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70-92 Boston Street - Environmental Site Assessment - Appendix C - October 2001 i Appendix C Removal Action Administrative Record File L2001-543 B-1 FLYNNTAN SITE (Identification Code - 015Y) REMOVAL ACTION ADMINISTRATIVE RECORD FILE AND INDEX Prepared For: U.S.Iffhvironmental Protection Agency Region I Emergency Planning and Response Branch John F. Kennedy Federal Building Boston, Massachusetts 02203 CONTRACT NO. 68-W5-0009 TDD NO. 98-07-0015 PCS NO. 5402 r► Prepared by: Roy F. Weston, Inc. Region I Superfand Technical Assessment and Response;Team 217 Middlesex Turnpike . Burlington, Massachusetts 01803 SEPTEMBER 19% i 1 INTRODUCTION This document is the Index to the Administrative Record File for the Flynntan Site Removal Action. The Index cites site-specific documents and guidance documents used by EPA staff in selecting a removal action at the site. The proposed actions will protect public health, welfare, and the environment by preventing people or animals from coming into contact with the contaminated areas of the site. The proposed actions are as follows: 1)Taking measures to prevent unauthorized access to the site, including repairing or installing additional security fencing and/or providing.24-hour security during removal activities; 2) conducting additional sampling of interior and exterior floor surfaces,and of drums,pails,and settling pits;3)sweeping up,consolidating,and staging hazardous waste contamination found on the floor surfaces; 4) categorizing, containerizing, and staging the contents of drums, vats, containers, and settling pits; and 5) collecting-and staging exterior lead- contaminated soil. Also, all wastestreams will be manifested and shipped off site for appropriate reuse or disposal at EPA-approved disposal facilities. The Administrative Record File is available for public review,by appointment, at the EPA Records Center,90 Canal Street,First Floor,Boston,Massachusetts,02114,and at the Salem Public Library, 370 Essex Street, Salem, Massachusetts, 01970. Questions concerning the Administrative Record File should be addressed to the EPA On-Scene Coordinator. The Administrative Record File is required by the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA), 42 U.S.C. § 9613 (k), and EPA's implementing regulations,40 CRF § 300.800.-825. or PLEASE NOTE: TIE FOLLOWING DOCUMENTS COMPILED IN THIS ADMINISTRATIVE RECORD HAVE BEEN MADE FROM THE BEST AVAILABLE COPIES SITE-SPECIFIC DOCUMENTS ADMINISTRATIVE RECORD FILE INDEX for the -Flynntan Site REMOVAL Removal Reports(Site File 2.02) l. "Removal Program Preliminary Assessment/Site Investigation Report for the Flynn Tan Site, Salem,Massachusetts, 14 April 1998",prepared by Roy F. Weston, Inc., Superfund Technical .Assessment and Response Team (START) for EPA Region I,June 1998. 2. Site Investigation Closure Memorandum from Athanasios Hatzopoulos,EPA On-Scene Coordinator, through Steven Novick, Section Chief, Site Evaluation&Response Section II,EPA Region I,to the Flynntan Site File, regarding the closure of the site investigation at the Flynntan Site, 70-92 Boston Street, Salem,MA,dated 28 April 1998. Pollution Reports (Site File 2.04) 3. Pollution Report No. 1, Flynntan Site, 70-92 Boston Street, Salem, Massachusetts, from U.S. EPA On-Scene Coordinator (OSC) A. Hatzopoulos, 20 July 1998. Action Memorandum(Site File 2.09) 4. Memorandum from Athanasios Hatzopoulos, On-Scene Coordinator, EPA Region I,through Steven R.Novick,Chief, Site Evaluation and Response II, to Patricia L.Meaney,.Director,Office of Site Remediation and Restoration, EPA Region I, concerning Request for a Removal Action at the Flynntan Site, Salem, Massachusetts, dated and signed 26 May 1998. (The Enforcement Section of the Memorandum is withheld as being CONFIDENTIAL). POTENTIALLY RESPONSIBLE PARTY(PRP) PRP-Specific Correspondence(Site File 11.09) 5. Letter to Salem Realty, LLC, c/o Jan Exman, Manager, 66 OId Blue Hill Road, Durham, Connecticut 06422, from Dennisses Valdez, Acting Chief, Emergency Planning and Response Branch, EPA Region 1, concerning notice of potential liability and invitation to perform or finance proposed cleanup activities: Flynntan Site, dated 4 May 1998. COMMUNITY RELATIONS .News Clippings/Press Releases (Site File 13.03). 6. "Administrative Record File Available for the Flynntan Site Removal. Action,"text of the advertisement as it was requested to appear.in the Salem Evening News, Salem,Massachusetts. w I l 11 SELECTED KEY GUIDANCE DOCUMENTS - EPA guidance documents may be reviewed at the EPA Superfund records room, Canal Street, Boston, Massachusetts. 1. Comprehensive Environmental Response Compensation: and Liability Act of 1980, as amended,42 U.S.C. § 9601 et seq. 2. "National Oil and Hazardous Substances Pollution Contingency Plan," Code of Federal Regulations (Title 40, Part 300) 1990. 3. "Action Memorandum Guidance", Superfund Removal Procedures, U.S. EPA, Office of Emergency and Remedial Response, OSWER Directive 9360.3-01, September 1990. 4. Superfund Amendments and Reauthorization Act of 1986. 1 i' i i I I ' i REMOVAL PROGRAM PRELIMINARY ASSESSNHM/ SITE INVESTIGATION REPORT FOR THE FLYNN TAN SITE SALEM, MASSACHUSETTS 14 APRIL 1998 Prepared For: U.S. Environmental Protection Agency Region I Emergency Planning and Response Branch John F. Kennedy Federal Building Boston, MA 02203 CONTRACT NO. 68-W540009 TDD NO. 98-05-0077 PCS NO. 5076 of DC NO. R-1523 Submitted By: Roy F. Weston, Inc. Superfund Technical Assessment and Response Team 217 Middlesex Turnpike Burlington, MA 01803 June 1998 TABLE OF CONTENTS I. Preliminary Assessment/Site Investigation Forms H. Narrative Chronology III. Appendices Appendix A - Site Location Map (Figure 1) Appendix B - Site Diagram(Figure 2) Appendix C - Sample Location Maps(Figures 3A and 3B) Appendix D - Chain-of-Custody Record Appendix E - Photodocumentation Log Appendix F - Volatile Organic Compound Analytical Data Appendix G - Semivolatile-Organic Compound Analytical Data Appendix H - pH Analytical Data Appendix I - Polychlorinated Biphenyls Analytical Data Appendix J - Metals Analytical Data Appendix K - Flashpoint Analytical Data I i i I. Preliminary Assessment/Site Investigation Forms w i i I A EPA REGION I REMOVAL PRELIMINARY ASSESSMENT Site Name and Location Name:Flynn Tan Location: 70-92 Boston Street Town:Salem County:Essex State: MA Site Status: ( )NPL ( -)NON-NPL ( )RCRA ( )TSCA ( )ACTIVE (X)ABANDONED ( )OTHER (X)Attached USGS Map of Location (X)Site I.D. No,. :015Y Latitude: 420- 31' 11.8" North Longitude: 700 54 ' 37. 9" West Referral ( )Citizen (X)City/Town ( )State ( )Preremedial ( )RCRA ( )Other: Name of referring party: City of Salem, Planning Department Phone:(978) 745-9595 Address: Planning Department, 1 Salem Green, Salem, 4Massachusetts ContactQ Identified 1)-Ms. Jane Guy - Salem Planning Department Phone: (978)745-9595 2)Mr. Charlie Latulippe - Town of Salem Fire Phone: (978)745-7777 Chief w Source of Information (X) Verbal: Conversations between Ms. Jane Guy, Salem Planning Department, and Chief Charles Latulippe of the Salem Fire Department with START member Patricia Coppolino. ( ) Report: ( ). Other: Potential Responsible Parties Owner: Mr. Jan Ex-man Phone: ( )Not Available Address: Operator: Mr. Jan Exman Phone: ( )Not Available Address: 70-92 Boston Street i i REMOVAL PRELIMINARY ASSESSMENT i Potential Threat (Concluded) iii . Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or other bulk storage containers, that may pose a threat of release. iv. High levels of hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate. V. Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate or be released. vi . Threat of fire or explosion. vii . The availability of other appropriate federal or state - response mechanisms to respond to the release. viii . Other situations or factors that may pose threats to public health or welfare or. the environment. Prior Response Activities ( ) PRP ( ) STATE ( ) FEDERAL ( ) OTHER Brief Description: None Available. Priority for Site Investigation (X) High ( ) Medium ( ) Low ( ) None Comments: The site building has been abandoned since 1988 and is located in a heavily populated residential area. The presence of unknown tannery waste poses a threat to the nearby population as well as to the North River Canal, which is located approximately 0.5 miles north of the site. Report Generation Originator: Patricia Coppolino Date: 13 April 1998 Affiliation: Roy F. Weston, Inc. (START) Phone: (781) 229-6430 TDD No. : 98-05-0077 PCS No. : 5076 i f 3 EPA REGION I REMOVAL SITE INVESTIGATION Inspection Information Site Name: Flynn Tan - Address: 70-92 Boston Street Town: Salem County: Essex State: MA Date of Inspection: 14,16 and 17 April 1998 Time of Inspection: 0900 hours Weather Conditions: Cloudy, 60OF Site Status at Time of Inspection: ( ) ACTIVE (%) INACTIVE Comments: The Flynn Tan Site (the site) currently is an inactive tannery facility.- Agencies/Personnel Performing Inspection Names Program (x) EPA: Athanasios Hatzopoulos Site Evaluation and Response Section II. Michael R. Usovicz Criminal Investigation Div. (x) EPA Contractor: Patricia Coppolino Roy F. Weston, Superfund Technical Assessment and Response Team (START) Todd Borci Roy F. Weston, START Stephen Amirault Roy F. Weston., START w ( ) State: (x) Other: Chief Charles Latulippe Salem Fire Dept. Current Owner Based on Field Interview: Jan Exman Physical Site Characteristics i Parameter _ _ Quantities/_Ext=t ( ) Cylinders: (x) Drums: Approximately 21 55-gallon steel and plastic drums were observed inside a site building.- Most were located on the first floor . and had various labels including flammable, corrosive, formic acid, degreasing solvent, chrome complex in isopropanol, SYN FOG insecticide, and sodium acetate. i REMOVAL SITE INVESTIGATION Physical Site Observations (Concluded) open concrete pit (which was sealed on 16 April 1998 by the City of Salem) was observed in the parking area. On 16 April 1988 signs were posted on every entrance to the site buildings by the City of Salem stating that the site buildings are structurally unsound for habitation. Most of the area outside the site buildings is paved except for one small area north of-the alleged USTs. This area had stressed vegetation and piles of animal hides adjacent to the southern external wall of the site building. The site is -fenced with a locked gate. The site is bordered to the north by-Goodhue Street, Beaver Street and a residential/commercial area; to the east by the intersection of Boston Road/Goodhue Street, and a residential/commercial area; to the south by Boston Street and a residential/commercial area; and to the west by a residential/commercial area. Field Sampling and Analysis Matrix Analytical Field Instrumentation Parameter CGI O RAD PID FID Background Readings: 0*LEL/20.9002 <15mrad <1 unit <1 ppm Drums: D-001 600 ppm D-007 180 ppm No other readings above background were noted. Field Quality Control Procedures . W SOP Followed ( ) Deviation From SOP Comments: ~� Description of Sampling Conducted i Samples collected on 16 April 1998 consisted of 11 drum samples (D- 001 through D-011) which were analyzed for metals,- pH, . flashpoint, semivolatile organic compounds . (SVOCs) , and volatile organic j compounds (VOCs) ; two soil samples (C-01 and C-02) which were analyzed for polychlorinated biphenyls (PCBs) ; ten soil samples (S- 001 through S-010) which were analyzed for metals; - and three tank samples, two liquid (T-001A and T-03) and one sludge (T-001B) , which were analyzed for metals. Samples S-001 through S-010, T- 001A, T-001B, and T-03 , were analyzed at RECRA Lab-Net Chicago ' located in University Park, IL. Samples D-001 through D7011, C-01 and C-02 were analyzed at the EPA New England Regional Laboratory (NERL) located in Lexington, MA. 3 REMOVAL SITE INVESTIGATION Site Determination (Concluded) ii. Hazardous substances or pollutants . or contaminants _.in drums, barrels, tanks, or other bulk storage containers, that may pose a threat of release. High levels of hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate. iv. Threat of fire or explosion. V. The availability of other appropriate federal or state response mechanisms to respond to the release. 4 Report Generation Originator: Patricia Coppolino Date: 01 May 1998 Affiliation: Roy F. Weston, Inc. (START) Phone: (781) 229-6430 TDD No. : 98-05-0077 PCS No. : 5076 I 5 II. Narrative Chronology w i I Narrative Chronology On 14 April 1998, Roy F. Weston, Inc. Superfund Technical Assessment and Response Team (START) members Patricia Coppolm and Todd Borci'mobilized to the Flynn Tan Property (the site) located at 70 - 92 Boston Street, Essex County, Massachusetts (see Appendix A - Site Location Map). The site is an old tannery that manufactured lamb skin products from the 1920s to 1988. After 1988 the site was abandoned. The site is approximately 1.89 acres, and is owned by Mr. Jan Exman. The City of'Salem alleges that portions of the site are being rented by Mr. Exman to tenants illegally(without certificate of occupancy). START personnel met with U.S. Environmental Protection Agency (EPA) On-Scene Coordinator (OSC) Tom Hatzopoulos to determine if there were any potential sources of contamination at the site to sample. Site activities were conducted in accordance with the site health and safety plan(HASP). The site HASP has been prepared as a separate document, entitled Removal Program Site Health and Safety: Plan for the Flynn Tan Site Preliminary Assessment/Site Investigation, Salem, Massachusetts. Prior to the initial walkthrough, START personnel calibrated a Radiation Meter, a Combustible Gas/Oxygen meter(CGI/02), an Organic Vapor Analyzer(OVA), and an Organic Vapor Monitor (OVM). Following equipment calibration, START personnel donned level C personal protection equipment (PPE) and conducted a site walk-through. START observed approximately 15 electrical capacitors, 21 55-gallon drums, and approximately 40 miscellaneous jars were.located in the site building. The drums were labeled"sodium acetate", "chrome complex in isopropanol", "SYN FOG insecticide", "flammable", "corrosive", "formic acid", and "degreasing solvent". Many of the jars contained what appeared to be different colored dyes, while others were labeled "pretan", "cirial G30", and "retan". ' Following the site walk-through, EPA and START personnel departed the site. On 16 April 1998, START members Coppolino, Borci, and Stephen Amirault mobilized to the site and met with OSC Hatzopoulos to conduct site investigation and perform sailing activities. Site activities were conducted in accordance with the site HASP. Prior to the walk-through, START personnel calibrated the Radiation Meter, the CGI/02, the OVA, and the OVM. Following the calibration of the air monitoring instruments, START members Coppolino and Borci donned level C PPE and entered the building to select drum sample locations. While in the building, Special Agent Michael R. Usovicz, from the EPA Criminal Investigation Division, Salem Fire Department Chief Charles Latulippe, and Deputy Chief Brophy met with OSC Hatzopoulos to discuss the fire hazards of the building and the current shipping and storing operations being conducted in the site building. Following drum sample location selection, START personnel donned Level B PPE and began collecting drum samples. Drum samples were collected from the following containers: sample D- 001 was collected from a blue 55-g4on plastic drum,.with a label that.read "corrosive, do not freeze", located in the storage room on'the first floor of the`facility and was analyzed for flashpoint, semivolatile organic compounds (SVOCs), and volatile organic compounds (VOCs); sample D-002 was collected from a blue 55-gallon plastic drum,with a label that read "coagulite", located in the storage room on the first floor of the facility and was analyzed for flashpoint, i On 17 April 1998, START members Coppolino and Borci returned to the site, donned level,C PPE, and photodowmented sample areas (see Appendix E-Photodocumentation Log). Samples were then subsequently delivered to the EPA New England Regional Laboratory (NERL) in Lexington, Massachusetts for pH, flasbpoint, VOC, SVOCs and PCB analyses by EPA Region I Method. In addition samples were also shipped via Federal Express to RECRA Lab-Net Chicago; located in University Park,. Illinois for Resource Conservation and Recovery Act (RCRA) metals analyses. (See Appendices F-Volatile Organic Compound Analytical Data, G- Semivolatile Organic Compound Analytical Data, H -,pH Analytical Data, I Polychlorinated Biphenyls Analytical Data, J=Metals Analytical Data, and K-Flasbpoint Analytical Data). i I ' i w I TABLE-1 Sample Descriptions (Concluded) 5 Ns tat NO + A k: v S-009 Soil Grab 0-3 Light Silty Decomposing material Brown S-010 Son Grab 0-3 Brown Silty Sod underr-a pile of hides C-001 Soil Grab N/A Brown Od -Soil-under a ca acitor C-002 Soil Grab N/A Brown Oily Soil on a transformer Pad *-If applicable. NA-Not applicable. w I _ I III. Appendices i or 1 1 - 1 • ' APPENDIX A Site Location Map (Figure:1) w %Zt 7 0 .w era A Y. -- & e; els 0 v- z P tils. FJ `Point.a ic;.-ood h � kS GoO CoCourseLobslter-RoC P 7 BEVI z HAR 4, L Fuxton F 42- % Al fire 1411/ to • Z ci < r Aarmany x 20� >11 3M VU L .:'Library �44 -8 Park Hill M Derrmorv, v w Sc ii r �F SI:. BO V Sc 7-. Derby R&ORS. Wh 4w an Q d 32 Y MAdow :Pow( J L s� N Lofta_Pt---6 f T, -Sa jzs i pd7ner % AN S -Ct*e IL V Substa A .9 Hasa,tg�'r LE�54 -!It .4 L LA Sr tb az "A 16 S: 2! 4 r r416 LS Fares.--et I,Z'2119,-,Peabc�dy _w '3r T, �ickerik - t \5i Em t iiiii co F.re If Course BASE MAP IS A PORTION OF THE FOLLOWING 7.5 X 15' U.S.G.S. QUAORANGLE(S): Salem. Mossachusa tts. 1985 • 1 MILE 1/2 0 1000 a 1000 2000 3000 4000 5000 6000 70w FEET GUACRAM=LOCAnON SITE LOCATION MAP Site Flynn Tan M.AGLIs W3EE1S/C0-SAJ-TS X REGION I SUPERFUNO TECHNICAL ASSESSMENT AND RESPONSE TEAM 70 .-92 Boston StreeT TOO DRAWN SY: Sclem , Mc'Issachusefts 98-05-0077 M. BUTTERWORTH _6/19/98 FILE NAME: R:\98040006\fig I.dwg FIGURE 1 APPENDIX B Site Diagram(Figure 2) a w a . i 00 r■ ~ \ N ■ � W O IN W DUNKIN Q a \ WW DONUTS `^ cr i (� V W Q a y = aQ U a m Q W i 3 m Lr x s � y¢�y cr W G �_ \ V Z IL \ cCD O Z W Q O a O O - � O (33 +n moo. Z � O '� � I zrn O ¢ o.00 j W m C7 - Q V)Of0 V) Z o V) W F- Li z U Lj Q O a : cr Q a o v, Q JO W C ~ I) V) 2 V) LLJ 0 Q O _ Z N Q� �2 a Z V7� J 0 d z Y a OI.- Li a) W W W .CC) Q O Z m 0 a O O Q Cl 0- V) ti U Q N W Z (7 1Z W Ld c, 0 0 N ® 3 Lr to Z W O h Q CD I— Li _Z > O ¢ w o W � Q Z y W C� O N m Z W z O C9 O C7 . U W W O F-. W Z 0 FL W Y W U O O a ' ZLti 5 O Z Q � Q p J a � O CO �i O r W U J V N Q Q .. V) : o Z �- W Z : W . J I �i APPENDIX C Sample Location Maps (Figures 3A and 3B) w LA1 a 00 V)Cl °' Q W o Z M O d � W Yf LD M 0 La Z Q' O H O J � z 1 0 o m r� Z C7 p`fJ �� m o M Of O V W LJ. m W Q0 �_ a 2 c, C9 p v W m a � y B�E:D) m 0 ` Q BOILER o Z ROOM o z 3 i 00 (n N in U � C7 C9 1 w ZY o a = o / of p U 0 ^ to �i-OQ 00 W 1 ® ® 0 ¢ O cr inoz iQ o ®®o 0 o I �r Q ^� �('� lal Q N C) o O moo 0 1 am p I O } '�00 Z/ Q U II (n .0 Am o� � W N J � p W N I = N LJ m © J p W 00 © 0 J Q Ul O N 01 Y L` d Q W 0 1.-- 'n 0� in m Z � C) 0.0 O (/) t/1 - _ \o F— ZZU o© a a 0 U <. 1— V)- ©© o � c' O �0 Z m 0 0 ©© V) 0 o w Z LaJ o p © n- —� LL- w O � < o � ao o 0 0 1 m N m w m o a m c, � Oz LLJ D © 0 0 1 Q Z 0 w 0 Z Z Q © L9 00 00 C) U J W `�'w Q U m J Q a J `7'CL ~_ 2 F- Z QQ0 tAi W QO Q N Cr �' Q m-i m Qp (D'o) r- to Q— U c) 0 acV 0 © ® � m © N W t� 8 3 2�(1 I 9£3SASlJ\9000V086\� =3►YYN 31U Sl13snHDVSS'VW W3-1 VS 86/OZ/lv a21.VHONVI8 11 LLOO-90-26 80013 aN003S 31Y0 `AM NM"G I ON am 133diS NO1S08 06—OL 1YY31 3SNOdS3S ONY LN3Y4SS3SSY IYOINH33L °NnJS3dns I N0193H 311 S N dl N N AI3 S1NV1Y15NO3/S!fl►O630 Sii37YHYn d'VW N011`d001 3IdWVS 31Y35 01 ION Ff r ' 30NVaIN3 A00a ONIOVOI W00H ® Ol ad3l I001 salviS 1 . W 0021 83lawni zoo—s • 01 a'V3I Salv1S f N008 I VA im SiVA i 00-5 j i i APPENDIX D Chain-of-Custody Record - s - - a . w - o Yl gi to cy-3 U2 -� Y y o o KK W -59 As E- � � N► � t- f- of sLLr� - -� Y 0 0 h E p v v UJ m o v t t o 'a Q a) c c 0 .a yW 1 1 c o GI �CCC J U. 4�� T W c� o a � tU d3 e�� `' +v Z U. z �, 3, c 0 1 N o t 0 Cc a o 0 �•� Z 5. ? p O > ^ V U G e I o Ob o o E O Z 1 r a Z a E _E E a � U / W c Q 7 0, i ] C WCL J—i e O W .� �. ` < .0 W O G o 0 0 f!1 cr Z � {{► � ` M N w 4� r2 Q 1LU Q 1 0 99 C C C U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I N9 65644 LAB CODE SOURCE h PERMIT NO PROJECT# -. CITY Su�Lr1, i`� COLLECTOR STATION # - d `WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) 1ndders SAMPLE TYPE:GRAB, T V_; AIR TEMP (°C): < 0% 0°-10% 11°-20°,> 21° COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW, TREATED Y Y M M D D Y Y M M D D (Circle One) Other ff VFOFq START END `'`•' ! PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. BOD NO2+3 COD Cd START END TSS _ TKN PCB Cu SAMPLE TEMP(°C) Turb T P 7 X-Ray Cr (f) Organics I OIG HOther VO& -Cr (+6) pH(SU) m . VOA's CN Fe Hg TOT 912(mg/1) ' FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (mlJl) None Ni Magmeter SIZE Pb Venturi m Sn FLOW METER EPA. SOURCE Parshal l Zn TOTALIZER -,V-Notch Inches/Degrees Other START \ Rectangular END her 7 EPA a�tz�o 3� 'Unpreserved sample MULTIPLIER . � U.S. ENVIRONMENTAL PROTECTION.AGENCY REGION I j1i0 65645 LAB CODE I SOURCE T n PERMIT NO. PROJECT # 's CITY COLLECTOR STATION # f WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) �dq&s SAMPLE TYP - AB T V AIR TEM P (°C): < 0°, 0°-10 11°-20°,> 21° COLLECTION DATE ' SAMPLE LOCATION:SUPPLY WATER, WASTEWATER: RAW,TREATED Y Y M M D D Y Y M M D D (Circle One) Other START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECT 2ION TIME Bacti NH3 Phenol Tot. Diss. O BOD N0.2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP (°C) Turb T P X-Ray. Cr(T) Organics O&G Other -Cr (+6) pH(SU) M °E] VOA's CN. Fe TOT C12(mg/1) FLOW MEASUREMENT M� SETTLEABLE SOLIDS (m l/l) None Ni Magmeter SIZE Pb Venturi•- m Sn FLOW METER EPA SOURCE Parshal l Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END Other •Unureserved sample MULTIPLIER U.S. ENVIRONMENTAL PROTECTION_AGENCY REGION I j�iQ 65648 LAB CODE SOURCE. �n PERMIT NO PROJECT# �e&M /�?ff COLLECTOR STATION # - - CITY _,,,,, WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) 1p Dols SAMPLE TYPE: J:r AB T V_ AIR TEMP ('C): < 00, 0'40% 11%200,>21" COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER,WASTEWATER: RAW,TREATED Y Y M M 0 D. Y Y M M 0 D (Circle One) Other j START END . : . PARAMETERS (CHECK APPROPRIATE) METALS COrL-L�ECT�ION. TIME Bacti NH3 Phenol Tot. Diss. CZLtJ BOD NO2+3 7 COD Cd START END Turb SS T PN X-Ray PCB u Cr SAMPLE TEMP ('C) Organics O&G Lj Other 'Cr(+6) pH(SU) [� •❑ VOA's CN . Hg TOT C12(mg/1) FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (mill) None Ni. Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshall Zn TOTALIZER V-Notch Inches/Degrees Other START _. Rectangular _ END EPA aOther 'Unpreserved sample MULTIPLIERI-7500-3 U.S. ENVIRONMENTAL PROTECTION AGENCY REGION I _ LAB CODE �'° 65649 SOURCE PERMIT NO_ PROJECT# CITY COLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) �dOf-s SAMPLE TYPE_GRABT V AIR TEMP ('C): < 00, 0'-10', 11'-200,> 21' COLLECT40N DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED Y Y M M D D YYMMDD (Circle One) Other 6 START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. BOD NO2+3 COO Cd START END TSS TKN PCB Cu SAMPLE TEMP VC) Turb T P X-Ray Cr(f) ' Organics I O&G Other��Svo 'Cr(+6) pH.(SU) m •�. VOA's- CN F Fe' TOT C12(m9/1) I�.J FLOW MEASUREMENT M� SETTLEABLE SOLIDS (m1/1) None Ni Magmeter SIZE Pb _ Venturi m Sn FLOW METER EPA SOURCE Parshall Zn TOTALIZER V-Notch Inches/Degrees Other START Rectangular END Other 'Unpreserved sample MULTIPLIER U.S. ENVIRONMENTAL PROTECTION AGENCY REGION i NO 65652 LAB CODE SOURCE Ninn PERMIT NO PROJECT# CITY COLLECTOR STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE) Thdo0rS SAMPLE TYPE' RA T V� AIR TEMP (°C): < 00, 0°-10°, 11°-20°,>21' COLLECTION DATE - .SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED YYMMDD YYMMDD (Circle One) Other START END PARAMETERS .(CHECK APPROPRIATE) METALS - COLLECTION TIME Bacti NH3 Phenol Diss. t Q BOO NO2+3 COD START END TSS TKN PCB Cu SAMPLE TEMP (°C) m Turb T P X-Ray Cr(T) Organics 08�G Other 'Cr(+6) pH(SU) [� .❑ VOA's CN Fe TOT C12(mgil) FLOW MEASUREMENT Mn SETTLEABLE SOLIOS.(ml/1) None Ni Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshal I Zn TOTALIZER V-Notch Inches/Degrees Other, START :Rectangular _ END Other •Unpreserved sample MULTIPLIER EPA RI-75OG-31 3 U.S. ENVIRONMENTAL PROTECTION AGENCY REGION IQ 67261 �. LAB CODE SOURCE Ofuhn fan PERMIT NO PROJECT# CITY .L COLLECTOR. JE�u STATION # WEATHER: CLEAR, RAIN, SNOW(CIRCLE ONE Ts SAMPLE TYPE:GRAB,__T V_ w AIR TEM P (°C): < 0°, 0 0-10 0, 11°-20°,> 21° COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER,WASTEWATER: RAW,TREATED YYMMDD Y Y M M,D D (Circle One) Other q a ¢1 START END PARAMETERS. (CHECK APPROPRIATE) METALS COLLECTION TIME Bacti NH3 Phenol Tot. Diss. t BOD NO2+3 COD Cd START END TSS TKN PCB Cu SAMPLE TEMP(°C) Turb T P X-Ray Cr (T) Organics 08�G Other fH 'Cr(+6) pH(SU) [11 -El VOA's CN Sva.G Fe TOT C12(mgll) . FLOW MEASUREMENT Mn SETTLEABLE SOLIDS(m1/1) None Ni Magmeter SIZE Pb • Venturi m Sn FLOW METER EPA SOURCE Parshal l Zn TOTALIZER V-Notch. Inches/Degrees Other START Rectangular END -- i _- - __ _ - _ ._ _•_ _-- _ _ . _____ a .- _ U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 1 11i0 67264- LAB CODE 1 SOURCE mn PERMIT NO PROJECT# CITY COLLECTOR STATION # O I WEATHER: CLEAR, RAIN. SNOW(CIRCLE ONE)- SAMPLE TYPE:GRAB,-X—T V_ AIR TEMP(QC): < 0°, 0 6=10°; 11 °-20°,> 21.0 COLLECTION DATE SAMPLE LOCATION: SUPPLY WATER, WASTEWATER: RAW,TREATED Y Y.M M D D Y Y M M D D (Circle One) Other191a f G Y START END PARAMETERS (CHECK APPROPRIATE) METALS COLLECTION TIME TIME Bacti NH3 Phenol Tot- Diss. �u BOD NO2+3 COD Cd START END ! TSS TKN PCB Cu SAMPLE TEMP (°C) j Turb T P X-Ray Cr M ' Organics O&G Other 'Cr(+6) pH(SU) ® .Q VOA's CN H Fe TOT C12(mg/l) f FLOW MEASUREMENT Mn SETTLEABLE SOLIDS (m111) None Ni ' Magmeter SIZE Pb Venturi m Sn FLOW METER EPA SOURCE Parshall TOTALIZER V-Notch Inches/Degrees Other START _:Rectangular END Other EPA RI-7500-31 •Unpreserved sample MULTIPL ER 1 ' i 3 i I APPENDIX E Photodocnmentation Log PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts D - 001 D-002 1 D- .0:3 D -004 �+ SCENE: View of sample locations D-00 i,D-002,D-003,and D-004 located in storage room on,the first floor. FRAME NUMBER: 1 DATE:4/17/98 TIME: 1000 SKY CONDITION: Inside PHOTO BY:Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 rnm FILM ROLL:95484 C - 02 SCENE: View facing west of former exterior transformer pad and sample location C-02- FRAME NUMBER:2 DATE:4/17/98 TIME: 1010 pKY CONDITION:Cloudy PHOTO BY:Patricia Coppolino WITNESS(ES):Todd Borci -tAMERA: Olympus SETTING: Automatic F LM[TYPE:35 mm FILM ROLL: 95484 Tnr%Ar, n0 Aw AA►.[ A..,_,. l -rc DI-Q AI.. CA7.0 PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts CA CITOR . SCENE:interior view of basement Engine Room. Two connected capacitors can be seen at center. Two identical connected capacitors are out of view to the right. FRAME NUMBER: 5 DATE:4/17/98 TM 1030 SKY CONDITION: Inside PHOTO BY:Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic .-IL.M TYPE:35 mm FILM ROLL:77270 i i I i SCENE: 'View facing east of southwestern portion of Flynn Tan building. 1AME NUMBER:6 DATE:4/17/98 TUM: 1040 SKY CONDMON:Cloudy PHOTO BY:Patricia Coppolino . WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 min FILM ROLL:77270 I Y - PHOTOGRAPHY LOG SHEET Flynn Tan Property Site, Salem, Massachusetts s- 0i0. SCENE: View facing-northeast of southern exterior portion of building,and sample locations S-009 and S-010. FRAME NUMBER:9 DATE:4/17/98 TIME: 1120 SKY CONDITION:Cloudy PHOTO BY:Patricia Coppolino WITNESS(ES): Todd Borci CAMERA: Olympus SETTING: Automatic F ,M TYPE:35 mm FILM ROLL:77270 i I SCENE: View of southern entrance to Flynn Tan building and sign posted by City of Salem building inspectors on 16 April 1998,stating building is condemned. -q AME NUMBER: 10 DATE:4/17/98 TIME: 1200 . ,XY CONDMON:Cloudy PHOTO BY:Patricia Coppolino WITNESS(ES):Todd Borci CAMERA: Olympus SETTING: Automatic FILM TYPE:35 nun FILM ROLL:77270 i Tnn u„ aR A-M I c P__ s rK P!'C Nn 5076 1I 1 i APPENDIX F Volatile Organic Compound Analytical Data w i US ENVIRONMENTAL PROTECTION AGENCY ' 60 Westview Street - Lexington, MA. 02173 DATE:May 1, 1998 SUBJECT:Flynntan Building,Salem,.MA Drums—Volatile Organic Analysis by GC/MS Samples Received. 65644, 65645,65646, 65647, 65649, 65650, 65651, 65652,67261, 67260 FROM:Joseph Montana, EIA TO:Tom Hatzopoulos, HBR ` Art- f �►' �It'I?� THRU:William Andrade, Ph.D.,Analytical Specialist PROJECT NUMBER: 98267 DATE(S)SAMPLES RECEIVED BY THE LABORATORY: 4/17/98 ANALYTICAL PROCEDURE: Drum: The samples were processed by Method 5035, High Concentration for Solid Waste and Nonaqueous Liquid Waste. .The extracts were analyzed by SW 846, Method 8260B, Rev 0,January 1995,(VOAGCMS. SOP 8/97). Data file reference: VOADRML.SOP i QUALITY CONTROL: 1. A method blank was analyzed prior to sample analysis. .2. Each sample was spiked with three surrogate compounds at 25 ppb concentration. The results for the surrogate recoveries are reported for-each sample. 3. Sample 65645 was'spiked in duplicate and analyzed to determine laboratory precision and accuracy. DATA FILE: J:ICHEMSTRYXREPORTSIVOA198267DR.WK4 p. 1 of 28 US ENVIRONMENTAL PROTECTION AGENCY { REGION I LABORATORY PROJECT AND REPORT FORM ' Chemist Reviewing Data: Wiliam J.Andrade, Ph.D. Method Modifications: None Limitations of Data: None Laboratory Blank Problems: None r _ Instrument Performance Problems: None Surrogate or Spike Recovery Problems: None Additional Comments: w There was no field trip blank sample for this analysis. A few target compounds did not meet the continuous calibration criteria for the analysis. These compounds were not observed in the samples analyzed. i i i p.3 of 28 FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID.: Lab Blank DILUTION FACTOR(S): 1 FILE NAME(S): 04228E3 DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppb Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/L) (ug/L) TARGET COMPOUNDS 747 7-3 34418 Chloromethane ND 5 74-83-9 34413 Bromomethane ND 5 75-01-4 39175 Vinyl Chloride ND 5 75-00-3 34311 Chloroethane ND 5 75-09-2 34423 Methylene Chloride ND 5 75-69-4 34488 Trichlorofluoromethane ND 5 75-35-4 34501 1,1-Dichloroethylene ND 5 75-34-3 34496 1,1-Dichloroethane ND 5 156-60-5 34546 1,2-Dichloroethylene isomers ND 5 67-66-3 32106 Chloroform ND 5 107-06-2 34531 1,2-Dichloroethane ND 5 '1-5.5-6 34506 1,1,1-Trichloroethane ND 5 56-23-5 32102 Carbon Tetrachloride ND 5 75-27-4 32101 Bromodichloromethane ND • 5 78-87-5 34541 1,2-Dichloropropane ND 5 10061-02-6 34699 t 1,3-Dichloropropene ND- 5 79-01-6 39180 Trichloroethylene ND 5 124-48-1 32105 Dibromochloromethane Nb 5 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 5 1,1-Dichloropropene 79-00-5 34511 1,1,2-Trichloroethane ND or 5 71-43-2 34030 Benzene ND 5 75-25-2 32104 Bromoform ND 5 127-18-4 34475 Tetrachloroethylene . ND 5 79-34-5 34516 . 1,1,2,2-Tetrachloroethane ND 5 108-88-3 34010 Toluene ND 5 108-90-7 34301 Chlorobenzene ND 5 100-41-4 34371 Ethylbenzene ND - 5 Dichlorobenzene isomers ND 5 1,1,2-Trichloro-1,2,2 trifluoroethane ND 5 67-64-1 .8.1552 Acetone 5 10. L 75-15-0 77041 Carbon Disulfide ND 15 (con't) P. 5 of 28 FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS- DRUM SAMPLE ID.: Method Blank SAMPLE WEIGHT: 0.097 g FILE NAME(S): 04228E4 DILUTION FACTOR(S): 50 DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/g) (ugig) TARGET COMPOUNDS 74 8.7-3 34418 Chloromethane ND 26 74-83-9 34413 Bromomethane ND 26 75-01-4 39175 Vinyl Chloride ND 26 75-00-3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488 Trichlorofluoromethane ND 26 75-35-4 34501 1,1-Dichloroethylene ND 26 75-34-3 34496 1,1-Dichloroethane ND 26 156-60-5 34546 1,2-Dichloroethylene isomers ND 26- 67-66-3 32106 Chloroform ND 26 107406-2 34531 1,2-Dichloroethane ND 26 '1-55-6 34506 1,1,1-Trichloroethane ND 26 56-23-5 32102 Carbon Tetrachloride ND 26 75-27-4 32101 Bromodichloromethane .ND 26 78-87-5 34541 1,2-Dichloropropane ND 26 10061-02-6 34699 t 1,3-Dichloropropene ND 26 79-01-6 39180 Trichloroethylene ND 26 124-48-1 32105 Dibromochloromethane ND 26 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 26 1,1-Dichloropropene 79-00-5 34511 1,1,2-Trichloroethane ND *26 71-43-2 34030 Benzene ND 26 75-25-2 32104 Bromoform ND 26 127-18-4 34475 Tetrachloroethylene ND 26 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 26 108-88-3 34010 Toluene ND 26 108-90-7 34301 Chlorobenzene ND 26 100-41-4 34371 Ethylbenzene ND 26 Dichlorobenzene isomers ND 26 1,1,2-Trichloro-1,2,2 -trifluoroethane ND 26 67-64-1 81552 Acetone ND _ 52 75-15-0 77041 Carbon Disulfide ND 78 (con't) P.7 of 28 FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION 1 LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65644 SAMPLE 1N)=1GFIP 0.079 g FILE NAME(S): 04228E13 DILUTION FACTOR(S): 5000 DATE OF-COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22198 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (uglgm) (uglgm) TARGET COMPOUNDS 74=87-3 34418 Chloromethane NO 3200 74-83-9 34413 Bromomethane ND • 3200 75-01-4 39175 Vinyl Chloride ND 3200 75-00-3 34311 Chloroethane NO 3200 75-09-2 34423 Methylene Chloride ND 3200 75-69-4 34488 Trichlorofluoromethane NO 3200 75-35-4 34501 1,1-Dichloroethylene NO 3200 75-34-3 34496 1,1-Dichloroethane ND 3200 156-60-5 34546 1,2-Dichloroethylene isomers NO 3200 67-66-3 32106 Chloroform NO 3200 107-06-2 34531 1,2-Dichloroethane NO 3200 71-55-6 34506 1,1,1-Tdchloroethane NO 3200 56-23-5 32102 Carbon Tetrachloride ND 3200 75-27-4 32101 Bromodichloromethane ND 3200 78-87-5 34541 1,2-Dichloropropane ND 3200 10061-02-6 34699 t 1,3-Dichloropropene ND 3200 79-01-6 39180 Trichloroethylene NO 3200 124-48-1 32105 Dibromochloromethane ND 3200 10061-01-5 34704 c-1,3-Dichloropropene and/or ND' 3206 1,1-Dichloropropene tr 79-00-5 34511 1,1,2-Trichloroethane ND 3200 71-43-2 34030 Benzene NO 3200 75-25-2 32104 Bromoform ND 3200 127-18-4 34475 Tetrachloroethylene ND 3200 79-34-5 34516 1,1,2,2-Tetrachloroethane NO 3200 108-88-3 34010. Toluene NO 3200 108-90-7 34301 Chlorobenzene ND- 3200 100-41-4 34371 Ethylbenzene ND 3200 Dichlorobenzene isomers NO 3200 1,1,2-Trichloro-1,2,2- trifluoroethane ND 3200 67-64-1 81552 Acetone ND 6400. 75-15-0 77041 Carbon Disulfide ND- 9600: (con't) i FACILITY.SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65645 SAMPLE WEIGHT: 0.139 g FILE NAME(S): 04228E5 DILUTION FACTOR(S): 50 DATE OF.COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS:.04/22/98 SAMPLE RESULTS: - ppm Reporting: CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74-87-3. 34418 Chloromethane NO 18 74 83-9 34413 Bromomethane NO 18 75-01-4 39175 Vinyl Chloride ND 18 75-00-3 34311 Chloroethane NO 18 75-09-2 34423 Methylene Chloride NO 18 75-694 34488 Trichlorofluoromethane NO 18 75-35-4 34501 1,1-Dichloroethylene NO 18 75-34-3 34496 1,1-Dichloroethane ND 18 156-60-5 34546 1,2-Dichloroethylene isomers ND 18 67-66-3 32106 Chloroform- ND 18 ,107-06-2 34531 1,2-Dichloroethane ND 18 71-55-6 34506. 1,1,1-Trichloroethane ND 18 56-23-5 32102 Carbon Tetrachloride NO 18 75-27-4 32101 Bromodchloromethane NO 18 78-87-5 34541 1,2-Dichloropropane NO 18 10061-02-6 -34699 t 1,3-Dichloropropene ND 18. 79-01-6 39180 Trichloroethylene NO 18 124-48-1 32105 Dibromochloromethane ND 18 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 18 1,1-Dichloropropene y 79-00-5 34511 1,1,2-Trichloroethane NO 18 71-43-2 34030 Benzene NO 18 75-25-2 32104 Bromoibrm NO 18 127-18-4 34475 Tetrachloroethylene ` ND 18 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 18 108-88-3 34010 Toluene NO 18 108-90-7 34301 Chlorobenzene NO 18 100-41-4 -34371 Ethylbenzene NO 18 Dichlorobenzene isomers ND' 18 i 1,2,2-Trichioro-1,2,2 trifluoroethane ND 18 67-64-1 81552 Acetone ND 36 75-15-0 77041 Carbon Disulfide NO 54 (con't) i p. 11 of 28 i FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEA13LE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65646 SAMPLE WEIGHT: 0.106 g FILE NAME(S): 04228E6 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm - Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 7487-3 34418 Chloromethane ND 24 74-83-9 34413 Bromomethane ND 24 75-01-4 39175 Vinyl Chloride ND 24 75-00-3 34311 Chloroethane ND 24 75-09-2 34423 Methylene Chloride ND 24 75-69-4 34488 Trichlorolluoromethane ND 24 75-35-4 34501 1,1-Dichloroethylene ND 24 75-34-3 34496 1,1-Dichloroethane ND 24 156-60-5 34546 1,2-Dichloroethylene isomers ND 24 67-66-3 32106 Chloroform ND 24 .. i 07-06-2 34531 1,2-Dichloroethane ND 24 71-55-6 34506 1,1,1-Trichloroethane ND 24 56-23-5 32102 Carbon Tetrachloride. ND 24 75-27-4 32101 Bromodichloromethane ND 24 78-87-5 34541 1,2-Dichloropropane ND 24 10061-02-6 34699 t-1,3-Dichloropropene ND 24 79-01-6 39180 Trichloroethylene ND 24 124-48-1 32105 Dibroinochloromethane ND 24 10061-01-5 34704 'c-1,3-Dichloropropene and/or ND 24 1,1-Dichloropropene or 79-00-5 - 34511 1,1,2-Trichloroethane ND 24 71-43-2 34030 Benzene ND 24. 75-25-2 32104 Bromoform ND 24 127-18-4 34475 Tetrachloroethylene ND 24 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 24 108-88-3 34010 Toluene ND 24 108790-7 34301 Chlorobenzene ND 24 100-41-4 34371 Ethylbenzene ND 24 Dichlorobenzene isomers ND 24 1,2,2-Trichloro-1,2,2 trifluoroethane ND 24 67-641 81552 Acetone ND; 48 75-15-0 77041 Carbon Disulfide ND 72 (con't) FACILITY SAMPLED:- FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65647 SAMPLE WEIGHT: 0.119 g FILE NAME(S): 04228E7 DILUTION FACTOR(S): 50 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 0412m8 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Cont. Limits Comments NO. NO, (ug/gm) (uglgm) TARGET COMPOUNDS 74-87-3 34418 Chloromethane ND 21 74=83-9 34413 Bromomethane ND 21 75-01-4 39175 Vinyl Chloride ND 21 75-00-3 34311 Chloroethane ND 21 75-09-2 34423 Methylene Chloride ND 21 75-69-4 34488 Trichlorofluoromethane ND 21 75-35-4 34501 1,1-Dichloroethylene ND 21 75-34-3 34496 1,1-Dichloroethane ND 21 156-60-5 34546 1,2-Dichloroethylene isomers ND 21 67-66-3 32106 Chloroform ND 21 07-06-2 34531 1,2-Dichloroethane ND 21 T1-55-6 34506 1,1,1-Trichloroethane ND 21 56-23-5 32102. Carbon Tetrachloride ND 21 75-27-4 32101 Bromodichloromethane ND 21 78-87-5 34541 1,2-Dichloropropane ND 21 10061-02-6 34699 tAi3-Dichloropropene ND 21 79-01-6 39180 Trichloroethylene ND 21 124-48-1 32105 Dibromochloromethane ND 21 10061-01-5 34704 c 1,3-Dichloropropene andlor ND 21 1,1-Dichloropropene or 79-00-5 34511 1,1,2-Trichloroethane ND 21 71-43-2 34030 Benzene -ND 21 75-25-2 32104 Bromoform ND 21 127-18-4 34475 Tetrachloroethylene ND 21- 79-34-5 34516 1,1,2,2-Tetrachloroethane ND 21 108-88-3 34010 Toluene ND. 21 108-90-7 34301 Chlorobenzene ND 21 100-41-4 34371 Ethylbenzene ND 21 Dichlorobenzerie isomers ND 21 I 1,22 Trichforo-1,2,2 trffluoroethane ND 21 67-64-1 81552 Acetone ND 42 75-15-0 77041 Carbon Disuffide ND 63 (con't) 1 _ n I A of 430 FACILITY SAMPLED: FLYNNTAN-BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65649 SAMPLE WEIGHT: 0.160 g FILE NAME(S): 0422BE11 DILUTION FACTOR(S): 1000 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: .04/22/98 SAMPLE RESULTS: pprn Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 7487-3 34418 Chloromethane ND 310 74=83-9 34413 Bromomethane ND 310 75-01-4 39175 Vinyl Chloride ND 310 75-00-3 34311 Chloroethane ND 310 75-09-2 34423 Methylene Chloride ND 310 75-69-4 34488 Trichlorofluoromethane ND 310 75-35-4 34-501 1,1-Dichloroethylene ND 310 75-34-3 34496 1.1-Dichloroethane ND 310 156-60-5 34546. 1,2-Dichloroethylene isomers ND 310 67-66-3 32106 Chloroform ND . 310 07-06-2 34531 1,2-Dichloroethane ND 310 71-55-6 34506 1,1,1-Trichloroethane ND 310 56-23-5 32102 - Carbon Tetrachloride ND 310 75-27-4 32101 Bromodichloromethane ND 310 78-87-5 34541 1,2-Dichloropropene ND 310 10061-02-6 34699 t 1,3-Dichloropropene ND 310 79-01-6 39180 Tdchloroethylene ND 310 12448-1 32105 Dibromochloromethane ND 310 10061-01-5 34704 a-1,3-Dichloropropene and/or ND 310 1,1-Dichloropropene or 79-00-5 34511 1,1,2-Trichloroethane ND 310 71-43-2 34030 Benzene ND 310 75-25-2 32104 Bromoform ND 310 127-18-4 34475 Tetrachloroethylene ND 310 79-34-5 34516 1,1,2,2-Tetrachloroethane 190 310 L 108-88-3 34010 Toluene ND 310 108-90-7 34301 Chlorobenzene ND 310 100-41-4 34371 Ethylbenzene ND -310 Dichlorobenzene isomers ND 310 1.2,2-Trichloro-1,2,2 trifluoroethane ND 310 67-64-1 81552 Acetone ND 620 75-15-0 77041 Carbon Disufflde ND 930 (con't) FACILITY SAMPLED: -FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65650 SAMPLE WEIGHT. 0.083 g FILE NAME(S): 04228E8 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE; Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 7"7-3 34418 Chloromethane ND 30 74-83-9 34413 Bromomethane ND 30 75-01-4 39175 Vinyl Chloride ND 30 75-00-3 34311 Chloroethane ND 30 75-09-2' 34423 Methylene Chloride NO 30 75-69-4 34488 Trichlorofluoromethane ND 30 75-35-4 34501 1,1-Dichloroethylene ND 30 75-34-3 34496 1,1-Dichloroethane ND 30 156-60-5 34546 1,2-Dichloroethylene isomers ND 30 67-66-3 32106 Chloroform ND 30 107-06-2 34531 1,2-Dichloroethane ND 30 71-55-6 34506 1,1,1-Tdchloroethane ND 30 56-23-5 32102 Carbon-Tetrachloride ND 30 75-27-4 32101 Bromodichloromethane ND 30 78-87-5 34541 1,2-Dichloropropane ND 30 10061-02=6 34699 t 1,3-Dichloropropene ND 30 79-01-6 39180 Trichloroethylene ND 30 124-48-1 32105 Dibromochloromethane ND 30 10061-0.1-5 34704 c-1,3-Dichloropropene and/or ND 30 1,1-Dichloropropene or 79-00-5 34511 1,1,2-Tdchloroethane ND 30 71-43-2 34030 Benzene ND 30 75-25-2 32104 Bromoform -ND 30 127-18-4 34475 Tetrachloroethylene ND 30 79-34-5 34516 1,1,2,2-Tetrachloroethane - ND 30 108-88-3 34010 Toluene ND 30 108-90-7 34301 Chlorobenzene ND 30 100-41-4 34371 Ethylbenzene ND 30 Dichlorobenzene isomers ND 30 1,2,2-Trichloro-1,2,2 trifluoroethane ND 30 67-64-1 81552 Acetone ND 60 75-15-0 7704.1 - Carbon Disulfide ND 90 (con't) FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65651 SAMPLE WEIGHT: 0.075 g FILE NAME(S): 04228E12 DILUTION FACTOR(S): 10000 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04I22/98 SAMPLE RESULTS: ppm Reporting CAS STORET : Compound Conc. Limits Comments NO. NO. (uglgm) (ug/gm) TARGET COMPOUNDS 74,47-3 34418 Chloromethane ND 6700 74-83-9 34413 Bromomethane ND . 6700 75-01-4 39175 Vinyl Chloride ND 6700 75-00-3 34311 Chloroethane ND 6700 75-09-2 34423 Methylene Chloride ND 6700 75-69-4 34488 Trichlorofluoromethane ND 6700 75-35-4 34501 1,1-Dichloroethylene ND 6700 75-34-3 34496 1,1-Dichloroethane ND 6700 156-60-5 34546 1,2-Dichloroethylene isomers ND 6700 67-66-3 32106 Chloroform ND 6700 107-06-2 34531 1,2-Dichloroethane ND 6700 71-55-6 34506 1,1,1-Trichloroethane ND 6700 56-23-5 32102 Carbon Tetrachloride ND 6700 75-27-4 32101 Bromodichloromethane ND 6700 78-87-5 34541 1,2-Dichloropropane ND 6700 10061-02-6 34699 t 1,3-Dichloropropene ND 6700 79-01-6 39180 Trichloroethylene ND 6700 124-48-1 32105 Dibromochloromethane ND 6700 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 6700 1,1-Dichloropropene 79-00-5 34511 1,1,2-Tdchloroethane ND 6709 71-43-2 34030 Benzene ND 6700 75-25-2 32104 Bromofonn ND 6706 127-18-4 34475 Tetrachloroethylene ND 6700 79-34-5 34516 1;1.2,2-Tetrachloroethane ND 6700 108-88-3 34010 Toluene ND 6700 108-90-7 34301 Chlorobenzene ND 6700 100-41-4 34371 Ethylbenzene ND 6700 Dichlorobenzene isomers ND -6700 1,2,2-Trichloro-1,2,2 trifluoroethane ND 6700 .67-641 81552 Acetone ND 13400 75-15-0 77041 Carbon Disulfide ND 20100 - (con't) ti FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 65652 SAMPLE WEIGHT: 0.095 g FILE NAME(S): 64228E9 DILUTION FACTOR(S): 50 DATE OF COLLECTION:04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (ug/gm) (ug/gm) TARGET COMPOUNDS 74=87-3 .34418 Chloromethane ND 26 74-83-9 34413 Bromomethane ND 26 75-01-4 39175 Vinyl Chloride ND 26 75-00-3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488 Trichlorofluoromethane ND 26 75-35-4- 34501 1,1-Dichloroethylene ND 26 75-34-3 34496 1,1-Dichloroethane ND 26. 156-60-5 34546 1,2-Dichloroethylene isomers ND 26. 67-66-3 32106 Chloroform ND 26 07-M2 34531 1,2-Dichloroethane . ND 26 71-55-6 34606 1,1,1-Trichloroethane ND 26 56-23-5 32102 Carbon Tetrachloride ND 26 75-27-4 32101 Bromodichloromethane ND- 26 78-87-5 34541 1,2-Dichloropropane. ND 26 10061-02-6 34699 t 1,3-Dichloropropane ND 26 79-01-6 39180 Trichloroethylene ND 26 124-48-1 32105 Dibromochloromethane . ND 26 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 26 1,1-Dichloropropene or 79-00-5 34511 1,1,2-Trichloroethane ND 26 71-43-2 34030 Benzene ND 26 75-25-2 32104 Bromoform ND 26 127-18-4 34475 Tetrachloroethylene ND 26 79-34-5 34516. 1,1,2,2-Tetrachioroethane ND 26 108-88-3 34010 Toluene ND 26 108-90-7 34301 Chlorobenzene' ND 26 100-41-4 34.371 Ethylbenzene ND 26 Dichiorobenzene isomers ND 26 1,2,2-Trichloro-1,2,2 trifluoroethane ND 26 67-64-1 81552 Acetone ND' 52 75-15-0 77041 Carbon Disulfide . ND 78 (con't) FACILITY-SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS -DRUM SAMPLE ID: 67261 SAMPLE WEIGHT: 0.080 g FILE NAME(S): 04228E14 -DILUTION FACTOR(S): 5000 DATE OF COLLECTION: 04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04122/98 SAMPLE RESULTS: ppm Reporting CA$ STORET Compound Conc. Limits Comments NO. NO, (ug/gm)" (ug/gm) TARGET COMPOUNDS 74-87-3 34418 Chloromethane NO 3100 7483-9 34413 Bromomethane ND 3100 75-01-4 39175 Vinyl Chloride NO 3100 75-00-3 34311 Chloroethane NO 3100 75-09-2 34423 Methylene Chloride NO 3100 75-69-4 34488 Trichlorofluoromethane NO 3100 75-35-4 34501 1,1-Dichloroethylene NO 3100 75-34-3 34496 1,1-Dichloroethane ND 3100 156-60-5 34546 1,2-Dichloroethylene isomers NO 3100 67-66-3 32106 Chloroform ND 3100 107-06-2 34531 1,2-Dichloroethane NO 3100 71-55-6 34506 1,1,1-Trichloroethane NO 3100 56-23-5 32102 Carbon Tetrachloride NO 3100 75-27-4 32101 Bromodichloromethane NO 3100 78-87-5 34541 1,2-Dichloropropane NO 3100 10061-02-6 34699 t 1,3-Dichloropropene NO 3100 79-01-6 39180 Trichloroethylene NO 3100 124-48-1 32105 Dibromochloromethane ND 3100 10061-01-5 34704 o-1,3-Dichloropropene and/or NO 3100 1,1-Dichloropropene of 79-00-5 34511 1,1,2-Trichloroethane NO 3100 71-43-2 34030 Benzene NO 3100 75-25-2 32104 Bromoform NO 3100 127-18-4 34475 Tetrachloroethylene NO 3100 79-34-5 34516 1,1,2,2-Tetrachloroethane NO 3100 108-88-3 34010 Toluene ND 3100 108-90-7 -34301 Chiorobenzene NO 3100 100-41-4 34371 Ethylbenzene NO 3100 Dichlorobenzene isomers NO 3100. 1,2,2-Trichloro-1,2,2 trifluoroethane ND 3100 67-64-1 81552 Acetone ND 6200 75-15-0 77041 Carbon Disulfide NO 9300 (con't) FACILITY SAMPLED: FLYNNTAN BUILDING US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS PURGEABLE ORGANIC ANALYSIS-DRUM SAMPLE ID: 67260 SAMPLE WEIGHT: 0.095 g FILE NAME(S): 0422BE10 DILUTION FACTOR(S): 50 DATE OF COLLECTION:-04/16/98 PRESERVATIVE: Cool to 4 C DATE OF ANALYSIS: 04/22/98 SAMPLE RESULTS: ppm Reporting CAS STORET Compound Conc. Limits Comments NO. NO. (u9/9m) (u9/9m) TARGET COMPOUNDS 74-$7-3 34418 Chloromethane ND 26 74483-9 34413 Bromomethane ND 26 75-01-4 39175 Vinyl Chloride ND 26 75-00-3 34311 Chloroethane ND 26 75-09-2 34423 Methylene Chloride ND 26 75-69-4 34488. Trichlorofluoromethane ND 26 75-35-4 34501 1,1-Dichloroethylene ND 26 ..75-34-3 34406 1,1-Dichloroethane ND 26 156-60-5 34546 1,2-Dichloroethylene isomers ND 26 67-66-3 32106 Chloroform ND 26 ;07-06-2 34531 1,2-Dichloroethane ND 26 71-55-6 34506 1,1,1-Tdchloroethane ND 26 56-23-5 32102 Carbon Tetrachloride ND 26 75-27-4 32101 Bromodichloromethane ND 26 78-87-5 34541 1,2-Dichloropropane ND 26 10061-02-6 34699 t 1,3-Dichloropropene ND 26 79-01-6 39180 Trichloroethylene ND 26 124-48-1 32105 Dibromochloromethane ND 26 10061-01-5 34704 c-1,3-Dichloropropene and/or ND 26 1,1-Dichloropropene or 79-00-5 34511 1,1,2-Trichloroethane ND 26 71-43-2 34030 Beniene ND 26 75-25-2 32104 Bromoform ND 26 127-18-4 34475 Tetrachloroethylene ND 26 79-34-5 34516 1,12,2-Tetrach1oroethane ND 26 108-88-3. 34010 Toluene ND 26 108-90-7 34301 Chlorobenzene ND 26 100-41-4 34371 Ethylbenzene ND 26 Dichlorobenzene isomers ND 26 1,22-Trichloro-1,22 trifluoroethane ND 26 67-64-1 81552 Acetone N0 52 75-15-0 77041 Carbon Disulfide ND 78. (con't) .. 97 of 7A APPENDIX G Semivblatile Organic Compound Analytical-Data 'w ; UN(TED STATES ENVIRONMENTAL PROTECTION AGENCY a % REGION 1 ENVIRONMENTAL SERVICES DIVISION 60 WESTVIEW STREET �c LEXINGTON,MASSACHUSETTS 02173-3185 )ATE: May 20, 1998 'UBJ: Gas Chromatography Analysis of Extractable Organics in a Aqueous Sample - FLYNN TANNERY ?ROM: Dick Siscakw, Chemistry Section PHRU4 Dr. William J_ Andrade, Advance 67 Analytical Chemistry Specialist l� TO: Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received and logged in by the laboratory according to . the SOP for Sample Log-in (EIA-ADMLOGNI.SOP, 7/97) . EPA Region 1 Procedure: Base Neutral Acids Extractables in Acrueous Samples, BNAWAHLI.SOP, 12/4/91. The samples are extracted using methylene chloride as the solvent. The. extracts are analyzed on a gas chromatograph equipped with a FID detector. Of The analytical support for this report was performed by ESAT contractors . Date (s) Samples Received by the Laboratory: 4/17/98- Date Analysis Started: 04/22/98 cc: Fil-e:. J: \CHEMSTRY\REPORTS\BNA\98267WB.WPD - O.rw1.A/R..vrl�hl�.Prb"d volt Vanet�m.n7 a-4 MIR nn V VPL Q—m4 A Panar(An%Padd=NM merf US ENVIRONMENTAL PROTECTION AGENCY 60 Westview Street Lexington, MA 02173 ANALYTICAL PARAMETERS INSTRUMENTS:! Hewlett Packard 5890 Gas Chromatograph Hewlett Packard 5987 Gas Chromatograph-Mass Spectrometer xGC/FID Screening Conditions: Gas: Hydrogen Capillary Column: DB-1, 30m, 25mm ID-, 0.25 micron film thickness Injection Mode: Splitless Temperature Program: Isothermal for 3 min at 40°C, programmed at 15'C/min to 3200C for 3 min GC-MS Conditions: Gas: Helium Capillary Column: DB-5, 60m, 25mm ID, 0.25. micron film thickness w " Injection Mode: Splitless Temperature Program: Isothermal for 4 min at 40°C, programmed at VC/min. to 3000C Injector, Transfer Temperatures: 290°C, 3000C Electron Energy: 70 V Mass Range: 35-550 Scan Rate: 6.9 seconds 3 I FACILITY SAMPLED: FLYNN TANK US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Matrix: Water DATE OF COLLECTION: NA Sample pH: N/A DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report -Factor: 25 SAMPLE RESULTS:. CAS ' Compound Conc. RL Qualifier NO. (ug/L) (�zg/L) or Comment ------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND 160 309-00=2- Aldrin ND 160 56-55-3 Benzo (a) anthracene ND 160 205-99-2 Benzo (b) fluoranthene ND 160 207-08-9 Benzo (k) fluoranthene ND 160 50-32-8 Benzo (a)pyrene. ND 160 191-24-2 Benzo (ghi)perylene ND 160. 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 319-86-8 delta-BHC ND 160 111-44-4 Bis (2-chloroethyl) ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND 160 117-81-7 Bis (2-ethylhexyl)phthalate ND 190 108-60-1 Bis'(2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene. ND 160 95-57-8 2-Chlorophenol ND-. 310 7005-72-3 4-Chlorophenylphenyl ether ND 160 218-01-9 Chrysene ND 160 72-54-8 4,4'-DDD ND 166 72-55-9 4, 4 ' -DDE ND 16.0 50-29-3 4, 4-'-DDT ND 160 53-70-3 Dibenzo(a,h)anthracene ND 160 84-74-2 Di-n-butylphthalate ND 160 541-73=1 1,3-Dichlorobenzene ND _ 160 (cont. ) 5 i US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Sample Results Continued: CAS Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment ------------------------------------------------------------------------ 120-82-1 1,2, 4-Trichlorobenzene ND 160 8B-06-2 2, 4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51-=6 Benzyl Alcohol ND 160 106-47-8 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND . 160 95-48-7 2-Methylphenol ND 166 106-44-5 4-Methylphen6l ND 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND 160 100-01-6 4-Nitroaniline ND 160. 95-95-4 2,4,5-Trichlorophenol, ND 160 Other Compounds Quantitated w Diphenylhydrazine ND 160 (azobenzene) Est. Tentatively Identified Conc. Compounds (ug/L) None detected ND 7 FACILITY SAMPLED: FLYNN TANK US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65646 Matrix: Water DATE OF COLLECTION: 04/16/98 Sample pH: NIA DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound Conc. AL Qualifier NO. (ug/L) (ug/L) or Comment ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND 160 :309-00-2 Aldrin ND 160 56-55-3 Benzo(a) anthracene ND 160 205-99-2 Benzo(b) fluoranthene ND 160 207-08-9 Benzo (k) fluoranthene ND 160 50-32-8 Benzo(a)pyrene. ND 160 191-24-2 Benzo(ghi)perylene ND 160 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 319-86-8 delta-BHC ND 160 1,11-44-4 Bis (2-chloroethyl)ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND 16& 117-81-7 Bis (2-ethy1hexyl)phtha1ate 40 160 L 108-60-1 Bis (2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene ND 160 95-57-8 . 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyl ether ND 160 218-01-9 Chrysene ND 160 72-54-8 4,4'-DDD ND 160 72-55-9 4, 4'-DDE ND 160 50-29-3 4, 4'-DDT ND 160 53-70-3 Dibenzo (a,h) anthracene ND 160 84-74-2 Di-n-butylphthalate ND 160 541-73-1 1,3-Dichlorobenzene ND 160 (cont. ) i 9 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65646 Sample Results Continued: `CAS Compound Conc. RL Qualifier NO. (ug/L) .(ud/L) or Comment ------------------------------------------------------------------------ 120-82-1 1,2,.4-Trichlorobenzene ND 160 88-06-2 2, 4, 6-Trichlorophenol ND - 310 Hazardous Substances 65-53=3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 :00-51-6 Benzyl Alcohol ND 160 106-47-8 . 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 1.60 91-57-6 2-Methylnaphthalene ND 160 95-48-7 2-Methylphenol ND 160 106-44-5 4-Methylphenol ND 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND 160 100-01-6 4-Nitroaniline ND 160y. 95-95-4 2, 4, 5-Trichlorophenol ND 160 Other Compounds Quantitated Diphenylhydrazine ND 160 (azobenzene) . Est. Tentatively Identified Conc. Compounds (ug/L) C12 Hydrocarbon 200, 000 J Organic Acid 100, 000 J Organic Acid C18 Hydrocarbon 100, 000 J Organic Acid (poss. C18) 30, 000 J - 11 FACILITY SAMPLED.: FLYNN TANN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652 Matrix: Water DATE OF COLLECTION: 04/16/98 Sample pH: :N/A DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound -Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND 160 309-00-2 Aldrin ND 160 56-55-3 Benzo (a) anthracene ND 160 205-99-2 Benzo (b) fluoranthene ND 160 207-08-9 Benzo (k) fluoranthene ND 160 50-32-8 Benzo(a)pyrene ND 160 191-24-2. Benzo (ghi)perylene - ND 160 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 319-86-8 delta-BHC ND 160 111-44-4 Bis (2-chloroethyl)ether ND 160 111-91-1 Bis (2-chloroethoxy)methane ND 160 117-81-7 Bis (2-ethylhexyl)phthalate ND 16t 108-60-1 Bis (2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene ND 160 95-57-8 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyl ether- ND 160 218-01-9 Chrysene ND 160 72-54-8 4, 4 '-DDD ND 160 72-55-9 4, 4 '-DDE ND 160 50-29-3 4, 41-DDT ND 160 53-70-3 Dibenzo(a,h) anthracene ND 160 84-74-2 Di-n-butylphthalate ND 160 541-73-1. 1, 3-Dichlorobenzene ND - 160 (cont. ) i - 13 , US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65652 Sample Results Continued: CAS * Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment --------------------------------------------- --------------------- iiO-82-1- 1, 2, 4-Trichlorobenzene ND 160 98-06-2 2, 4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51=6 Benzyl Alcohol ND 16.0 106-47-8 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND 160 95-48-7 2-Methylphenol ND 160 106-44-5 4-Methylpllenol ND- 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND i60 100-01-6 4-Nitroaniline ND 160 95-95-4 2, 4, 5-Trichl6rophenol ND 160 Other Compounds Quantitated w Diphenylhydrazine ND 160 (azobenzene) Est. Tentatively Identified Conc. Compounds (ug/L) Unknown 100 J C12 Hydrocarbon 200 J Methylene bis (dimethyl diethyl) methyl phenol 200 - J i 15 FACILITY SAMPLED: FLYNN TANN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67260 Matrix: Water DATE OF COLLECTION: 04/16/9.8 Sample' pH: N/A DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor: None VOLUME EXTRACTED: 40 mL Report Factor: 25 SAMPLE RESULTS: CAS Compound Conc. Rh Qualifier NO. (ug/L) (ug/L) or Comment ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 160 208-96-8 Acenaphthylene ND 160 120-12-7 Anthracene ND. 160 309-00-2 Aldrin ND 160 56-55-3 Benzo(a) anthracene - ND 160 205-99-2 -Benzo (b) fluoranthene ND 160 207-08-9 Benzo (k) f luoranthene ND 160 50-32-8 Benzo (a)pyrene ND 160 191-24-2 Benzo.(ghi)perylene ND 160 85-68-7 Butyl Benzyl Phthalate ND 160 319-85-7 beta-BHC ND 160 .319-8.6-8 delta-BHC ND 160 111-44-4 Bis (2-chloroethyl)ether ND 160 ill-91-1 Bis (2-chloroethoxy)methane ND. 16% 117-81-7 Bis (2-ethylhexyl)phthalate ND 160 108-60-1 Bis (2-chloroisopropyl) ether ND 160 101-55-3 4-Bromophenylphenyl ether ND 160 86-74-8 Carbazole ND 160 59-50-7 4-Chloro-3-methylphenol ND 310 91-58-7 2-Chloronaphthalene ND 160 95-57-8 2-Chlorophenol ND 310 7005-72-3 4-Chlorophenylphenyl ether ND _ 160 218-01-9 Chrysene ND 1.60 72-54-8 4, 4 '-DDD ND 160 72-55-9 4, 4'-DDE ND 160 50-29-3 4, 4'-DDT ND 160 53-70-3 Dibenzo (a,h) anthracene ND 160- 84-74-2 'Di-n-butylphthalate ND _ 160 541-73-1 • 1, 3-Dichlorobenzene ND 160 (cont.) 17 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67260 Sample Results Continued: CAS Compound Conc. RL Qualifier NO. (ug/L) (ug/L) or Comment -;----.------------------------------------------------------------------ 120-82-1 1,2, 4-Trichlorobenzene ND 160 &8-06-2 2,4, 6-Trichlorophenol ND 310 Hazardous Substances 65-53-3 Aniline ND 160 65-85-0 Benzoic Acid ND 310 100-51-6 Benzyl Alcohol ND 160 106-47-8 4-Chloroaniline ND 160 132-64-9 Dibenzofuran ND 160 91-57-6 2-Methylnaphthalene ND 160 - 95-48-7 2-Methylphenol ND 160 106-44-5 4-Methylphenol ND 160 88-74-4 2-Nitroaniline ND 160 99-09-2 3-Nitroaniline ND - 160 100-01-6 4-Nitroaniline ND 160 95-95-4 2,4,5-Trichlorophenol ND 160 Other Compounds Quantitated w Diphenylhydrazine ND 160 (azobenzene) Est. Tentatively Identified Conc: Compounds (ug/L) None detected ND i i 19 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 1 ENVIRONMENTAL SERVICES DIVISION F 60 WESTVIEW STREET �c £ LEXINGTON,MASSACHUSETTS 02173,318s DATE: May 21, 1998 SUBJ: Gas Chromatography-Mass Spectrometry Analysis of Extractable Organics in Soils and Sediments - FLYNN TAN FROM: Dick Siscanaw;" Chemistry Section THRU,: Dr. William J. Andrade, Advai)ced. Analytical Chemistry Specialist TO: Tom Hatzopoulos, PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received and logged in by the laboratory according to the SOP for Sample Log-in (EIA-ADMLOGN1.SOP., 7/97). . EPA Region I Procedure: High Level BNA Analyses for Drum andtor Pure Product Samples, BNADRML2.SOP. The modules used for this procedure were: GC/FID_ Screening of BNA Extracts, BNASCRE4.BNA, Gas Chromatography/Mass Spectrometry Analysis-of Semivolatile Organics, BNAENVII.MOD, Quality Control -Module, QC3.MOD. All Values are reported out on a dry weight basis. w The analytical support for this report was performed by ESAT contractors. Date (s) Samples Received by the Laboratory: 04/17/98 Date Analysis Started: 04/22/98 cc: File: J: \CHEMSTRY\REPORTS\BNA\98267DB.WPD R•cvdedM-7dab10.PdMed with Vegetable OI Based toles on 100%Recvdad Paper(40%Postaonsumeo 1 - f 7 U.S. EPA REGION I LABORATORY Semivolatile Organic Analyses WATER MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Sample No. : Dates) Analyzed: Spike Sample MS QC Added Conc. -Conc. MS $ Limits Compound (ug/L) (ug/L) (ug/L) Rec Rec Phenol 1562 0 1400 90 12-110 2-Chlorophenol 1562 0 1500 96 27-123 s1, 4-Dichlorobenzene 781 0 760 97 36-97 N-Nitroso-di-n-prop. (1) 781 0 710 gl 41-1I6 `1, 2, 4-Trichlorobenzene 781 0 670 86 39-98 - 4-Chloro-3-methylphenol 1562 0 1200 77 23-97 Acenaphthene 781 0 660 85 46-1.18 4-Nitrophenol 1562. 0 1200 77 10-80 2, 4-Digitrotoluene 781 0 490 63 24-96 Pentachlorophenol 1562 0 1300. 83 9-103 Pyrene 781 0 690 88 26-127 Spike MSD Added Conc. MSD % % QC LIMITS Compound (ug/L) (ug/L) Rec RPD RPD Rec Phenol 1562 1600 102 13 42 12-110 2-Chlorophenol 1562 1600 102 6 40 -27-123 1, 4-Dichlorobenzene 781 780 100 3 28 36-97 j N-Nitroso-di-n-prop. (I) 781 770 99 8 38 41-116 1, 2, 4-Trichlorobenzene 781 730 93 8 2W 39-98 4-Chloro-3-methylphenol 1562 1360 83 8 42 23-97 Acenaphthene 781 710 91 7 31 46-118 4-Nitrophenol 1562 1300 83 8 50 10-80 2, 4-Dinitrotoluene 781 490 63 0 38 24-96 Pentachlorophenol 1562 1300 83 0 50 9-103 Pyrene 781 730 93 5 31 26-127 (1) N-Nitroso-di-n-propylamine- *_ Values outside of QC limits RPD: 0 out of 11 outside limits Spike Recovery: - 0 out of 22 outside limits 1 ' e US ENVIRONMENTAL PROTECTION AGENCY ! 60 Aestview Street i Lexington, MA 02173 ANALYTICAL PARAMETERS INSTRUMENTS: Hewlett Packard 5890 Gas Chromatograph Hewlett Packard 5987 Gas Chromatograph-Mass Spectrometer: GC/FID Screening Conditions: Gas: Hydrogen ' Capillary Column: DB-1, 30m, 25mm ID, 0.25 micron film thickness Injection Mode: Splitless Temperature Program! Isothermal for -3 min at 40°C, programmed at 150C/min to 3200C for 3 min GC-MS. Conditions: Gas: Helium Capillary Column: DB-5, 60m, 25mm PD, 0.25 micron film thickness Injection Mode: Splitless Temperature Program: Isothermal for 4 min at 40`C, programmed at 7°C/min to - 300°C Injector, Transfer. Temperatures: 290°C, 3000C Electron .Energy: 70 V. Mass Range: 35-550 i Scan Rate: 0.9 seconds I 5 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Matrix: Drum DATE OF COLLECTION: Not Applicable Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 1 mL DATE OF- ANALYSIS: . 04/24/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.200 g Report Factor 1 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------- Priority Pollutants 83-32-9 Acenaphthene ND 300 208--96-8 Acenaphthylene ND 300 120-12-7 Anthracene ND 300 309-00-2 Aldrin ND 300 56-55-3 Benzo (a)anthracene ND 300 205-99-2 Benzo (b) fluoranthene ND 300 207"08-9 Benzo (k) fluoranthene ND 300 50-32-8 Benzo (a)pyrene ND 300 191-24-2 Benzo (ghi)perylene -ND 300 85-68-7 Butyl Benzyl Phthalate ND 300 319-85-7 beta-BHC ND 300 319-86-8 delta-BHC ND 300 111-44-4 Bis (2-chloroethyl)ether ND 30gr 111-91-1 Bis (2-chloroethoxy)methane ND 300 117-81-7 Bis (2-ethylhexyl)phthala,te ND 300 108-60-1 Bis (2-chloroisopropyl) ether ND 300 101-55-3 4-Broinophenylphenyl ether ND 300 86-74-8 Carbazole ND 300 59-50-7 4-Chloro-3-methylphenol - ND 600 91-58-7 2-Chloronaphthalene ND 300 95-57-8 2-Chlorophenol ND 600 7005-72-3 4-Chlorophenylphenyl ether ND 300 218-01-9 Chrysene ND 300 72-54-8 4, 4'-DDD ND 300 72-55=9 4,-4--DDE ND 300 50-29-3 4, 4 '-DDT ND 300 53-70-3 Dibenzo(a,h)anthracene ND 300 (con Tt) 7 i i US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : BLANK Results Continued: ; . CAS Compound . Conc. - RL Qualifier -NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ 120-82-1 1,2, 4-Trichlorobenzene ND 300 88-06-2 214, 6-Trichlorophenol ND 600 Hazardous Substances 65-53-3 Aniline ND _ 300 65-85-0 Benzoic Acid ND 600 100-51-6 Benzyl Alcohol ND 300 106-47-8 4-Chloroaniline ND 300 132-64-9 , Dibenzofuran ND 300 91-57-6 2-Methylnaphthalene ND 300 95-48-7 2-Methylphenol ND 300 106-44-5 4-Methylphenol ND 300 88-74-4 2-Nitroaniline ND 300 99-09-2 3-Nitroaniline ND 300 100-01-6 4-Nitroaniline ND 300. 95-95-4 2,4, 5-Trichlorophenol ND 300r Other Compounds Quantitated None detected ND 300 Est. Tentatively Identified Conc. ' Compounds (mg/Kg) None detected ND i 9 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.256 g Report Factor 0.78 RESULTS: GAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acehaphthene ND 230 208-96-8 Acenaphthylene ND 230 120-12-7 Anthracene ND 230 309-00-2 Aldrin ND 230 56-55-3 Benzo(a) anthracene ND 230 205-99-2 Benzo(b) f luoranthene ND 230 207-08-9 Benzo (k) fluoranthene ND 230 50-32-8 Benzo (a)pyrene ND 230 191-24-2 Benzo (ghi)perylene ND 230 85-68-7 Butyl Benzyl Phthalate ND 230 319-85-7 beta-BHC ND 230 319-86-8 delta-BHC ND 230 111-44-4 Bis (2-chloroethyl) ether ND 23W. 111-91-1 Bis (2-chloroethoxy)methane Nb 230 117-81-7 Bis (2-ethylhexyl)phthalate ND 230 108-60-1 Bis (2-chloroisopropyl)ether ND 230 101-55-3 4-Bromophenylphenyl ether ND 230 86-74-8 -Carbazole ' ND -230 59-50-7 4-Chloro-3-methylphenol ND 470 91-58-7 2=Chloronaphthalene ND 230 95-57-8 2-Chlorophenol ND 470 7005-72-3 4-Chlorophenylphenyl ether ND 230 218-01-9 Chrysene ND 230 72-54-8 4, 4 '-DDD ND 230 72-55-9 4, 4 '-DDE ND 230 50-29-3 -4, 4'-DDT ND 230 53-70-3 Dibenzo (a,h) anthracene ND 230 (con't) i� US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65645 Results Continued: CAS Compound Conc. RL. Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------ 120-82-1 1, 2,4-Trichlorobenzene ND 230 88-06-2 2, 4, 6-Trichlorophenol ND �470 Hazardous Substances 65-53-3 Aniline ND 230 65-85-0 Benzoic Acid . ND 470 100-51-6 Benzyl Alcohol ND 230 106-47-8 4-Chloroaniline ND 230 132-64-9 Dibenzofuran ND 230 91-57-6 2-Methylnaphthalene ND 230 95-48-7 2-Methylphenol ND 230 106-44-5 4-Me.thylphenol ND 230 88-74-4 2-Nitroaniline ND 230 99-09-2 3=Nitroaniline ND 230 100-01-6 4-Nitroaniline ND 230 95-95-4 2, 4,5-Trichlorophenol ND 230 ---------------------------- Other Compounds Quantitated w ---------------------------- None detected ND 230 • ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- None detected ND i i 13 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65647 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor None . WET WEIGHT EXTRACTED: 0.87 g Report Factor 0.87 RESULTS: CAS'- AS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------- Priority Pollutants 83-32-9 Acenaphthene ND 260 208-96-8 Acenaphthylene ND 260 120-12-7 Anthracene ND 260 309-00-2 Aldrin . ND 260 56-55-3 Benzo(a) anthracene ND 260. 205-99-2 Benzo (b) fluoranthene ND 260 207-08-9 Benzo (k) fluoranthene ND 260 50-32-8 - Benzo(a)pyrene ND. 260 191-24-2 Benzo (ghi)perylene . ND 260 85-68-7 Butyl Benzyl Phthalate ND 260 319-85-7 beta-BHC ND 260 319-86-8 delta-BHC ND 26W 111-44-4 Bis (2-chloroethyl)ether ND 260 111-91=1 Bis (2-chloroethoxy)methane ND 260 117-81-7 Bis (2-ethylhexyl)phthalat.e ND 260 108-60-1 Bis (2-chloroisopropyl) ether ND 260 101-55-3 4-Bromophenylphenyl ether ND 260 86-74-8 Carbazole ND 260 59-50-7 4-Chloro-3-methylphenol ND 520 91-58-7 2-Chloronaphthalene ND 260 95-57-8 2-Chlorophenol ND 520 7005-72-3 4-Chlorophenylphenyl ether ND 260 218-01-9 Chrysene ND 260 72-54-8 4,4'-DDD ND 260 72-55-9 4,4'-DDE ND 260 50-29-3 4,4'-DDT ND _ 260 53-70-3 Dibenzo (a.h) anthracene ND 260 (con't) 1.5 1 - US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC. ANALYS-IS SAMPLE NO. : 65647 Results Continued: CAS Compound Conc. RL Qualifier NO, (mg/Kg) (mg/Kg) or Comment ----------------------------------------------------------- --------- 1'20-82-1 1,2, 4-Trichlorobenzene ND .260 88-06-2 2, 4, 6-Trichlorophenol ND � 520 ---------------------------- Hazardous Substances ----------- - ---- 65-53-3 Aniline ND 260 65-85-0 Benzoic Acid ND 520 100-51-6 Benzyl Alcohol ND 260 106-47-8 4-Chloroaniline ND 260 132-64-9 . Dibenzofuran NO 260 91-57-6 2-Methylnaphthalene ND 260 95-48-7 2-Methylpheno1 ND 260 106-44-5 4-Methylphen0'1 ND 260 88-74-4 2-Nitroaniline ND 260 99-09-2 3-Nitroaniline ND 260 100-01-6 4-Nitroaniline ND 260 95-95-4 2, 4,5-Trichlorophenol ND 260. ---------------------------- Other Compounds Quantitated rr ---------------------------- None detected ND 260 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Cyclotetra siloxane, octa methyl 2800 J Cyclopenta siloxane, deca methyl 2000 J Cyclohexa siloxane, dodeca methyl 5000 J Siloxane product 3600 J Siloxane product 810 J 17 FACILITY SAMPLED: FLYNN TAN- US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY. GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/24/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.172 g Report Factor- 1 .16 a - RESULTS: GAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 350 208-96-8 Acenaphthylene ND 350 .120-12-7 Anthracene ND 350 309-00-2 Aldrin ND 350 56-55-3 Benzo (a) anthracene ND 350 205-99-2 Benzo (b) fluoranthene ND 350 207-08-9 Benzo (k) fluoranthene ND 350 50-32-8 Benzo (a)pyrene ND 350 191-24-2 Benzo (ghi)perylene ND 350 85-68-7 Butyl Benzyl Phthalate ND 350 319-85-7 beta-BHC ND 350 319-86-8 delta-BHC ND 35% 111-44-4 Bis (2-chloroethyl) ether ND 350 111-91-1 Bis (2-chloroethoxy)methane ND 350 117-81-7 Bis (2-ethylhexyl)phthalate ND 350 108-60-1 Bis (2-chloroisopropyl) ether ND 350 101-55-3 4-Bromophenylphenyl ether ND 350 86-74-8 Carbazole ND 350 59-50-7 4-Chloro-3-methylphenol ND 700 91-58-7 2-Chloronaphthalene ND 350 95-57-8 2-Chlorophenol ND 700 7005-72-3 4-Chlorophenylphenyl ether ND 350 . 218-01-9 Chrysene. ND 350 72-54-8- 4, 4'-DDD ND 350 72-55-9 4, 4'-DDE ND 350 50-29-3 4,4'-DDT ND _ 350 j 53-70-3 Dibenzo (a,h) anthracene ND 350 (con't) I - 19 OS ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65649 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment 120-82-1 1,2, 4-Trichlorobenzene ND 350 88-06-2 2, 4, 6-.Trichlorophenol. ND 700 ---------------------------- Hazardous Substances 65-53-3 Aniline ND 350 65-85-0 Benzoic Acid ND 700 100-51-6 Benzyl Alcohol ND 350 106-47-8 4-Chloroaniline ND 350 132-64-9 Dibenzofuran ND 350 91-57-6 2-Methylnaphthalene ND 350 95-48-7 2-Methylphenol ND 350 .106-44-5 4=Methylphenol ND -350 88-74-4 2-Nitroaniline ND 350 99-09-2 3-Nitroaniline ND 350 100-01-6 4-Nitroaniline ND 350 95-95-4 2,4, 5-Trichlorophenol ND 350rr ---------------------------- Other Compounds Quantitated. i ---------------------------- None detected ND 350 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Hydrocarbon 2000 J C12 Hydrocarbon 5000 J Hydrocarbon 2000. J C12 Hydrocarbon 2000 _ jr C12 Hydrocarbon 3000 J note: light petroleum product i . 21 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY - GC /MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65651 Matrix: Drum DATE . OF COLLECTION: - 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol . 10 mL DATE OF. ANALYSIS: 04/30/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.151 g - Report Factor 1.3 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments --------------------------------------- -------------------- Priority Pollutants 83-32-9 Acenaphthene ND 390 208-96-8 Acenaphthylene ND 390 120-12-7 Anthracene ND 39.0 309-00-2 Aldrin ND 390 56-55-3 ; Benzo(a)anthracene ND 390 205-99-2 Benzo(b) fluoranthene ND 390 207-08-9 Benzo(k.) fluoranthene- ND 390 50-32-8 Benzo(a)pyrene ND 390 191-24-2 Benzo(ghi)perylene . ND 390 85-68-7 Butyl Benzyl Phthalate ND 390 319-85-7 beta-BHC ND 390 319-86-8 delta-BHC ND 39% 111-44-4 Bis (2-chloroethy-1)ether ND 390 111-91-1 Bis ('2-chloroethoxy)methane ND .390 117-81-7 Bis (2-ethylhexyl)phthalate ND 390 108-60-1 Bis (2-chloroisopropyl) ether ND 390. 101-55-3 4-Bromophenylphenyl ether ND 390 86-74-8 Carbazole ND 390 59-50-7 4-Chloro-3-methylphenol ND 780 91-58-7 2-Chloronaphthalene ND 390 95-57-8 2-Chlorophenol ND 780 7005-72-3 4-Chlorophenylphenyl ether ND 390 218-01-9 Chrysene ND 390 72-54-8 4, 4'-DDD ND -390 72-55-9 4, 4'-DDE ND 390 50-29-3 4, 4'-DDT ND _ ..390 ;53-70-3 Dibenzo(a,h) anthracene ND 390 (con't) i 23 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65651 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment --------------------------------------------------------------------- 120-82-1 1,2, 4-Trichlorobenzene ND 390 88-06-2 .2, 4, 6-Trichlorophenol ND 780 ---------------------------- Hazardous Substances ---------------------------- 65-53-3 Aniline ND 390 65-85-0 Benzoic 'Acid ND 780 100-51-6 Benzyl Alcohol ND 390 106-47-8 4-Chloroaniline ND 390 132-64-9 Dibenzofuran ND 390 91-57-6 2-Methylnaphthalene 90 390 L 95-48-7 2-Meth ND 390 106-44-5 4-Methylphenol ND -390 88-74-4 2-Nitroaniline ND 390 99-09-2 3-Nitroaniline ND 390 100-01-6 4-Nitroaniline ND 390 95-95-4 2,4, 5=Trichlorophenol_ ND 390 ---------------------------- Other Compounds Quantitated w ------------------- None detected ND 390 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Nonane 3000 J Hydrocarbon (C10) 3000 _ J Benzene Alkyl (C3) 3000 J C12 Hydrocarbon 9000 J C12 Hydrocarbon 5000 J note: light petroleum product 25 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65644 Matrix: Drum DATE. OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/30/98 Dilution Factor 1: 10 WET WEIGHT EXTRACTED: 0.178 g Report Factor 11 RESULTS: CAS Compound Conc. kL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ----------------------------- ------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND 3300 208-96-8 Acenaphthylene ND 3300 120-12-7 Anthracene ND 3300 309-00-2 Aldrin ND 3300' 56-55-3 Benzo (a) anthracene ND 3300 205-99-2 Benzo(b) fluotanthene ND 3300 207-08-9 Benzo (k) fluoranthene ND 3300 50-32-8 Benzo(a)pyrene ND 3300 191-24-2 Benzo (ghi)perylene ND 3300 85-68-7 Butyl Benzyl Phthalate ND 3300 319-85-7 beta-BHC ND 3.300 319-86-8 delta-BHC ND 33000 111-44=4 Bis (2-chloroethyl) ether ND 3300 111-91-1 Bis (2-chloroethoxy)methane ND 3300 117-81-7 Bis (2-ethylhexyl)phthalate ND 3300 108-60-1 Bis (2-chloroisopropyl) ether ND 3300 101-55-3 4-Bromophenylphenyl ether- ND 3300 86-74-8 Carbazole. ND 3300 59-50-7 4-Chloro-3-methylphenol ND 6600 91-58-7 2-Chloronaphthalene ND 3300 95-57-8 2-Chlorophenol ND 6600 7005-72-3 4-Chlorophenylphenyl. ether ND 3300 218-01-9 Chrysene ND 3300 72-54-8 4, 4'-DDD ND 3300- 72-55-9 4, 4--DDE ND 3300 50-29-3 4,4'-DDT ND 3300 53-70-3 Dibenzo (a,h)anthracene ND 3300- (con't) i 27 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65644 Results Continued: CAS Compound Conc. RL Qualifier NO. .(mg/Kg) (mg/Kg) or Comment 120-82-1 1,2, 4=Trichlorobenzene ND .3300 88-06-2 2,4, 6-Trichlorophenol ND 6600 ---------------------------- _ Hazardous Substances ---------------------------- 65-53-3 Aniline ND 3300 65-85-0 Benzoic Acid ND 6600 100-51-6 Benzyl Alcohol ND 3300 106-47-8 4-Chloroaniline ND 3300 132-64-.9 Dibenzofuran -ND 3300 91-57-6 2-Methylnaphthalene 2000 3300 L 95-48-7 2-Methylphenol ND 3300 106-44-5 4-Methylphenol ND 3300 88-74-4 2-Nitroaniline . ND 3300 99-09-2 3-Nitroaniline ND 3300 100-01-6 4-Nitroaniline ND 3300 95-95-4 2, 4, 5-Trichlorophenol ND 3300 ---------------------------- Other Compounds Quantitated or ---------------------------- None detected ND 3300 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Hydrocarbon (C8) 6000 J C14- Hydrocarbon 6000 J C16 Hydrocarbon 6000 J C16 Hydrocarbon 6000 J C18 Hydrocarbon 10000 - J note: Petroleum Product. Possible mix of light petroleum and fuel no. 2. 29 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : ' 67261 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 mL DATE OF ANALYSIS: 04/30/98 Dilution Factor 1:10 WET WEIGHT EXTRACTED: 0.164 g Report_ Factor 12 RESULTS: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comments ---------------------------------------------------------------------=-- Priority Pollutants 83-32-9 Acenaphthene ND 3600 208-96-8 Acenaphthylene ND 3.600 120-12-7 Anthracene. ND 3600 309-00-2 Aldrin ND 3600 56-55-3 Benzo (a) anthracene. ND 3600 205-99-2- Benzo (b) fluoranthene ND 3600 207-08-9 Benzo (k) f luoranthene ND 3600 50-32-8 Benzo (a)pyrene ND 3600 191-24-2 Benzo(ghi)perylene ND 3600 85-68-7 Butyl Benzyl Phthalate ND 3600 319-85-7 beta-BHC ND 3600 319-86-8 delta-BHC ND 360Qw 111-44-4 Bis (2-chloroethyl)ether ND 3600 111-91-1 Bis (2-chloroethoxy)methane : ND 3600 117-81-7 Bis (2-ethylhexyl)phthalate ND. 36.00 108-60-1 Bis (2-chloroisopropyl)ether ND 3600 101-55.-3 4-Bromophenylphenyl ether ND 3600 86-74-8 Carbazole ND 3600 59-50-7 4-Chloro-3-methylphenol ND 7200 91-58-7 2-Chloronaphthalene ND 3600 95-57-8 2-Chlorophenol ND 7200 7005-72-3 4-Chlorophenylphenyl ether ND 3600 218-01-9 Chrysene ND 3600 72-54-8- 4, 4'-DDD ND 3600 72-55-9 4,4'-DDE ND 3600 50-29-3 4,4'-DDT ND 3.600. 53-70-3 Dibenzo (a,h) anthracene ND 3600 i (con't) i 31 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GUMS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 67261 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg)- (mg/Kg) or Comment 120-82-1 1,2,-4-Trichlorobenzene ND 3600 88-06-2 2, 4, 6-Trichlorophenol ND 7200 ---------------------------- Hazardous Substances ------------------------ 65-53-3 Aniline ND 3600 65-85-0 Benzoic Acid ND 7200 100-51-6 Benzyl Alcohol ND 3600 106-47--8 4-Chloroaniline ND 3600 132-64-9 Dibenzofuran ND 3600 91-57-6 2-Methylnaphthalene 900 3600 L 95-48-7 2-Methylphenol ND .3600 106-44-5 4-Methylpheno1 ND 3600 88-74-4 2-Nitroaniline ND 3600 99-09-2 3-Nitroaniline ND 3600 100=01-6 4-Nitroaniline ND 3600 95-95-4 2, 4, 5-Trichlorophenol ND 3600 Other Compounds Quantitated w ------------------------- None detected ND 3600 ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Hydrocarbon 10,000 J Decane 40,000 J C12 Hydrocarbon 10, 000 J C12 Hydrocarbon 10,000 J C12 Hydrocarbon 30, 000 J note: Possible light petroleum product and smaller amount of fuel #2. 33 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTI.ON AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65650 Matrix: Drum DATE OF COLLECTION: 04/16/98 Density DATE OF EXTRACTION: 04/22/98 Conc. Final Vol. 10 ML DATE OF ANALYSIS : ' 04/30/98 Dilution Factor None WET WEIGHT EXTRACTED: 0.196. g Report Factor 1.02 RESULTS: CAS Compound Conc. RL Qualifier NO. -(mg/Kg) (mg/Kg) or Comments ------------------------------------------------------------------------ Priority Pollutants 83-32-9 Acenaphthene ND . 310 208-96-8 Acenaphthylene ND 310- 120-12-7 Anthracene ND 310 309-00-2 Aldrin. ND 310 56-55-3 Benzo (a)anthracene ND 310 205-99=2 Benz o (b) fluoranthene ND 310 207-08-9 Benzo (k) fluoranthene ND 310 50-32-8 Benzo (a)pyrene ND 310 191-24-2 Benzo (ghi)perylene ND 310 85-68-7 Butyl Ben_zyl Phthalate ND 310 319-85-7 beta-BHC ND 310 319-86-8 delta-BHC ND 31(k 111-44-4 Bis (2-chloroethyl) ether ND 310 111-91-1 Bis (2-chloroethoxy)methane ND 310 117-81-7 Bis (2-ethylhexyl)phthalate ND 310 108-60-1 Bis (2-chloroisopropyl) ether ND- 310 101-5573 4-Bromophenylphenyl ether ND 310 86-74-8 Carbazole ND 310 59-50-7 4-Chioro-3-methylphenol ND 610 91-58-7 2-Chloronaphthalene ND 310 95-57-8 2-Chlorophenol ND 610 7005-72-3 4-Chlorophenylphenyl ether ND 310 218-01-9 Chrysene ND 310 72-54-8 4, 4 '-DDD ND 310 72-55-9 4, 4'-DDE ND 310 . 50-29-3 4, 4'-DDT ND 310 53-70-3 Dibenzo (a,h) anthracene ND 310 (con't) 35 US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GC/MS EXTRACTABLE ORGANIC ANALYSIS SAMPLE NO. : 65650 Results Continued: CAS Compound Conc. RL Qualifier NO. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ 120-82-1 1,2, 4-Trichlorobenzene ND 310 88-06-2 2, 4, 6-Trichlorophenol ND - 610 ---------------------------- Hazardous Substances ---------------------- 65-53-3 Aniline ND 3.10 65-85-0 Benzoic Acid ND 610 100-51-6 Benzyl Alcohol ND 310 106-47-8 4-Chloroaniline ND 310 132-64-9 Dibenzofuran ND 310 91-57-6 2-Methylnaphthalene ND 310 95-48-7. 2-Methylphenol ND 310 106-44-5 4-Methylphenol ND 310 88-74-4 2-Nitroaniline ND 310 99-09-2 3-Nitroaniline ND 310 j 100-01-6 4-Nitroaniline ND 310 95-95-4 2, 4, 5-Trichlorophenol ND 310 ---------------------------- Other Compounds Quantitated ---------------------------- None detected - ND 310 - rr ---------------------------- Est. Tentatively Identified Conc. Compounds (mg/Kg) ---------------------------- Tetradecanoic acid methyl . ester 1700 J 9-Hexadecanoic acid methyl- -ester 3200 J Hexadecanoic acid methyl ester 2900 J Octadecanoic acid isomer 3400 J Octadecanoic acid isomer 28000 J Octadecenoic acid methyl ester 1200 J Unknown 1900 J 37 :. APPENDIX H pH Analytical Data w . 1 . Please note: The laboratory performing the drum pH analysis incorrectly identified the site name as"Sponge Von the"SUBJ:"line of the analytical data memorandum. The analytical data contained in this memorandum are the drum pH results for the Flynntan site in Salem,Massachusetts and can be verified by the EPA sample numbers (65646, 65647, 65648, 65650, 65651, 65652, 65660, and 65661) which correspond to the chain-of- custody record(Appendix D, Section 1) and the project number (98267) which was assigned to this site by the laboratory. w .i2dl� UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION I 60 WESTVIEW STREET, LEXINGTON, MASSACHUSETTS 02173 MEMORANDUM PN: 98267 DATE: April 23, 1998 SUBJ: Sponge % = Drum pH Results FROM: Hugh Curran 04 Chemist TO: Tom Hatzopoulos LL � MRU: Dr. William J. ade Senior Chemistry Analytical. Specialist Analytical References: Methods 9040B and 9045C, from "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW-8461 3rd ed. , Final Update IIB, Rev. 2 and 3, 1/95." (SOP I-16, Rev. 3/92) Date Samples Received by Laboratory: 04/17/98 ?ate Samples Analyzed by Laboratory: 04/20/98 File name: 98267dr.pH i - -3- Quali.ty Assurance\Quality Control Laboratory Duplicates: Sample 65646 ale 65646 Dup. Average RPD 11.45 11.50 11.48 0.4% same ie 65652 maple 65652 Dup. Average RM Y3.35 3 .40 3.38 1.5a Sample 67260 Sample 67260 Dup. Average RPD 7.60 7.60 7.60 0.0% Samgle .67261 sawle 6726.1 Duo: Average BAIL 4.75 4.80 4.78 1.0% i - F i APPENDIX I Polychlorinated Biphenyl Analytical Data UNITED STATES ENVIRONMENTAL PROTECTION AGENCY . A % REGION 1 ENVIRONMENTAL SERVICES DIVISION j 60 WESTVIEW STREET �'�c LDQNGTON,MASSACHUSETTS 02173.3185 )ATE: April 28, 1998 sUBJ: Analysis of PCBs in Soils - FLYNN TAN ?ROM: PeterrPhilbrook, Investigations and Analysis, Chemistry Section =U, Dr. William J. Andrade,. Advancel Analytical Chemistry Specialist TO: Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received. and logged in by the laboratory according- to the SOP for Sample Log-In (EIA-ADMLOGNI.SOP, 7/97) .. EPA Region 1 Procedure: Polychlorinated .Biphenyls in Soil Samples, Mid Level` Method, PCBSOML6.SOP. The modules used for this . procedure were: XL 2020 Heat Systems Sonicator-, SONICAT2 .MOD, Chlorinated Pesticides and PCB Screening, 8500ECI.MOD,. 5880 Gas Chromatographs, 5880EC2.MOD. Results are reported out in dry weight. The analytical support for this report was performed by NCOA contractors. w -Date Samples Received by the Laboratory: 04/17/98 Date Analysis' Started: 04/21/98 cc: File: J: \CHEMSTRY\REPORTS\PCB-PEST\98267SO.PCB Reoyeted/Recydable.Pdnted wKhh Vegetable 01 Based Ws on t00%Regded Paiper(40%Postoonsumer) US ENVIRO 'AL PROTECTION AGENCY 60 Westview Street Lexington, NA 02173 Chemist who reviewed data: Peter Philbrook Holding time meet (Y/N) : Yes Extraction (Water - 7 days, Sail - 14 days) Analytical (40 days after -extraction) Method modifications: None Limitations of data: Detection limits for sample 67265 were increased due. to oily matrix. Laboratory blank- problems: None Instrument performance problems: None Surrogate and spike recovery problems: Surrogate- recoveries for sample 67264 could not be determined due to dilutions required to quantitate target -compounds. Additional comments: None 3 FACILITY SAMPLED: FLYNN TAN US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY Polychlorinated Biphenyls SAMPLE NO. : 67264 DATE OF COLLECTION: 04/16/98 Matrix: Soil DATE OF EXTRACTION: 04/22/98. Final Volume: 5 mL DATE OF ANALYSIS: 04/24/98 Percent Moisture - 7.3 DRY WEIGHT EXTRACTED: 2.78 g Dilution Factor: 100 WET WEIGHT EXTRACTED: 3.00 g Report Factor: 105 .8 SAMPLE RESULTS-: CAS Compound Conc. , RL Qualifier No. (mg/Kg) (mg/Kg) or Comment ------------------------------------------------------------------------ 12674-11-2 Aroclor-1016 ND 18 11104-28-2 Aroclor-1221 ND 18 11141-16-5 Aroclor-1232 ND 18 53469-21-9 Aroclor-1242 ND 18 12672-29-6 Aroclor-1248 ND 18 11097-69-1 Aroclor-1254 180 18 11096=82-5 'Aroclor-1260 ND 18 11100-14-4 Aroclor-1262 ND 18 37324-23-5 Aroclor-1268 ND 18 Sample Recovery for Observed Surrogate Compound: Recoveries M ------------------------------------------------------------------------ Decachlorobiphenyl NA 2,4,-5,6-Tetrachloro-m-xylene NA -----------=-----------------------------------------------�----------- 1 5 APPENDIX J Metals Analytical Data i - • w N O Z '�N��ON CM c;C, N �- 1 0 O O UV� I I cm W Ei 1��J� liJ O 1 » O�� .Q ONi000/0000.v N•- NO CYCYm C) v0m 40 c,m 0m m n.0 Cb %rwo<v N(Oo _ LL.Q �� N i 0 p am or` oo.rmom0000m.- Q� �m maDN�arr-Cj C* oQ ci CM W W a U p Z W N W Z� V) N Og� O�EOOmIO"f 00DO,6ANNFAR LLO InOQOmwmabrco�0 OW N co C.) 1 Q !NO - m Q�' J °a M� o p 0 o W c �» » > Wrn � Q NO r` NQQOOr�OIr'OCQ NN Dj Q m Q9 � C4 tn C4-1OVOmaD O� OQ 0 w °a aWU co CD �Z F-t- r Q w O W W O Z' -a-» >-> > 0tu Uhilu- Q �Q 1U cq M N O r N V O o000Om r� JJY d0 CO M C.4V m��Or�r 0�li 00 4�� NN t'OZZ. W Q Q FO,� O FhW-N Z tz X W W 0 Q Z J J W CL »� '..yam » *�! 0 W ' Z qtmNfr $ r►m0M.WN M' ■ jf N CD oEir �-N _ QQC4 c�— oo w J O U) � W OW p� OQONNOOOPfOOPN W CM�QOp} Qm O�<01MO�NNm0�0 �" w Q-" On .- 0� ' 0 0 W Z Z' a m p 0�� NoQo�om0 el NRoo a r�_j cr E v a � aaaaaaadac�ida �Z wZwo cCD Qco0 �DOC ZOZH a' (� W-irz 0 j dQW -JW U W }0.. U C.)Za� da�K WW W� - LL IL IL ZOFO- m V ' U�a� N. J IL :�.LLvU. �O OQ N OQ�ONCNI N• O G V~ cm MCI W E a Up W W � Q F- g z W ca Z N 0 5 <0: gH z - Q o 0? p > pM z W W J 0 ca �WW y' 0 UQ UJ UU Q J >>>> >>>>>> �}}V W W Q 2 QD m-a0 E ma0Q01-0--0e-o I-acl z CM4 a9QOp rOOO—r-00CN5000 OQzz O J'Y < cl QO E ZZ W tiv p o N co Z�» i Q Cl) IL z J J W - 0 » > »> 'o—» a:LU to 1h 490E OI h N N N m N N O to CD N H a 0 W- O ror0p n]Ot000Q4.NPdj000 ' Q Z ILF=QON LOGO tp 0450od - �� N Q N r r0 j p V) t0 W � d' t7) >>>>>>>>>>7 C.)< 'It0 Q')OtYbOmo L O p 0 r 0 00 o~C r C C 0 O U pU.�C-4 o Z z y CD Co. 0 Z _o Q M�""F_ t`C CIO R',v +100tooVN n pW� NQOo4r6NNOIOr cc r E 000 .O O O.O O W J tu- aaaaaaaaat�iaa I= WQ_ 1 Wo 4 2~2o �6�C 0- 9 Z.0 Z F- pD aoc,pc� �w�w z p Q o a I ZJIL �O w g JZs> Gom 1Q ZZ22:52 ZjZ� zUV jW�CJKZpOK.T> Q - • - ao �S z a°d�caic�c=i� Mw i au-a0 I r 0 F-Z ONOrONOmOr.--N m U O 0 N 0 0 0 CID 1�~~� r r a f W`L �UpJ E W W a F 2 Z F W N W H N ` Oui H 2 F-a Z m �Q O = OC3 U O a, W w O W �. co a Q Q MQ' �WW O Y ZUU mn FA U W m co w E Z- CL z ui zz at Q w F.� Q Z�Ww N Z a C7 >> N w >D. . 'T Os-010000rOOQ1�D Ul r W O o0 aD .. d0O N C-A co-t0 rCDO.rC7N 0 LL N(O ry r aR Z N 1- b n co W co O a� rF-ZC p�ONm��MO�ObltN .- N pAr Q �w. J E N000 ONONOGO � V 0 ' aaaaaaaaaUaa "=- i MZ IL M—mO LL �Q2o CL 0 ZUZ� 0 LU I QQ 201� 0..Wj0U W ¢O th O CL us rww� U $d' �a w �a3> zha aD$ U _ 2 Jzp-aW. 9 IJf.p� ZU mm22>>2 W>>� UUV' Qm O �mmo2go QQQ=ZUp��'�; Z . m O�awwd v' wvg z QamnUU�J��o�v,, au.ao APPENDIX K Flashpoint Analytical Data i UNITED STATES ENVIRONMENTAL PROTECTION AGENCY { REGION 1 10 d ENVIRONMENTAL SERVICES DIVISION s 60 WESTVIEW.STREET LEXINGTON,MASSACHUSETTS 02173-3185 DATE: April 29, 1998 SUBJ: Flash Point Determination - FLYNN TAN FROM: Peter PPhilbrook, Chemistry ect'o yed Analytical Chemist S Specialist L'HRII: _ Dr. William J. Andrade, d nced Chemistry p TO: Tom Hatzopoulos PROJECT NUMBER: 98267 ANALYTICAL PROCEDURE: All samples were received and logged in by the laboratory according to the SOP for Sample Log-in*. (EIA-ADMLOGNI.SOP, 7/97) . The flash points were determined by the EPA Region 1 method, Flashpoint - Setaf lash Closed-Cup Method, FLASH3...SOP. Reference: ASTM-Method D3278-78 The analytical support. for this report was performed by NCOA contractors. . Date Samples Received by the Laboratory: 04/17/98-- w Date Analysis Started: 04/21/98 cc I File.- J: \CHEMSTRY\REPORTS\MISC\98267DR.FP i US ENVIRONMENTAL PROTECTION AGENCY 60. Westview Street Lexington, MA 02173 KEY: > = Greater than < = Less than ' s Less than or equal to Approximate * = The duplicate analyses did not agree within 1 degree Centigrade (possibly due to sample variation) so the flashpoint was repeated for a total of 5 or 6 values. NA = Not Applicable.. _The flash/no flash test is not done for the duplicates, only the finite flash point is determined. i SAMPLES ANALYZED: 65644.., -.65645, 65646; 65647, 64649; 65650, 65651, 656521 672601 67261 1 I .MEMORANDUM DATE: April 28, 1998 SUBJ: Site Investigation Closure Flynntan Site 70-92 Boston Street Salem, MA r FROM: Athanasios Hatzopoulos, On-Scene Coordinator Site Evaluation Evaluation & Response Section II TO,:- Flynntan Site File THRU-: Steven Novick, Section Chief Site Evaluation & Response Section II In accordance with section 300 .400 of the NCP, a Removal Site Evaluation, consisting of a Preliminary Assessment and Site Investigation (PA/SI) , has been undertaken for .the Flynntan Site in Salem, Massachusetts. The findings - of the Removal Site Evaluation, . recorded in a PA/SI Report, have been evaluated under the criteria set forth in section 300 .415 of the NCP and section 104 (a) and (b) of CERCLA, 42 U.S .C. 9 9604 (a) and (b) . The Removal Site Evaluations has led to the determination that a Removal Action is appropriate at this time. The findings of the Removal Site Evaluation are as follows: - 1. Source and nature of the release or threat ofrelease: a. Please refer to the document entitled "Removal Program Preliminary Assessment/Site Investigation for the Flynntan Site, Salem, Massachusetts" by Roy F. Weston - Superfund Technical Assistance & Response Team (May, 1998) . i b. The major hazardous substances, pollutants, and/or contaminants that are being released or for which there is threat of release: Substances Media pH>12 liquids in drums Flammable liquids in drums I _ i . -3- 4 . As. reflected in Section 3 . above, the Removal Site Evaluation was terminated due to its completion and not for other reasons. Therefore, the following factors. were considered in determining tthe .appropriateness of a Removal Action pursuant to section 300 .415 (b) (2) of the NCP_: (X) Actual or potential exposure to nearby human populations, animals, or the food chain from hazardous substances or pollutants or contaminants; ( ) Actual or potential contamination of drinking water supplies- or sensitive ecosystems; (X) Hazardous substances or pollutants or contaminants in drums, barrels, tanks, or other bulk storage containers, that may pose a threat of release; ( ) High levels of-hazardous substances or pollutants or contaminants in soils largely at or near the surface, that may migrate; ( ) Weather conditions that may cause hazardous substances or pollutants or contaminants to migrate or be released; (X) Threat of fire or explosion; (X) The availability of other appropriate Federal or State response mechanisms to respond to the release; 'and (X) Other situations or factors that may pose threats to public health or welfare or the environment.. w 5 . The existence of the conditions specified in Section 4 . above suggest that a Removal Action under section 300 .415 of the NCP is necessary. 6. In light of the magnitude of the threat or potential threat to health-, welfare, or the environment, the Removal Action should be undertaken as a: Emergency Time-Cr itical_X Non-.Time-Critical j cc: Dave McIntyre, Chief, SERS I Jane Guy, Salem Planning Department Anthony Guarciariello, MADEP ..Dennis Gagne, Chief, Technical Support & Site Assessment i U.S. ENVIRONMENTAL PROTECTION AGENCY POLLUTION REPORT I . HEADING DATE: JULY 20, 1998 SUBJECT:- FLYNNTAN SITE - POLREP #1 LOCATION: 70-92 BOSTON STREET, SALEM, MA SITE ID NUMBER: 015Y CERCLIS NUMBER: MA0002333433 OSC: A. HATZOPOULOS, USEPA, OFFICE OF SITE REMEDIATION AND RESTORATION, SECT. II OFFICE PHONE # : -617-573-5759 (OFFICE) ACTION MEMO STATUS: FUND LEAD INCEPTION DATE: JULY 6, 1998 DEMOBILIZATION DATE: TBD II . BACKGROUND The Site is located at 70-92 Boston Street in Salem, Massachusetts . The Site is approximately 1.90 acres and is an abandoned leather tanning factory located in a heavily populated residential/commercial area of Salem, Massachusetts. The Site is fenced with locking gates at several entrances of the Site. However, the fence does not preclude unauthorized access. Evidence from'graffitti - and other vandalism activities that children and others had been entering the Site. - The closest residential property is less than 100 feet away from the Site. An estimated 1, 000 people reside/work .25 miles of the -Site. A day care facility -is located .2 miles west of the Site. Within a 1-mile radius there are 5 other schools, one of which is Salem High School . Most of the windows and doors of the entire structure are either broken, missing or have been replaced by. temporary plywood. The primary threats that will be removed from the Site %onsist of ignitable and caustic substances in drums/tanks as well as leaking electrical capacitors and metal tanning residues/dust such as chromium and lead on the floors, drains, settling pits and exterior grounds. Contaminants found at the site. include but are not limited to polychlorinated biphenyls (PCBs) , lead and chromium. III . ACTIONS On July. 6, 1998, the ERCS contractor .and the START contractor mobilized to the site. To date FRCS has : 1) . established security, 2) prepared the Site for the removal action activities i.e. set up utilities (phones, fax, electricity, water etc) UNITED STATES ENVIRONMENTAL PROTECTION AGENCY . _ Z REGION 1 W 0 JOHN F.KENNEDY FEDERAL BUILDING �F BOSTON, MASSACHUSETTS 02203-0001 r Enforcement Confidential 'Materials Attached MEMORANDUM DATE: May 26, 1998 SUBJECT: Request for a Removal -Action at the Flynntan Site, r Salem, Massachusetts - ACTION MEMORANDUM FROM: Athanasios Hatzopoulos, On-Scene Coordinator 441- Site Evaluation and >s' e Section II THRU: Steven R. Novick, Chie Site Evaluation and Respo se II TO: Patricia L. Meaney, Director Office of Site Remediation and Restoration. I. -PURPOSE The -purpose of this Action- Memorandum is to. request and document approval of the proposed removal action at the Flynntan Site (the Site) , which is located at 70-92 Boston Street in Salem, Essex County, Massachusetts. Hazardous substances present in drums. and on the floors of the ma-nufacturing building, if not addressed by implementing the response actions selected in this Action Memorandurff, will continue to pose a threat to human health and the environment. There are no nationally. si.gnificant or precedent-setting issues associated with this Site, and there has been no use of the OSC' s $50, 000 warrant authority. . II. SITE -CONDITIONS AND BACKGROUND CERCLIS Identifier: MA0002333433 SITE Identifierc015Y Category of 'Removal: Time-Critical Itttemet Address(URL)•httpJ/www.epe-96v Recycled/Recyctabla•Printed with Vegetable 04 Based Inks on Recycled Paper(Minimum 25%Postconsumer) latitude and longitude of the Site are 4203i' 12"N and 7005413811W. The Site is bordered to the north by Goodhue and Beaver Streets; to the south by Boston Street; to the west by a residential/commercial area; and to the east by the intersection of Boston Street and Goodhue Street. Private residences are located within 100 feet of the Site boundaries. Land use in the immediate vicinity is mixed residential/commercial . The Site is situated less than half of a mile from the North River Canal which flows into the Salem Sound. 3 . Site Characteristics The Site is approximately 1. 9 acres and it is fenced. However, evidence of graffiti and other vandalism activities,.-clearly indicates that trespassing is a common occurrence. A large wood/brick structure and several parking areas are located within the Site. . This structure is made- up of two buildings which are joined. One portion is a 4-story wood/metal frame building and was used for the leather tanning operations (building-a) . The building's exterior is covered by asbestos shingles that are falling off. The interior has sustained 2 fire.s . The rest of the structure is made up of a newer 2-story, brick sided building that is in better structural condition (building-b) . Building-a is not occupied. However, building-b on the day of the PA/SI, was illegally occupied by two tenants (a construction company and a storage/shipping business) . Most of the windows and doors 'of the entire structure are either broken, missing or have been replaced by temporary plywood. The Site has three parking areas that are adjacent to the structure. Hi.storical information indicates that the Site contains 4-6 underground storage tanks possibly containing heating oil . rr The PA/SI revealed that approximately 21, 55-gallon drums are located inside the Site' s structure. Most were on. the first floor of building-a,' and had various labels such as: flammable, corrosive, formic acid, degreasing solvent, chrome complex in isopranol, SYN FOG insecticide, and sodium acetate. The first floor and its drains are littered with powders and tanning process residues. There is an approximately 101x15 ' settling pit that is filled with 51 - of liquid and about 1' of sludge. The rest of the floors are littered with boxes, paper, and trash from vandalism and other trespassing activities. Building-b contains another I pit that is filled. with liquid and sludge like -material . 3 i S. NPL Status The Site is currently not listed on the National Priorities- List. The Site is not, at this time, being evaluated by the Agency for Toxic Substances and Disease Registry (ATSDR) . B. Other Actions to Date 1. Previous Actions . From 1-996, the City of Salem has been in contact with the owner regarding the cleaning and possible redevelopment of the Site. In October 1997, the City's Building. Department, due- to a complaint received by the Salem neighborhood Improvement Task Force, `had conducted a building inspection of the Site. The City on' October 15, 1997, notified the owner -of illegal rental of the property. 2 . Current Actions This will be EPAs first removal action conducted at the Site. C. State and. Local Authorities' Roles. The City of Salem has assisted EPA in collecting background information. The MADEP has been contacted by EPA and is expected to assist EPA by providing technical comments on the proposed removal action. and generating a list of regulations for consideration as applicable or relevant and appropriate. Neither state nor local authorities have the resources to remove the hazardous substances abandoned at the Site. III. THREATS TO" PUBLIC HEALTH OR WELFARE OR THE ENVIRONMENT, AND STATUTORY AND REGULATORY AUTHORITIES A. Threats to Public Health or Welfare There is clear. evidence from graffiti and other vandalism activities that children and others are entering the Site. The area around the Site is heavily populated both residentially -and commercially. The closest residential property is less than 100 feet away from the Site. An estimated 1, 000 people reside/work .25 miles of the Site. A 5 I i paper and other trash from vandalism and other trespassing activities .. These conditions pose a threat of fire or explosion. If a fire does occur in the building, the substances present would be released in the atmosphere . 40 CFR 300 .415 (b) (2) (vii) The availability of other appropriate federal or state response mechanisms to respond to the release Neither state nor local authorities have the resources to address the contaminated surface soils at the Site. Chromium-Children who come in contact with Chromium contamination may be at increased risk of developing noncancerous health effects possibly including skin irritation and contact dermatitis. Inhalation of airborne dust particles is a possible route of exposure. PCBs- Exposure to PCBs pose a variety -of health impacts . PCBs are classified as a B2 probable human carcinogen, are liver toxins and possibly cause peripheral neuropathy (nerve disease in extremities) . PCBs have been found to cause rashes (edema of face and hands, simple erythematous eruptions with pruritus, acute eczematous contact dermatitis; and chloracne) subcutaneous edema and- hyperpigmentation of skin and mucous membranes; excessive secretions from the eyelids (hyperactive Meibomian glands; conjunctivitis; and - edema of the eyelids) ; formation of keratin cysts in and hyperplasia of epithelial layer of hair- follicles; increase in liver size (hepatic hypertrophy) ; .decreases: in number of red- blood cells and hemoglobin; serum hyperlipidemia; and increases in numbers of white blood cells .in the body (leukocytosis) . Pr . . Various studies have found that exposure to PCBs may cause _irregular menstrual cycles, and increased PCB serum levels may cause pathological pregnancies (toxemia of ' pregnancy, and abortions) stillbirths, underweight births, etc . Mother's milk contaminated with PCB' s appears to be a source of exposure for infants. Developmental abnormalities have been observed in PCB-intoxicated infants. LEAD- Lead. is a probable human carcinogen, •since it has been proven to cause kidney cancer in -laboratory animals . Exposure to high levels .of lead can cause brain and kidney damage. Lead exposure may increase blood pressure in middle-aged men and has been known to 7 f Neither state nor local authorities have the resources. to address the contaminated surface soils at the Site. IV. ENDANGERMENT DETERMINATION Actual or threatened releases of hazardous substances at or from this Site, if not addressed by implementing the response action selected in this Action Memorandum, may present an imminent- and substantial endangerment to public health, or welfare, or the environment. V. PROPOSED ACTIONS AND ESTIMATED COSTS A. Proposed Actions 1. Proposed Action Description The actions required to mitigate the threats outlined . herein, are given below. - At this time, indications are that the PRPs will not perform this work. The proposed actions will protect public health, welfare and the environment by preventing people or animals to come into contact with the contaminated areas of the Site. The proposed actions are as follows: 1) take measures to prevent unauthorized access to. the Site. These measures may include repairing or installing additional security fencing and/or providing 24 hour security during the removal activities; 2) conduct additional sampling of interior and .exter_ ior floor surfaces as well as drums, pails and settling pits;. 3) the hazardous waste contamination on the .flgor surfaces will be swept up, consolidated and staged. The content of drums, vats, containers and settling pits, will be categorized, containerized, and staged. " The exterior lead contaminated soil .-will be collected and staged. All waste streams will be manifested and shipped off-site for appropriate re-use or disposal- at an EPA-approved disposal facility. 2. Contribution to Remedial .Performance Performing this removal action will contribute to remedial performance and protect public health and the environment by eliminating the potential for exposure to contaminated areas of the Site and preventing the i 9 268-270 Hazardous and Solid Waste Amendments Land Disposal Restrictions Rule 40 CFR Part 300 .440 Procedures for Planning and Implementing Off-Site Response Actions (Off-Site Rule) 40 CFR Part 761 .60 and Parts 761.202-218 : TSCA requirements for disposal of PBS 49 CFR Parts 171-179 : Department of Transportation Regulations for Transport of Hazardous Materials The OSC has requested that the Massachusetts Department of Environmental Protection identify State ARARS for consideration by the. OSC. B-. Estimated Costs and Schedule The OSC has prepared an independent government estimate of the cost associated with carrying out the proposed actions outlined above. A summary of this estimate is given below. The action is anticipated to be complete within eight months of its commencement . EXTRAMURAL COSTS: ERGS COSTS: Labor & Equipment $ 75, 000 Lab Analysis j $ 5., 000 Transportation & Disposal $ 50, 000 ERCS COST TOTAL $ ..130,000 START COSTS: S 50 . 000 w SUBTOTAL, EXTRAMURAL COSTS $ 180, 000 EXTRA COSTS CONTINGENCY (20°s of Subtotal, Extramural costs) +S 36, 000 TOTAL EXTRAMURAL COSTS $ 216, 000 INTRAMURAL COSTS• Labor, Expenses, Subsistence $ 70, 000 TOTAL, REMOVAL PROJECT. CEILING $ 286, 000 11 I recommend you approve $ 286, 000 to initiate the removal action proposed above, of which as much as . $ 156,000 is from the EPA removal allowance. Expenditure will be limited to the categories of START and Intramural for the purpose of :monitoring compliance with an Administrative--Order, should the' PRP perform the cleanup. APPROVAL DATE: / DISAPPROVAL• DATE- } i w 13 JpIEo srgs UNITED STATES ENVIRONMENTAL PROTECTION AGENCY _� yW REGION 1 i f JOHN F.KENNEDY FEDERAL BUILDING ;F BOSTON,MASSACHUSETTS 02203-0001 URGENT LEGAL MATTER -- PROMPT REPLY NECESSARY VIA FEDERAL EXPRESS - OVERNIGHT DELIVERY 5/4/98 Salem Realty, LLC c/o Jan Exman, Manager 66 Old Blue Hill Road Durham, Connecticut 06422 Re: NOTICE OF POTENTIAL LIABILITY AND INVITATION TO PERFORM OR FINANCE PROPOSED CLEANUP ACTIVITIES: Flynntan Site Dear Mr. Exman: This letter serves to notify Salem Realty, LLC of potential liability regarding the Flynntan Site, Salem, Massachusetts ( "Site" ) , as defined by Section 107 (a) of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980,. as amended ("CERCLAr') , 42 U.S.C. § 9607 (a) . This letter also notifies Salem Realty, LLC of forthcoming removal activities at the Site which Salem Realty, LLC is. invited to perform or finance. and which you may be ordered to perform at a later date. NOTICE OF POTENTIAL LIABILITY The United States Environmental Protection Agency ("EPA") has documented the release or threatened release -of hazardous substances or pollutants or contaminants at the Site, which is located at 70. -92 Boston Street, Salem, Massachusetts. The Site is further- defined in Book 13751, Page 323, Essex County Registry of Deeds, in Salem, Massachusetts . w Hazardous substances involved •in the release or threat of release at the Site include, but are not limited to, flammable and caustic substances . EPA has spent- or is considering spending public funds on actions to investigate and control such releases - or threatened releases at the Site. Unless a potentially . responsible party ("PRP") or parties commit to properly performing or financing such actions, EPA may perform these actions pursuant to Section 104- of CERCLA, 42 U.S.C: § 9604 . Under Sections 106 (a). and 107 (a) of CERCLA; 42 U.S.C. §§ 9606 (a) and 9607 (a) , Section 7003 of the- Resource Conservation and .Recovery Act. ("RCRA'r) , 42 U.S.C. § 697.3 , and other laws, liable parties may be obligated to implement response actions deemed necessary. by EPA .to protect public, health, welfare, or the environment and may be liable for all costs incurred by the Internet Address(URL)• httpJlwww.epa.gov Recycled/Recyclable•Printed wdh Vegetable 01 Based Inks on Recycled Paper(Minimum 25%Postconsumer) i i required by such an order. - . Be advised that even if Salem Realty, LLC does not indicate a .willingness to perform or finance necessary response actions, P; may order you to undertake such actions under Section 106 of CERCLA, 42 U.S.C. § 9606. Failure to. comply. with a Section 106 (a) administrative order may result in a fine of up to $27, 500 per day under Section 106 (b) or imposition of treble damages under Section 107 (c) (3) of CERCLA. Further, you may be held, liable under Section 107 (a) for the cost of the response activities EPA performs at the Site and for any damages to natural resources. In addition, by virtue of Section li3 -.of CERCLA, 42 U.S.C. § 9613 , other PRPs who agree to perform the necessary response action may seek contribution protection. PRP RESPONSE AND EPA CONTACT i You should contact EPA within- ten (10) business, days after receipt of this letter to indicate your willingness to perform or finance the response activities outlined above. If EPA does not receive a response within that time, EPA will assume that you do not wish to negotiate a resolution of your liabilities in connection with the response and that you have declined any involvement in performing response activities: Be advised, however, that liability under CERCLA is joint and- several; therefore, , each PRP_ is potentially liable for undertaking all response actions or reimbursing the Government for the entire amount of its response costs . Please -provide the name, address, and telephone number of a designated contact- for future communications . Your written response, including any technical comments or questions concerning the proposed response activities, should be directed to the EPA On-Scene Coordinator (OSC) for the Site: Athanasios Hatzopoulos U.S . Environmental Protection Agency +� Site Evaluation & Response Section II JFK Federal Building' -' Mail Code HBR Boston, Massachusetts 02203 Legal questions and all communications from counsel should be directed to: Cynthia A. Lewis U.S. Environmental Protection Agency Office of Environmental Stewardship JFK Federal Building .-- SES Boston, Massachusetts 02263 (617) -565-3285 i PURPOSE AND USE OF THIS NOTICE LETTER The factual and legal discussions contained in this letter .are intended solely to provide. notice and information. Such discussions are not intended to be, and cannot be, relied upon as "EPA' s final position on any matter set forth herein. Due to the seriousness of . the environmental and legal problems posed by conditions at the Site, EPA urges that you give immediate attention and provide a prompt response to this letter. By copy of this letter EPA is notifying the Commonwealth of Massachusetts and the Natural Resources Trustees of EPA' s intent to perform, or to enter. into negotiations for the performance or financing of, response actions at the Site. Thank you for your attention to this matter.. Sinc rel , Dennisses Val es, Acting Chief Emergency Planning and Response Branch Enclosures CC: Athanasios Hatzopoulos, EPA On-Scene Coordinator - OSRR Sharon C. •Fennelly, EPA Enforcement Coordinator - OSRR Holly Inglis, EPA Administrative Records Coordinator - OSRR Jane Guy, Salem Planning Department Anthony Guarciariello, MADEP . Andrew Raddant, Acting .Environmental Officer, U.S. Department of the Interior Ken Finkelstein, National Oceanic and..Atmospheric Administration N Administrative Record File Available for the Flynntan Site Removal Action The U.S. Environmental Protection Agency(EPA)announces that the Administrative Record File for the removal action at the Flynntan Site located in Salem, Massachusetts is available for review. EPA seeks to inform the public of the availability of the Administrative Record File and to encourage the public to review and comment on it. The proposed actions will protect public health, welfare, and the environment by preventing people or animals from coming into contact with the contaminated areas of the site. The proposed actions are as follows: 1)Taking measures to prevent unauthorized access to the site, including repairing or installing additional security fencing and/or providing 24-hour security during removal activities; 2) conducting additional sampling of interior and exterior floor surfaces,and of drums,pails, and settling pits; 3)sweeping up, consolidating,-and staging hazardous waste contamination found on the floor surfaces;4) categorizing,containerizing, and staging the contents of drums,vats, containers, and settling pits; and 5)collecting and staging exterior lead-contaminated soil. Also, all wastestreams will be manifested and shipped off site for appropriate reuse or disposal at EPA-approved disposal facilities. The Administrative Record File'is the collection of documents that formed the basis for the selection of a removal action at the site. Documents in the Administrative Record File include the Preliminary Assessment/Site Investigation Report and the Action Memorandum. The Administrative Record File is available for review at the: • -EPA Records Center, 90 Canal Street, First Floor, Boston, Massachusetts, 'U.S.2114, (617) 573-5729,by appointment. Salem Public Library, 370 Essex Street, Salem, Massachusetts, 01970, (978) 744- 0860. Written comments on the Administrative Record File should be sent to: On-Scene Coordinator Athanasios Hatzopoulos,U.S.EPA,Region I,MailCode HBR,John F. Kennedy Federal Building; Boston, Massachusetts, 02203. Comments should be sent to the On-Scene CoorAnator within 30 days of this announcement.