol ND 7200 60-57-1 Dieldrin ND 3600 84-66-2 Diethylphthalate ND 3600 105-67-9 2-4-Di.methylphenol ND 7200 131-11-3 Dimethylphthalate ND 3600 51-28-5 2, 4-Dinitrpphenol ND 7200 121-14-2 2, 4-Dinitrot6luene ND 3600 606-20-2 2, 6=Dinitrotoluene ND 3600 86-73-7 - Fluorene ND 3600 76-4.4-8 Heptachlor ND 3600 1024-57-3 Heptachlor epoxide _ND 3600 118-74-1 Hexachlorobenzene ND 3600 87-68-3 Hexachlorobutadiene ND 3600rr 77-47-4 Hexachlorocyclopentadiene ND 3600 67-72-1 Hexachloroethane ND 3600 193-39-5 Indeno (1, 2, 3-cd)pyrene ND 3600 78-.59-1 Isophorone ND 3600 534-52-1 2-methyl-4,6-dinitrophenol ND 7200 91-20-3 Naphthalene 900 3600 L 98-95-3 Nitrobenzene ND - 3600 88-75-5 2-Nitrophenol ND 7200 100-02-7 4-Nitrophenol ND 7200 86-30-3 N-nitrosodiphenylamine ND 3600 621-64-7 N-Nitrosodi-n-propylamine ND 3600 87-86-5 Pentachlorophenol ND 7200 .85-01-8 Phenanthrene ND 3600 \ 108-95-2 Phenol ND _ 1200 J 129-00-0 Pyrene ND 3600 { (con't) - °" US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67261 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg)' (mg/Kg) ors Comment 120-82-1 1,2,-4-Trichlorobenzene ND 3600 88-06-2 2, 4, 6-Trichlorophenol ND 7200 ---------------------------- Hazardous Substances ---------------------------- 65-53-3 Aniline ND 3600 65-85-0 Benzoic Acid ND 7200 100-51-6 Benzyl Alcohol ND 3600 106-47-8 . 4-Chloroaniline ND 9600 . 132-64-9 Di-benzofuran ND 3600 91-57-6 2 Methylnaphthalene 900 3600 L 95-48-7 2 Methylphenol ND .3600 106-44-5 4-Methylphenol ND 3600 { 88-74-4 2-Nitroaniline ND 3600 99-09-2 3-Nitroaniline ND 3600 100=01-6 4-Nitroaniline ND 3600 95-95-4 2, 4,5-Trichlorophenol ND 3600 Other Compounds Quantitated rr ---------------------------- None detected ND 3600 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Hydrocarbon 10,000 J Decane 401000 J C12 Hydrocarbon ' 10, 000 jr C12 Hydrocarbon 10,000 J C12 Hydrocarbon 30, 000 J note: Possible light petroleum product and smaller amount of fuel #2 . 33 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67261 Results Continued: Sample Recoveries For Recoveries QC Range .Surrogate Compounds: M M --------------------------------------------------------- ------------ 2-Fluorophenol NA 25-121 Phenol,d5 NA 24-113 Nitrobenzene,d5 NA 23-120 Fluorobiphenyl NA 30-115 2, 4, 6-Tribromophenol NA 19-122 p-Terphenyl,d14 NA 18-137 2-Chlorophenol-d4 NA , 20-130 1,2-Dichlorobenze-d4 NA 20-130 \ FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65656 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/30/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.196 g Report Factor 1 .02 RESULTS : CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 310 208-96-8 Acenaphthylene ND 310- 120-12-7 Anthracene ND 310 309-00-2 Aldrin ND 310 56-55-3 Benzo(a)anthracene ND 310 205-99-2 Benzo(b) fluoranthene ND 310 207-08-9 Benzo(k) fluoranthene ND 310 50-32-8 Benzo(a)pyrene ND 310 191-24-2 Benzo (ghi)perylene ND 310 85-68-7 Butyl Benzyl Phthalate ND 310 319-85-7 beta-BHC ND 310 319-86-8 delta-BHC ND 31% 111-44-4 Bis (2-chloroethyl) ether ND 310 111-91-1 'Bis (2-6hloroethoxy)methane ND 310 117-81-7 Bis (2-ethylhexyl)phthalate ND 310 108-60-1 Bis (2-chloroisopropyl) ether ND- 310 101-5573 4-Bromophenylphenyl -ether ND 310 86-74-8 Carbazole ND 310 59-50-7 4-Chloro 3-methylphenol ND 610 91-58-1 2-Chloronaphthalene ND 310 95-57-8 2-Chlorophenol ND 610 7005-72-3 4-Chlorophenylphenyl ether ND 310 218-01-9 Chrysene ND 310 72-54-8 4, 4'-DDD ND 310 72-55-9 4, 4 '-DDE ND 310 '0--29-3 4., 4 '-DDT. ND 310 -,3-70-3 Dibenzo (a,h) anthracene ND 310 (con't) 35 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS .EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : . 65650 Results Continued: CAS . Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg)- or Comment ------------------------------------------------------------------------ 84-74-2 Di-n.=butylphthalate ND 310 117-84-0 Di-n-octylphthalate ND 310 541-73-1 1, 3-Dichlorobenzene ND 310 95-50-1 1,2-Dichlorobenzene ND 310 106-46-7 - 1, 4-Dichlorobenzene ND 310 91-94-1 3, 31-Dichlorobenzidine ND 31.0 120-93-2 2, 4-Dichlorophenol ND 610 60-57-1 Dieldrin ND 310 84=66-2 Diethylphthalate ND 310 ) 105-67-9 2-4-Dimethylphenol ND 610 131-11-3 Dimethylphthalate ND 310 51-28-5 - 2, 4-Dinitrophenol ND 610 121-14-2 2, 4-Dinitrotoluene ND i 310 606-20-2 2, 6-Dinitrotoluene ND 310 86-73-7 Fluorene ND. 310 76=44-8 Heptachlor ND 310- 1024-57-3 Heptachlor epoxide ND 310 118-74-1 Hexachlorobenzene ND 310 87-68-3 Hexachlorobutadiene ND. 31% 77-4-7-4 Hexachlorocyclopentadiene ND 310 67-72-1 Hexachloroethane ND 310 193-39-5 Indeno (1, 2, 3-cd)pyrene ND 310 78-59-1 Isophorone ND 310 534-52-1 2-methyl-4, 6-dinitrophenol ND 610 91-20-3 Naphthalene ND 310 98-95-3 Nitrobenzene ND 310 88-75-5 2-Nitrophenol ND 610 100-02-7 4-Nitrophenol ND 610 86-30-3 N-nitrosodiphenylamine ND 310 621-64-7 N-Nitrosodi-n-propylamine ND 310 87-86--5 Pentachlorophenol ND 610 -85-01-8 Phenanthrene ND 310 .108-95-2 Phenol ND 610 129-00-0 Pyrene ND 310 (con't). 4. US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65650 Results Continued: CAS Compound Conc'. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------=----------------------------------------------------------- 120-8-2-1 11 2, 4-Trichlorobenzene ND 310 88-06-2 2, 4, 6-Trichlorophenol ND : 610 - ------------------- Hazardous Substances -------------------- ----- 65-53-3 Aniline ND 3.10 - 65-85-0 Benzoic Acid. ND 610 100-51-6 Benzyl Alcohol ND 310 106-47-8 4-Chloroaniline ND 310 132-64-9 Dibenzofuran ND 310 91-57-6 2-Methylnaphthalene ND 310 95-48-7. 2-Methylphenol ND 310 ?06-44-5 4-Methylphenol ND 310 88-74-4 2-Nitroaniline ND 310 99-09-2 3-Nitroaniline ND 310 100-01-6 4-Nitroaniline ND 310 95-95-4 2, 4, 5-Trichlorophenol ND 310 ---------------------------- Other Compounds Quantitated ----------------------------- None detected , ND 310 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Tetradecanoic acid methyl - ester 1700 J 9-Hexadecanoic acid methyl ester 3200 J Hexadecanoic acid methyl ester 2900 J Octadecanoic acid isomer 3400 J Octadecanoic acid isomer 28000 J Octadecenoic acid methyl ester 1200 J Unknown 1900 J 37 r US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY ' = :GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65650 " Results Continued: _ ------------------------------------------------------------------------ Sample Recoveries For Recoveries QC Range, Surrogate Compounds: f%) M 2-Fluorophenol 93 25-121 Phenol,d5 92 24-113 Nitrobenzene,d5 78 .23-120 Fluorobiphenyl 87 30-115. 2, 4, 6-Tribromophenol 41 19-122 p-Terphenyl,d14 90 18-137 2-Chlorophenol-d4 101 20-130 1, 2-Dichlorobenze-d4 102 20-130 ------------------------------------------------------------------------ \ rr 38 APPENDIX H pH Analytical Data �r E � � 1 . ;� Please note: The laboratory performing the drum pH analysis incorrectly identified the site name as"Sponge X on the "SUBJ:"line of the analytical data memorandum. The analytical data contained in this memorandum are the drum pH results for the Flynntan site in Salem, Massachusetts and can be verified by the EPA sample numbers (65646, 65647, 65648; 65650, 65651, 65652, 65660, and 65661) which correspond to the chain-of- custody record (Appendix D, Section 1.) and the project number (98267) which was assigned to this site by the.laboratory. z � ` d �� fZaP UNITED STATES ENVIROMMML PROTECTION AGENCY REGION I 60 WESTVIEW STREET, LESINGTON, MASSACHUSETTS 02173 MEMORANDUM PN: 98267 DATE: April 23, 1998 j SUBJ: Sponge % - Drum pH Results FROM: Hugh Curran 0L Chemist TO: Tom Hatzopoulos L �HRII: Dr. William.. Ad�fade y - senior Chemistry Analytical. Specialist { AnalyticAl References: Methods 9040B and 9045C, from "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW-846, 3rd ed. , Final Update IIB, Rev. 2 and 3, 1/95." (SOP I=16, Rev. 3/92) Date Samples e eived b abo ato : 04/17/98 Date Samples Analyzed by Laboratory: 04/20/98 File name: 48267dr.pH - Results Value reported as aqueous pH measured in water at 25 degrees C. - 65646(ave) 11.48 65647 >13 65652 (ave) 3.38 67260(ave) 7.60. 1 Values reported as waste pH measured in water at. 25 degrees C. Sample PH 65648 3.30 65650 -6.83 65651 4.55 67261(ave) 4.78 -3- Quality Assurance\Quality Control r - - Labbratory Dullicatesr_ Sample 65646. $maple 65646 Dup. Average RPD 11.45 11.50 11.48 0.4% Samvie 65657 $=p1e 65652 Dup. Averaae RPD Y3.35 3 .40 3.38 1.50 Sam=le 67260 $amble 67260 Dup. Average U2 7. 60 7.60 7.60 0..01 Satiple 67261 pzple 6726i. Dup: Average. RPD 4.75 4.80 4.78 1.0% w -4- Data Quality Statements Data review chemist: Bill Andrade Method modifications.: Amounts less than- the 20 grams required by the method were used for samples 65648 and 67261- DUP due to insufficient amounts of those samples. ' An amount less than the 20 grams required by the method was used for sample 65650 due to the formation of a suspension when water was added. - Limitations of data: None Comments: Samples 65648,- 6.5650, - 65651 and 67261. were stirred with water and the pH of aqueous phase was taken. Instrument performance Problems: None • w chain. of custody Abnormalities: None APPENDIX I PolychIorinated Biphenyl Analytical Data i . 1 ; .. �- � \V/ A UNITED STATES ENVIRONMENTAL PROTECTION AGENCY j a � - REGION, ��4-2-a 'O'N ENVIRONMENTAL SERVICES DIVISION 60 WESTVIEW STREET LEXINGTON,MASSACHUSETTS 02173-3185 )ATE:. April 28, 1998 WW: Analysis of PCBs in Soils - FLYNN TAN FROM: Peter Philbrook, Investigations and Analysis, Chemistry Section =U, Dr. William J-. Andrade,. Advance` Analytical Chemistry Specialist TO: Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received. and logged in by the laboratory according to the SOP for Sample Log-In (EIA-ADMLOGNI.SOP, 7/97) . EPA Regional Procedure: Polychlorinated _Biphenyls in Soil Samples, Mid Level" Method, . PCBSOML6.SOP: The modules used for this; Procedure were: XL 2020 Heat Systems Sonicator, SONICAT2.MOD,. Chlorinated Pesticides and PCB Screening, 850.0EC1.MOD,. 5880 Gas Chromatographs, 5880EC2.MOD. Results are reported out -in dry weight. The analytical support for this report was performed by NCOA contractors. +� _ Date Samples Received by the Laboratory: 04/17/98 Date Analysis' Started: 04/21/98 cc: File: J: \CHEMSTRY\REPORTS\PCB-PEST\98267SO.PCB US ENV IRONMENTAI. .PROTECTION AGENCY l 60 Westview Street / Lexington, MA 02173- QUALITY CONTROL: 1: One method blank was included in the analysis. 2. Each sample was spiked with the surrogate compounds, tetrachloroxylene and decachlorobiphenyl, at approximately 0.2 mg[Kg.. The results for the surrogate recoveries are reported out with each sample. 3. . One sample, 67265, was spiked as a matrix spike with Aroclor-1260 at approximately 1.0 mg/Kg. The recovery Is listed below. PCB Recovery QC Range Aroclor 1260 84* 46 - 15.3 . * = Matrix recovery was determined using a single T&W DB=5 column. Recovery .could not be, determined on-the confirmatory DB-1701 column, due to interference from a.:.large unresolved complex.. matrix. The sample had ah. .oily matrix. w 2. '�-' US ENVIRONMENTAL PROTECTION AGENCY 60 Westview Street Lexington, MA 02173 Chemist who reviewed data: Peter Philbrook Holding time meet (YIN) : Yes Extraction (Water - 7 days, Soil - 14 days) Analytical (40 days after extraction) Method modifications: None Limitations of data: Detection limits for sample 67265 were increased due to oily matrix. Laboratory blank. problems: .None Instrument performance problems: None rr Surrogate and spike recovery problems: surrogate recoveries for sample 67264 could not be' determined due to dilutions required. t.o quantitate target compounds. Additional Comments:- None 3 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY. Polychlorinated Bipheriyls SAMPLE NO..: 67265 DATE OF COLLECTION: 04/16/98 - Matrix: Soil DATE OF EXTRACTION: 04/22/98 Final Volume: 5 mL DATE OF ANALYSIS: 04/24/98 Percent Moisture 37 DRY WEIGHT EXTRACTED: 2.21 g Extract Dilution . 1 WET WEIGHT EXTRACTED: 3 .50 g Report Factor: 1.3 - SAMPLE RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ----------------------------------------------------------------------- 12674-11-2 Aroclor-1016 - ND 2.00 Y11104-28-2 Aroclor-1221 ND, 2.00 11141-16-5 Aroclor-1232 ND 2.00 53469-21-9 Aroclor-1242 ND 2.00 12672-29-6 Aroclor-1248 ND 2.00. 11091-69-1 Aroclor-1254 ND 2.00 11096-82--5 Aroclor-1260 ND 2.00 11100-14-4 Aroclor-1262 ND 2 .00 37324-23-5 Aroclor-1268 ND 2.00 ------------------------------------------------------------------------- \ Sample Recovery for Observed Surrogate Compound: Recoveries (�) Decachlorobiphenyl 58 2,4,5,6-Tetrachloro-m-xylene 65 ------ ------------------------------------------------------------------ Notes: RL = Reporting level ND ..= None detected = Approximate w < = Less than > = Greater than NA = Not applicable due to high sample dilutions or sample interferences E = Estimated value exceeds the calibration range L = Estimated value is below the- calibration range B = Analyte is associated- with the lab blank or trip blank contamination. Values are qualified when the observed, concentration of the contaminant .in the sample extract is less than ten times the concentration in the blank. P = The confirmation value exceeded 3.5% difference and is less than 100%. The lower value is reported. D = Detected but too low to quantitate. C = The identification has been confirmed by. GC/MS. F, 4. ` ` FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I. LABORATORY Polychlorinated Biphenyls SAMPLE NO. : 672.64 DATE OF COLLECTION: 04/16/98 Matrix: Soil DATE OF EXTRACTION: 04/22/98. Final Volume: 5 mL DATE OF ANALYSIS: 64/24/98 Percent Moisture .7.3 DRY WEIGHT EXTRACTED: 2.78 g _ Dilution Factor: 100 WET WEIGHT EXTRACTED: 3.0.0 g Report Factor: 105.8 SAMPLE RESULTS: CAS Compound Conc. , RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment --------------------------------------------------------------. - ---- 12674-11-2 Aroclor-1016 ND 18 11104-28-2 - Aroclor-1221 ND 18 11141-16-5 Aroclor-1232 ND 18 53469-21-9 Aroclor-1242 ND 18 '12672-29-6 Aroclor-1248. ND 18 11097-69-1 Aroclor-1254 180 18 11096-82-5 Aroclor-1260 ND 18 11100-14-4 Aroclor-1262 ND 18 37324-23-5 Aroclor-1268 ND 18 ----- -----=-------------------- ------ ------ ----=----------------- Sample Recovery for Observed Surrogate Compound: Recoveries R) Decachlorobiphenyl NA 2,.4,5,6-Tetrachloro-m-xylene NA -----------------------------------------------------------�----------- 5 i FACILITY SAMPLED: FLYNN TAN J US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY Polychlorinated Biphenyls SAMPLE NO. : BLANK DATE OF COLLECTION: Not Applicable Matrix: Soil DATE OF EXTRACTION: 04/22/98 Final Volume: 5 mL DATE OF ANALYSIS: 04/22/98 Percent Moisture 0 DRY WEIGHT. EXTRACTED: 3 .00 g Dilution Factor: 1 WET WEIGHT EXTRACTED: 3 .00 g Report Factor: 1.0 SAMPLE RESULTS: CAS Compound Conc. RL _Qualifier NO. (mg/Kg) (Mg/Kg) or Comment ------------- ---------------------------------------------------------- .12674-11-2 Aroclor-1016 ND 0.17 11104-28-2 Aroclor-1221 ND .0.,17 11141-16-5 Aroclor-1232 ND 0.17 53469-21-9 Aroclor-1242 ND 0.17 12672-29-6 Aroclor-12.48 ND 0.17 11097-69-1 Aroclor-1254 ND 0.17 \ 11096-82-5 Aroclor-1260 ND 0.17 ) 1110'0-14-4 Aroclor-1262 ND 0..17 37324-23-5 Aroclor-1268 ND 0.17 . ------------------------------------------------------------------------- Sample Recovery for Observed Surrogate Compound: Recoveries (%) Decachlorob.iphenyl 98 2,4,5,6-Tetrachloro-m-xylene 65 ------------------------------------------------------------------------ . 1 6 APPENDIX J Metals Analytical Data r a - . w N Z v Q 00 N p 00 C r r O U Q rW a O uul'' E UO W r ti� ON CD OO W000.v N� N O 8CA W <O C'0 tq 019m�7r a.0 dr co IT1U OY hCD0OCDr Q n N O � O P 7> n CO O m ti 00 O W 0000 W r N co M dr7m Wt-O tD.N C7 r - �000 W Nr CDnr,-W to C _ L aW� co r Nrth O O o w H LL i w O W r -W-W ID'O O W CO W O O'O 0 0 v to ;; y aO W Ul CWONCW9WW000 0�. O toD m cq a � 0 _ a P O< U to I.- w I.- Q tDn*t- ;V WaO CD 0000 mao —> w o ° romno.° CLC aor-wo [3� LL pb0 W F ¢0 W W a Q.0: 3 J wo0U O Z WU 12 wQ �Q t0 C* r)04 C r VOG 00O00 r- }} 0 - wJO NO gM nCVON vOOn W R^r ZF-OQ Z mp.o 069 ^Ht°NOnto 0 0�00 O Nr H3 5T ~ Z 1- 3:LULu 0 P Q - z a Z wW N.t- n0NtD 00h;CbaMCON II / ■ a NO r V-d.6Otpo, IOrNWr _ a_ a4 N CD �Nmrrr 6c; 1 . D? W O d J - a w »> co co r otoNNoo0t000ncV LLI tii LL9A_ w��40o01c4mo�a o p 0 C2 r n Z Z a to co a000rvmawv N 0 NGgq CN0NOoo O 0- 0 W aaaaaaCLCLCL IL a. � crw d.4m ttuoWO dOqq ��W O ..K ZOZ G .J Z Z AL W� aaOW' ru WOOS a lu x. SE. 0 a Z� 00 U_ �. �: Z v S -> D co .. a .J O } U. � ZZ�?�2 W>Z>w �LLV[1.. Q WD a mW�mUOZOZOU5,w WtAm 0 3W 09KO ow-3 J :.. Z< + f '. go �tai5 zI Q�d vc�v--J'.m2wuj0: <tr.ILV_ z . ScqCT0"a©8®-" 0 e �� Wit« . . `• w 9 E \ - o | w w § a C3 ' § z ■ . �& § §� Z < o z .I .e . . <�ci0 _ ww RZvv . - J COD■wo 0 _< - �0 6� 6 7�0002 �_ 0m ®/kk ut 7 . � � CL S@_©r�8C14C, §�ZZw ) - -© oo�N w�� I�§ « $Jzzjx� w �0 2 ' E■■■■« ■ z - . P=iu_■J- 0 n. ' - • .J�-j 2J &. . &->§/Z z to e _ o Int-&ooM.o-toa : 11, . . � LL co kC-4 Cld10-c; � 2��« ■ � z � - � 2 2 R§i� @2R�«Satoco # LL ■nC©�V3r- o k o G & z z § �000-�no_677 0 �3G��o®C3 10 ■ C; ■ �� 0 0j ■ k §� E Q� . b �aaaan.&aavacL Q$ ujBwo . . .lu $-§ _ $ J6=coo . . � E/E ® 6 ' . Co. IL -Jwoc® :§ 0 $Cc xe� .moo& Amw < ' E § IL w « > k2o �k § 5o `�&% /.w :31 . k§� U z-��S u�- #2.. ■o 2 &@3eo2: mow§ K - § K2© o D2W ®io O§w2 z ` ■g� ■ �a_2k0�%$I■e «��U ^ 2 T }ON I. �N IO`..'p NN C OlO 00Tr N I �JI G O T T 10W £ a W w z f w co all zW — Ow Q 0 J Q Z O V W D o W 0 W a0 Q U y WW ui �zUv Q W U L-F Z ZcD W�n 0— f0 0 t0 e0 0lP O T T W n t0 r OTC E rNOO W G�j�nj O T O Z— v . Z W� .o6 GGo�'r� ocoGGG OQOO 0 J coY QLL Nr E'�ZZ W �� 0 c•� $ QQ Hfl E � �W-N I z N QZJJ w oLU » -> > »M d—» a O. rO0-il.TG CD O N01DOO,�et1�-G000 Q Q N J b W co W :2QTo E va��oNnr�ocvomm ui tii LL cp 5000 G'do- c G COC 0~n� O Z Z Q N O co a)' Z O n OW E IV OO�TviO4C40 le ccl 7 �J E GGG .0 O GOtu dz �Zd0) In Luowo Wad. 5 �co O*C 1Z-O Z� a� boU d pW -JtilW Z O Q - aw� - W _ 0 W UJ }}. a 2naoG` - : U -. < 0 g z 5o 222 maw. Md0 aCiUg• Z ads OQ Um = O�W.a,O � v vj� Q W , . ao Qu.Mo 0 F-Z O N O r O N O W Orr N UO c v. Oo "6000 0n V~ r r c t¢w_� �{ Ow UD _U W {L a F � Z f W N W . Z9 Go W Q ct: J FZ In O F- F_ 0 OO W W ui ui w O W D >- Qi 0 D z Wo a a ww °° �ZWW O Y F- D a� E WtOiF� Go 0 �aoo a Qazz w t9 -w W m W , w _ ZXww < a Z J J J 'a-» m w D>. ' Qmo �o -mwmg oQoMIDvtL 4�N R�r� ao IL $ 7 $,_ .�PlN O Z DOd ~� y v o C o z OOp O V}"ZC CD O N m e-v n o�o W v N 0 W. � .AjvOO�r�NNOt'7r O C O O O p o o _ O W aaaa(Lmm& 8m& �"Z &:k am' w_ow.[3 m m.j wa g 2 20. W0 5 �� W450 - UJJ}Z.. D J .0 �. Z0a w' a��v. w = O �+ 2a2K 2ww w w m w �ag.�. a q g D.0 2— m.wD UDU0U. N Wm 2w.2gv.OZoza J C I �g ? Qamocaic=iJLUJ a1eJi i aU.ac�i w .- - � :� APPENDIX K Flasbpoint.AmlyticaI Data 4 \� w �� • A UNITED STATES ENVIRONMENTAL PROTECTION AGENCY �� = REGION 1 ' ENVIRONMENTAL SERVICES DIVISION gyp= 60 WESTVIEW-STREET LEXINGTON,MASSACHUSETTS 02173-3185 DATE: April 29, 1998 SUBJ: Flash Point Determination - FLYNN TAN pep FROM: Peter Philbrook, ChemiAdc&d cyt PHRII, , Dr. .-William J. Andrade, 'oAn alyticalChemistry _Specialist , TO': Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received and logged in by the laboratory according to the SOP for Sample Log=in'. (EIA-ADMLOGNI.SOP, 7/97) . The flash points were determined. by the EPA Region 1 method, Flashpoint Setaflash Closed-Curs Method, FLAS$3,..SOP.. Reference: ASTM-Method D3278-78 The analytical support for this report was performed by NCOA contractors. . Date Samples Received by the Laboratory: 04/17/98. �r Date Analysis Started: 04/21/98 cc: Files J: \CHEMSTRY\REPORTS\MISC\98267DR.FP - 0�....�e�weO�...i..1.N� DeMe�.del.Vwwel:.e.e�Iv tl'.. i:..i_e..�:•.wr n�_.m�esr__•.i.ai nr_._..Y..r:c. US EN7IRONMMTAL PROTECTION AGENCY 60 Westview Street .Lexington, MA 02173 QUALITY CONTROL: 1. The flash point' of p-xylene was determined each day, prior to the sample analysis. Observed Accepted Average Date Flash Range Flash Points (°C) Point (°C) _ 27.2 ± 0.8- (°C) 04/21/98 (1st) 27.5 ` 04-/21/98 (last) '27.'5 . 27.5 RESULTS: Sample Date Flash/ Observed Average Comments . No Flash Flash Flash 1 . .Test Point -Point (60°C) -(°C) (°C) 65644 04/21/981 No Flash 65645 04/21/98 No Flash 65.646 04/21/98 No Flash 65647 04/21/98 Flash 19°C 65647DUP 04/21/98 Flash 18°C 18.5°C M 65649 04/21/98 No Flash. 65650 04/21/98 No Flash 65651 04/21/98 Flash 47.5°C 65651DUP 04/21/98 Flash 48°C -480C 65652 64/21/98 No Flash 67260 04/21/98 No Flash 67261 04/21/98 Flash 550 67261DUP 04/21/98 Flash . 550 55°C -- --- ---------------------------------------------------------------- 1 1 ' .i J US ENVIRONMENTAL PROTECTION AGENCY 60. Nestview Street Lexington, MA 02173 > = Greater than = Less than ' s = Less than or equal to -- = Approximate * = The duplicate analyses did not -agree within 1 degree Centigrade (possibly due to sample variation) so the flashpoint. was repeated for a total of 5 or 6 values. NA = Not Applicable. The flash/no flash test is not done for the duplicates, only the finite flash point is determined. I N SAMPLES ANALYZED: 65644., -65645, 65645; 6564-7, 64649, 65650, 65651, 65652; 672601 67261 us M14MOEMENTAL PROTECTION AGENCY 60 Westview Street Lexington, MA 02173 Chemist who reviewed data: 'Peter Phil-brook Method modifications: Our SOP has been modified to include.-solids in. the analysis: All the4 steps and quality control are the same as in the EPA RCRA method: 'Test. Methods for Evaluating Solid Waste' , Setaflash Closed Tester, method 1020, Second edition, 1982. This Method is based 4 on ASTM Method D327-78. Limitations of data: None Laboratory blank problems: None Instrument performance .problems: None Surrogate and spike -recovery problems: None w Additional comments: Sample 65647 Flashed and was. soluble in water. According to ASTM methodology this sample required a % water determination. : This test was performed on• 4-28-98 using a Karl Fisher. titration. Sample 65657 is 81% water. The density of sample 65657 is 1140 mg/mL. MEMORANDUM DATE: April 2.8, 1998 SUBJ: Site Investigation Closure Flynntan Site 70-92 Boston Street Salem, MA f FROM: Athanasios Hatzopoulos, On-Scene Coordinator : Site Evaluation & Response Section II TO: , Flynntan Site File THRU-. Steven Novick, Section Chief , Site Evaluation & Response Section II Iri accordance with section 300.400 of the NCP, a Removal Site Evaluation, consisting of a Preliminary Assessment and Site Investigation (PA/SI) , has been undertaken for the Flynntan Site in Salem, Massachusetts. The findings -of the Removal Site Evaluation, recorded in a PA/SI Report, have been evaluated under the- criteria set forth in section 300.-415 of the NCP and section 104.(a) and. (b) of CERCLA, 42 U.S.C. § 9604 (a) and (b) . The Removal Site Evaluati.oA has; led to the determination that �a Removal Action is appropriate at this time. The findings of the Removal Site Evaluation are as follows: 1. Source. and nature. .of the release or threat of release: a . Please refer :to the document entitled Removal Program Preliminary Assessment/Site Investigation for the Flynntan Site, Salem, Massachusetts" by Roy F. We Superfund Technical Assistance & Response Team .(May, 1998). . b. The major hazardous substances, pollutants, and/or contaminants that are being released or for which there is threat -of release: Substances Media pH>12 liquids in drums Flammable liquids in drums 2 . Evaluation of the threat to _public health: welfare and the ) environment: a. Federal Agency for Toxic Substances and Disease. Registry: 'Threat No Threat Evaluation x Not Necessary . b. Endangerment to the ecosystem: Threat No Threat Evaluation x Not Necessary T 3 . The Removal Site Evaluation was terminated pursuant to 4 section 300 .410 a of the NCP foie the fol owini reason(s) [CHOOSE THE APPROPRIATE REASON(S) AND DELETE THE REST. IF SITE IS ON THE NPL, SKIP FIRST FOUR CHOICES.] ( ) There is no release. ( j The source is neither a "vessel" nor a "facility" as defined .in section 300.5 of the NCP. ) ( ) The release involves neither a hazardous substance, nor a pollutant or contaminant that may present an imminent and substantial danger to public health or welfare. ( ) The amount, quantity, .or concentration released does not warrant Federal -response. ( ) The release consists of a situation specified in section 300 .400 (b) subject to limitations on response. ( ) A party responsible for the release, or any other person, is providing appropriate response, and on-scene monitoring by the government-Js not required. (X) The Removal Site Evaluation is complete. -3- 4 . As reflected in Section 3 . above, the Removal Site Evaluation was terminated due to its completion and not for other reasons . _ Therefore, the following factors. were considered in determining- the.appropriateness of a Removal Action pursuant to section 300.415 (b) (2) of the NCP.: (X) .Actual or potential exposure to nearby human populations, animals, or the food. chain from hazardous substances or pollutants or contaminants; ( ) Actual or potential contamination of drinking water supplies or sensitive ecosystems; (X) Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or. other'bulk storage containers, that may. pose a threat of release; ( ) High levels of -hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate; ( ) Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate or be released; (X) Threat of fire or explosion; i (X) The availability of- other appropriate. Federal or State response mechanisms to respond to the release; and (X) Other- situations or factors that may pose threats to public health or welfare or the environment-. rr 5 . The existence of the conditions specified in Section 4 . above suggest that a Removal Action under section 300 .415 of the NCP is necessary. 6 . In light of the magnitude of the threat or potential threat to health-, 'welfare, or the environment, the Removal Action should- be undertaken as a: Emergency Time-Critical X Non-.Time.-Critical cc : Dave McIntyre, Chief, SERS I Jane Guy, Salem Planning Department Anthony Guarciariello,. MADEP .-Dennis Gagne, Chief, Technical Support & Site Assessment U.S.. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT I. HEADING DATE: JULY 20, 1998 SUBJECT:- FLYNNTAN SITE - POLREP #1 LOCATION: 70-92 BOSTON STREET, SALEM, MA SITE ID NUMBER: 015Y CERCLIS NUMBER: MA0002333433 OSC: A. HATZOPOULOS, USEPA, OFFICE OF SITE REMEDIATION AND RESTORATION, SECT. II OFFICE PHONE #: 617-573-5759 (OFFICE) ACTION MEMO STATUS: - FUND LEAD INCEPTION DATE: JULY 6, 1998 DEMOBILIZATION DATE: TBD II . BACKGROUND The Site is- located at 7-0-92 Boston Street in Salem, Massachusetts. The Site is approximately 1..90 'acres and is an abandoned leather tanning factory located in a heavily populated residential/commercial area of Salem, Massachusetts. The Site is fenced with locking gates at several entrances of the Site. However, the fence does not preclude unauthorized access. Evidence from -graffitti -and other vandal-ism activities that children and others had been entering the Site.' The closest residential property is less than 100 feet away from the Site. An estimated 1, 000 people reside/work .25 .miles of the .Site. A day care facility "is located .2 miles west of the Site. Within a 1-mile radius there are 5 other schools, one of .which is Salem High School . Most of the windows and doors- of the entire structure are either broken, missing or have been replaced by temporary plywood. The primary threats that will be removed from the Site gpnsist of ignitable and caustic substances in drums/tanks as well as. leaking electrical capacitors and metal tanning residues/dust such as chromium and lead on the floors, drains, settling pits- and exterior grounds. Contaminants found at the site- include but- are not limited to polychlorinated biphenyls (PCBs) , lead and chromium. III . ACTIONS On July 6, . 1998, the ERCS contractor and the START contractor mobilized to the site. To date ERCS has: 1) established security, 2) prepared the Site for the removal action activities i .e. set up utilities .(phones, fax, electricity, water etc) 2 3) cleared and staged the debris. from the manufacturing floor, 4) began the consolidating the . floor and drain waste, 5) categorized and staged -the hazardous materials found in drums/containers, 6) disassembled,staged and containerized all PCB contaminated electrical components, 7) prepared and put out bids for the transportation and disposal of the hazardous materials IV. FINANCIAL The removal -project ceiling defined in the Action Memorandum is $286, 000.00 CEILING. CHARGED BALANCE ERCS $130, 000 $32, 000 $98, 000 EPA $ 70, 000 $11, 000 $59, 000 START $ 50,000 $10,000 $40., 000 CONTINGENCY $ 36, 000 -0- $36, 000 TOTAL - $286,000 $53,000 $233., 000 1 The above cost estimate is based on figures known .to the OSC at the time this POLREP was written. The cost accounting does not necessarily- represent an exact monetary figure which the government may include in any claim for cost recovery. V. FUTURE PLANS ERCS will continue to cnsolidate the contaminants on the floors, drains and pits for transportation and dislbbsal . CASE PENDS �s' UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 2� Y° REGION 1 JOHN F.KENNEDY FEDERAL BUILDING o= BOSTON, MASSACHUSETTS 02203-0001 0 Enforcement Confidential Materials Attached MEMORANDUM DATE: May 26, 1998 SUBJECT: Request for a Removal -Action at the Flynntan Site, Salem, Massachusetts - ACTION MEMORANDUM FROM: At.hanasios Hatzopoulos, On-Scene Coordinator Site Evaluation and s )se Section II THRU: Steven R. Novick, .Chie Site Evaluation and Respo II TO: Patricia L. Meaney, Director Office of Site Remediation and Restoration. . I. -PURPOSE The purpose of .this Action- Memorandum. is to. request and document approval of the proposed removal action at the Flynntan Site ' (the Site) , which- is located at 70-92 Boston Street in Salem, Essex County, Massachusetts: Hazardous substances present in drums and on the floors of the manufacturing building, if not addressed by implementing the response actions selected in this Action MemoranduTff, will continue to pose a threat to human health and .the environment. There are no nationally- significant or precedent-setting issues associated with this Site, and there - has been no use of- the OSC's $50, 000 warrant authority. II._ SITE CONDITIONS AND BACKGROUND CERCLIS Identifier: MA0002333433 SITE Identifier:015Y Category of Removal: Time-Critical Intemet Address(URL)• httpJ/www.epa.gbv . Recycled/Recyclable•Printed with Vegetable ON Based Inks on Recycled Paper(Mlntnum 259E Postconsumer) A. Site Description 1. Removal Site Evaluation In November of 1997, the .City of Salem, Planning Department (the City) referred this Site to the Emergency Planning and Response Branch (EPRB) . The City's concern was that hazardous wastes may have. existed on-Site . Since 1996 the City had repeatedly informed the owner that the City's primary goal is to see the Site environmentally cleaned up and returned to productive use. Furthermore, the City was concerned that portions of the Site were rented -illegally to tenants and other portions of the building. were used by - children as a clubhouse. On December 4, 1997, EPA sent a request for access to the property owner for the purposes of couduc.ting a Preliminary Assessment/Site Investigation (PA/SI) . The owner refused EPA access. Consequently, on March 26, 1998, EPA issued a Unilateral Administrative Order to the property owner, after which access was granted. On April; 14 & 16, 1998, the Emergency Planning and Response Branch (EPRB) conducted a PA/SI which- included sampling of drums, soils, liquid samples from pits, 1 interior floors and drains of the manufacturing building. Based on this investigation, EPA documented that ,several of the drums are flammable and several other drums contain caustic. substances. Sampling analysis also revealed that the. floors and settling pits- from . the structure on the_ Site are contaminated with chromium- as well polychlorinated biphenyls (PCBs) . In addition, lead contaminated soil was detected under a pile of 'animal hides on the exterior grounds sof the Site adjacent to the. structure. The PA/SI was concluded, -and a removal action was recommended in the closure memorandum dated April 28, 1998, to remove the contaminated substances . The results of the PA/SI are documented in the report entitled Removal Program Preliminary- Assessment -Site . Investigation for the FlyLintan Site -Salem Massachusetts, dated May, 1998-. 2 . Physical Location The Site is located at 70-92- Boston Street- in Salem; Essex county; Massachusetts. The Site .is further defined in Book 13751, Page 323, Essex County Registry of Deeds, Salem, Massachusetts. The approximate 2 latitude .and longitude of the Site are 4203i' 12"N and 70054138"W. The Site is bordered to the north by Goodhue and Beaver Streets; to the south by Boston Street; to the west by a residential/commercial area; and to the east by the intersection of Boston Street and Goodhue Street. Private residences are located within 100 feet of the Site boundaries. Land use in the immediate vicinity is 'mixed residential/commercial . The Site is situated less than half of a mile from the North River Canal which flows into the Salem Sound. 3 . Site Characteristics The Site is approximately 1. 9 acres and it is fenced. However, evidence of .graffit�i and other vandalism activities. -clearly indicates that trespassing is a common occurrence . A large wood/brick . structure and ' several parking areas are located within the Site. . This structure is made up -of two buildings which are joined. One portion is a 4-story wood/metal frame building and was used for the leather tanning operations (building-a) . The building's exterior is covered by asbestos shingles that are falling off. . The interior has sustained 2 fires. The rest of the structure is made up of a newer 2-story, brick sided building that is in better structural condition (building-b) . Building-a is not occupied. However, building-b on the day of the PA/SI, was illegally occupied by two tenants (a construction company and a storage/shipping. business) . Most of the windows and' doors of the entire structure are either broken, missing or have been replaced by temporary plywood. The Site has .three parking areas that are adjacent to the structure. Historical information indicates that the Site . contains 4-6 underground storage tanks , possibly containing heating oil . rr The PA/SI revealed that approximately 21, 55-gallon drums are located- inside the Site ' s structure. Most were on the first floor of building-a, and had various labels such as : flammable, corrosive, formic acid, degreasing solvent, chrome complex in isopranol, SYN FOG insecticide, and sodium acetate.. * The first floor and its drains are littered with powders and tanning process residues. There is an approximately 101x15 ' settling pit that is filled with 51 - of liquid and about 1 ' of sludge. The rest of the floors are littered with boxes, paper, and trash from vandalism and other trespassing activities. Building-b contains another pit that is filled with liquid and sludge like -material . 3 The exterior grounds of the Site are paved 'except for one small area that is adjacent to south portion of building-a. This area showed signs of stressed vegetation, soil. discoloration and also had a pile of decomposing animal hides. During the day of the PA/SI the City's Fire and Building Departments visited and inspected the Site.- After their inspection the Building Department determined the entire structure unsound for habitation and condemned it .by posting signs on every entrance to the Site. 4 . Release or Threatened Release. into the Environment of a Hazardous Substance or Pollutant or Contaminant The following hazardous substances as defined in CFR 261.2 and 302 . 4 as seen- in Table 1 were detected in samples collected during'-the PA/.SI conducted at :the Site. The concentrations listed are matched to the EPA list of hazardous substances and the Massachusetts Department of Environmental Protection' s (MADEP) .Soil category standards . They are the highest ones reported for that particular waste stream. TABLE 1 �. MEDIA HAZARDOUS CONCENTRATION MADEP SOIL EPA SUBSTANCE IN DRY WEIGHT CATEGORY CFR ppm STANDARDS Min sludge from lead. 2,630 300-600 vats w residues/ chromium 23,000 1,000-5,000 dirt on floors& arsenic 26.1 30 drains drums ignitables 190 <60°C corrosive >13 pH >_12.5 soil lead 1,450 300-600 4 5. NPL Status The Site As currently not listed on the National Priorities' List. The Site is not, . at this time, being evaluated by the Agency for Toxic Substances and Disease Registry (ATSDR) . B. Other Actions to Date 1. Previous Actions From 1996, the City of Salem has been in contact with the owner regarding the cleaning and possible redevelopment of the Site. In October 1997, the City's Building. Department', due- to a complaint received by the E • Salem neighborhood Improvement Task Force, `had . conducted a building inspection of the Site. The City on' October .15, 1997, notified the owner .of illegal rental of the property. 2 . Current Actions This will be EPAs first removal action conducted at the Site. C. State and Local Authorities' Roles. The City of Salem has assisted EPA in. collecting background information. The MADEP has been contacted by EPA and is expected to assist EPA by providing _ . . technical comments on the proposed removal action. and generating a list of regulations for consideration as applicable or relevant and appropriate. Neither state nor local authorities have the resources to remove the hazardous substances abandoned at the Site. III. THREATS TO PUBLIC HEALTH OR WELFARE OR THE ENVIRONMENT, AND STATUTORY AND REGULATORY AUTHORITIES A. 'Threats to. Public Health or Welfare There is clear. evidence from graffiti and other vandalism activities that children and others are entering -the Site. The area around the Site is heavily populated both residentially and commercially. The closest residential property is less than 100 feet away from the Site. An estimated 1, 000 people reside/work .25 miles of the Site. A 5 day care facility is located .2 miles west of the Site. Within a 1-mile radius there are 5 other schools, one of l which is Salem High School . The g primary human receptors of concern are children who may enter the Site, and come into Contact with the contaminants, and others who work and/or engage in recreational activities on the adjacent properties. Based on Site conditions and information available on the hazardous substances present, the Site poses the following threats to public health or welfare. 40 CFR 300 .415 (b) (2) (i) Actual or potential exposure to nearby human populations, animals, or the food chain from hazardous substances or pollutants or contaminants Chromium, PCB and lead contamination on the floors and settling pits. of building-a, pose a direct contact threat to individuals who. may enter. the Site . These constituents may also escape to the exterior by means of open pathways. Corrosive and ignitable substances in building-a pose a direct contact threat to children or trespassers entering the Site 40 CFR 300.415 (b) (2) (iii) Hazardous substances or ) pollutants or contaminants in drums, barrels, tanks, or other bulk storage. containers, that may pose a threat of release Ignitable and corrosive substances in drums may pose a direct contact threat to 'individuals entering the Site. 40. CFR 300.415 (b) (2) (iv) High. levels of hazardous- substances or- pollutants or contaminants in soils largely at or near the surface, that may migxwte Lead on surface soils may migrate via wind or surface runoff onto adjacent properties. The Site is adjacent to private residential properties and less than .5 miles away from the North River Canal which flows into the Salem Sound. The proximity of the contaminated areas of the Site may increase this threat of migration to the adjacent properties . 40 CFR 300 .415 (b) (2). (vi) Threat of fire or explosion Ignitable hazardous substances in drums exist at the Site. The structure has clearly been vandalized by .trespassers. Building-a' s floors are covered with 1 s paper. and other trash from vandalism and other trespassing activities .. These conditions pose a threat of fire or explosion. If a fire does occur in the building, the substances present would be released in the atmosphere. 40 CFR 300 .415 (b) (2) (vii) The availability of, other appropriate federal or state response mechanisms to respond to the release Neither state not local authorities have the resources to address the contaminated surface soils at the Site. Chromium-Children .who come in contact with Chromium contamination. may be at increased. risk of developing noncancerous health effects possibly including skin irritation and contact dermatitis. Inhalation of airborne dust particles 'is a possible route of exposure. PCBs- Exposure . to PCBs pose a variety .of health impacts . PCBs are classified as a B2 probable human carcinogen, are liver toxins and possibly cause peripheral neuropathy (nerve disease in extremities) . PCBs- have been found to cause rashes (edema of face and hands, simple erythematous eruptions with pruritus, acute eczematous contact dermatitis, and chloracne) subcutaneous edema .and. hyperp.igmentation of skin and mucous membranes.; excessive secretions from the eyelids (hyperactive Meibomian glands; conjunctivitis;. and edema of the eyelids) ; formation of keratin cysts in and hyperplasia of epithelial layer of .hair follicles; increase in liver size (hepatic hypertrophy) ; decreases in. number of red blood cells and hemoglobin; serum - hyperlipidemia; and increases in numbers of white blood cells ..in the body (leukocytosis) . w Various studies have found that exposure to PCBs may cause :irregular menstrual cycles, and increased PCB serum levels may cause pathological pregnancies (toxemia of ' pregnancy, and abortions) stillbirths, underweight births, etc . Mother's milk. contaminated with PCB ' s appears to be a source of exposure for infants. Developmental abnormalities have been observed in PCB-intoxicated infants. LEAD- Lead. is a probable human carcinogen, 'since it has - been proven to' cause kidney cancer in 'laboratory animals . Exposure to high levels -of lead can cause - brain and kidney damage. Lead exposure may increase blood pressure in middle-aged men and has been known to damage parts of .the male. reproductive system. Lead is / also well known for its effects on young children, who are more likely to be exposed to lead due to hand-to- mouth activity. . In children, lead exposure has been shown to decrease intelligence (IQ) scores, slow their growth, and cause hearing problems . If a pregnant .woman is exposed to lead, it". can be carried to the unborn child and cause premature birth, low birth weight, or even abortion. ARSENIC- Inorganic arsenic is a human poison. The DHHS has determined that arsenic is a known carcinogen. Breathing inorganic arsenic increases the risk of lung cancer. .Ingesting inorganic arsenic increases the risk of skin cancer and tumors of the bladder, kidney, liver and lung. B. Threats to the Environment ' The Site is situated less than one half of a mile from the North River Canal which flows into the Salem Sound. Potential receptors of the contaminants may include fish and other organisms such as shell fish dependent upon the North River Canal and Salem Sound. Portions of the river and sound are used for recreational activities such as swimming and recreational fishing. The Site poses the following threats to the environment: 4.0 CFR 300.415 (b) (2) (i) Actual or potential exposure to nearby human populations, animals, or the food chain from hazardous substances or pollutants or contaminants" PCBs, lead. and chromium contamination at the Site may pose a contact threat to ecological receptorsyfand may enter- the food chain. 40 CFR 300 .4.15 (b) (2) (i.v) "High levels of hazardous substances or pollutants or contaminants in soils largely at' or near the surface, that may migrate] .. Lead contamination -in surface soils may migrate via surface runoff. The, proximity .of the contaminated areas to the surface waters may increase this threat of migration 40. CFR 300.415.(b) (2) (vii) The availability of other appropriate. federal ,or state response mechanisms to respond to the release l a. 8 '` Neither state nor local authorities have the resources, toaddress the contaminated surface soils at the Site. IV. ENDANGERMENT DETERMINATION Actual or threatened releases of hazardous substances at or from this Site, if not addressed -by implementing the response action selected in this Action Memorandum, may present an imminent- and substantial endangerment to public health, or welfare, or the environment. V. PROPOSED ACTIONS AND ESTIMATED COSTS A. Proposed Actions 1. Proposed Action Description The actions. required to mitigate the threats outlined . herein, are given below. . At this time, indications are that the PRPs will not perform this work. The proposed actions will protect public health, welfare and the environment by preventing people or animals to come into contact with the contaminated areas of the Site. The proposed actions are as follows: 1) take measures to prevent unauthorized access to. -the Site. These measures may include repairing or instal Iing additional security fencing and/or providing 24 hour security during the removal activities; 2) conduct additional sampling of interior and .exterior floor surfaces -as well as drums, pails and settling pits;. 3} the hazardous waste contamination on the fl6or surfaces will be swept up, consolidated and staged. The -content of drums, vats, containers and settling pits, will. be categorized, containerized, and staged. The exterior lead contaminated soil will be collected and staged. All waste streams will be manifested and shipped off-site for appropriate re-use or disposal- at an-EPA-approved disposal facility. 2. Contribution to Remedial Performance Performing this removal action will contribute to remedial. performance and. protect public health and the environment by eliminating the potential for exposure to contaminated areas of the Site and preventing the 9 further release of hazardous substances to- the 1 environment. 3 . . Applicable or Relevant and Appropriate Regulations The cleanup standards, standards of control, and- other —substantive requirements that have been identified to- date, are listed below, and are applicable within the confines -of EPA Publication 540/P-91/011, "Superfund Removal Procedures : Guidance on the Consideration of ARARs During Removal Actions. " FEDERAL; .ACTION-SPECIFIC 29 CFR Parts 1910 1926 and 1904 : OSHA Health 'and Safety Regulations '40 CFR Part 262 Standards Applicable to Generators of Hazardous Waste: Subpart B - The Manifest 262 .20 : General requirements for manifesting 262 .21 : Acquisition of manifests 262.22 : Number of copies of manifests 262 .23 : Use of the manifest ) SUhRart C Pre-Transport Requirements 262 .30 :Packaging 262 .31 : .Labeling 262.32 : Marking Subpart D - Recordkee]aing and Re ortin 262.40 :- Recordkeeping 40 CFR Part 264 Standards for Owners and Operators of Hazardous waste Treatment-, Storage, and. Dispogal Facilities: Subpart I - Use and Management of Containers 264 .171 : Condition of containers 264 .172 : Compatibility of waste with containers 264 .173 : Management of containers .264 .174 : -Inspections of containers- 264 .177 : Special requirements for incompatible wastes 40 CFR Part 264 Hazardous Waste Regulations - RCRA Subtitle C: 1 J 10 268-270 Hazardous and Solid Waste Amendments Land Disposal Restrictions Rule 40 CFR Part 300 . 440 Procedures for Planning and Implementing Off-Site Response Actions (Off-Site Rule) 40 CFR Part . 761.60 and Parts 761 .202-218 : TSCA requirements for disposal of PBS _ 49 CFR Parts 171-179 : Department of .Transportation Regulations for Transport of Hazardous Materials The OSC has requested that the Massachusetts Department of Environmental Protection identify State ARARS for consideration by the. OSC. B-. Estimated Costs and Schedule The OSC has prepared an independent government estimate of the cost associated with carrying out the proposed actions. outlined above. A summary of this estimate is given below. The action is anticipated to be complete within eight months of its commencement . EXTRAMURAL COSTS: ERCS COSTS: Labor & Equipment $ 75, 000 Lab Analysis $ 5., 000 Transportation & Disposal $ 50, 000 ERCS COST TOTAL $ -.130,.000 START COSTS: $ 50, 000 K SUBTOTAL, EXTRAMURAL COSTS $ 180, 000 EXTRA COSTS CONTINGENCY (20a of Subtotal, Extramural costs) + 36, 000 TOTAL EXTRAMURAL COSTS $ 216, 000 INTRAMURAL. COSTS Labor Expenses, Subsistence .$ 70, 000 TOTAL, REMOVAL PROJECT- CEILING $ 286, 0.0 0 11 VI. EXPECTED- CHANGE IN THE SITUATION SHOULD ACTION BE DELAYED OR NOT TAKEN In the absence of the removal action described herein, conditions at the Site can be expected. to remain unaddressed, and threats associated with the abandoned hazardous substances will persist . VII. OUTSTANDING POLICY ISSUES _There are no known policy issues that are outstanding with respect to this removal action. VIII. ENFORCEMENT ATTACHED TO THIS DOCUMENT - FOR INTERNAL DISTRIBUTION ONLY IX. RECOMMENDATION This decision document- represents the selected removal action for the Flynntan Site in Salem, Massachusetts, developed in accordance with CERCLA, as amended, and not inconsistent with the National Contingency Plan (NCP) . The basis for this decision will be documented in the Administrative Record to be established for this Site. Conditions at the Site meet the NCP Section 300 .415 (b) (2) criteria for a removal. due to the following: "Actual or potential exposure to nearby human populations, animals, or the food chain from hazardous substances or pollutants or contaminants" [§300.415 (b) (2) (i) ] , W "Threat of fire or explosion" [§300.415 (b) (2) (vi) ] "Hazardous substances or pollutants or contaminants .in drums, barrels, tanks, or other bulk storage containers, that ,may pose a threat of release" [§300.4.15 (b) (2) (iii) ) . "Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate- or be released" [§300 .415 (b) (2) (v) ] "The availability of other .appropriate. federal or state. response mechanisms to respond to the release (5300 .415 (b) (2) (vii) ] . 12 I recommend you approve $ 286, 000 to initiate the removal action proposed above, of which - as much as. $ 156,000 is from the EPA removal allowance. . Expenditure will be limited to the categories of START and Intramural for the purpose of monitoring compliance with an Administrative.Order, should the' PRP' perform the cleanup. APPROVAL _ , DATE: ��(/�; D.ISAPPROVAL- DATE 4 13 tEo sr.��s- �' UNITED STATES ENVIRONMENTAL PROTECTION AGENCY ?� YV W REGION 1 o JOHN F.KENNEDY FEDERAL BUILDING 'yF BOSTON,MASSACHUSETTS 02203-0001 URGENT LEGAL MATTER -- PROMPT REPLY NECESSARY VIA FEDERAL EXPRESS -_OVERNIGHT DELIVERY 5/4,/98 Salem Realty, LLC c/o Jan Exman, Manager 66 Old Blue Hill Road Durham, Connecticut 064.22 Re : NOTICE OF POTENTIAL LIABILITY AND INVITATION TO PERFORM OR FINANCE PROPOSED CLEANUP ACTIVITIES: Flynntan Site Dear Mr. Exman: This letter serves to notify Salem Realty, LLC of potential liability regarding the Flynntan Site, Salem, Massachusetts ( "Site" ) , as defined by Section 107 (a) of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980, as amended (rrCERCLA") , 42 U.S.C. § 9607 (a) . This letter .also - notifies Salem Realty, LLC of forthcoming removal activities at the Site .which Salem Realty, LLC is invited to perform or finance and which you may be ordered to perform at a later date. NOTICE OF POTENTIAL LIABILITY The United States Environmental Protection Agency ("EPA." ) has documented the release or threatened release -of hazardous substances or pollutants or contaminants at the Site, which is located at 70- -92 Boston Street, Salem, Massachusetts.. The Site is further defined in Book 13751, -Page 323, Essex County Registry of Deeds, in Salem, Massachusetts. K Hazardous substances involved in the release or threat of release .at the Site include, but are not limited to, flammable and caustic substances. EPA has spent- or is considering spending public funds on actions to investigate and -control such releases . or threatened releases at the Site. ' Unless a potentially , -responsible party ("PRP") or parties commit to properly performing or financing such actions, EPA may perform these actions pursuant to Section 104- of CERCLA, 42 U.S.C. § 9604 . Under Sections 106 (a) and 107 (a) of CERCLA, 42 U.S.C_ §§ 9606 (a.) and 9607 (a) , Section 7003 o.f the- Resource Conservation and .Recovery Act ( "RCRA") , 42 U.S .C. §- 69:7:3, and other laws, liable parties may be obligated to implement response actions deemed necessary_ by EPA .to protect public: health, welfare, or the environment and may be liable for all costs incurred by the Intemet Address(URL)+ http://www.epa.gov Recycled/Recyclable.Printed with Vegetable Of Based Inks on Recycled Paper(MlnUnum 25%Postconsumeh Government in responding to- any release or threatened release at 1 the Site. Such actions and costs may include, .but are not limited to, expenditures for investigations, planning, response., oversight, and enforcement activities. Responsible parties under CERCLA include current and former owners and operators of the Site, persons who arranged for disposal or treatment of hazardous substances found at the Site (often called "generators" ) , and persons who accepted hazardous substances for transport to the Site (often called "transporters") . EPA has evaluated evidence- gathered during investigations of the Site. ,' Based on this evidence EPA has information indicatin that Salem Rea ty, LLC is a potentially r.esl2onsible 12arty, under Section 107.(a) of CERCLA with respect to the Site. Specifically, EPA has reason- to believe that Salem Realty, LLC is the current owner/operator of the Site. By this letter, EPA notifies Salem Realty, LLC of its potential liability and urges Salem Realty, LLC to voluntarily perform or finance those response activities that EPA determines are necessary at the Site_ OUTLINE OF S.ITE .RESPONSE ACTIVITIES In accordance with CERCLA and -other authorities, EPA has undertaken certain actions and incurred. certain costs in response to conditions at the Site. These response actions have included conducting site assessments as well as other investigations which have revealed the presence .of hazardous substances at the Site. i Due . to the presence of hazardous substances at. the Site, - and in light of other conditions, EPA has determined that there may be an imminent and subs tantialmendangerment to public health, welfare, or the environment.. In response, EPA is plannincr, to ' conduct the following immediate removal activities at the Site : .1) overpack, stage, manifest and properly dispose of th%,. drums and other containers present at several locations mwithin the Site boundaries, at an EPA-approved disposal facility; and, 2) take other appropriate actions based on EPA's . sampling results. INVITATION TO PERFORM SITE RESPONSE ACTIVITIES Before EPA spends additional public .funds to undertake a removal action at the Site, EPA urges Salem Realty, LLC to voluntarily perform or finance the removal. activities outlined above . Any such work performed by you in your capacity as a PRP must be conducted pursuant to an administrative order and an EPA- approved workplan as authorized by Section 106(a) of CERCLA, 42 U.S..C. § 9606 (a) . Prior to final issuance of such an. order, a draft order will be sent 'to you or your representative for review and comment. Enclosed herewith. is a copy of a- summary of -a- generic Scope of Work. This document ' should provide 'you with an understanding of the types of plans and activities typically ``� required by such an order. Be advised that even if Salem Realty, LLC does not - indicate a willingness to perform or finance necessary response actions, EPA may order you to undertake such actions under Section 106 of CERCLA, 42 U.S.C. § 9606. Failure to comply with a Section 106 (a) administrative order may result in a fine of up to $27, 500 per. day under Section 106(b) or imposition of treble damages under Section 107 (c) (3) of CERCLA. Further, you may be held liable _under Section 107 (a) - for the cost of the response activities EPA performs at the Site and for any damages to natural resources. In addition, by- :virtue of Section 113 ' of CERCLA, 42 U.S .C. § 9613, other PRPs who agree to perform the necessary response action may seek contribution protection, PRP RESPONSE AND EPA CONTACT You should contact EPA within- ten (10) business, days after receipt of this letter to indicate your willingness to perform or finance the response activities outlined above. If EPA does .not receive a response within that time, EPA will assume that you do not wish. to negotiate a resolution of your liabilities in connection with the response and that you have declined any involvement in performing response activities.- Be advised, however,- that liability under CERCLA is- joint and- several; therefore, each PRP is potentially liable for undertaking all response, actions or reimbursing the Government for the entire amount of its response costs. Please -provide the name, address, and telephone number of a designated contact for future -communications. Your written response, including any technical comments or questions concerning the proposed response activities, should be directed to the EPA On-Scene Coordinator (OSC) for the Site: Athanasios Hatzopoulos U.S. Environmental Protection Agency �- Site Evaluation & Response Section II JFK Federal Building - Mail Code HBR Boston, Massachusetts 02203. Legal questions and all communications from counsel should be directed to: Cynthia A. Lewis U.S . Environmental Protection Agency Office of Environmental Stewardship JFK Federal Building. -- SES Boston, Massachusetts 02203 (617) -565-3285 DECISION NOT TO USE SPECIAL NOTICE under Section 122 (e) of CERCLA, 42 U.S.C. § 9622 (e) , EPA has the discretionary authority to invoke special notice procedures to formally negotiate the terms of an agreement between EPA and PRPs to conduct or finance response activities. The- use of special notice procedures triggers a -moratorium on certain EPA - activities. at the Site while formal negotiations between EPA and the PRPs are conducted. Due. to the exigencies posed by "conditions present at the Site, removal activities must be conducted as expeditiously as possible . - EPA has therefore decided not to invoke the Section 122 (e) special notice procedures with respect. to CERCLA removal actions at this Site. . Nonetheless, EPA is willing to discuss settlement opportunities without invoking a moratorium, but will initiate the response action as planned if such discussions do not lead to settlement expeditiously. ADMINISTRATIVE RECORD Pursuant to Section 113 (k) of CERCLA, 42 U.S.C. § 9613 (k) , EPA will -establish an administrative record .containing documents that form the basis of EPA' s decision on the selection of response actions for the Site. The administrative record files may be inspected and comments may be submitted by contacting the OSC for the Site. The Administrative Record Files with corresponding index. should be' available for inspection at a repository. -near the Site within sixty (60) days of initiation of on-site removal activities . SITE ACTIVITY OUTSIDE EPA ACTIONS If Salem Realty, LLC is already involved in discussions with . state or other local authorities or involved in "a lawsuPt regarding this Site, Salem Realty; LLC' should continue such activities. as .it sees fit. This letter is not intended to advise or direct you to restrict or discontinue any such activities . However, Salem Realty, LLC is advised to report the status of any such discussions or actions in its response to this letter and to provide a copy of its response to any other parties involved in" those discussions or actions. CONSENT TO ACCESS EPA requests access to your property, the Site, to perform or oversee the response actions discussed above. This request is .enclosed. PURPOSE AND USE OF THIS NOTICE LETTER The. factual and legal discussions contained in this letter are intended solely to provide. notice and information. Such discussions are not intended to be, and. cannot be, relied upon as " EPA' s final position on any matter set forth herein. Due to the seriousness of the environmental and legal problems posed by conditions at the Site, EPA urges that you give immediate attention and provide a prompt response to this letter. By copy of this letter EPA is notifying the Commonwealth of Massachusetts and the Natural Resources Trustees of EPA' s intent to perform, or to enter into negotiations for the performance or financing .of, _ response actions at the Site. Thank you for your attention to this matter. 4 Sinc rel , Dennisses Val es, Acting Chief Emergency Planning and Response Branch Enclosures cc: Athanasios Hatzopoulos, EPA On--Scene Coordinator - OSRR Sharon C. Fennelly, EPA Enforcement Coordinator - OSRR Holly Inglis, EPA Administrative Records Coordinator - OSRR Jane Guy, Salem Planning Department . Anthony Guarciariello, MADEP Andrew Raddant, Acting Environmental Officer, U.S. Department of the Interior .Ken Finkelstein, National Oceanic and Atmospheric Administration -yf SUMMARY OF GENERIC SCOPE OF WORK Phis summary of the Generic .Scope of Work is provided for informational purposes only. More detailed provisions will be set forth in the site- specific Scope of Work. Provisions may vary from site to site.. \ 4hen EPA determines that a Potentially Responsible Party (PRP) has the ability �o promptly and properly prevent, mitigate, or eliminate -the threats posed by .iazardous substances at the Site.,.. EPA may issue an Administrative Order (Order) to such party (the Respondent) with an attached Scope of Work (SOW). . Phe Order and SOW, among other things, compel the Respondent to develop a plan :o clean the Site . The components of the plan (also called a "deliverable") nust be submitted to EPA for approval before implementation. Detailed h Lnstructions for generating eac component shall be provided in the SOW. The Man shall . consist of the components listed below. L) Site Security - The Respondent shall provide on-site security service. Site security shall be maintained until EPA determines- the threats posed by conditions at the -Site are eliminated or substantially mitigated. �) Notification of Contractor Selection - The Respondent shall notify EPA of :he proposed. cleanup contractor selected to perform work required under the )rder.. 3) Site-Specific Health and Safety Plan (HASP) - The Respondent shall develop and implement a HASP for all activities to be conducted at the..Site. The HASP. 3hall .be developed to protect all on-site personnel and must comply with all applicable health and safety regulations. ) 6) Quality Assurance Plan (QAP). - The Respondent shall develop a QAP to be itilized in conducting all field and laboratory. analysis. The QAP shall insure that analytical results generated are of known .qua�ity. 3) Site Assessment Plan (SAP) - The Respondent shall develop a SAP specifying :he overall strategy of the field investigative work necessary to characterize Ate contamination. ;) Site Assessment - A Site Assessment shall be conducted following EPA ,ipproval of the' SAP_ rr 7) Site Assessment Report and Cleanup Plan (SAR/CP) - Following completion of :he Site Assessment, the Respondent shall develop a SAR/CP . that summarizes the Site Assessment and proposes cleanup methods necessary' to substantially Litigate and/or eliminate the threats posed by hazardous substances present at :he Site. 3) Site Cleanup - The Site Cleanup shall be conducted according to the EPA approved Cleanup Plan. 3) Completion of Work Report (CWR) - Upon completion of the Site Cleanup, the tespondent shall submit a CWR summarizing the work performed under the Order and SOW and outlining any remaining contamination. kt any time prior to or after the completion of the work specified in this .3 EPA may determine that -additional tasks 'are necessary in order to achie <�.- -he objectives of the Order, the SOW and CERCLA. Administrative Record File Available for the Flynntan Site Removal Action The U.S. Environmental Protection Agency(EPA) announces that the Administrative Record File for the removal action at the Flynntan Site located in Salem, Massachusetts is available for review. EPA seeks to inform the public of the availability of the Administrative Record File and to encourage the public to review and comment on it. The proposed actions will protect public health, welfare, and the environment by preventing people or animals from coming into contact with the contaminated areas of the.site. The proposed actions are as follows: 1)Taking measures to prevent unauthorized access to the site, including repairing or installing additional security fencing and/or providing 24-hour security during.removal activities;2) conducting.additional sampling of interior and exterior floor surfaces, and of drums,pails,and settling pits; 3)sweeping up, consolidating,-and staging hazardous waste contamination found on the floor surfaces;4) categorizing, containerizing, and staging the contents of drums,vats, containers, and settling pits; and 5)collecting and staging exterior lead-contaminated soil. Also, all wastestreams will be manifested and shipped-off site for PP P _ a ro riate reuse or disposal at EPA-approved disposal facilities. - The Administrative Record File'is the collection of documents.that formed the basis for the selection of a removal action.at the site. Documents in the Administrative Record File include the Preliminary Assessment/Site Investigation Report and the Action Memorandum. The Administrative Record File is available for review at the: U.S.-EPA Records Center, 90 Canal Street, First Floor, Boston, Massachusetts, 02114, (617) 573-5729, by appointment. Salem Public Libr ary, 370 Essex Street, Salem, Massachusetts, 01970, (978) 744- 0860. Written comments on the Administrative.Record File should be sent to: On-Scene Coordinator Athanasios Hatzopoulos,U.S. EPA,Region I,MailCode HBR,John F. Kennedy Federal Building, Boston, Massachusetts, 02203. Comments should be sent to the On-Scene Coord1mator within 30, .days of this announcement. i CHRONOLOGICAL SUMMARY REPORT FOR THE FLYNNTAN SITE SALEK MASSACHUSETTS 22 June-thr-augt 2-7—- Prepared for: U.S. Environmental Protection Agency Region I Emergency Planning and Response Branch John F. Kennedy Federal Building Boston,MA 02203, CONTRACT NO. 68-W5-0009 TDD NO. 98-06-0013B PCS NO. 5671 DC NO. R-1674 Submitted by: Roy F. Weston, Inc. Superfund Technical Assessment and Response Team 217 Middlesex Turnpike Burlington, MA 01803 December 1998 TABLE OF CONTENTS 1.0 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... . . . . . . . . . . . . . . . 1 2.0 SITE CONDITIONS AND BACKGROUND . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . 1 2.1 Site Location and Description . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . 1 2.2 Site History/Previous Actions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2.3 EPA Removal Program Preliminary Assessment/Site Investigation . . . . . . . . . . . 2 3.0 SUMMARY OF FEDERAL RESPONSE ACTIONS. . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 3.1 Mobilization and Site Preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 3.2 Trenches and Pits . . . . . . . . . . . . . . . . . . _. . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3.3 Drums and Containers . . . ... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 3.4 Electrical Capacitors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 3.5 Interior Extent-of-Contamination Sampling Survey . . . . . . . . . . . . . . . . . . . . . . . 6 3.6 Aboveground and Underground Storage Tanks . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 3.6.1 Aboveground Storage Tanks. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 3.6.2 Underground Storage Tanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 3.7 Lead-and Chromium-Contaminated Surface Soil . . . . . . . . . . . . . . . . _. . . . . . 6 3.8 Automotive Batteries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 3.9 Leather Hides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .... . . . . . . . . . . . 7 3.10 Contaminated Personal Protective Equipment . . . . . ... . . . . . . . . . . . . . . . . . . . . 7 3.11 Site Shutdown Activities and Demobilization . . .. . . . . . . . . . . . . . . . . . . . . . . . . 7 ii LIST OF APPENDICES Appendix A Site Location Map (Figure 1) Appendix B Site Diagram(Figure 2) Appendix C Sample Location Diagram(Figure 3) Appendix D On-site Metals Screening Report Appendix E Photodocumentation Log Appendix F Metals Analytical Data Appendix G Semivolatile Organic Compounds Analytical Data Appendix H Chain-of-Custody Documentation Appendix I Manifest/Bill of Lading Log Appendix J Manifests/Bills of Lading Appendix K Polychlorinated Biphenyls Analytical Data Appendix L Asbestos Analytical Data iii 1.0 INTRODUCTION 1 The Flynntan site (the site) is located at 70 - 92 Boston Street in Salem, Essex County, Massachusetts (See Appendix A - Site Location Map, Figure 1). The site consists of an approximately 1.89-acre property located on the northern side of Boston Street in a mixed residential/commercial'area in the western portion of Salem. The North River Canal,considered to be a sensitive ecosystem,is located approximately 0.5 miles north of the site. The Endicott School, a daycare center with an enrollment of approximately 200 children, is located approximately 0.2 miles west of the site. The site was referred to the U.S. Environmental Protection Agency (EPA) by the City of Salem Planning Department. On 14, 16, and 17 April 1998, EPA and personnel from the Roy F. Weston, Inc.,Region I Superfund Technical Assessment and Response Team(START)conducted a Removal Program Preliminary Assessment/Site Investigation(PA/SI)at the site. Laboratory analytical results of samples collected from drums, capacitors, surface soils, sludges, and free liquids indicated elevated concentrations of lead, chromium, and polychlorinated biphenyls(PCBs), and low levels of volatile organic compounds(VOCs)and semivolatile organic compounds(SVOCs). Laboratory results for samples analyzed for pH and flashpoint indicated a pH range of 3.30 to >13 and flashpoints ranging from 19 to 55 degrees Celsius. EPA subsequently determined that.a.removal action was warranted based on the substantial threat of release to the environment,and the imminent threat to public health and welfare presented by the hazardous substances at the site. 2.0 SITE CONDITIONS AND BACKGROUND 1 2.1 Site Location and Description The site is located at 70 - 92 Boston Street in Salem, Essex County, Massachusetts, at latitude 42" 31' 11.8" North and longitude 70' 54' 37.9" West. The site is located in a mixed residential/commercial zone-and is bordered to the north by Goodhue Street; to the east by the intersection of Boston Road/Goodhue Street; to the south by Boston Street; and to the west by Beaver Street. There are four buildings located on the 1.89-acre site (See Appendix B - Site Diagram, Figure 2). The tannery building consists of one four-story wood and metal frame building that has sustained two fires; one two-story brick building, and two storage buildings constructed as additions to the original two buildings. 2.2 Site History/Previous Actions Flynntan was an operational tannery from 1920 through 1988,during which time the facility manufactured lamb-skin products. In 1988,the site was abandoned. The current owner of the site is Mr. Jan Exman. The City of Salem alleges that portions of the site were being rented by Mr. Exman to.tenants illegally(without certificates of occupancy). On 16 April 1988, signs were posted on every entrance to the site buildings by the City of Salem stating that the site buildings are structurally unsound for habitation. An open concrete pit,located in.the parking area adjacent to the southwest portion of the-buildings, was sealed on 16 April 1998- by the City of Salem. The EPA Emergency Planning and Response Branch(EPRB)received a request for assistance from the City of Salem Planning Department to determine if removal activities.were warranted at the site. On 14, 16,and 17 April 1998,EPA and START personnel conducted a Removal Program PA/SI at the site(see Section 2.3). . 2.3 EPA Removal Program Preliminary Assessment/Site Investigation On 14, 16, and 17 April 1998, EPA and START personnel conducted a Removal Program PA/SI at the site. Chief Charles Latulippe of the City of Salem Fire Department was also present. During the PA/SI, observations were made of evidence of trespassing, including extensive graffiti throughout the building interior and exterior, as well as several broken windows and doors. These observations were made even though the site was surrounded by a chain-link fence with locked gates. Indications of the presence of hazardous materials within the site buildings included the presence of at least 21 drums, some of which were labeled as follows:"flammable","corrosive","formic acid","degreasing solvent","chrome complex in isopropanol", "SYN FOG insecticide", and "sodium acetate". In addition, at least 15 capacitors suspected ofcontaining PCBs,as well as.numerous small containers,were observed throughout the buildings. An open concrete pit was observed in the parking area adjacent to the southwest portion of the buildings and was sealed on 16 April 1998 by City of Salem. Most of the area outside the site buildings was paved except for a small area north of an area which allegedly contain underground storage tanks (USTs). The unpaved area was noted to contain stressed vegetation and limited areas of animal hides adjacent to the southern external wall of the site building. During the PA/SI,the following samples were collected: 11 drum samples(D-001 through D-011) which were analyzed for metals, pH, flashpoint, SVOCs, and VfDCs; two.-soil samples(C-01 and C-02)which were analyzed for PCBs; 10 soil samples(S-001 through S- 010)which were analyzed for metals; and three pit samples,two liquid(T-001A and T-03) and one sludge(T-001B) which were analyzed for metals. Samples S-001 through S-010, T-001 A,T-001 B,and T-03 were analyzed-at R£C-RA Lab=NetChicagcrlocated-in University Park, IL. Samples D-001 through'D-011, C-01 and C-02 were analyzed at the EPA New England Regional Laboratory(NERL) located in Lexington,MA. Laboratory analytical results of the samples collected during the PA/SI indicated that the highest concentrations of chromium were detected in sludges located within trenches and pits inside the site buildings, as well as at one surface soil sample located adjacent to the southwest portion of the site buildings. The highest concentrations of lead were detected at one location on the floor of the building, as well as at one exterior soil sample location. PCBs (Aroclor 1254) were detected in one sample located on a building floor adjacent to capacitors. The maximum concentrations of all substances detected in samples collected during the-PA/SI were as follows: aluminum (7,470 milligrams per kilogram [mg/kg]), arsenic(30.3 mg/kg),barium(2,23.0 mg/kg),cadmium(500 mg/kg),calcium(12,300 mg/kg), chromium (31,300 mg/kg), iron (287,000 mg/kg), lead (2,630 mg/kg), magnesium (4,040 mg/kg), mercury (4.4 mg/kg), selenium (64.2 mg/kg), silver (18.2 mg/kg), PCB (Aroclor 2 1254)(180 mg/kg), 1,3,5-trimethylbenzene(3,500 mg/kg), 1,2,4-trimethylbenzene(13,000 mg/kg),1,1,2,2-tetrachloroethane(190 mg/kg),xylenes(total)(170 mg/kg),n—propylbenzene l (1,000 mg/kg), . sec-isopropyltoluene (1,600 mg/kg); naphthalene (950 mg/kg), 2- / methylnaphthalene(2,000 mg/kg), and bis-2-ethylhexylphthalate(40 mg/kg). Based on the analytical data generated during PA/SI activities,EPA On-Scene Coordinator -(OSC)Athanasios Hatzopoulos determined that a removal action was necessary at the site. Criteria used for this, determination included the substantial threat of release to the. environment and the imminent and substantial danger to public health and welfare presented by the hazardous substances. 3.0 SUMMARY OF FEDERAL RESPONSE ACTIONS 3.1 Mobilization and Site Preparation On 22 June 1998,.OSC Hatzopoulos,EPA Health and Safety Officer(HSO)Robert Hinten, EPA representative Sylvia Kirsch,and START member Jenifer Sullivan arrived at the site. In addition,representatives of the EPA Region I Emergency Response and Cleanup Services (ERCS) contractor, OHM Remediation Services, Inc. including Response Manager(RM) Joseph Coleman, and ERCS Transportation and Disposal (T and D) Coordinator Barry Taggart. A site walk-through was conducted to determine a suitable location.for a command post,as well as to determine any health and safety hazards that needed to be addressed as part. of site preparation activities. ) On 29 June 1998, START members Sullivan and Brenda Operach arrived on site and met with OSC Hatzopoulos,ERCS RM Coleman,and ERCS T and D Coordinator Taggart,who had been performing an additional site walk-through in preparation for the planned removal action. At the request of OSC Hatzopoulos,START mobilized an x-ray fluorescence(XRF) analyzer to the site to screen solid samples for metals in an effort to further characterize the contamination at the site. START personnel collected samples(TR 020,TR-021,TR-022, and TR-025 through TR-029)from trenches located within the two garage areas in the north- central portion of the site building. Two sludge/solid samples(TR-023 and TR-024)were also collected from a storm drain and trench located at the exterior of the northernmost garage, and three surface soil samples(SS-020, SS-021, and SS-022)were collected from the exterior of the southern side of the building. Surface soil sample locations were chosen by OSC Hatzopoulos based on results of the PA/SI conducted at the site which indicated high levels of metals in this area. Sampling was conducted in accordance with the site-specific sampling plan,. which is a separate document produced by START personnel entitled Removal Program Sampling Quality Assurance/Quality Control Plan for the Flynntan Site (See Appendix C - Sample Location Diagram, Figure 3). Results of on-site screening indicated that there were only low levels of metals present in material within the exterior trenches. Surface soils were shown to have slightly elevated concentrations of lead and chromium. Sludge material collected from within the interior trenches was found to contain elevated levels of lead and chromium as well as other metals (See Appendix D - On-site Metals Screening Report). 3 On 6 July 1998, OSC Hatzopoulos, ERCS RM Joseph Coleman, and two ERCS laborers arrived at the site. The process of installation or activation of utilities(telephone,electrical, and water)as well as the delivery and staging of ERCS equipment and expendables was initiated at that time. On 7 July 1998, START member Sullivan arrived at the site. The site-specific removal health and safety plan(HASP)was reviewed by-all site personnel. In addition, emergency phone numbers. and directions to the hospital were posted, and site work zones were delineated. All site activities were performed inappropriate personal protective equipment (PPE),.as detailed in the HASP. The site HASP was prepared by START personnel as a separate document, entitled Health and Safety Plan for the Flynntan Site, Salem, Essex County, Massachusetts. Off-hours site security was initiated with the Data Quest Security Company. START personnel photodocumented site activities during site preparation activities and throughout the remainder of the removal action (see Appendix E - Photodocumentation Log). Additional,site preparation activities included the clearing of debris from the interior garage areas at the north side of the building as well as all other work areas. The ERCS crew hooked up lights within the basement of the site building and covered pits and trenches in that area with.polyethylene sheeting and caution tape. The contamination reduction zone (CRZ) was also delineated within the northernmost garage. On 8 July 1998, START personnel collected three sludge samples (TR-025, TR-030, and TR-031)and one liquid sample.(TR-025A)for laboratory analyses at EPA NERL. Analytical parameters included metals screening ofall four samples-,and SVOC analysis ofsamples TR- 030 and TR-031 (see Attachments F - Metals Analytical Data and Attachment G - Semivolatile Organic Compounds Analytical Data). Chain-of-Custody documentation for all samples collected during the removal action is included in Appendix H - Chain-of- Custody Documentation. On 13 July 1998,ERCS personnel set up an area for drum staging in a room located near the small garage within the building. In addition,Levine-Fricke Recon,Inc.initiated a 5-day-air sampling survey for the presence of lead and chromium. Air sampling results for each of the 5 days indicated no concentrations above the established action levels for lead and chromium. Copies of the air sampling laboratory reports are available in the EPA Flynntan site files. 3.2 Trenches and Pits Wooden and metal grates were removed from interior trenches, and solid/sludge material within the trenches was removed by hand and staged in piles pending removal with a vactor truck. Material located in the deep pits within the building was left in place due to its wet consistency pending removal with the vactor truck. To allow access by the vactor truck to the sludge material within the pits,a vacuum truck was utilized.to remove any standing water existing as a layer on top of the sludge. 4 On 4 August and 14 August 1998, Franklin Environmental Services of Wrentham, MA removed a total of approximately 5,438.gallons of water from the pits. The 1,843 gallons of water removed on 4 August 1998 were transported to Environmental Compliance Corporation(ECC) in Stoughton, Massachusetts for disposal. The 3,595 gallons of water removed on 14 August 1998 was transported to United Oil. Recovery in Meriden, Connecticut for disposal. On 9 September 1998, Cyn Environmental Services, Inc. of Stoughton,MA removed a total of approximately 1,100 gallons of water and transported it to ECC for disposal. Information regarding all waste transported off site for disposal or recycling during the removal action is included in Appendix I-Manifest/Bill of Lading Log and Appendix J-Manifests/Bills of Lading. On 9 September.1998, J.F. Walton Systems of Chelsea, MA,as a subcontractor to Capitol Environmental Services, utilized a vactor truck to transfer material from the trenches and pits, as well as the contaminated surface soil which had been excavated and staged within the building, into.two sludge boxes. Confined space entry procedures were utilized during the removal of material from the pits. Corn-cob absorbent material was added to the sludge as it was transferred into sludge boxes to reduce moisture.content. On 10 September 1998, the material was transported by AmeriTech Environmental Services (AES) of South Portland, ME to the Waste Management Disposal Services - Crossroads (Waste Management) facility in Norridgewock,ME for disposal. 3.3 Drums and Containers Beginning on 13 July 1998, drums.and containers were staged within the site building. Hazard categorization testing was performed on samples collected from the drums and containers in order to establish disposal waste streams and to determine potential compatibility for possible consolidation of materials. Small (<5 gallon capacity) containers were laboratory packaged, and materials from two drums were consolidated and staged pending disposal. In addition, two drums labelled as isopropanol, and chromium complex, respectively, were overpacked and staged pending disposal. On 20 August 1998, approximately 50 drums were transported off site by Clean Venture/Cycle.Chem,Inc.(CV/CC)of Elizabeth,NJ to the CV/CC facility in Elizabeth,NJ. 3.4 Electrical Capacitors Results of laboratory analysis performed on a sample collected during the PA/SI from beneath a capacitor indicated that the subject capacitor contained PCB oil. On 14 July 1998, ERCS personnel initiated the removal of capacitors from various locations throughout the site buildings. On 21 July 1998,this task was completed, and a total of 21 capacitors along with their casings and related components were placed into two drums and staged pending disposal. On 20 September 1998,the drums were transported offsite for disposal along with all other drums (see Section 3.3). 5