Loading...
70-92 Boston Street - Site Investigation Summary Report - Aqueous sample 1MITKEII CORPORATION "Environmental Testing For The New Millennium" I January 27, 2005 TRC Solutions, Inc. Foot of John Street Lowell, MA 01852 Attn: Ms. Liz Denly RE: Client Project: Flynn Tan, Salem, Aqueous Samples Lab Project#: C1600 j Dear Ms. Denly: Enclosed please find the data report of the required analyses for the samples associated with the above referenced project. If you have any questions regarding this report, please call me. We appreciate your business. Sine el , Edward A. Lawler Laboratory Operations Manager i i I I , i 175 Metro Center Boulevard • Warwick, Rhode Island 02886-1755 ! (401) 732-3400 • Fax (401) 732-3499 • wwwmitkem.com * Data Summary Pack < J7 bo Cd Qr ca O CY AT� rl x, cn I ai 0 z A suatzvjxoa-40# u P. U ti �Lb -flos Go C� Ifalvm ;> F. E[vd9 El z allsodwoD 0 0 i� El 4� —Y. 4K Cl) C/2 cy z 0 cn ri ul Cd CL "Ns fQ rn TI I g 4 e A. 1 0 :D CK t. 4n N M p z Q, u SH3MVINOD ao Ztb u ul tA U a tr- C; I (S R k- im 'A -e 0,0 WaHlo 14 T-r Z r4 n 10, zi "I - -Ilos 0 iN 00 'RAJIVM > 00 t 00 glisodwoz) 0 0 C=) at: CA tn 0 cn M r- El Ol A '4 z 0 Q u S 04 i Analytical Data Package for TRC Solutions, Inc. Client Project: Flynn Tan, Salem, Aqueous Samples Mitkem Project ID: C 1600 January 27, 2005, Revised 2/10/05 i Prepared For: TRC Solutions, Inc. Foot of John Street Lowell, MA 01.852 Attn: Ms. Liz Denly f Prepared By: Mitkem Corporation 175 Metro Center Boulevard Warwick, RI 02886 (401) 732-3400 1 i 1 000 �- SDG Narrative Mitkem Corporation submits the enclosed data package in response to TRC Solutions' Flynn Tan aqueous sample project. Under this deliverable, analysis results are presented for five samples that were received on December 28 and 29,2004 and logged in under Mitkem Work Order Number C1600. Analyses were performed per instruction in the chain of custody form. For reference, a copy of the Mitkem Work Order form is included for cross-referencing the client sample ID and laboratory sample ID. The analyses were performed according to Massachusetts DEP and EPA SW-846 methods, with results presented in a Level 4 format deliverable. The following observation and/or deviations are observed for the following analyses: 1. Volatile Organic Analyses: Samples were analyzed by Method 8260B. Surrogate standards: four surrogate standards were spiked into each analysis_ Surrogate recoveries were within the MADEP and Mitkem QC limits. Mitkem's statistical QC limits listed on the surrogate report form are wider than the MADEP 70%-130% limits for d4-1,2-dichloroethane. Lab control sample/lab control sample duplicate: spike recoveries were within the MADEP 70%- 130%limits with the exception of low recovery for 1,4-dioxane in V6WLCS and its duplicate and V6XLCS and its duplicate. This compound is also outside of the calibration acceptance criteria. A few compounds were recovered outside of the Mitkem statistical QC limits in V6XLCS and its duplicate. Lab fortified blank: laboratory fortified blanks at the 1 ug/L concentration level were analyzed to support a reduced reporting limit for vinyl chloride and.1,1-dichloroethene. Percent recoveries for both compounds in both LFB were within the QC limits. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Percent,recoveries and replicate RPDs were within the MADEP 70%- 130% limits, as well as the Mitkem statistical QC limits, with the exception of low recovery for for styrene in both the MS and MSD. Replicate RPD exceeded the MADEP 30% limit for vinyl acetate. Sample analysis: samples MW-2 and MW-3 were reanalyzed at 2X and 10X dilutions respectively. No other unusual occurrences were noted during sample analysis. ©06J I 2. MADEP VPH Analysis: Samples were analyzed by VPH Method 1.1. All samples were properly preserved. Surrogate standards:percent recoveries were within the QC limits. Lab control sample: spike recoveries were within the QC limits for the lab control sample s and duplicate lab control sample. Matrix spikelmatrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. .Percent recoveries and replicate RPDs were within the QC limits. Sample analysis: no unusual occurrences were noted during sample analysis. i 3. Semivolatile Organic Analyses: l Samples were extracted by Method 3520C continuous liquid-liquid extraction, and analyzed by Method 8270C. Surrogate standards: six surrogate standards were spiked into each analysis. All surrogate recoveries were within the Mitkem QC limits. All compounds are within the MADEP 30-130%limits for base/neutral and 15-110% limits for acid compounds with the exception of tribromophenol in samples MW-5, MW-6MS and MW-X recovered above the MADEP I 10% QC limit.. Lab control sample: spike recoveries were within the MADEP well as the Mitkem statistical QC limits with the exception of hexachlorocyclopentadiene recovered above the Mitkem limit but within the MADEP limit. Mitkem LCS QC limits are generally within the MADEP 40-140% limits for base/neutral and 30-130% limits for acid compounds with the exception of difficult analytes. These QC limits and the difficult compounds have been statistically determined per method requirements. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Percent recoveries were within the MADEP 40-140%limits for base/neutral and 30-130% limits for acid compounds with the exception of unusually low recovery for 3,3'dichlorobenzidine in the MS and MSD. A few compounds were outside of the Mitkem statistical QC limits. Replicate RPDs were within the MADEP and Mitkem limits with the exception of 3,3'-dichlorobenzidine. Sample analysis: the compounds aniline, azobenzene and acetophenone were not included on the analyte list for this project. No other unusual occurrences were noted during sample analysis. C/V 4. MADEP EPH Analysis: Samples were extracted by Method 3510C, separatory funnel extraction, and analyzed by EPH Method 04/1.1. Surrogate recovery: recoveries were within the QC limits. Laboratory control sample: spike recoveries in lab:control sample and duplicate LCS met the acceptance criteria of the method. Matrix spike/matrix spike duplicate: duplicate matrix spikes were performed on sample MW-6. Spike recoveries were within the QC limits with the exception of nonane recovered at 19% in the MSD and decane recovered at 39% and 27%respectively in the MS/MSD. This indicates some potential low bias for the lower molecular weight aliphatic range. Please note that Mitkem's reporting limits.for this range are significantly below the MCP standards, and that much of this range is also detectable in the VPH analysis. Sample analysis: a contaminant.in the EPH fractionation cartridges was present in the aliphatic and aromatic ranges. The identity of this contaminant has been confirmed by GUMS, and has been subtracted from the appropriate EPH Range results. The method blank and several samples contained C 11-C22 Aromatic Range organics above the reporting limit. This is due to a pattern of peaks typically due to EPH fractionation cartridge contamination. No other unusual occurrences were noted during sample analysis. 5. PCB Analysis: Samples were extracted by Method 3510C, separatory funnel, and analyzed by Method 8082. Surrogate standards: all percent recoveries were within the Mitkem statistical and MADEP QC limits. Mitkem's statistical QC limits listed on the surrogate report form are slightly different from the MADEP 30%-150%limits. Lab control sample: spike recoveries were within the QC limits in the LCS/LCS duplicate. Mitkem's statistical QC limits listed on the LCS report form are tighter than the MADEP 40%-I40%limits. Sample analysis: sample extracts were concentrated to 2mL final volume to provide reduced reporting limits. No other unusual occurrences were noted during sample analysis. 000�(L 6. Metals/Cyanide Analysis: Samples were analyzed by methods 601013, 7470 and 9012B. Lab control sample: spike recoveries were within the QC limits with the exception of cyanide recovery at 77.3%,which was below the 80%limit. A matrix spike and matrix duplicate were analyzed instead of a duplicate LCS. Matrix spike: matrix spike analysis was performed on sample MW-6. Spike recoveries. were within the QC limits with the exception of low recovery for cyanide. A post- digestion spike was performed for cyanide with significantly higher recovery. Cyanide results are qualified with the"N"flag. Duplicate: duplicate analyses were performed on sample MW-6. Replicate RPDs were within the QC limits. Sample analysis: no unusual occurrences were noted during sample analysis. All pages in this report have been numbered consecutively, starting with the title page and ending with a page saying only"Last Page of Data Report". I certify that this data package is in compliance,both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the laboratory manager or his designee,as veri d by the following signature. Edward A. Lawler Laboratory Operations Manager 1/27/05, Revised 2/10/05 MADEP MCP ANALYTICAL METHOD REPORT CERTIFICATION FORM Laboratory Name: , �'-� C� Project Ak Project Location: sc{lPdyj MADEP RTN': This Form provides certifications for the following data set: (list Laboratory Sample ID Number(s)J sew jCLbr�a�c�Pi ��e�f �/6 60 Sample Matrices. �rouaterSoil/Sediment Drinking Water Other. MCP SW-846 826OB-0 8151A( ) 8330( ) 6010B -7470A/lA Methods Used 8270C 8081A( ) VPH 6020( ) 9014M Z As specified in MADEP 8082 8021 B( ) EPH 7000 S3( ) 7196A( ) Compendium of - Analytical Methods. 1 List Release Tracking Number(RTN), if known 2 M-SW-846 Method 9014 or MADEP Physiologically Available Cyanide(PAC)Method (check all that apply) 3 S-SW-846 Methods 7000 Series List individual method and analyte. An affirmative response to questions A, B, C and D is required for"Presumptive Certainty"status j A Were all samples received by the laboratory in a condition consistent with Yes No' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical methods) B included in this report followed, including the requirement to note and Yes No' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for "Presumptive Certainty", as described in Section 2.0 (a), (b), (c) and Yes No' (d) of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? p VPH and EPH Methods only Was the VPH or EPH Method conducted Yes No ' without significant modifications "see Section 11.3 of respective Methods) A response to questions E and F below is required for"Presumptive Certainty"status E Were all analytical QC performance standards and recommendations for Yes No' the specified methods achieved? F Were results for all analyte-list compounds/elements for the specified .Yes No' method(s)reported? All Negative responses must be addressed in an attached Environmental Laboratory case narrative. 1, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical rep",,, to the best of my nowledge and belief, accurate and complete. Signature: - Position: Printed Name: &!�/lx- t) '� �' � Date: 7�r - - ----- CAM VII A.rev- 3.2 April 2004 006 CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 12/28/2004 Analysis: MADEP VPH 1.1 Date Received: 12/28/2004 Client ID: MW-5 Date Analyzed: 12/29/2004 Lab ID: C1600-01 B Aliquot Used for Analysis: 5 ml Matrix: Aqueous Sample pH: <2 Concentration in: ug/L Dilution Factor_ 1 Reporting Target Analvtes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xyiene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene ND 5 QC Batch: 16283 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 102 2,5-Dibromotoluene(PID)- 100 ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes_ Page 1 of 1 C 1600-01 B CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 12/29/2004 Analysis: MADEP VPH I A Date Received: 12/29/2004 Client ID: MW-6 Date Analyzed: 12/31/2004 Lab ID: C1600-02B Aliquot.Used for Analysis: 5 ml Matrix: Aqueous Sample.pH:<2 Concentration in: ug/L Dilution Factor_ 1 Reporting Target Analytes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene ND 5 QC Batch: 16321 VPH.Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 103 2,5-Dibromotoluene(PID) 98 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-02B l IT KEINI , tO•PO• Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 12/29/2004 Analysis: MADEP VPH 1.1 Date Received: 12/29/2004 Client ID: MW-X Date Analyzed: 12/31/2004 Lab ID: C1600-03B Aliquot Used for Analysis:5 ml Matrix: Aqueous Sample pH: <2 Concentration in: ug/L Dilution Factor: 1 Reporting Target Analytes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene ND 5 QC Batch: 16321 VPH Ranges C5-C8 Aliphatics ND 10.0 C9 -C10 Aromatics 100 100 C9 -C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 114 2,5-Dibromotoluene(PID) 109 ND=Not Detected . Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA1QC procedures were achieved. No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1600-03B IT KE _NI CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Date Collected: 12/29/2004 Analysis: MADEP VPH 1.1 Date Received: 12/29/2004 Client ID: MW-3 Date Analyzed: 12/31/2004 Lab ID: C1600-04B Aliquot Used for Analysis: 5 ml Matrix: Aqueous Sample pH:<2 Concentration in: ug/L Dilution Factor_ 1 Reporting Target Analytes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene 12 5 m-and p-Xylenes 36 5 MTBE ND 5 Naphthalene 48 5 QC Batch: 16321 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics 3,800 100 C9-C12 Aliphatics 1,100 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 98 2,5-Dibromotoluene(PID) 93 ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C 1600-04 B MIT KEM CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC_MA Date Collected: 12/29/2004 Analysis: MADEP VPH 1.1 Date Received: 12/29/2004 Client ID: MW-2 Date Analyzed: 12/31l2004 Lab ID: C1600-05B Aliquot Used for Analysis: 5 ml Matrix: Aqueous Sample pH:<2 Concentration in: ug/L Dilution Factor. 1 Reporting Target Analytes Results Limit Benzene ND 5 Ethylbenzene 62 5 Toluene ND 5 o-Xylene 8 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene 11 5 QC Batch: 16321 VPH Ranges C5-C8 Aliphatics ND 100 C9 -C10 Aromatics 750 100 C9-C12 Aliphatics 620 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 99 2,5-Dibromotoluene(PID) 96 ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. I i VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-05B I i • ' i• Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Analysis: MADEP VPH 1.1 Client ID: VBLK4H Date Analyzed: 12/29/2004 Lab ID: MB-16283 Aliquot Used for Analysis: 5 ml Matrix: Aqueous Concentration in:ug/L Dilution Factor 1 Reporting Target Analytes Results Limit Benzene NO 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND' 5 Naphthalene ND 5 QC Batch: 16283 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9'-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene (FID) 97 2,5-Dibromotoluene(PID) 93 ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Pagel of 1 C1600-MB 1 i MIT KE III ! CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Client: TRC MA Analysis: MADEP VPH 1.1 Client ID: VBLK4J Date Analyzed: 12/30/2004 Lab ID: MB-16311 Aliquot Used for Analysis: 5 ml Matrix: Aqueous Concentration in:ug/L Dilution Factor: 1 Reporting Target Analytes Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 Naphthalene ND 5 QC Batch: 16311 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 106 2,5-Dibromotoluene(PID) 107 ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the VPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. No significant modifications were made to this method. f VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes. Page 1 of 1 C 1600-MB CORPORATION Analysis Report:Volatile Petroleum Hydrocarbons Client: TRC MA Analysis: MADEP VPH 1-1 Client ID: VBLK4L Date Analyzed: 12/31/2004 Lab ID: MB-16321 Aliquot Used for Analysis: 5 ml Matrix: Aqueous Concentration in:ug/L Dilution Factor_ 1 Reporting Target Mal es Results Limit Benzene ND 5 Ethylbenzene ND 5 Toluene ND 5 o-Xylene ND 5 m-and p-Xylenes ND 5 MTBE ND 5 -Naphthalene ND 5 QC Batch: 16321 VPH Ranges C5-C8 Aliphatics ND 100 C9-C10 Aromatics ND 100 C9-C12 Aliphatics ND 100 Surrogate Recovery(%): 2,5-Dibromotoluene(FID) 102 2,5-Dibromotoluene(PID) 96 ND=Not Detected Except where noted in*the Project Narrative, all QA/QC procedures required by the VPH method were followed,and all performance/acceptance standards for the required QA/QC procedures were achieved_ No significant modifications were made to this method_ VPH ranges are adjusted to exclude the concentration of target and QC(surrogate)analytes_ Page 1 of 1 C1600-MB 'i CORPORATION a Analysis Report: Volatile Petroleum Hydrocarbons Matrix Spike Summary Client: TRC MA Client ID: MW-6 Matrix: Aqueous Lab ID for Matrix Spike: C1600-02BMS Analysis Date for Matrix Spike: 12/30/2004 Lab ID for MS Duplicate: C1600-02BMSD Analysis Date for MS Duplicate: 12/30/2004 Analysis: MADEP VPH 1.1 % Recovery Anal a Matrix Spike Matrix Spike Duplicate RPD(%1 Benzene 93 92 1 Ethylbenzene 88 90 2 Toluene 88 90 2 o-Xylene 90 91 1 m-and p-Xylenes 86 87 1 MTBE 100 101 0 Naphthalene 98 102 4 VPH Ranges C5-C8 Aliphatics 111 113 2 C9-C10 Aromatics 109 104 5 C9-C12 Aliphatics 71 70 1 Page 1 of 1 C1600-MS/MSD CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client: TRC_MA Matrix: Aqueous Lab ID for Blank Spike: LCS-16283 Analysis Date for Blank Spike: 12/29/2004 Lab ID for BS Duplicate: LCSD-16283 Analysis Date for BS Duplicate: 12/29/2004 Analysis: MADEP VPH 1.1 % Recovery Anal)de Blank Sc)ike Blank Spike Duplicate RPD Benzene 106 98 7 Ethylbenzene 103 96 7 Toluene 105 97 7 o-Xylene 103 96 7 m-and p-Xylenes 104 97 6 MTBE 106 99 6 Naphthalene 92 82 11 VPH Ranges C5-C8 Aliphatics 118 108 9 C9-C10 Aromatics 100 95 5 C9-C12 Aliphatics 99 90 10 QC Batch: 16283 Page 1 of 1 C1600-LCS i i MIT KE .NI CORPORATION Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client: TRC_MA Matrix: Aqueous Lab ID for Blank Spike: LCS-16311 Analysis Date for Blank Spike: 12/30/2004 Lab ID for BS Duplicate: . LCSD-16311 Analysis Date for BS Duplicate: 12/30/2004 Analysis: MADEP VPH I A % Recovery Anal a Blank Spike Blank.Sjke Duplicate RPD(%? Benzene 104 96 8 Ethylbenzene 104 96 8 Toluene 104 95 9 o-Xylene 104 97 6 m-and p-Xylenes 105 97 7 MTBE 111 106 4 Naphthalene 116 115 0 VPH Ranges C5-C8 Aliphatics 116 103 12 C9-C10 Aromatics 103 97 6 C9-C12 Aliphatics 99 90 10 QC Batch: 16311 Page 1 of 1 C1600-LCS O. O. Analysis Report: Volatile Petroleum Hydrocarbons Lab Control Summary Client: TRC MA Matrix: Aqueous Lab ID for Blank Spike: LCS-16321 Analysis-Date for Blank Spike: 12/31/2004 Lab ID for BS Duplicate: LCSD-16321 Analysis Date for BS Duplicate: 12/31/2004 Analysis: MADEP VPH 1.1 % Recov_ery Anal a Blank S��ike Blank Strike Duplicate RPD Benzene 105 100 4 Ethylbenzene 104 100 3 Toluene 104 100 3 o-Xylene 104 100 3 m-and p-Xylenes 104 101 2 MTBE 106 107 0 Naphthalene 103 112 8 VPH Ranaes C5-C8 Aliphatics 119 111 7 C9-C10 Aromatics 102 101 1 C9-C12 Aliphatics 105 100 5 QC Batch: 16321 Page 1 of 1 C1600-LCS 1 CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/28/04 Client ID: MW-5 Date Received: 12/28/04 Lab ID: C1600-01C Date Extracted: 1/10/05 Matrix. Aqueous Date Analyzed: 1/17/05 F1, 1/17/05 F2 Concentration in: ug/L Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics ND .200 C19-C36 Aliphatics. ND 200 C11 -C22 Aromatics 260, 100 Target Analytes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a) anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a) pyrene ND 5 Indeno(1,2,3-cd) pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 78% o-Terphenyl 80% 2-Fluorobiphenyl 79% 2-Bromonaphthalene 68% ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and.QC(surrogate)analytes. Page 1 of 1 C1600-01C CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/29/04 Client ID: MW-6 Date Received: 12/29/04 Lab ID: C1600-02C Date Extracted: 1/10/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17/05 F2 Concentration in: ug/L Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics ND 200 C19-C36 Aliphatics ND 200 C11 -.C22 Aromatics 120 100 Target Analytes Naphthalene ND 5 2-Methyinaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi) perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 78% o-Terphenyl 78% 2-Fluorobiphenyl 74% 2-13romonaphthalene 67% ND= Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-02C CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/29/04 Client ID: MW-X Date Received: 12/29/04 Lab ID: C1600-03C Date Extracted: 1/10/05 Matrix: Aqueous Date Analyzed: Ill7105 F1, 1/17/05 F2 Concentration in: ug/L Dilution: 1 Reporting EPH Ranqes Results Limits C9-C18 Aliphatics ND 200 C19-C36 Aliphatics ND 200 C11 -C22 Aromatics ND 100 Target Anal des Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a) pyrene ND 5 Indeno(1,2,3-cd) pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 83% o-Terphenyl 84% 2-Fluorobiphenyl 77% 2-Bromonaphthalene 72% ND=Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved_ EPH ranges are adjusted to exclude concentration of target and QC(surrogate) analytes_ Page 1 of 1 C1600-03C CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/29/04 Client ID: MW-3 Date Received: 12/29/04 Lab ID: C1600-04C Date Extracted: 1/10/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17105 F2 Concentration in:ug/L Dilution: 1 Reporting EPH Ranaes Results Limits C9-C18 Aliphatics 430 200 C19-C36 Aliphatics ND 200 C11 -C22 Aromatics . ND 100 Target Analytes Naphthalene 19 5 2-Methyl naphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a) anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo (a) pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 70% o-Terphenyl 74% 2-Fluorobiphenyl 82% 2-Bromonaphthalene 67% ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC (surrogate)analytes_ Page 1 of 1 C1600-04C Ood�?-� MIT KE -NI ' CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/29/04 Client ID: MW-2 Date Received: 12/29/04 Lab ID: C1600-05C Date Extracted: 1/10/05 Matrix: Aqueous Date Analyzed: 1/17/05 F1, 1/17105 F2 Concentration in:ug/L Dilution: 1 Reporting EPH Ramses Results Limits C9-C18 Aliphatics ND 200 C19-C36 Aliphatics ND 200 C11 -C22 Aromatics 100 100 Target Analytes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND - 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b)Fluoranthene ND 5 Benzo(k)Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi) perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 79% o-Terphenyl 79% 2-Fluorobiphenyl 75% 2-Bromonaphthalene 69% ND=Not Detected Except where noted in the Project Narrative,all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC(surrogate)analytes. Page 1 of 1 C1600-05C CORPORATION Analysis Report: Extractable Petroleum Hydrocarbons Client: TRC_MA Analysis: MADEP EPH 04/1.1 Date Collected: 12/28/04 Client ID: Date Received: 12/28/04 Lab ID: MB-16432 Date Extracted: 1/10/05 Matrix. Aqueous Date Analyzed: 1/17/05 F1, 1/17/05 F2 Concentration in: ug/L Dilution: 1 Reporting EPH Ranges Results Limits C9-C18 Aliphatics ND 200 C19-C36 Aliphatics ND 200 C11 -C22 Aromatics 310 100 Target Analytes Naphthalene ND 5 2-Methylnaphthalene ND 5 Acenaphthylene ND 5 Acenaphthene ND 5 Fluorene ND 5 Phenanthrene ND 5 Anthracene ND 5 Fluoranthene ND 5 Pyrene ND 5 Benzo(a)anthracene ND 5 Chrysene ND 5 Benzo(b) Fluoranthene ND 5 Benzo(k) Fluoranthene ND 5 Benzo(a)pyrene ND 5 Indeno(1,2,3-cd)pyrene ND 5 Dibenzo(a,h)anthracene ND 5 Benzo(ghi)perylene ND 5 QC Batch: MB-16432 Surrogate Recovery: Chlorooctadecane 92% o-Terphenyl 92% 2-Fluorobiphenyl 72% 2-Bromonaphthalene 69% ND= Not Detected Except where noted in the Project Narrative, all QA/QC procedures required by the EPH method were followed, and all performance/acceptance standards for the required QA/QC procedures were achieved. EPH ranges are adjusted to exclude concentration of target and QC (surrogate) analytes. Page 1 of 1 MB-16432 CORPORATION Analysis Report: Lab Control Sample Client TRC Date Extracted for LCS/LCSD: 1/10/06 Matrix: Aqueous Date Analyzed for LCS: 1/17/05 Lab ID for Lab Control Sample(LCS): LCS-16432 Date Analyzed for LCSD: 1117/05 Lab ID for Lab Control Sample Duplicate(LCSD): LCSD-16432 Analysis: MADEP EPH 04-1.1 MADEP EPH - F1 -ALIPHATICS Ana e % Recovery LCS LCSD % RPD Nonane C9 32 39 20 Decane C10 41 44 9 Dodecane C12 50 51 1 Tetradecane C14 60 61 2 Hexadecane C16 72 71 1 Octadecane C18 79 76 4 Nonadecane C19 81 78 4 Eicosane C20 87 84 4 Docosane C22 85 82 4 Tetracosane C24 83 79 5 Hexacosane C26 84 80 5 Octacosane C28 84 80 5 Triacontane.C30 83 79 5 Hexatriacontane C36 82 78 5 C9-C18 Aliphatics 56 57 3 C19-C36 Aliphatics 84 80 5 Surrogate Recovery LCS LCSD Chlorooctadecane 100% 92% % Naphthalene Breakthrough: 0-0 0.0 %2-methyinaphtalene Breakthrough: 0.0 0.0 i Page 1 of 2 eph.lcs I i MIT KE -NI CORPORATION .• /, ! • Analysis Report: Lab Control Sample Client: TRC Date Extracted for LCS/LCSD: 1110/05 Matrix: Aqueous Date Analyzed for LCS: 1/17/05 Lab ID for Lab Control Sample(LCS): LCS-16432 Date Analyzed for LCSD: 1/17/05 Lab ID for Lab Control Sample Duplicate(LCSD): LCSD-16432 Analysis: MADEP EPH 04-1.1 MADEP EPH - F2 -AROMATICS Anal a % Recovery LCS LCSD % RPD Naphthalene 50 53 7 2-Methylnaphthalene 50 .52 5 Acenaphthylene 63 63 1 Acenaphthene 70 71 1 Fluorene 72 72 1 Phenanthrene 80 80 1 Anthracene 80 82 1 Fluoranthene 83 84 0 Pyrene 83 83 0 Benzo(a)anthracene 80 80 1 Chrysene 87 87 1 Benzo(b)Fluoranthene 82 80 1 Benzo(k) Fluoranthene 82 81 2 Benzo(a) pyrene 84 83 1 Indeno(1,2,3-cd)pyrene 81 80 1 Dibenzo(a,h)anthracene 74 73 1 Benzo(ghi) perylene 79 78 1 C11 -C22 Aromatics 75 76 0 Surrogate Recovery: LCS LCSD o-Terphenyl 91% 89% 2-Fluorobiphenyl 76% 76% 2-Bromonaphthalene 72% 71% Page 2 of 2 eph.lcs E i CORPORATION 1 j Analysis Report: Matrix Spike Client TRC Date Extracted for MS/MSD: 1/10/05 Matrix: Aqueous Date Analyzed for MS: 1/17/05 Client ID: MW-6 Date Analyzed for MSD: 1/17/05 Lab ID for Matrix Spike(MS): C1600-02CMS Lab ID for Matrix Spike Duplicate(MSD): C1600-02CMSD Analysis:MADEP EPH 04-1.1 MADEP EPH - F1 -ALIPHATICS Anal e % Recovery MS MSD % RPD Nonane C9 30 19 45 Decane C10 39 27 38 Dodecane C12 51 43 17 Tetradecane C14 58 50 15 Hexadecane C16 70 65 8 Octadecane C18 77 73 5 Nonadecane C19 79 76 4 Eicosane C20 86 84 2 Docosane C22 86 84 2 Tetracosane,C24 83 82 1 Hexacosane C26 84 83 1 Octacosane C28 83 82 1 Triacontane C30 83 82 1 Hexatriacontane C36 83 81 2 C9-C18 Aliphatics 54 46 16 C19-C36 Aliphatics 83 82 2 Surrogate Recovery MS MSD Chlorooctadecane 97% 95% Page 1 of 2 eph.ms/msd i 114 CORPORATION Analysis Report: Matrix Spike Client: TRC Date Extracted for MS/MSD: 1/10/05 Matrix: Aqueous Date Analyzed for MS: 1/17/05 Client ID: MW-6 Date Analyzed for MSD: 1117/05 Lab ID for Matrix Spike(MS): C1600-02CMS Lab ID for Matrix Spike Duplicate(MSD): C1600-02CMSD Analysis: MADEP EPH 04-1.1 - MADEP EPH - F1 - AROMATICS Analyte % Recovery MS MSD % RPD Naphthalene 50 43 16 2-Methylnaphthalene 52 45 15 Acenaphthylene 66 60 9 Acenaphthene 72 66 8 Fluorene 74 70 7 Phenanthrene 82 79 3 Anthracene 83 81 3 Fluoranthene 84 84 0 Pyrene 84 84 0 Benzo(a)anthracene 81 82 2 Chrysene 87 89 3 Benzo(b) Fluoranthene 81 84 4 Benzo (k) Fluoranthene 82 84 2 Benzo(a) pyrene 83 85 3 Indeno (1,2,3-cd)pyrene 79 82 3 Dibenzo(a,h)anthracene 72 76 6 Benzo(ghi)perylene 78 80 3 C11 -C22 Aromatics 76 75 1 Surrogate Recovery_: MS MSD o-Terphenyl 89% 88% 2-Fluorobiphenyl 81% 81% 2-Bromonaphthalene 84% 85% Page 2 of 2 eph.ms/msd j 12/15/04 Fractionation Checks I LOT: 409070-QL Conc Recovery Conc Recovery ALIPHATICS (ng/uL) (%) AROMATICS (ng/uL) (%) Nonane C9 8.794 70 Naphthalene 10.007 80 Decane C10 9.998 80 2-Methyinaphthalene 10.077 81 Dodecane C12 10.103 81 Acehaphthylene 10.388 83 Tetradecane C14 10.307 82 Acenaphthene 10.402 83 Hexadecane C16 10.027 80 Fluorene 10.646 85 Octadecane C1.8 10.78 86. Phenanthrene 10.996 88 Nonadecane C19 10.234 82 Anthracene. 11.721 94 Eicosane C20 10.552 84 Fluoranthene 11.26 90 Docosane C22- 10.251 82 Pyrene 11.155 89 Tetracosane C24t 10.367 83 Benzo(a)anthracene 11.319 91 Hexacosane C26 10.064 81 Chrysene 11.268 90 Octacosane C28 10.297 82 Benzo(b)Fluoranthene 11.279 90 . Triacontane C30 10.267 82 Benzo(k)Fluoranthene 10.835 87 Hexatriacontane C36 9.122 73 Benzo-(a)pyrene 11.77 94 Indeno(1,2,3-cd)pyrene 11.325 91 C9-C18 Aliphatics 80 Dibenzo(a;h)anthracene 10.542 .84. C19-C36 Aliphatics 81 Benzo(gh7 perylene 11.219 90 C11-C22 Aromatics 88. lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5105 Level: - (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4-------- Trichlorofluoromethane 5 U 75-35-4-------- 1,1-Dichloroethene 1 U 67-64-1---------Acetone 2 J 74-88-4---------Iodome e 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 1 J 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2 Lab Name: MITKEM CORPORATION Contract: f Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5105 Level: (low/med) LOW Date Received: 12/29/04 s Moisture: not dec. bate Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9-----= 1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 64 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene _ 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 15 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 24 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 8 95-63-6---------1,2,4-Trimethylbenzene 180 135-98-8--------sec-Butylbenzene 14 99-87-6---------4-Isopropyltoluene . 4 J 541-73-1---------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 1 J 104-51-8---------n-Butylbenzene 9 95-50-1---------1,2-Dichlorobenzene 2 J 96-12-8----------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87=68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 13 FORM I VOA O1,M03:0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5105 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7----------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tent-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM. I VOA OLM03.0 { lA EPA SAMPLE NO. f VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2DL j Lab Name: MITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5139 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 2.0 Soil Extract Volume: - (uL) Soil Aliquot Volumes _(uL) CONCEN`IRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 10 U 74-87-3---------Chloromethane 10 U 75-01-4---------Vinyl Chloride 4 U 74-83-9---------Bromomethane 10 U 75-00-3---------Chloroethane 10 U 75-69-4---------Trichlorofluoromethane 10 U 75-35-4---------1,1-Dichloroethene 2 U 67-64-1---------Acetone 10 U 74-88-4---------Iodomethane 10 U 75-15-0---------Carbon Disulfide 10 U 75-09-2---------Methylene Chloride 10 U 156-60-5--------trans-1,2-Dichloroethene 10 U 1634-04-4-------Methyl tert-butyl ether 10 U 75-34-3------- 1,1-Dichloroethane 10 U 108-05-4--------Vinyl acetate 10 U 78-93-3---------2-Butanone 10 U 156-59-2--------cis-1,2-Dichloroethene 10 U 590-20-7--------2,2-Dichloropropane 10 U 74-97-5---------Bromochloromethane 10 U 67-66-3---------Chloroform 10 U 109-99-9--------Tetrahydrofuran 10 U 71-55-6---------1,1,1-Trichloroethane 10 U 563-58-6--------1,1-Dichloropropene 10 U 56-23-5---------Carbon Tetrachloride 10 U 107-06-2--------1,2-Dichloroethene 10 U 71-43-2---------Benzene 10 U 79-01-6---------Trichloroethene 10 U 78-87-5---------1,2-Dichloropropane 10 U 74-95-3---------Dibromomethane 10 U 75-27-4---------Bromodichloromethane 10 U 10061-01-5------cis-1,3-Dichloropropene 10 U 108-10-1--------4-Methyl-2-pentanone 10 U 108-88-3--------Toluene 10 U 10061-02-6------trans-1,3-Dichloropropene 10 U FORM I VOA OLM03.0 1 . 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-2DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5139 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 2.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 10 U 142-28 9--------1,3-Dichloropropane 10 U 127-18-4--------Tetrachloroeth_ ene 10 U 591-78-6--------2-Hexanone 10 U 124-48-1--------Dibromochloromethane 10 U 106-93-4--------1,2-Dibromoethane 10 U 108-90-7--------Chlorobenzene 57 D 630-20-6--------1,1,1,2-Tetrachloroethane 10 U 100-41-4--------Euhylbenzene 10 U ----------------m,p-Xylene _ 10 U 95-47-6---------o-Xylene 10 U 1330-20-7-------Xylene (Total) 10 U 100-42-5--------Styrene 10 U 75-25-2---------Bromoform 10 U 98-82-8---------Isopropy nzene 13 D 79-34-5---------1,1,2,2-Tetrachloroethane 10 U 108-86-1--------Bromobenzene 10 U 96-18-4---------1,2,3-Trichloropropane__ 10 U 103-65-1--------n-Propylbenzene 23 D 95-49-8------- 2-Chlorotoluene 10 U 108-67-8--------1,3,5-Trimethy nzene 10 U 106-43-4--------4-Chlorotoluene 10 U 98-06-6---------tert-Butylbenzene 6 DJ 95-63-6---------1,2,4-Trimethylbenzene 220 D 135-98-8--------sec-Butylbenzene 13 D 99-87-6---------4-Isopropyltoiuene 4 DJ 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 104-51-8--------n-Butylbenzene_ 9 DJ 95-50-1---------1,2-Dichlorobenzene 10 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 87-68-3---------Hexachlorobutadiene -10 U 91-20-3---------Naphthalene 14 D FORM I VOA OLM03.0 i 7A EPA SAMPLE NO. j VOLATILE ORGANICS -ANALYSIS DATA SHEET MW-2DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No_ : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-05ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5139 1 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 2.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 10 U 60-29-7---------Ether 10 U 108-20-3--------Diisopropyl Ether_ 10 U 637-92-3--------Ethyl tert-butyl ether 10 U 994-05-8--------tert-Amyl methyl ether 10 U 123-91-1--------1,4-Dioxane 200 U i 1 i , i i I i 1 FORM I VOA OLM03.0 i iA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5104 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: - __(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chlorotnethane 5 U 75-01-4---------Vinyl Chloride _ 2 U 74-83-9---------Bromomethane _ 5 U 75-00-3---------Chloroethane 1 J 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene__ 1 U 67-64-1---------Acetone 4 J 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate__ 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane_ 5 U 74-97-5---------Bromochloromethane_ 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropene 5 U 74-95-3---------Dibromomethane _ 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5104 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (Mm) Dilution Factor: 1.0 Soil Extract Volume: {uL) Soil Aliquot Volume: __(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q i 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3=Dichloropropane 5 U 121-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromet e 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1, 1,1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene 5 U ----------------m,p-Xylene 34 95-47-6---------o-Xylene 11 1330-20-7-------Xylene (Total) 45 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 4 J 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U. 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 310 E 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 10 95-63-6---------1,2,4-Trimethylbenzene 480 E 135-98-8--------sec-Butylbenzene 10 99-87-6---------4-Isopropyltoluene 44 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 2 J 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 6 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 54 I - I FORM I VOA OLM03.0 I i I _ 1A . EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5104 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl .tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5145 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 10.0 Soil Extract Volume: (uL) Soil Aliquot Volume: AUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 50 U 74-87-3--------- Chloromethane 50 U 75-01-4---------Vinyl Chloride 20 U 74-83-9---------Bromomethane 50 U 75-00-3---------Chloroethane 50 U 75-69-4---------Trichlorofluoromethane 50 U 75-35-4---------1,1-Dichloroethene 10 U 67-64-1---------Acetone' 50 U 74-88-4---------Iodomet e 50 U 75-15-0-------=-Carbon Disulfide 50 U 75-09-2---------Methylene Chloride 50 U 156-60-5--------trans-1,2-Dichloroethene 50 U 1634-04-4-------Methyl tert-butyl ether 50 U 75-34-3---------1,1-Dichloroethane 50 U 108-05-4---- ---Vinyl acetate 50 U 78-93-3---------2-Butanone 50 U 156-59-2--------cis-1,2-Dichloroethene 50 U 590-20-7--------2,2-Dichloropropane 50 U 74-97-5---------Bromochloromethane 50 U 67-66-3---------Chloroform 50 U 109 99-9--------Tetrahydrofuran 50 U 71-55-6---------1,1,1-Trichloroethane 50 U 563-58-6--------1,1-Dichloropropene 50 U 56-23-5---------Carbon Tetrachloride 50 U 107-06-2--------1,2-Dichloroethane 50 U 71-43-2---------Benzene 50 U 79-01-6---------Trichloroethene 50 U 78-87-5---------1,2-Dichloropropane _ 50 U 74-95-3---------Dibromomethane 50 U 75-27-4----------Bromodichloromet e w 50 U 10061-01-5------cis-1,3-Dichloroprcpene 50 U 108-10-1--------4-Methyl-2-pentanone _ 50 U 108-88-3--------Toluene 50 U 10061-02-6------trans-1,3-Dichloropropene 50 U FORM I VOA OLM03.0 I lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3DL Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5145 Level: (low/med) LOW Date Received: 12/29/04 °s Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 10.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCEN' RATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 50 U 142-28-9--------1,3-Dichloroprcpane 50 U 127-18-4--------Tetrachloroethene 50 U 591-78-6--------2-Hexanone 50 U 124-48-1--------Dibromochloromethane 50 U 106-93-4--------1,2-Dibromoethane 50 U 108-90-7--------Chlorobenzene 50 U 630-20-6--------1,1, 1,2-Tetrachloroethane 50 U 100-41-4--------Euhylbenzene 50 U ----------------m,p-Xylene 26 DJ 95-47-6---------o-Xylene 50 U 1330-20-7-------Xylene (Total) 26 DJ 100-42-5--------Styrene 50 U 75-25-2---------Bromoform 50 U 98-82-8---------Isopropylbenzene 50 U 79-34-5---------1,1,2,2-Tetrachloroethane 50 U 108-86-1--------Bromobenzene 50 U 96-18-4---------1,2,3-Trichloropropane 50 U 103-65-1--------n-Propylbenzene 50 U 95-49-8---------2-Chlorotoluene 50 U 108-67-8--------1,3,5-Trimethylbenzene 470 D 106-43-4--------4-Chlorotoluene 50 U 98-06=6---------tert-Butylbenzene 50 U 95-63-6---------1,2,4-Trimethylbenzene 1200 D 135-98-8--------sec-Butylbenzene 50 U 99-87-6---------4-Isopropyltoluene 50 U 541-73-1--------1,3-Dichlorobenzene 50 U 106-46-7--------1,4-Dichlorobenzene _ 50 U 104-51-8------- n-Butylbenzene 50 U 95-50-1---------1,2-Dichlorobenzene 50 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 50 U 120-82-1--------1,2,4-Trichlorobenzene 50 U 87-68-3---------Hexachlorobutadiene 50 U 91-20-3---------Naphthalene 58 D FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-3DL Lab Name: MITKEM CORPORATION Contract: 1 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-04ADL Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5145 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 10.0 Soil Extract Volume: -(uL) Soil Aliquot Volume: - _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 50 U 60-29-7---------Ether 50 U 108-20-3--------Diisopropyl Ether 50 U 637-92-3--------Ethyl tert-butyl ether 50 U 994-05-8--------tert-Amyl methyl ether 50 U 123-91-1--------1,4-Dioxane 1000 U i i , i i i i FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG NO. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5099 Level: (low/med) LOW Date Received: 12/28/04 Moisture: ,not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate_ 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 j IA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5099 Level: (low/med) LAW Date Received: 12/28/04 Moisture: not dec. Date Analyzed: 01/04/05 i GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 1 79-00-5-------.--1, 1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone _ 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1, 1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 2 J 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-.Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1, 2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U i FORM I VOA OLM03:0 i lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5099 Level: (low/med) LOW Date Received: 12/28/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume:. __ JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-.6---------1,2,3-Trichlorobenzene _ _ 5 U 60-29-7---------Ether _ 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA' SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5100 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q i 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene_ _ 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1, 1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene '5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6-------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 i i I i - - lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: MITKEM CORPORATION Contract: MW-6 Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02A Sample wt/vol: .5.000 (g/mL) ML Lab File ID: V6D5100 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution- Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1, 1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5----------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene _ 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03 .0 lA EPA SAMPLE NO. 1 -VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5100 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. . Date Analyzed: 01/04/05 i GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _.JUL) CONCENTRATION UNITS: i CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q i 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMS Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5143 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (am) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: JUL) CONCEDI`IRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 48 74-87-3---------Chloromethane 49 75-01-4---------Vinyl Chloride 48 74-83-9---------Bromomethane _ 55 75-00-3---------Chloroethane 46 75-69-4---------Trichlorofluoromethane 58 75-35-4---------1,1-Dichloroethene 50 67-64-1---------Acetone 30 74-88-4---------Iodomethane 55 75-15-0---------Carbon Disulfide 43 75-09-2---------Methylene Chloride 51 156-.60-5--------trans-1,2-Dichloroethene 40 1634-04-4-------Methyl tert-butyl ether 78 75-34-3---------1,1-Dichloroethane 39 108-05-4--------Vinyl acetate 66 78-93-3---------2-Butanone 33 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropane 37 74-97-5---------Bromochloromethane 44 67-66-3---------Chloroform 42 109-99-9--------Tetrahydrofuran 54 71-55-6---------1,1,1-Trichloroethane 40 563-58-6--------1,1-Dichloropropene 43 56-23-5---------Carbon Tetrachloride 39 107-06-2--------1,2-Dichloroethane 42 71-43-2---------Benzene 43 79-01-6---------Trichloroethene 43 78-87-5---------1,2-Dichloropropane _ 42 74-95-3---------Dibromomethane 45 75-27-4---------Bromodichloromethane 39 10061-01-5------cis-1,3-Dichloropropene 38 108-10-1--------4-Methyl-2-pentanone 37 108-88-3--------Toluene 44 10061-02-6------trans-1,3-Dichloropropene 37 FORM I VOA OLM03 .0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMS Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5143 Level: (low/med) LOW Date Received: .12/29/04 °s Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 45 142-28-9--------1,3-Dichloropropane 46 121-18-4--------Tetrachloroethene 51 591-78-6--------2-Hexanone 35 124-48-1--------Dibromochloromethane 40 106-93-4--------1,2-Di.bromoethane 48 108-90-7--------Chlorobenzene 49 630-20-6--------1, 1,1,2-Tetrachloroethane 44 100-41-4--------Ethylbenzene 47 ----------------m,p-Xylene 92 95-47-6---------o-Xylene 46 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 31 75-25-2---------Bromoform 35 98-82-8---------Isopropylbenzene 46 79-34-5---------1,1,2,2-Tetrachloroethane 52 108-86-1--------Bromobenzene 50 96-18-4---------1,2,3-Trichloropropane 44 103-65-1--------n-Propylbenzene 50 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 44 106-43-4--------4-Chlorotoluene 51 98-06-6---------tert-Butylbenzene 50 95-63-6---------1,2,4=Trimethylbenzene 44 135-98-8--------sec-Butylbenzene 50 99-87-6---------4-Isopropyltoluene 50 541-73-1--------1,3-Dichlorobenzene 51 106-46-7--------1,4-Dichlorobenzene 52 104-51-8------ n-Butylbenzene 52 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3--chloropropane 45 120-82-1--------1,2,4-Trichlorobenzene 50 87-68-3---------Hexachlorobutadiene 47 91-20-3---------Naphthalene 52 FORM I VOA OLM03:0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMS Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5143 Level: (low/med) LAW Date Received: 12/29/04 96 Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: _ -(uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 50 60-29-7---------Ether 49 108-20-3--------Diisopropyl Ether 44 637-92-3--------Ethyl tert-butyl ether 42 994-05-8--------tert-Amyl methyl ether 46 123-91-1--------1,4-Dioxane 630 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMSD Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5144 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 45 74-87-3---------Chloromethane 48 75-01-4---------Vinyl Chloride 45 i 74-83-9---------Bromomethane 52 75-00-3---------Chloroethane 46 75-69-4-------- Trichlorofluoromethane 56 75-35-4---------1,1-Dichloroethene 49, 67-64-1---------Acetone 33 74-88-4---------Iodomet e 53 75-15-0---------Carbon Disulfide 53 75-09-2---------Methylene Chloride 50 156-60.-5--------trans-1,2-Dichloroethene 40 1634-04-4-------Methyl tert-butyl ether 81 75-34-3---------1,1-Dichloroethane 38 108-05-4--------Vinyl acetate 41 78-93-3---------2-Butanone 35 156-59-2--------cis-1,2-Dichloroet ene 42 590-20-7--------2,2-Dichloropropane 35 74-97-5---------Bromochloromethane 44 67-66-3---------Chloroform 42 109-99-9--------Tetrahydrofuran 59 71-55-6---------1,1,1-Trichloroethane 39 563-58-6--------1,1-Dichloropropene 42 56-23-5---------Carbon Tetrachloride 37 107-06-2--------1;2-Dichloroethane 42 i 71-43-2---------Benzene 43 79-01-6---------Trichloroethene 43 78-87-5---------1,2-Dichloropropane 42 74-95-3---------Dibromomethane 45 75=27-4---------Bromodichloromethane 38 10061-01-5------cis-1,3-Dichloropropene 38 108-10-1--------4-Methyl-2-pentanone 39 108-88-3--------Toluene 43 10061-02-6------trans-1,3-Dichloropropene 37 t i FORM I VOA OLM03 :0 I lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMSD Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5144 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 46 142-28-9--------1,3-Dichloropropane 48 127-18-4--------Tetrachloroethene_ 50 591-78-6--------2-Hexanone 40 124-48-1--------Dibromochloromethane 40 106-93-4--------1,2-Dibromoethane_ 50 108-90-7--------Chlorobenzene 49 630-20-6--------1,1, 1,2-Tetrachloroethane 44 100-41-4--------Ethylbenzene 46 ----------------m,p-Xylene 91 95-47-6---------o-Xylene 45 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 30 75-25-2---------Bromoform 36 98-82-8---------Isopropylbenzene 46 79-34-5---------1,1,2,2-Tetrachloroethane 54 108-86-1--------Bromobenzene 50 96-18-4---------1,2,3-Trichloropropane_ 42 103-65-1--------n-Propylbenzene 48 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 43 106-43-4--------4-Chlorotoluene 151 98-06-6---------tert-Butylbenzene 48 95-63-6---------1,2,4-Trimethylbenzene 43 135-98-8--------sec-Butylbenzene 49 99-87-6---------4-Isopropyltoluene 48 541-73-1--------1,3-Dichlorobenzene 51 106-46-7--------1,4-Dichlorobenzene _ 52 104-51-8--------n-Butylbenzene 49 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3-chloropropane_ 47 120-82-1--------1,2,4-Trichlorobenzene 50 87-68-3---------Hexachlorobutadiene 45 91-20-3---------Naphthalene 55 FORM I VOA OLM03:0 J lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02AMSD i Sample wt/vol: 5.000 (g/mL) ML Lab File ID: VGD5144 Level: (low/med) -LOW Date Received: 12/29/04 °s Moisture: not dec. Date Analyzed: 01/05/0.5 1 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 50 60-29-7---------Ether 54 108-20-3--------Diisopropyl Ether 44 637-92-3--------Ethyl tert-butyl ether_ _ 44 994-05-8--------tert-Amyl methyl ether 47 123-91-1--------1,4-Dioxane 830 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5101 Level: (low/med) LOW Date Received: 12/29/04 °s Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume:..--- (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane _ 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane _ 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone _ 5 U 74-88-4---------Iodomethane 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochlorcmethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethene 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropene 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 100.61-02-6------trans-1,3-Dichloropropene 5 U I FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5101 Level: (low/med) LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (nun) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L. or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U. 95-47-6---------o-Xylene . 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8----------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene_ 5 U !, 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene_ 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03.0 I I i j lA EPA SAMPLE NO.. VOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix:-(soil/water) WATER Lab Sample ID: C1600-03A Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5101 Level: (low/med) .LOW Date Received: 12/29/04 Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U ' 60-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U { i i 1 1 FORM I VOA OLM03:0 I i lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5094 Level: (low/med) LOW Date Received: OW Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: WL.) CONCENTRATION.UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichiorodifluoromethane 43 74-87-3---------Chloromethane 44 75-01-4---------Vinyl Chloride 45 74-83-9---------Bromomethane 54 75-00-3---------Chloroethane 47 75-69-4---------Trichlorofluoromethane 51 75-35-4---------1,1-Dichloroethene 47 67-64-1---------Acetone 44 74-88-4---------Iodomethane 51 75-15-0---------Carbon Disulfide 46 75-09-2---------Methylene Chloride _ 49 156-60-5--------trans-1,2-Dichloroethene 45 1634-04-4-------Methyl tert-butyl ether 86 75-34-3---------1,1-Dichloroethene_ 44 108-05-4--------Vinyl acetate 45 78-93-3---------2-Butanone 38 156-59-2--------cis-1,2-Dichloroethene 46 590-20-7--------2,2-Dichloropropane 44 74-97-5---------Bromochloromethane 48 67-66-3---------Chloroform 47 109-99-9--------Tetrahydrofuran 48 71-55-6---------1,1,1-Trichloroethane 45 563-58-6--=-----1,1-Dichloropropene 48 56-23-5---------Carbon -Tetrachloride 45 107-06-2--------1,2-Dichloroethene 45 71-43-2---------Benzene 47 79-01-6---------Trichloroethene 48 78-87-5---------1,2-Dichloropropane_ 46 74-95-3---------Dibromomethane 47 75-27-4---------Bromodichloromethane 45 10061-01-5------cis-1,3-Dichloropropene 45 108-10-1--------4-Methyl-2-pentanone 38 108-88-3--------Toluene_ 48 10061-02-6------trans-1,3-bichloropropene 44 FORM I VOA OLM03 A lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16366 Sample wt/vol: 5.000 (g/mL) ML. Lab File ID: V6D5094 Level: (low/med) LOW Date Received: _ °s Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mate) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: __(UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1',2-Trichloroethane 47 142-28-9--------1,3-Dichloropropane 46 127-18-4--------Tetrachloroethene 48 591-78-6--------2-Hexanone 37 124-48-1--------Dibromochloromethane w 45 106-93-4--------1,2-Dibromoethane 47 108-90-7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetrachloroethane 46 100-41-4--------Ethylbenzene 48' ----------------m,p-Xylene 97 95-47-6---------o-Xylene 48 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 49 75-25-2---------Bromoform 43 98-82-8---------Isopropylbenzene 47 79-34-5---------1,1,2,2-Tetrachloroethane 44 108-86-1--------Bromobenzene 46 96-18-4---------1,2,3-Trichloropropane 43 103-65-1--------n-Propylbenzene 47 95-49-8---------2-Chlorotoluene 47 108-67-8--------1,3,5-Trimethylbenzene 47 106-43-4--------4-Chlorotoluene 47 98-06-6---------tert-Butylbenzene 46 95-63-6---------1,2,4-Trimethylbenzene 47 135-98-8--------sec-Butylbenzene 47 99-87-6---------4-Isopropyltoluene 48 541-73-1--------1,3-Dichlorobenzene 47 106-46-7--------1,4-Dichlorobenzene 47 104-51-8--------n-Butylbenzene 47 95-50-1---------1,2-Dichlorobenzene 47 96-12-8---------1,2-Dibromo-3-chloropropane_ 38 120-82-1--------1,2,4=Trichlorobenzene_ 46 87-68-3---------Hexachlorobutadiene 44 91-20-3---------Naphthalene 41 FORM I VOA 012403.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEEP V6WLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5094 Level: (low/med) LOW Date Received: !° Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: . _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 46 60-29-7---------Ether 49 108-20-3--------Diisopropyl Ether 48 637-92-3--------Ethyl tert-butyl ether 48 994-05-8--------tert-Amyl methyl ether 50 123-91-1--------1,4-Dioxane 190 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5095 i Level: (low/med) LOW Date Received: o Moisture: . not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 45 74-87-3---------Chloromethane 46 75-01-4---------Vinyl Chloride 46 74-83-9---------Bromomethane 55 75-00-3---------Chloroethane 48 75-69-4---------Trichlorofluoromethane 52 75-35-4---------1,1-Dichloroethene 49 67-64-1---------Acetone 43 74-88-4---------Iodomethane 52 • 75-15-0---------Carbon Disulfide 47 75-09-2---------Methylene Chloride 50 156-60-5--------trans-1,2-Dichloroethene 46 1634-04-4-------Methyl tert-butyl ether 90 75-34-3---------1,1-Dichloroethane 45 108-05-4--------Vinyl acetate 77 78-93-3---------2-Butanone 38. 156-59-2--------cis-1,2-Dichloroethene 48 590-20-7--------2,2-Dichloropropane 43 74-97-5---------Bromochloromethane 49 67-66-3---------Chloroform 47 109-99-9--------Tetrahydrofuran 47 71-55-6---------1,1,1-Trichloroethane 45 563-58-6--------1, 1-Dichloropropene 48 56-23-5---------Carbon Tetrachloride 44 ' 107-06-2--------1,2-Dichloroethene _ 46 71-43-2---------Benzene 47 79-01-6---------Trichloroethene 48 78-87-5---------1,2-Dichloropropane 46 74-95-3---------Dibromomethane 48 75-27-4---------Bromodichloromethane 46 10061-01-5------cis-1,3-Dichloropropene 46 108-10-1--------4-Methyl-2-pentanone 40 108-88-3--------Toluene 48 10061-02-6------trans-1,3-Dichloropropene 45 FORM I VOA OLM03:0 t i lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VGWLCSD Lab Name: MITKEM CORPORATION Contract: Lab- Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5095 Level: (low/med) LOW Date Received: OW Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 48 142-28-9--------1,3-Dichloropropane 47 127-18-4--------Tetrachloroethene __ 49 591-78-6--------2-Hexanone 37 124-48-1--------Dibromochloromethane 44 106-93-4--------1,2-Dibromoethane__ 48 108-90-7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetrachloroethane 45 100-41-4--------Ettylbenzene 47 ----------------m,p-Xylene 94 95-47-6---------o-Xylene 48 1330-20-7-------Xylene (Total 140 100-42-5--------Styrene 48 75-25-2---------Bromoform 43 98-82-8---------Isopropyl nzene 47 79-34-5---------1,1,2,2-Tetrachloroethane 45 108-86-1--------Bromobenzene 46 96-18-4---------1,2,3-Trichloropropane 43 103-65-1--------n-Propylbenzene 46 95-49-8---------2-Chlorotoluene 47 108-67-8----- 1,3,5-Trimethylbenzene_ 46 106-43-4--------4-Chlorotoluene 46 98-06-6---------tert-Butylbenzene 45 95-63-6---------1,2,4-Trimethylbenzene 46 135-98-8--------sec-Butylbenzene 46 99-87-6---------4-Isopropyltoluene 46 541-73-1--------1,3-Dichlorobenzene 47 106-46-7--------1,4-Dichlorobenzene 47 104-51-8--------n-Butylbenzene 46 95-50-1---------1,2-Dichlorobenzene 47 96-12-8---------1,2-Dibromo-3-chloropropane_ 39 120-82-1--------1,2,4-Trichlorobenzene 46 87-68-3---------Hexachlorobutadiene 43 91-20-3---------Naphthalene- 46 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) LATER Lab Sample ID: LCSD-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5095 Level: (low/med) LOW Date Received: o Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q i 87-61-6---------1,2,3-Trichlorobenzene 46 60-29-7---------Ether 53 108-20-3--------Diisopropyl Ether 50 637-92-3--------Ethyl tert-butyl ether 50 994-05-8--------tert-Amyl methyl ether 52 123-91-1--------1,4-Dioxane 540 i I FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6WLFB Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No..: MC1600 Matrix: (soil/water) WATER Lab Sample ID: LFB-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5096 Level: (low/med) IOW Date Received: Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (um) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: - JUL) CONC YIRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-01-4---------Vinyl Chloride 0.8 J 75-35-4---------1,1-Dichloroethene 1 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16380 i Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5134 Level: (low/med) LOW Date Received: o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 48 74-87-3---------Chloromethane 43 75-01-4---------Vinyl Chloride 45 74-83-9---------Bromomethane 58 75-00-3---------Chloroethane 47 75-69-4---------Trichlorofluoromethane 59 75-35-4---------1,1-Dichloroethene 50 67-64-1----------Acetone 46 74-88-4---------Iodomethane 55 75-15-0---------Carbon Disulfide 48 75-09-2---------Methylene Chloride 51 156-60-5--------trans-1,2-Dichloroethene 42 1634-04-4-------Methyl tert-butyl ether 79 75-34-3---------1,1-Dichloroethane_ 40 108-05-4--------Vinyl acetate 69 78-93-3---------2-Butanone 38 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropene` 38 74-97-5---------Bromochloromethane 45 67-66-3---------Chloroform 44 109-99-9--------Tetrahydrofuran _ 52 71-55-6---------1, 1,1-Trichloroethane 41 563-58-6--------1,1-Dichloropropene 44 56-23-5---------Carbon Tetrachloride 42 107-06-2--------1,2-Dichloroethane 43 71-43-2---------Benzene _ 44 79-01-6---------Trichloroethene 44 78-87-5---------1,2-Dichloropropane 43 74-95-3---------Dibromomethane 45 75-27-4---------Bromodichloromethane 41 10061-01-5------cis-1,3-Dichloropropene 40 108-10-1--------4-Methyl-2-pentanone 36 108-88-3--------Toluene 45 10061-02-6------trans-1,3-Dichloropropene 40 FORM I VOA O1,M03:0 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16380 -Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5134 Level: (low/med) LAW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 45 142-28-9--------1;3-Dichloropropane 48 127-18-4--------Tetrachloroethene 54 591-78-6--------2-Hexanone 39 124-48-1--------Dibromochloromethane 45 106-93-4--------1,2-Dibromoethane 48 108-90-7--------Chlorobenzene 50 630-20-6--------1,1,1,2-Tetrachloroethane 46 100-41-4--------Ethylbenzene 49 ----------------m,p-Xylene_ 99 95-47-6---------o-Xylene 50 1330-20-7--------Xylene (Total) 150 100-42-5--------Styrene 50 75-25-2---------Bromoform 42 98-82-8---------Isopropylbenzene 49 79-34-5---------1,1,2,2-Tetrachloroethane 49 108-86-1--------Bromobenzene 49 96-18-4---------1,2,3-Trichloropropane 46 103-65-1--------n-Propylbenzene 51 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 50 106-43-4--------4-Chlorotoluene 51 98-06-6---------tert-Butylbenzene 49 95-63-6---------1,2,4-Trimethylbenzene 51 135-98-8--------sec-Butylbenzene 51 99-87-6---------4-Isopropyltoluene 52 541-73-1--------1,3-Dichlorobenzene 52 106-46-7--------1,4-Dichlorobenzene 52 104-51-8--------n-Butylbenzene _ 52 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3-chloropropane_ 41 120-82-1--------1,2,4-Trichlorobenzene 49 87-68-3---------Hexachlorobutadiene 47 91-20-3---------Naphthalene 46 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5134 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (nun) Dilution Factor: 1.0 Soil Extract Volume:_ (uL) Soil Aliquot Volume: JUL) CONCTNTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 50 60-29-7---------Ether 51 108-20-3--------Diisopropyl Etlier 45 637-92-3--------Ethyl tert-butyl ether 44 994-05-8---=----tert-Amyl methyl ether 46 123-91-1--------1,4-Dioxane 650 } I i I FORM I VOA OLM03:0 I I lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No: : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5135 Level: (low/med) LOW Date Received: %s Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _ (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 44 74-87-3---------Chloromethane 44 75-01-4---------Vinyl Chloride _ _ 47 74-83-9---------Bromomethane 58 75-00-3---------Chloroethane _ 48 75-69-4---------Trichlorofluoromethane 58 75-35-4---------1, 1-Dichloroethene _ 51 67-64-1---------Acetone 41 74-88-4---------Iodomethane 55 75-15-0---------Carbon Disulfide 48 75-09-2---------Methylene Chloride 51 156-60-5--------trans-1,2-Dichloroethene 41 1634-04-4-------Methyl tert-butyl ether 79 75-34-3---------1,1-Dichloroethene 39 108-05-4--------Vinyl acetate 39 78-93-3---------2-Butanone 36 156-59-2--------cis-1,2-Dichloroethene 42 590-20-7--------2,2-Dichloropropane 38 74-97-5---------Bromochloromethane 45 67-66-3---------Chloroform 43 109-99-9--------Tetrahydrofuran 52 71-55-6---------1,1,1-Trichloroethane 41 563-58-6--------1,1-Dichloropropene 44 56-23-5---------Carbon Tetrachloride 40 107-06-2--------1,2-Dichloroethane 42 71-43-2---------Benzene 43 79-01-6---------Trichloroethene 43 78-87-5---------1,2-Dichloropropane 42 74-95-3---------Dibromomethane 44 75-27-4---------Bromodichloromethane 41 10061-01-5------cis-1,3-Dichloropropene 40 108-10-1--------4-Methyl-2-pentanone 36 108-.88-3--------Toluene 44 10061-02-6------trans-1,3-Dichloropropene 39 FORM I VOA OLM03.0 1 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLCSD Lab Name: MITKEM CORPORATION Contract: Lab Coder MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5135 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1,1,2-Trichloroethane 44 142-28-9--------1,3-Dichloropropane_ 46 127-18-4--------Tetrachloroethene 52 591-78-6--------2-Hexanone 37 124-48-1--------Dibromochloromethane 43 106-93-4--------1,2-Dibromoethane 47 108-90-7--------Chlorobenzene 48 630-20-6--------1,1,1,2-Tetrachloroethane 44 100-41-4--------Ethylbenzene 48 --------------m,p-Xylene 97 95-47-6---------o-Xylene _ 48 1330-20-7-------Xylene (Total) 140 100-42-5--------Styrene 49 ` 75-25-2---------Bromoform 40 98-82-8---------Isopropylbenzene 47 79-34-5---------1,1,2,2-Tetrachloroethane 50 108-86-1--------Bromobenzene 50 96-18-4---------1,2,3-Trichloropropane 46 ` 103-65-1--------n-Propylbenzene 50 95-49-8---------2-Chlorotoluene 50 108-67-8--------1,3,5-Trimethylbenzene 51 106-43-4--------4-Chlorotoluene 52 98-06-6---------tert-Butylbenzene 49 95-63-6---------1,2,4-Trimethylbenzene 50 135-98-8--------sec-Butylbenzene 51 99-87-6---------4-Isopropyltoluene 51 541-73-1--------1,3-Dichlorobenzene 52 106-46-7--------1,4-Dichlorobenzene 51 104-51-8---------n-Butylbenzene 52 95-50-1---------1,2-Dichlorobenzene 52 96-12-8---------1,2-Dibromo-3-chloropropane 42 I 120-82-1--------1,2,4-Trichlorobenzene 49 87-68-3---------Hexachlorobutadiene__ 47 ' 91-20-3---------Naphthalene- 50 i FORM I VOA OLM03:0 i 1 i 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEEP V6XLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5135 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _ UL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 49 60-29-7---------Ether 53 108-20-3--------Diisopropyl Etter 45 637-92-3--------Ethyl tert-butyl ether 44 994-05-8--------tert-Amyl methyl ether 47 123-91-1--------1,4-Dioxane 630 FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET V6XLFB Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 i Matrix: (soil/water) WATER Lab Sample ID: LFB-16380 Sample wt/vol: ' 5.000 (g/mL) ML Lab File ID: V6D5136 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: O1/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uQ CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-01-4---------Vinyl Chloride 0.8 J 75-35-4---------1,1-Dichloroethene 1 FORM I VOA OLM03:O 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3107 Level: (low/med) LOW Date Received: 12/28/04 Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.-0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 10 U 111-44-4--------bis(2-Chloroethyl) Ether 10 U 95-57-8---------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108-60-1--------2,2' -oxybis(1-Chloropropane) 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine_ 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone _ 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U, 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy)methane_ 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 19 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate _ _ 10 U 208-96-8--------Acenaphthylene 10 U 606-20-2---------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3107 Level: (low/med) LOW Date Received: 12/28/04 15 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: , 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether 10 U 86-73-7---------Fluorene 10 U 100-01-6--------4-Nitroaniline 20 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 20 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 10 U 101-55-3--------4-Bromophenyl-phenylether 10 U 118-74-1--------Hexachlorobenzene 10 U 87-86-5---------Pentachlorophenol 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene_ 10 U 129-00-0--------Pyrene 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3' -Dichlorobenzidine 10 U. 56-55-3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis (2-Ethylhexyl phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10' U 205-99-2--------Benzo(b) fluoranthene 10 U 207-08-9--------Benzo(k) fluoranthene 10 U 50-32-8---------Benzo(a)pyrene_ 10 U 193-39-5--------Indeno(1,2,3-cd)pyr ene 10 U 53-70-3---------Dibenzo(a,h)anthracene 10 U 191-24-2--------Benzo(g,h,i)perylene 10 U (1T--- Cannot be separated from Diphenylamine FORM I SV-2 0LM03:0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3108 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 10 U 111-44-4--------bis(2-Chloroethyl Ether 10 U 95-57-8---------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108-60-1--------2,2' -oxybis(1-Chloropropane 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine_ 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy)methane 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 10 U 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene 10 U 606-20-2--------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3108 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: - decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol_ 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether 10 U 86-73-7---------Fluorene_ 10 U 100-01-6--------4-Nitroaniline 20 U 534-52-1--------4,6-Dinitro-2-methylphenol 20 U 86-30-6---------N-Nitrosodiphenylamine .(1)_ 10 U 101-55-3--------4-Bromophenyl-phenylether 10 U 118-74-1--------Hexachlorobenzene _ 10 U 87-86-5---------Pentachlorophenol_ 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole _ 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene 10 U 129-00-0--------Pyrene_ _ 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3' -Dichlorobenzidine___ 10 U 56-55-3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis(2-Ethylhexyl)phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b) fluoranthene T 10 U 1 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene 10 U 193-39-5--------Indeno(1,2,3-cd)pyrene 10 U 53-70-3---------Dibenzo(a,h)anthracene 10 U 191-24-2--------Benzo(g,h,i)perylene 10 U i (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 z i 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3109 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor. 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 38 111-44-4--------bis(2-Chloroethyl)Ether 42 95-57-8---------2-Chlorophenol 34 541-73-1--------1,3-Dichlorobenzene 35 106-46-7--------1,4-Dichlorobenzene 36 95-50-1---------1,2-Dichlorobenzene 37 95-48-7---------2-Methylphenol 45 108-60-1--------2,2' -oxybis(1-Chloropropane) 44 106-44-5--------4-Methylphenol 48 621-64-7--------N-Nitroso-di-n-propylamine 50 67-72-1---------Hexachloroethane 35 98-95-3---------Nitrobenzene 45 78-59-1---------Isophorone 47 88-75-5---------2-Nitrophenol 43 105-67-9--------2,4-Dimethylphenol 63 120-83-2--------2,4-Dichlorophenol 44 120-82-1--------1,2,4-Trichlorobenzene 41 91-20-3---------Naphthalene 43 106-47-8--------4-Chloroaniline 48 111-91-1--------bis(2-Chloroethoxy methane_ 46 87-68-3---------Hexachlorobutadiene 39 59-50-7---------4-Chloro-3-Methylphenol 48 91-57-6---------2-Methylnaphthalene 45 77-47-4---------Hexachlorocyclopentadi ne y 56 88-06-2---------2,4,6-Trichlorophenol 50 95-95-4---------2,4,5-Trichlorophenol 48' 91-58-7---------2-Chloronaphthalene 48 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate 48 208-96-8--------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 50 99-09-2---------3-Nitroaniline 44 83-32-9---------Acenaphthene 48 FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3109 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05. Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 50 100-02-7--------4-Nitrophenol 49 132-64-9--------Dibenzofuran 47 121-14-2--------2,4-Dinitrotoluene 48 84-66-2---------Diethylphthalate 49 7005-72-3-------4-Chlorophenyl-phenylether 48 86-73-7---------Fluorene 49 100-01-6--------4-Nitroaniline 44 534-52-1--------4, 6-Dinitro-2-methylphenol 50 86-30-6---------N-Nitrosodiphenylamine (1)__ 60 101-55-3--------4-Bromophenyl-phenylether 49 118-74-1--------Hexachlorobenzene 50 87-86-5---------Pentachlorophenol 61 85-01-8---------Phenanthrene 49 120-12-7--------Anthracene 50 86-74-8---------Carbazole 54 84-74-2---------Di-n-butylphthalate 50 206-44-0--------Fluoranthene 50 129-00-0--------Pyrene 48 85-68-7----------Butylbenzylphthalate 48 91-94-.1---------3,3 ' -Dichlorobenzidine 1 J 56-55-3---------Benzo(a)anthracene 52 218-01-9--------Chrysene 51 117-81-7--------bis(2-Ethylhexyl)phthalate 48 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b)fluoranthene 43 207-08-9--------Benzo(k) fluoranthene 54 50-32-8---------Benzo(a)pyrene 48 193-39-5--------Indeno(1,2,3-cd)pyrene 46 53-70-3---------Dibenzo(a,h)anthracene 46 191-24-2--------Benzo(g,h,i)perylene 47 (1) - Cannot be separated from Diphenylamine FORM I SV-2 01-M03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: (low/med) LOW Date Received: 12/29/04 o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 36 111-44-4--------bis(2-Chloroethyl)Ether 44 95-57-8---------2-Chlorophenol 31 541-73-1--------1,3-Dichlorobenzene 38 106-46-7--------1,4-Dichlorobenzene 39 95-50-1---------1,2-Dichlorobenzene 40 95-48-7---------2-Methylphenol 44 108-60-1--------2,2'-oxybis(1-Chloropropane) 45 106-44-5--------4-Methylphenol 47 621-64-7--------N-Nitroso-di-n-propylamine 49 67-72-1---------Hexachloroethane 38 98-95-3---------Nitrobenzene 46 78-59-1---------Isophorone 47 88-75-5---------2-Nitrophenol 39 105-67-9--------2,4-Dimethylphenol 63 120-83-2--------2,4-Dithlorophenol 39 120-82-1--------1,2,4-Trichlorobenzene 41 91-20-3---------Naphthalene 44 106-47-8--------4-Chloroaniline 48 111-91-1--------bis(2-Chloroethoxy)methane 47 87-68-3---------Hexachlorobutadiene 39 59-50-7---------4-Chloro-3-Methylphenol 47 91-57-6---------2-Methylnaphthalene 44 77-47-4---------Hexachlorocyclopentadiene 54 88-06-2---------2,4,6-Trichlorophenol 46 95-95-4---------2,4,5-Trichlorophenol 47 91-58-7---------2-Chloronaphthalene 48 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate 48 208-96-8--------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 50 99-09-2---------3-Nitroaniline 41 83-32-9---------Acenaphthene 48 FORM I SV-1 OLM03.0 1C EPA SAMPLE No. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: (low/med) LOW Date Received: 12/25/04 °s Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 -- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 48 100-02-7--------4-Nitrophenol 45 132-64-9--------Dibenzofuran 48 121-14-2--------2,4-Dinitrotoluene 49 84-66-2---------Diethylphthalate 50 7005-72-3-------4-Chlorophenyl-phenylether 47 86-73-7---------Fluorene 50 100-01-6--------4-Nitroaniline 44 534-52-1--------4,6-Dinitro-2-methylphenol_ 48 86-30-6---------N-Nitrosodiphenylamine (1) 59 101-55-3--------4-Bromophenyl-phenylether 49 118-74-1--------Hexachlorobenzene 50 87-86-5-----=---Pentachlorophenol 59 85-01-8---------Phenanthrene 49 120-12-7--------Anthracene 51 86-74-8---------Carbazole 54 84-74-2---------Di-n-butylphthalate 50 206-44-0--------Fluoranthene 49 129-00-0--------Pyrene _ 50 85-68-7---------Butylbenzylphthalate 49 91-94-1---------3,3 ' -Dichlorobenzidine 2 J 56-55-3---------Benzo(a)anthracene 48 218=01-9--------Chrysene 52 117-81-7--------bis(2-Ethylhexyl)phthalate_ 48 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b) fluoranthene 44 207-08-9--------Benzo(k) fluoranthene 49 50-32-8---------Benzo(a)pyrrene 46 193-39-5--------Indeno(1,2,3-cd)pyrene 46 53-70-3---------Dibenzo(a,h)anthracene 46 191-24-2--------Benzo(g,h,i)perylene 47 (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 10 U 111-44-4--------bis(2-Chloroethyl) Ether 10 U 95-57-8---------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1----------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108-60-1--------2,2'-oxybis(1-Chloropropane) 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine_ 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy)methane_ 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7---------4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 10 U 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene 10 U 606-20-2--------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline_ 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET — MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 _- GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether_ 10 U 86-73-7---------Fluorene_ 10 U 100-01-6--------4-Nitroaniline 20 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 20 U 86-30-6---------N-Nitrosodiphenylamine (1) 10 U 101-55-3--------4-Bromophenyl-phenyletHer 10 U 118-74-1--------Hexachlorobenzene 10 U i 87-86-5---------Pentachlorophenol 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole 10 U 84-74-2---------Di-n-butylphthalate 10 U 206-44-0--------Fluoranthene 10 U 129-00-0--------Pyrene 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3' -Dichlorobenzidine 10 U 56-55-3---------Benzo(a)anthracene 10 U 218-01-9--------Chrysene 10 U 117-81-7--------bis(2-Ethylhexyl�phthalate 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b)fluoranthene _ 10 U 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene 10 U 193-39-5--------Indeno(1,2,3-cd)pyrene 10 U 53-70-3---------Dibenzo(a,h)anthracene _ 10 U 191-24-2--------Benzo(g,h,i)perylene— - 10 U (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 1B EPA. SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET S2QLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3100 Level: (low/med) LOW Date Received: Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 --_ GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol 41 111-44-4--------bis(2-Chloroethyl)Ether 43 95-57-8---------2-Chlorophenol 37 541=73-1--------1,3-Dichlorobenzene 37 106-46-7--------1,4-Dichlorobenzene 37 95-50-1---------1,2-Dichlorobenzene 39 95-48-7---------2-Methylphenol 44 108-60-1--------2,2- -oxybis (1-Chloropropane) 45 106-44-5--------4-Methylphenol 46 621-64-7--------N-Nitroso-di-n-propylamine_ 49 67-72-1---------Hexachloroethane 36 98-95-3---------Nitrobenzene 45 78-59-1---------Isophorone 47 88-75-5---------2-Nitropheno 44 105-67-9--------2,4-Dimethylp enol 54 120-83-2--------2,4-Dichlorophenol 43 120-82-1--------1,2,4-Trichlorobenzene 40 91-20-3---------Naphthalene 43 106-47-8--------4-Chloroaniline 57 111-91-1--------bis(2-Chloroethoxy methane_ 47 87-68-3-------.--Hexachlorobutadiene 38 59-50-7---------4-Chloro-3-Methylphenol 46 91-57-6---------2-Methylnaphthalene 43 77-47-4---------Hexachlorocyclopentadiene 58 88-06-2---------2,4,6-Trichlorophenol 46 95-95-4---------2,4,5-Trichlorophenol 44 91-58-7---------2-Chloronaphthalene 47 88-74-4---------2-Nitroaniline 48 131-11-3--------Dimethylphthalate 49 208-96-8--------Acenaphthylene 49 606-20-2--------2,6-Dinitrotoluene 49 99-09-2---------3-Nitroanilin_e 49 83=32=9---------Acenaphthene 48 FORM I SV-1 OLM03.0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I S2QLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEMM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3100 Level: (low/med) LOW Date Received: Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL). Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: ' CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol 29 100-02-7----- 4-Nitrophenol 37 132-64-9--------Dibenzofuran 48 ? 121-14-2--------2,4-Dinitrotoluene 51 84-66-2---------Diethylphthalate 49 7005-72-3-------4-Chlorophenyl-phenylether 48 86-73-7---------Fluorene 48 100-01-6--------4-Nitroaniline 47 534-52-1--------4,6-Dinitro-2-methylphenol 41 86-30-6---------N-Nitrosodiphenylamine (1)_ 60 101-55-3--------4-Bromophenyl-phenylether 48 118-74-1--------Hexachlorobenzene 49 ! 87-86-5---------Pentachlorophenol 33 85-01-8---------Phenanthrene 47 120-12-7--------Anthracene 51 86-74-8---------Carbazole 49 84-74-2---------Di-n-butylphthalate 49 206-44-0--------Fluoranthene 49 129-00-0--------Pyrene 50 85-68-7---------Butylbenzylphthalate 51 91-94-1---------3,3 ' -Dichlorobenzidine 55 56-55-3---------Benzo(a)anthracene 49 218-01-9--------Chrysene 54 117-81-7--------bis(2-Ethylhexyl)phthalate 50 117-84-0--------Di-n-octylphthalate 46 205-99-2--------Benzo(b) fluoranthene 45 207-08-9--------Benzo(k) fluoranthene 48 50-32-8---------Benzo(a)pyrene 47 193-39-5--------Indeno(1,2,3-cd)pyrene 47 53-70-3---------Dibenzo(a,h)anthracene 47 191-24-2--------Benzo(g,h,i)perylene 49 (1) - Cannot be separated from Diphenylamine FORM I SV-2 OLM03:0 DATA PACKAGE ADDENDUM SEMIVOLATILE ORGANICS C 1600 Data Summary Forms, followed by Full Data Package Pages. 1B EPA SAMPLE NO. SEMIVOLATILE' ORGANICS ANALYSIS DATA SHEET MW-5 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-01D Sample wt/vol: 1000 .(g/mL) ML Lab File ID: S2E3107 Level: (low/med) LOW Date Received: 12/28/04 Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U 1 I FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No..: MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3108 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No: : SDG No. : MC1600 i Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMS Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3109 j Level: (low/med) LOW Date Received: 12/29/04 o Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 59 103-33-3--------Azobenzene 48 98-86-2---------Acetophenone 10 U i 1 FORM I SV-1 OLM03:0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-6MSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02DMSD Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3110 Level: (low/med) LOW Date Received: 12/29/04 Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/06/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 60 103-33-3--------Azobenzene 49 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03.0 j 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET MW-X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 i Matrix: (soil/water) WATER Lab Sample ID: C1600-03D Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3111 Level: (low/med) LOW Date Received: 12/29/04 wk Moisture: _ decanted: (YIN) Date Extracted:01/03/05 i Concentrated Extract Volume: 1000 (UL) Date Analyzed: 01/06/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCED]TRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U 1 i S i 1 f S 1 i i FORM I SV-1 OLM03.0 . 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEEP S2QLCS Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3100 Level: (low/med) IOW Date Received: Moisture: decanted: (YIN) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0 (uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline _ 64 103-33-3--------Azobenzene 47 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 i Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Aniline 50 0.0 59 118 40-140 Azobenzene 50 0.0 48 96 40-140 s SPIKE MSD MSD ADDED CONCENTRATION o a QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ --------- ------ ------ ------ ------ Aniline 50 60 120 2 — 40-140 Azobenzene 50 49 98 2 g.p4-&-- 40-140 f i # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out of 4 outside limits COMMENTS: I FORM III SV-1 OLM03.0 FORM 3 WATER SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION a LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. Aniline 50 64 128 40-140 Azobenzene 50 47 94 40-140 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits C01MENTS: FORM III SV 4B. EPA SAMPLE NO. SEMIVOLATILE METHOD BLANK SLM4ARY SBLK2Q Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID: S2E3101 Lab Sample ID: MB-16345 Instrument ID: S2 Date Extracted: 01/03/05 Matrix: (soil/water) WATER Date Analyzed: 01/05/05 Level: (low/med) LOW Time Analyzed: 1954 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED ------------ -------------- -------------- ---------- 01 S2QLCS LCS-16345 S2E3100 01/05/05 02 MW-5 C1600-01D S2E3107 01/05/05 03 MW-6 C1600-02D S2E3108 01/05/05 04 MW-6MS C1600-02DMS S2E3109 01/05/05 05 MW-6MSD C1600-02DMSD S2E3110 01/06/05 06 MW-X C1600-03D S2E3111 01/06/05 07 08 09 10 11 — - 12 13 _ 14 15 16 17 18 19 20 21 22 23 24 25 26 —— 27 28 29 30 C014ME TS: page 1 of 1 l FORM IV SV OLM03.0 i 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SBLK2Q Lab Name: MITKEM CORPORATION Contract: Lab Code: 'MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3101 Level: (low/med) LOW Date Received: Moisture: _ decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: 01/05/05 Injection. Volume: 1.0(uL) Dilution Factor: 1. 0 GPC Cleanup: (YIN) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 62-53-3---------Aniline 10 U 103-33-3--------Azobenzene 10 U 98-86-2---------Acetophenone 10 U FORM I SV-1 OLM03.0 FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET MW-6 Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: C1600-02D Sample wt/vol: 1000 (g/ml) ML Lab File ID: E2E3242F Moisture: decanted: (YIN) Date Received: 12/29/04 Extraction: (SepF/Copt/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 --. GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L .or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 0.20 U 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor-1248 _ 0.20 U 11097-69-1------Aroclor-1254 _ 0.20 U 11096-82-5------Aroclor-1260 _ 0.20 U i i i i I FORM I PCB FORK[ 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET P2PLCS Lab Name: MITKIEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: LCS-16376 Sample wt/vol: 1000 (g/ml) ML Lab File ID: E2E3240F Moisture: decanted: (YIN) Date Received: Extraction: (SepF/font/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 - GPC Cleanup: (YIN) N pH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 1.9 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6--- Aroclor-1248 _ 0.20 U 11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 2.0 FORM I PCB FORM 1 CLIENT SAMPLE NO. PCB ORGANICS ANALYSIS DATA SHEET P2PLCSD Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: LCSD-16376 Sample wt/vol: 1000 fg/ml) ML Lab File ID: E2E3241F a Moisture: decanted: (YIN) Date Received: Extraction: (SepF/font/Sonc) SEPF Date Extracted:01/05/05 Concentrated Extract Volume.. 2000 (uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (YIN) N pH: Sulfur Cleanup: (YIN) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 2.0 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor-1242 0.20 U 12672-29-6------Aroclor-1248 0.20 U '11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 2.0 FORM I PCB U-S- EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DNPA SHEOF -- { I Lab Name: Mitkem Corporation Contract: 28367-005 Mw-5 Lab Code: MITkEM Case No- SAS No-: SDG No. : MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600-01 Level (low/med) : MED Date Received: 12/28/04 $ Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7440-36-0 Antimony 20 U P 7440-38-2 Arsenic__ 20 U P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium 5.6 U P 7440-47-3 Chromium 25.6 P 7439-92-1 Lead 10 ul P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7440-28-D Thallium 20 U P 7440-62-2 Vanadium 50 U P 7440-66-6 Zinc 50 U P 7439-97-6 Mercury 0.28 U Cv Cyanide Q U N CA Comments: FORM I - IN SW846 {��y{yr 0085P I I i 1 U_S_ EPA - CLP f 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET I MWI-b Lab Name: Mitkem Corporation Contract: 28367-005 i - Lab Code: MITKEM Case No. SAS No. : SDG No- : MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600=02 Level (low/med) : MED Date Received: 12/29/04 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L I CAS No. Analyte Concentration C Q M 7440-36-0 Antimony 20 U P 7440-38-2 Arsenic 20 U. _P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium 5.0 U P 7440-47-3 Chromium 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7440-28-0 Thallium 20 U P 7440-62-2 Vanadium 50 U P 7440-66-6 Zinc _ _50 U P_ 7439_-_97-6 Mercury 0.31 U Cv Cyanide U N CA Comments: FORM I - IN SW846 0086 1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET -- - Lab Name: Mitkem Corporation Contract 28367-005 i�1W-X Lab Codes MITREM Case No. SAS No. : SDG No- : MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600-03 Level (low/med) : MED Date Received: 12/29/04 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7440-36-0 timony 20 U p 7440-38-2 Arsenic 20 U p 7440-39-3 Barium 200 U _ P 7440-41-7 Beryllium _ 5.0 U p 7440-43-9 cadmium 5.0 U P 7440-47-3 Chromium 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U p 7440-22-4 Silver 30 .u..- p. 7440-28-0 Thallium _ 20 U p 7440-62-2 vanadium 50 U P 7440-66-6 Zinc 50 U_ P 7439-97-6 Mercury_ 0.29 U CV Cyanide - �Q 0 U N CA Comments: FORM I - IN SW846 0VO l i U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Mw-3 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No_ SAS No_: SDG No_ : MC1600 Matrix (soil/water) : WATER Lab Sample ID: C1600-04 Level (low/med) : MED Date Received: 12/29/64 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No_ Analyte Concentration J16T M 7440-36-0 timony 20 P 7440-38-2 Arsenic 20 U P 7440-39-3 Barium _ 200 U P 7440-41-7 jBeryllium 5.0 U P 7440-43-_9 ICadmium 5.0 U P 7440-47-3 Chromium _ 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7440-28-0 Thallium 20 U P 7440-62'-2 Vanadium 50 U P 7440-66-6 Zinc _ 50 U P 7439-97-6 Mercury 0.30 U_ CV i Cyanide U N- CA Comments: FORM I - IN SW846 0088 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Mw-2 Lab Name: Mitkem Corporation Contract: 28367-005 Lab Code: MITKEM Case No. SAS No.: SDG No. : MC1600 Matrix (soil/water) : WATER Lab Sample ID_ . C1600-05 Level (low/med) : MED Date Received: 12/29/04 $ Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7440-36-0 Antimony 20 U P 7440-38-2 Arsenic 20 U P 7440-39-3 Barium 200 U P 7440-41-7 Beryllium 5.0 U P 7440-43-9 Cadmium _ 5.0 U P 7440-47-3 Chromium 20 U P 7439-92-1 Lead 10 U P 7440-02-0 Nickel 50 U P 7782-49-2 Selenium 30 U P 7440-22-4 Silver 30 U P 7440-28-0 Thallium 20 U _ P 7440-62-2 Vanadium _ 50 U P 7440-66-6 Zinc _ SO U P 7439-974 Mercury 0.30 U Cv Cyanide rp U N— CA 10104 Comments: FORM I - IN SW846 0 0 8 91'� 1 U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE i Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Solid LCS Source: Aqueous LCS Source: LCS-16324 Aqueous (ug/L) Solid (mg/kg) Analyte True Found %R True Found C Limits %R Mercury 4.6 4.91 106.7 I i I FORM VII - IN SW846 i U.S_ EPA - CLP 7 LABORATORY CONTROL SAMPLE Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No_ : SDG No MC1600 Solid LCS Source: Aqueous LCS Source: LCS-16327 I Aqueous (ug/L) Solid (mg/kg) Analyte True Found %R True Found C Limits %R Antimony 455.0 463.48 101.9 Arsenic 455.0 468.29 102.9 Barium 9100.0 9385.42 103.1 Beryllium 227.0 237.12 104.5 Cadmium 227.0 236.77 104.3 Chromium 910.0 929.59 102.2 Lead 455.0 472 .16 103.8 Nickel 2270.0 2364.12 104.1 Selenium 455.0 463.94 102.0 Silver 1130.0 1206.18 106.7 Thallium 455.0 453.31 99.6 Vanadium 2270.0 2327.93 102.6 Zinc 2270.0 2380.19 104.9 FORM VII - IN SW846 U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Solid LCS Source: Aqueous LCS Source: LCS-16385 Aqueous (ug/L) Solid (mg/kg) Analyte True Found %R True Found C Limits %R Cyanide 100.0 77.28 77.3 t , I i i I FORM VII - IN SW846 I - 2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO. # (DCE)# (TOL)# (BFB)## OUT ------------ ------ ------ ------ ------ --- ------------ ------ ------ ------ ------ --- 01 VBLK6W 101 100 102 96 0 02 V6WLCS 96 97 96 96 0 03 V6WLCSD 97 100 95 95 0 04 V6WLFB 101 103 102 97 0 05 MW-5 99 97 98 94 0 - 06 MW-6 98 9.7 97 95 0 07 MW-X 101 98 97 94 0 08 MW-3 97 98 96 96 0 09 MW-2 94 96 92 91 0 10 VBLK6X 101 102 ill 101 0 11 V6XLCS 97 98 106 104 0 12 V6XLCSD 95 96 102 100 0 13 V6XLFB 98 99 106 97 0 14 MW-2DL 97 100 102 100 0 15 MW-6MS 97 100 105 103 0 16 MW-6MSD 96 102 105 102 0 17 MW-3DL 95 98 107 99 0 18 _ 19 20 21 22 23 24 25 26 27 28 29 301 QC LIMITS SMC1 = Dibromofluoromethane (78-117) SMC2 (DCE) = 1,2-Dichloroethane-d4 (62-124) SMC3 (TOL) = Toluene-d8 (81-116) OTHERR(BFB) = Bromofluorobenzene (74-126) # Column to be used to flag recovery values * Values outside of contract required QC limits page 1 of 1 FORM II VOA-1 OLM03.0 2C WATER SEMIVOLATILE SURROGATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 i EPA S1 S2 S3 S4 S5 S6 S7 S8 TOT SAMPLE NO. (NBZ)# (FBP)# (TPH)## (PHL)# (2FP)# (TBP)# # # OUT ------------ ------ ------ ------ ---- 01 S2QLCS 90 94 102 73 46 96 0 02 SBLK2Q 86 90 96 74 49 81 0 03 MW-5 90 96 94 77 47 114 0 04 MW-6 91 94 97 59 24 99 0 05 MW-6MS 91 96 100 71 36 112 --0 06 MW-6MSD 93 96 98 66 33 105 0 07 MW-X 97 100 103 88 84 116 0 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 QC LIMITS S1 (NBZ) = Nitrobenzene7d5 (48-106) S2 (FBP) = 2-Fluorobiphenyl (38-120) S3 (TPH) = Terphenyl-d14 ( 0-147) S4 (PHL) =Phenol-d5 ( 0-120) S5 (2FP) = 2-Fluorophenol ( 1-103) S6 (TBP) = 2,4,6-Tribromophenol (37-122) # Column to be used to flag recovery values * Values .outside of contract required QC limits D Surrogate diluted out page 1 of 1 FORM II SV-1 OLM03.0 i i FORM 2 WATER PCB SURROGATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 GC Column(1) : RTXCLPPEST ID: 0.53 (mm) GC Column(2) : RTXCLPPEST 2 ID: 0.53 (mm) CLIENT TCX 1 TCX 2 DCB 1 DCB 2 OTHER OTHER TOT SAMPLE NO. %REC # .REC # .REC # .REC # (1) (2) OUT ------------ ------ ------ ------ ------ ------ ------ --- 01 PBLK2P 80 84 102 99 0 02 P2PLCS 89 88 108 106 _ 0 03 P2PLCSD 90 89 97 102 0 04 MW-6 81 104 100 102 0 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 ADVISORY QC LIMITS S1 (TCX) = Tetrachloro-m-xylene (29-158) S2 (DCB) = Decachlorobiphenyl (30-164) # Column to be used to flag recovery values * Values outside of QC limits D Surrogate diluted out page 1 of 1 FORM II PCB FORM 3 WATER VOLATILE MATR.IX. SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MIIMN CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ --------- ------------- ------------- ------ ------ ------------------------ --------- ------------- ------------- ------ ------ Dichlorodifluoromethane 50 0.0 48 96 48-135 Chloromethane 50 0.0 49 98 60-118 Vinyl Chloride 50 0.0 48 96 65-113 Bromomethane 50 0.0 55 110 73=122 Chloroethane 50 0.0 46 92 72-118 Trichlorofluoromethane 50 0.0 58 116 68-129 1,1-Dichloroethene 50 0.0 50 100 67-121 ! Acetone 50 0.0 30 60 38-161 Iodomethane 50 0.0 55 110 72-130 Carbon Disulfide 50 0.0 43 86 53-137 Methylene Chloride 50 0.0 51 102 59-132 trans-1,2-Dichloroethen 50 0.0 40 80 71-124 Methyl tert-butyl ether 100 0.0 78 78 75-123 1,1-Dichloroethane 50 0.0 39 78* 83-116 Vinyl acetate 50 0.0 66 132 44-160 2-Butanone 50 0.0 33 66 64-139 cis-1, 2-Dichloroethene 50 0.0 42 84 83-120 2,2-Dichloropropane 50 0.0 31 74 70-129 Bromochloromethane 50 0.0 44 88 85-124 t Chloroform 50 0.0 42 84* 89-118 Tetrahydrofuran 50 0.0 54 108 76-126 1,1,1-Trichloroethane 50 0.0 40 80* 81-122 1,1-Dichloropropene 50 0.0 43 86 76-122 Carbon Tetrachloride 50 0.0 39 78* 79-125 1,2-Dichloroethane 50 0.0 42 84 83-123 Benzene 50 0.0 43 86 81-120 Trichloroethene 50 0.0 43 86 77-121 1,2-Dichloropropane 50 0.0 42 84 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COM1A=S: ! page 1 of 6 FORM III VOA i FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKE4 Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 -- SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ----------------- -- - Dibromomethane 50 0.0 45 90 86-124 Bromodichloromethane 50 0.0 39 78* 90-114 cis-1,3-Dichloropropene 50 0.0 38 76* 78-119 4-Methyl-2-pentanone 50 0.0 37 74 57-138 Toluene 50 0.0 44 88 817121 trans-1,3-Dichloroprope 50 0.0 37 74* 85-118 1,1,2-Trichloroethane 50 0.0 45 90 44-159 1,3-Dichloropropane 50 0.0 46 92 79-125 Tetrachloroethene 50 0.0 51 102 73-121 2-Hexanone 50 0.0 35 70 53-145 Dibromochloromethane 50 0.0 40 80 80-124 1,2-Dibromoethane 50 0.0 48 96 80-124 Chlorobenzene 50 0.0 49 98 82-118 1,1,1,2-Tetrachloroetha 50 0.0 44 88 84-121 Ethylbenzene 50 0.0 47 94 80-122 Xylene (Total) 150 0.0 140 93 81-121 Styrene 50 0.0 31 62* 77-128 Bromoform 50 0.0 35 70* 77-130 Isopropylbenzene 50 0.0 46 92 58-148 1,1,2,2=Tetrachloroetha 50 0.0 52 104 76-125 Bromobenzene 50 0.0 50 100 76-124 1,2,3-Trichloropropane 50 0.0 44 88 57-140 n-Propylbenzene 50 0.0 50 100 72-119 2-Chlorotoluene 50 0.0 50 100 75-120 1,3,5-Trimethylbenzene 50 0•.0 44 88 76-116 4-Chlorotoluene 50 0.0 51 102 78-116 tert-Butylbenzene 50 0.0 50 100 71-115 1,2,4-Trimethylbenzene 50 0.0 44 88 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COWENTS: page 2 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION a LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # ..REC. sec-Butylbenzene 50 0.0 50 100 67-117 4-Isopropyltoluene 50 0.0 50 100 68-118 1,3-Dichlorobenzene 50 0.0 51 102 80-116 1,4-Dichlorobenzene 50 0.0 52 104 80-114 n-Butylbenzene 50 0.0 52 104 58-121 1,2-Dichlorobenzene 50 0.0 52 104 81-116 1,2-Dibromo-3-chloropro 50 0.0 45 90 71-126 1,2,4-Trichlorobenzene 50 . 0.0 50 100 67-114 Hexachlorobutadiene 50 0.0 47 94 50-111. Naphthalene 50 0.0 52 104 58-133 1,2,3-Trichlorobenzene 50 0.0 50 100 64-118 Ether 50 0.0 49 98 70-130 Diisopropyl Ether 50 0.0 44 88 70-13b Ethyl tert-butyl ether 50 0.0 42 84 70.-130 tert-Amyl methyl ether 50 0.0 46 92 70-130 1,4-Dioxane 1000 0.0 630 63* 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD f MSD ADDED CONCENTRATION % % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dichlorodifluoromethane 50 45 90 6 40 48-135 Chloromethane 50 48 96 2 40 60-118 Vinyl Chloride 50 45 90 6 40 65-113 Bromomethane 50 52 104 6 40 73--1-22 Chloroethane 50 46 92 0 40 72-118 Trichlorofluoromethane 50 56 112 4 40 68-129 1,1-Dichloroethene 50 49 98 2 40 67-121 Acetone 50 33 66 10 40 38-161 Iodomethane 50 53 106 4 40 72-130 Carbon Disulfide 50 53 106 21 40 53-137 Methylene Chloride 50 50 100 2 40 59-132 trans-1,2-Dichloroethen 50 40 80 0 40 71-124 Methyl tert-butyl ether 100 81 81 4 40 75-123 1,1-Dichloroethane 50 38 76* 2 40 83-116 Vinyl acetate 50 41 82 47* 40 44-160 2-Butanone 50 35 70 6 40 64-139 cis-1,2-Dichloroethene 50 42 84 0 40 83-120 2,2-Dichloropropane 50 35 70 6 40 70-129 Bromochloromethane 50 44 88 0 40 85-124 Chloroform 50 42 84* 0 40 89-118 Tetrahydrofuran 50 59 118 9 40 76-126 1,1,1-Trichloroethane 50 39 78* 2 40 81-122 1,1-Dichloropropene 50 42 84 2 40 76-122 Carbon Tetrachloride 50 37 74* 5 40 79-125 1,2-Dichloroethane 50 42 84 0 40 83-123 Benzene 50 43 86 0 40 81-120 Trichloroethene 50 43 86 0 40 77-121 1,2-Dichloropropane 50 42 84 0 40 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION o % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dibromomethane 50 45 90 0 40 86-124 Bromodichloromethane 50 38 76* 2 40 90-114 cis-1,3-Dichloropropene 50 38 76* 0 40 78-119 4-Methyl-2-pentanone 50 39 78 5 40 57-138 Toluene 50 43 86 2 40 81-121 trans-1,3-Dichloroprope 50 37 74* 0 40 85-118 1,1,2-Trichloroethane 50 46 92 2 40 44-159 1,3-Dichloropropane 50 48. 96 4 40 79-125 Tetrachloroethene 50 50 100 2 40 73-121 2-Hexanone 50 40 80 13 40 53-145 Dibromochloromethane 50 40 80 0 40 80-124 1,2-Dibromoethane 50 50 100 4 40 80-124 Chlorobenzene 50 49 98 0 40 82-118 1,1,1,2-Tetrachloroetha 50 44 88 0 40 84-121 Ethylbenzene 50 46 92 2 40 80-122 Xylene (Total) 150 140 93 0 40 81-121 Styrene 50 30 60* 3 40 77-128 Bromoform 50 36 72* 3 40 77-130 Isopropylbenzene 50 46 92 0 40 58-148 1,1,2,2-Tetrachloroetha . 50 54 108 4 40 76-125 Bromobenzene 50 50 100 0 40 76-124 1,2,3-Trichloropropane 50 42 84 5 40 57-140 n-Propylbenzene 50 48 96 4 40 72-119 2-Chlorotoluene 50 50 100 0 40 75-120 1,3,5-Trimethylbenzene 50 43 86 2 40 76-116 4-Chlorotoluene 50 51. 102 0 40 78-116 tert-Butylbenzene 50 48 96 4 40 71-115 1,2,4-Trimethylbenzene 50 43 86 2 40 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COH ENTS: page 5 of 6 FORM III VOA FORM 3 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITC94 Case No. : SAS No. : SDG No_ : MC1600 Matrix Spike - Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION °s o QC LIMITS-- COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. sec-Butylbenzene 50 49 98 2 40 67-117 4-Isopropyltoluene 50 48 96 4 40 68-118 1,3-Dichlorobenzene 50 51 102 0 .40 80-116 1,4-Dichlorobenzene 50 52 104 0 40 80-114 n-Butylbenzene 50 49 98 6 40 58-121 1,2-Dichlorobenzene 50 52 104 0 40 81-116 1,2-Dibromo-3-..chloropro 50 47 94 4 40 71-126 1,2,4-Trichlorobenzene 50 50 100 0 40 67-114 Hexachlorobutadiene 50 45 90 4 40 50-111 Naphthalene 50 55 110 6 40 58-133 1,2,3-Trichlorobenzene 50 50 100 0 40 64-118 Ether 50 54 108 10 40 70-130 Diisopropyl Ether 50 44 88 0 40 70-130 Ethyl tert-butyl ether 50 44 88 5 40 70-130 tert-Amyl methyl ether 50 47 94 2 40 70-130 1,4-Dioxane 1000 830 83 27 40 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 72 outside limits Spike Recovery: 19 out of 144 outside limits C )MMENTS: page 6 of 6 FORM III VOA t FORM 3 WATER VOLATILE LAB CONTROL SAMPLE i Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS —� SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. j Dichlorodifluoromethane 50 43 .86 48-135 Chloromethane 50 44. 88 60-118 Vinyl Chloride 50 45 90 65-113 Bromomethane 50 54 108 73-122 Chloroethane 50 - 47 94 72-118 Trichlorofluoromethane 50 51 102 68-129 1,1-Dichloroethene 50 47 94 67-121 Acetone 50 44 88 38-161 Iodomethane 50 51 102 72-130 Carbon Disulfide 50 46 92 53-137 Methylene Chloride 50 49 98 59-132 trans-1,2-Dichloroethen 50 45 90 71-124 Methyl tert-butyl ether 100 86 86 75-123 1,1-Dichloroethene 50 44 88 83-116 Vinyl acetate 50 45 90 44-160 2-Butanone 50 38 76 64-139 cis-1,2-Dichloroethene 50 46 92 83-120 2,2-Dichloropropane 50 44 88 70-129 Bromochloromethane 50 48 96 85-124 Chloroform 50 47 94 89-118 Tetrahydrofuran 50 48 96 76-126 1,1,1-Trichloroethane 50 45 90 81-122 1, 1-Dichloropropene 50 48 96 76-122 Carbon Tetrachloride 50 45 90 79-125 1,2-Dichloroethane 50 45 90 83-123 Benzene 50 47 94 81-120 j Trichloroethene 50 48 96 77-121 1,2-Dichloropropane 50 46 92 81-116 Column to be used to flag recovery and RPD values with an asterisk i * Values outside of QC limits COD24EN 'S: i i page 1 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. -- --------- ------------- ------------- ------ ------ Dibromomethane 50 47 94 86-124 Bromodichloromethane 50 45 90 90-114 cis-1,3-Dichloropropene 50 45 90 78-119 4-Methyl-2-pentanone 50 38 76 57-138 Toluene 50 48 96 81-121 trans-1,3-Dichloroprope 50 44 88 85-118 1,1,2-Trichloroethane 50 47 94 44-159 1,3-Dichloropropane 50. 46 92 79-125 Tetrachloroethene 50 48 96 73-121 2-Hexanone 50 37 74 53-145 Dibromochloromethane 50 45 90 80-124 1,2-Dibromoethane 50 47 94 80-124 Chlorobenzene 50 48 96 82-118 1,1,1,2-Tetrachloroetha 50 46 92 84-121 Ethylbenzene 50 48 96 80-122 Xylene (Total) 150 140 93 81-121 Styrene 50 49 98 77-128 Bromoform 50 43 86 77-130 Isopropylbenzene 50 47 94 58-148 1,1,2,2-Tetrachloroetha 50 44 88 76-125 Bromobenzene 50 46 92 76-124 1,2,3-Trichloropropane 50 43 86 57-140 n-Propylbenzene 50 47 94 72-119 2-Chlorotoluene 50 47 94 75-120 1,3,5-Trimethylbenzene 50 47 94 76-116 4-Chlorotoluene 50 47 94 78-116 tert-Butylbenzene 50 46 92 71-115 1,2,4-Trimethylbenzene 50 47 94 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS page 2 of 6 FORM III VOA 1 FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENI'R.ATION o LIMTTS - COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. sec-Butylbenzene 50 47 94 67-117 4-Isopropyltoluene 50 48 96 68-118 1,3-Dichlorobenzene 50 47 94 80-116 1,4-Dichlorobenzene 50 47 94 80-114 n-Butylbenzene 50 47 94 58-121 1,2-Dichlorobenzene 50 47 94 81-116 1,2-Dibromo-3-chloropro 50 38 76 71-126 1,2,4-Trichlorobenzene 50 46 92 67-114 Hexachlorobutadiene 50 44 88 50-111 Naphthalene 50 41 82 58-133 1,2,3-Trichlorobenzene 50 46 92 64-118 Ether 50 49 98 70-130 Diisopropyl Ether 50 48 96 70-130 Ethyl tert-butyl ether 50 48 96 70-130 tert-Amyl methyl ether 50 50 100 70-130 1,4-Dioxane 1000 190 19* 70-130. # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits C )MMENTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE LCSD LCSD ADDED CONCENTRATION a o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD ## RPD REC. Dichlorodifluoromethane 50 45 90 4 40 48-135 Chloromethane 50 46 92 4 40 60-118 Vinyl Chloride 50 46 92 2 40 65-113 Bromomethane 50 55 110 2 40 73-122 Chloroethane 50 48 96 2 40 72-118 Trichlorofluoromethane 50 52 104 2 40 68-129 1,1-Dichloroethene 50 49 98 4 40 67-121 Acetone 50 43 86 2 40 38-161 Iodomethane 50 52 104 2 40 72-130 Carbon Disulfide 50 47 94 2 40 53-137 Methylene Chloride 50 50 100 2 40 59-132 trans-1,2-Dichloroethen 50 46 92 2 40 71-124 Methyl tert-butyl ether 100 90 90 4 40 75-123 1,1-Dichloroethane 50 45 90 2 40 83-116 Vinyl acetate 50 77 154 52* 40 44-160 2-Butanone 50 38 76 0 40 64-139 cis-1,2-Dichloroethene 50 48 96 4 40 83-120 2,2-Dichloropropane 50 43 86 2 40 70-129 Bromochloromethane 50 49 98 2 40 85-124 Chloroform 50 47 94 0 40 89-118 Tetrahydrofuran 50 47 94 2 40 76-126 1, 1,1-Trichloroethane 50 45 90 0 40 81-122 1,1-Dichloropropene 50 48 96 0 40 76-122 Carbon Tetrachloride 50 44 88 2 40 79-125 1,2-Dichloroethane 50 46 92 2 40 83-123 Benzene 50 47 94 0 40 81-120 Trichloroethene 50 48 96 0 40 77-121 1,2-Dichloropropane 50 46 92 0 40 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE LCSD LCSD ADDED CONCENTRATION % o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dibromomethane 50 48 96 2 40 86-124 Bromodichloromethane 50 46 92 2 40 90-114 cis-1,3-Dichloropropene 50 46 92 2 40 78-119 4-Methyl-2-pentanone 50 40 80 5 40 57-138 _ Toluene 50 48 96 0 40 81-121 trans-1,3-Dichloroprope 50 45 90 2 40 85-118 1,1,2-Trichloroethane 50 48 96 2 40 44-159 1,3-Dichloropropane 50 47 94 2 40 79-125 Tetrachloroethene 50 49 98 2 40 73-121 2-Hexanone 50 37 74 0 40 53-145 Dibromochloromethane 50 44 88 2 40 80-124 1,2-Dibromoethane 50 48 96 2 40 80-124 Chlorobenzene 50 48 96 0 40 82-118 1,1,1,2-Tetrachloroetha 50 45 90 2 40 84-121 Ethylbenzene 50 47 94 2 40 80-122 Xylene (Total) 150 140 93 0 40 81-121 Styrene 50 48 96 2 40 77-128 Bromoform 50 43 86 0 40 77-130 Isopropylbenzene 50 47 94 0 40 58-148 1,1,2,2-Tetrachloroetha 50 45 90 2 40 76-125 Bromobenzene 50 46 92 0 40 76-124 1,2,3-Trichloropropane 50 43 86 0 40 57-140 n-Propylbenzene 50 46 92 2 40 72-119 2-Chlorotoluene 50 47 94 0 40 75-120 1,3,5-Trimethylbenzene 50 46 92 2 40 76-116 4-Chlorotoluene 50 46 92 2 40 78-116 tert-Butylbenzene 50 45 90 2 40 71-115 1,2,4-Trimethylbenzene 50 46 92 2 40 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA i FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS .No. SDG No. : MC1600 Matrix Spike - Sample No. : V6WLCS SPIKE LCSD LCSD ADDED CONCENTRATION 's °s QC LIMITS COMPOUND (ug/L) (ug./L) REC # RPD # RPD REC. -------- --- --- ----- ------ ------ ------ ------ sec-Butylbenzene 50 46 92 2 40 67-117 4-Isopropyltoluene 50 46 92 4 40 68-118 1,3-Dichlorobenzene 50 47 94 0 40 80-116 1,4-Dichlorobenzene 50 47 94 0 40 80-114 n-Butylbenzene 50 46 92 2 40 58-121 1,2-Dichlorobenzene 50 47 94 0 40 81-116 1,2-Dibromo-3-chloropro 50 39 78 2 40 71-126 1,2,4-Trichlorobenzene 50 46 92 0 40 67-114 Hexachlorobutadiene 50 43 86 2 40 50-111 Naphthalene 50 46 92 11 40 58-133 1,2,3-Trichlorobenzene 50 46 92 0 40 64-118 Ether 50 53 106 8 40 70-130 Diisopropyl Ether 50 50 100 4 40 70-130 Ethyl tert-butyl ether 50 50 100 4 40 70-130 tert-Amyl methyl ether 50 52 104 4 40 70-130 1,4-Dioxane 1000 540 54* 96* 40 707130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 2 out of 72 outside limits Spike Recovery: 2 out of 144 outside limits COMMENTS: page 6 of 6 FORM III VOA I FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6WLFB I I SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ------------------------ --------- ------------- ------------- ------ ------ ----------------------- ------------- ------ ------ Vinyl Chloride 1 0.8 80 60-120 1, 1-Dichloroethene 1 1 100 60-120 i i l # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits COMMENTS: j 1 FORM III VOA I FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION a LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ------------------------ --------- ------------- ------------- ------ ------ ------------------------ --------- ------------- ------------- ------ ------ Dichlorodifluoromethane 50 48 96 48-135 Chloromethane 50 43 86 60-118 Vinyl Chloride 50 45 90 65-113 Bromomethane 50 58 116 737122 .. Chloroethane 50 47 94 72-118 Trichlorofluoromethane 50 59 118 68-129 1,1-Dichloroethene 50 50 100 67-121 Acetone 50 46 92 38-161 Iodomethane 50 55 110 72-130 Carbon Disulfide 50 48 96 53-137 Methylene Chloride 50 51 102 59-132 trans-1,2-Dichloroethen 50 42 84 71-124 Methyl tert-butyl ether 100 79 79 75-123 1,1-Dichloroethane 50 40 80* 83-116 Vinyl acetate 50 69 138 44-160 2-Butanone 50 38 76 64-139 cis-1,2-Dichloroethene 50 42 84 83-120 2,2-Dichloropropane 50 38 76 70-129 Bromochloromethane 50 45 90 85-124 Chloroform 50 44 88* 89-118 Tetrahydrofuran 50 52 104 76-126 1,1,1-Trichloroethane 50 41 82 81-122 1,1-Dichloropropee 50 44 88 76-122 Carbon Tetrachloride 50 42 84 79-125 1,2-Dichloroethene 50 43 86 83-123 Benzene 50 44 88 81-120 Trichloroethene 50 44 88 77-121 1,2-Dichloropropane 50 43 86 81-116 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CON24ENTS: page 1 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Dibromomethane 50 45 90 86-124 Bromodichloromethane 50 41 82* 90-114 cis-1,3-Dichloropropene 50 40 80 78-119 4-Methyl-2-pentanone 50 36 72 57-138 .. Toluene 50 45 90 81-121 trans-1,3-Dichloroprope 50 40 80* 85-118 1,1,2-Trichloroethane 50 45 90 44-159 1,3-Dichloropropane 50 48 96 79-125 Tetrachloroethene 50 54 108 73-121 2-Hexanone 50 39 78 53-145 Dibromochloromethane 50 45 90 80-124 1,2-Dibromoethane . 50 48 96 80-124 Chlorobenzene 50 50 100 82-118 1,1,1,2-Tetrachloroetha 50 46 92 84-121 Ethylbenzene 50 49 98 80-122 Xylene (Total) 150 150 100 81-121 Styrene 50, 50 100 77-128 Bromoform 50 42 84 77-130 Isopropylbenzene 50 49 98 58-148 1,1,2,2-Tetrachloroetha 50 49 98 76-125 Bromobenzene 50 49 98 76-124 1,2,3-Trichloropropane 50 46 92 57-140 n-Propylbenzene 50 51 102 72-119 2-Chlorotoluene 50 50 100 75-120 1,3,5-Trimethylbenzene 50 50 100 76-116 4-Chlorotoluene 50 51 102 78-116 tert-Butylbenzene 50 49 98 71-115 1,2,4-Trimethylbenzene 50 51 102 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III VOA 1 FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No..: V6XLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ---- --------- ------------- ------------- ------ ------ sec-Butylbenzene 50 51 102 67-117 4-Isopropyltoluene 50 52 104 68-118 1,3-Dichlorobenzene 50 52 104 80-116 1,4-Dichlorobenzene 50 52 104 80-114 n-Butylbenzene 50 52 104 58-121 1,2-Dichlorobenzene 50 52 104 81-116 1,2-Dibromo-3-chloropro 50 41 82 71-126 1,2,4-Trichlorobenzene 50 49 98 67-114 Hexachlorobutadiene 50 47 94 50-111 Naphthalene 50 46 92 58-133 1,2,3-Trichlorobenzene 50 50 100 64-118 Ether 50 51 102 70-130 Diisopropyl Ether 50 45 90 70-130 Ethyl tert-butyl ether 50 44 88 70-130 tert-Amyl methyl ether 50 46 92 70-130 1,4-Dioxane 1000 650 65* 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 3 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS SPIKE LCSD LCSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ ---- Dichlorodifluoromethane 50 44 88 9 40 48-135 Chloromethane 50 44 88 2 40 60-118 Vinyl Chloride 50 47 94 4 40 65-113 Bromomethane 50 58 116 0 40 73-.122 Chloroethane 50 48 96 2 40 72-118 Trichlorofluoromethane 50 58 116 2 40 68-129 1,1-Dichloroethene 50 51 102 2 40 67-121 Acetone 50 41 82 11 40 38-161 Iodomethane 50 55 110 0 40 72-130 Carbon Disulfide 50 48 96 0 40 53-137 Methylene Chloride 50 51 102 0 40 59-132 trans-1,2-Dichloroethen 50 41 82 2 40 71-124 Methyl tert-butyl ether 100 79 79 0 40 75-123 1,1-Dichloroethane 50 39 78* 2 40 83-116 Vinyl acetate 50 39 78 56* 40 44-160 2-Butanone 50 36 72 5 40 64-139 cis-1,2-Dichloroethene 50 42 84 0 40 83-120 2,2-Dichloropropane 50 38 76 0 40 70-129 Bromochloromethane 50 45 90 0 40 85-124 Chloroform 50 43 86* 2 40 89-118 Tetrahydrofuran 50 52 104 0 40 76-126 1,1,1-Trichloroethane 50 41 82 0 40 81-122 1,1-Dichloropropene 50 44 88 0 40 76-122 Carbon Tetrachloride 50 40 80 5 40 79-125 1,2-Dichloroethane 50 42 84 2 40 83-123 Benzene 50 43 86 2 40 81-120 Trichloroethene 50 43 86 2 40 77-121 1,2-Dichloropropane 50 42 84 2 40 81-116 # Column to .be' used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: i i page 4 of 6 FORM III VOA i I FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEMM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : VGXLCS SPIKE LCSD LCSD ADDED CONCENTRATION °s % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dibromomethane 50 44 88 2 40 86-124 Bromodichloromethane 50 41 82* 0 40 90-114 cis-1,3-Dichloropropene 50 40 80 0 40 78-119 4-Methyl-2-pentanone 50 36 72 0 40 57-138 _ Toluene 50 44 88 2 40 81-121 trans-1,3-Dichloroprope 50 39 78* 2 40 85-118 1,1,2-Trichloroethane 50 44 88 2 40 44-159 1,3-Dichloropropane 50 46 92 4 40 79-125 Tetrachloroethene 50 52 104 4 40 73-121 2-Hexanone 50 37 74 5 40 53-145 Dibromochloromethane 50 43 86 4 40 80-124 1,2-Dibromoethane 50 47 94 2 40 80-124 Chlorobenzene 50 48 96 4 40 82-118 1, 1,1,2-Tetrachloroetha 50 44 88 4 40 84-121 Ethylbenzene 50 48 96 2 40 80-122 Xylene (Total) 150 140 93 7 40 81-121 Styrene 50 49 98 2 40 77-128 Bromoform 50 40 80 5 40 77-130 Isopropylbenzene 50 47 94 4 40 58-148 1,1,2,2-Tetrachloroetha 50 50 100 2 40 76-125 Bromobenzene 50 50 100 2 40 76-124 1,2,3-Trichloropropane 50 46 92 0 40 57-140 n-Propylbenzene 50 50 100 2 40 72-119 2-Chlorotoluene 50 50 100 0 40 75-120 1,3,5-Trimethylbenzene 50 51 102 2 40 76-116 4-Chlorotoluene 50 52 104 2 40 78-116 tert-Butylbenzene 50 49 98 0 40 71-115 1,2,4-Trimethylbenzene 50 50 100 2 40 77-117 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 5 of 6 FORM III VOA FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLCS 's i SPIKE LCSD LCSD ADDED CONCENTRATION o QC LIMITS-.. COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ ------ sec-Butylbenzene 50 51 102 0 40 67-117 I 4-Isopropyltoluene 50 51 102 2 40 68-118 1,3-Dichlorobenzene 50 52 104 0 40 80-116 1,4-Dichlorobenzene 50 51 102 2 40 80-114 n-Butylbenzene 50 52 104 0 40 58-121 1,2-Dichlorobenzene 50 52 104 0 40 81-116 1,2-Dibromo-3-chloropro 50 42 84 2 40 71-126 1,2,4-Trichlorobenzene 5.0 49 98 0 40 67-114 Hexachlorobutadiene 50 47 94 0 40 50-111 Naphthalene 50 50 100 8 40 58-133 1,2,3=Trichlorobenzene 50 49 98 2 40 64-118 Ether 50 53 106 4 40 70-130 Diisopropyl Ether 50 45 90 0 40 70-130 Ethyl tert-butyl ether 50 44 88 0 40 70-130 tert-Amyl methyl ether 50 47 94 2 40 70-130 1,4-Dioxane 1000 630 63* 3 40 70-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 72 outside limits Spike Recovery: 10 out of 144 outside limits COMMENTS: -- i page 6 of 6 FORM III VOA I FORM 3 WATER VOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : V6XLFB SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ---------------- --------- ------------- ------------- ------ ---=-- - Vinyl Chloride 1 0.8 80 80-120 1,1-Dichloroethene 1 1 100 80-120 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: . 0 out of 0 outside limits Spike Recovery: 0 out of 2 outside limits COMMENTS: FORM III VOA 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Phenol 50 0.0 38 76 0-127 bis(2-Chloroethyl)Ether 50 0.0 42 84 46-109 2-Chlorophenol 50 0.0 34 68 22-117 1,3-Dichlorobenzene 50 0.0 35 70 28-103 1,4-Dichlorobenzene 50 0.0 36 72 28-104 1,2-Dichlorobenzene 50 0.0 37 74 29-107 2-Methylphenol 50 0.0 45 90 40-104 2,21-oxybis(1-Chloropro 50 0.0 44 88 10-134 4-Methylphenol 50 0.0 48 96 35-106 N-Nitroso-di-n-prop. (1) 50 0:0 50 100 44-122 Hexachloroethane 50 0.0 35 70 24-104 Nitrobenzene 50 0.0 45 90 47-112 Isophorone 50 0.0 47 94 48-118 2-Nitrophenol 50 0.0 43 86 29-122 2,4-Dimethylphenol 50 0.0 63 126* 14-109 2,4-Dichlorophenol 50 0.0 44 88 31-122 1,2,4-Trichlorobenzene 50 0.0 41 82 33-108 Naphthalene 50 0.0 43 86 38-117 4-Chloroaniline 50 0.0. 48 96 0-152 bis (2-Chloroethoxy)meth 50 0.0 46 92 49-112 Hexachlorobutadiene 50 0.0 39 78 28-109 4-Chloro-3-Methylphenol 50 0.0 48 96 48-117 2-Methylnaphthalene 50 0.0 45 90 43-113 Hexachlorocyclopentadie 50 0.0 56 112* 34-103 2,4,6-Trichlorophenol 50 0.0 50 100 34-127 2,4,5-Trichlorophenol 50 0.0 48 96 32-131 2-Chloronaphthalene 50 0.0 48 96 47-116 2-Nitroaniline 50 0.0 48 96 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: i page 1 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Dimethylphthalate 50 0.0 48 96 53-124 Acenaphthylene 50 0.0 49 98 50-119 2,6-Dinitrotoluene 50 0.0 50 100 52-122 3-Nitroaniline 50 0.0 44 88 47-115 Acenaphthene 50 0.0 48 96 50-121 2,4-Dinitrophenol 50 0.0 50 100 0-144 4-Nitrophenol 50 0.0 49 98 0-160 Dibenzofuran 50 0.0 47 94 51-122 2,4-Dinitrotoluene 50 0.0 48 96 52-126 Diethylphthalate 50 0.0 49 98 53-126 4-Chlorophenyl-phenylet 50 0.0 48 96 50-124 Fluorene 50 0.0 49 98 52-125 4-Nitroaniline 50 0.0 44 88 47-117 4,6-Dinitro-2-methylphe 50 0.0 50 100 3-151 N-Nitrosodiphenylamine 50 0.0 60 120 48-121 4-Bromophenyl-phenyleth 50 0.0 49 98 51-124 Hexachlorobenzene 50 0.0 50 100 52-124 Pentachlorophenol 50 0.0 61 122 5-125 Phenanthrene 50 0.0 49 98 52-128 Anthracene 50 0.0 50 100 52-127 Carbazole 50 0.0 54 108 54-126 Di-n-butylphthalate 50 0.0 50 100 56-132 Fluoranthene 50 0.0 50 100 53-130 Pyrene 50 0.0 48 96 53-131 Butylbenzylphthalate 50 0.0 48 96 54-128 3,31-Dichlorobenzidine 50 0.0 1 2* 41-117 Benzo(a)anthracene 50 0.0 52 104 56-124 Chrysene 50 0.0 . 51 102 53-123 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 6 FORM III SV-1 OLM03 .0 3C f WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY j Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 i i - -SPIKE SAMPLE MS MS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. ------------------------ ------ bis (2-Ethylhexyl)phthal 50 0.0 48 96 56-127 Di-n-octylphthalate 50 0.0 46 92 59-138 Benzo(b) fluoranthene 50 0.0 43 86 58-126 Benzo(b) fluoranthene 50 0.0 54 108 60-124 Benzo(a)pyrene 50 0.0 48 96 61-121 Indeno(1,2,3-cd)pyrene 50 0.0 46 92 23-152 Dibenzo(a,h)anthracene 50 0.0 46 92 60-122 Benzo(g,h,i)perylene 50 0.0 47 94 57-124 I (1) N-Nitroso-di-n-propylamine i # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COD44ENTS: i page 3 of 6 FORM III SV-1 OLM03 .0 I 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 ' - - SPIKE MSD - - MSD ADDED CONCENTRATIONS o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Phenol 50 36 72 5 40 0-127 bis (2-Cbloroethyl)Ether 50 44 88 5 40 46-109 2-Chlorophenol 50 31 62 9 40 22-117 1,3-Dichlorobenzene 50 38 76 8 40 28-103 1,4-Dichlorobenzene 50 39 78 8 40 28-104 1,2-Dichlorobenzene 50 40 80 8 40 29-107 2-Methylphenol 50 44 88 2 40 40-104 2,21 -oxybis(1-Chloropro 50 45 90 2 40 10-134 4-Methylphenol 50 47 94 2 40 35-106 N-Nitroso-di-n-prop. (1) 50 49 98 2 40 44-122 Hexachloroethane 50 38 76 8 40 24-104 Nitrobenzene 50 46 92 2 40 47-112 Isophorone 50 47 94 0 40 48-118 2-Nitrophenol 50 39 78 10 40 29-122 2,4-Dimethylphenol 50 63 126* 0 40 14-109 2,4-Dichlorophenol 50 39 78 12 40 31-122 1,2,4-Trichlorobenzene 50 41 82 0 40 33-108 Naphthalene 50 44 88 2 40 38-117 4-Chloroaniline 50 48 96 0 40 0-152 bis(2-Chloroethoxy)meth 50 47 94 2 40 49-112 Hexachlorobutadiene 50 39 78 0 40 28-109 4-Chloro-3-Methylphenol 50 47 94 2 40 48-117 2-Methy1naphthalene 50 44 88 2 40 43-113 Hexachlorocyclopentadie 50 54 108* 4 40 34-103 2,4,6-Trichlorophenol 50 46 92 8 40 34-127 2,4,5-Trichlorophenol 50 47 94 2 40 32-131 2-Chloronaphthalene 50 48 96 0 40 47-116 2-Nitroaniline 50 48 96 0 40 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 4 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION % QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. Dimethylphthalate 50 48 96 0 40 53-124 Acenaphthylene 50 49 98 0 40 50-119 2,6-Dinitrotoluene 50 50 100 0 40 52-122 3-Nitroaniline 50 41 82 7 40 47-115 - Acenaphthene 50 48 96 0 40 50-121 2,4-Dinitrophenol 50 48 96 4 40 0-144 4-Nitrophenol 50 45 90 8 40 0-160 Dibenzofuran 50 48 96 2 40 51-122 2,4-Dinitrotoluene 50 49 98 2 40 52-126 Diethylphthalate 50 50 100 2 40 53-126 4-Chlorophenyl-phenylet 50 47 94 2 40 50-124 Fluorene 50 50 100 2 40 52-125 4-Nitroaniline 50 44 88 0 40 47-117 4,6-Dinitro-2-methylphe 50 48 96 4 40 3-151 N-Nitrosodiphenylamine 50 59 118 2 40 48-121 4-Bromophenyl-phenyleth 50 49 98 0 40 51-124 Hexachlorobenzene 50 50 100 0 40 52-124 Pentachlorophenol 50 59 118 3 40 5-125 Phenanthrene 50 49 98 0 40 52-128 Anthracene 50 51 102 2 40 52-127 Carbazole 50 54 108 0 40 54-126 Di-n-butylphthalate 50 50 100 0 40 56-132 Fluoranthene 50 49 98 2 40 53-130 Pyrene 50 50 100 4 40 53-131 Butylbenzylphthalate 50 49 98 2 40 54-128 3,31-Dichlorobenzidine 50 2 4* 67* 40 41-117 Benzo(a)anthracene 50 48 96 8 40 56-124 Chrysene 50 52 104 2 40 53-123 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits CONHENTS: page 5 of 6 FORM III SV-1 OLM03.0 3C WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Lab Name: MITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. :, MC1600 Matrix Spike - EPA Sample No. : MW-6 SPIKE MSD MSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ --------- ------------- ------ ------ ------ ------ ------------------------ --------- ------------- ------ ------ ------ ------ bis(2-Ethylhexyl)phthal 50 48 96 0 40 56-127 Di-n-octylphthalate 50 46 92 0 40 59-138 Benzo(b) fluoranthene 50 44 88 2 40 58-126 Benzo(k)fluoranthene 50 49 98 10 40 60-124 Benzo(a)pyrene 50 46 92 4 40 61-121 Indeno(1,2,3-cd)pyrene 50 46 92 0 40 23-152 Dibenzo(a,h)anthracene 50 46 92 0 40 60-122 Benzo(g,h,i)perylene 50 47 94 0 40 57-124 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and. RPD values with an asterisk * Values outside of QC limits RPD: 1 out of 64 outside limits Spike Recovery: 6 out of 128 outside limits CODg4ENTS: page 6 of 6 FORM III SV-1 OLM03.0 FORM 3 WATER SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS SPIKE SAMPLE LCS LCS QC- ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC ## REC. ------------------------ ------- Phenol 50 41 82 0-127 bis(2-Chloroethyl)Ether 50 43 86 46-109 2-Chlorophenol 50 37 74 22-117 1,3-Dichlorobenzene 50 37 74 28-103 1,4-Dichlorobenzene 50 37 74 28-104 1,2-Dichlorobenzene 50 39 78 29-107 2-Methylphenol 50 44 88 40-104 2,21 -oxybis(1-Chloropro 50 45 90 10-134 4-Methylphenol 50 46 92 35-106 N-Nitroso-di-n-prop. (1) 50 49 98 44-122 Hexachloroethane 50 36 72 24-104 Nitrobenzene 50 45 90 47-112 Isophorone 50 47 94 48-118 2-Nitrophenol 50 44 88 29-122 2,4-Dimethylphenol 50 54 108 14-109 2,4-Dichlorophenol 50 43 86 31-122 1,2,4-Trichlorobenzene 50 40 80 33-108 Naphthalene 50 43 86 38-117 4-Chloroaniline 50 57 114 0-152 bis (2-Chloroethoxy)meth 50 47 94 49-112 Hexachlorobutadiene 50 38 76 28-109 4-Chloro-3-Methylphenol 50 46 92 48-117 2-Methylnaphthalene 50 43 86 43-113 Hexachlorocyclopentadie 50 58 116* 34-103 2,4,6-Trichlorophenol 50 46 92. 34-127 2,4, 5-Trichlorophenol 50 44 88 32-131 2-Chloronaphthalene 50 47 94 47-116 2-Nitroaniline 50 48 96 51-120 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 1 of 3 FORM III SV FORM 3 WATER SEM[IVOLATILE- LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS .SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Dimethylphthalate 50 49 98 53-124 Acenaphthylene 50 49- 98 50-119 2,6-Dinitrotoluene 50 49 98 52-122 3-Nitroaniline 50 49 98 47-115 Acenaphthene 50 48 96 50-121 2,4-Dinitrophenol. 50 29 58 0-144 4-Nitrophenol 50 37 74 0-160 Dibenzofuran 50 48 96 51-122 2,4-Dinitrotoluene 50 51 102 52-126 Diethylphthalate 50 49 98 53-126 4-Chlorophenyl-phenylet 50 48 96 50-124 Fluorene 50 48 96 52-125 4-Nitroaniline 50 47 94 47-117 4,6-Dinitro-2-methylphe 50 41 82 3-151 N-Nitrosodiphenylamine 50 60 120 48-121 4-Bromophenyl-phenyleth 50 48 96 51-124 Hexachlorobenzene 50 49 98 52-124 Pentachlorophenol 50 33 66 5-125 Phenanthrene 50 47 94 52-128 Anthracene 50 51 102 52-127 Carbazole 50 49 98 54-126 Di-n-butylphthalate 50 49 98 56-132 Fluoranthene 50 49 98 53-130 Pyrene . 50 50 100 53-131 Butylbenzylphthalate 50 51 102 54-128 3,31 -IDichlorobenzidine 50 55 110 41-117 Benzo(a)anthracene 50 49 98 56-124 Chrysene 50 54 108 53-123 (1) N-Nitroso-di-n-propylamine # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits COMMENTS: page 2 of 3 FORM III SV FORM 3 WATER SEMIVOLATILE LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix Spike - Sample No. : S2QLCS i I SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION % LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. bis(2-Ethylhexyl)phthal 50 50 100 56-127 Di-n-octylphthalate 50 46 92 59-138 Benzo(b)fluoranthene 50 45 90 58-126 Benzo(k)fluoranthene 50 48 96 60-124 Benzo(a)pyrene 50 47 94 61-121 Indeno(1,2,3-cd)pyrene 50 47 94 23-152 Dibenzo(a,h)anthracene 50 47 94 60-122 Benzo(g,h,i)perylene 50 49 98 57-124 (1) N-Nitroso-di-n-propylamine # Column- to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of . 0 outside limits Spike Recovery: 1 out of 64 outside limits COMMENTS: page 3 of 3 FORM III SV FORM 3 WATER PCB LAB CONTROL SAMPLE Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix Spike - Sample No. : P2PLCS SPIKE SAMPLE LCS LCS QC. ADDED CONCENTRATION CONCENTRATION o LIMITS COMPOUND (ug/L) (ug/L) (ug/L) REC # REC. Aroclor-1016 2.0 1.9 95 45-162 Aroclor-1260 2.0 2.0 100 54-159 SPIKE LCSD LCSD ADDED CONCENTRATION o o QC LIMITS COMPOUND (ug/L) (ug/L) REC # RPD # RPD REC. ------------------------ --------- -------=----- ------ ------ ------ ------ ------------------------ --------- ------------- ------ ------ ------ ------ Aroclor-1016 2.0 2.0 100 5 40 45-162 Aroclor-1260 2.0 2.0 100 0 40 54-159 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 2 outside limits Spike Recovery: 0 out of 4 outside limits COMMENTS: FORM III PCB U.S_ EPA - CLP i j 5A EPA SAMPLE NO SPIKE SAMPLE RECOVERY - MW-6 Lab Name: Mitkem Corporation Contract: 28367-0050- Lab Code: MITKEM Case. No- SAS No. : SDG No_ : MC1600 ] Matrix (soil/water) : WATER Level (low/med) : MED i — $ Solids for Sample: 0.0 II -- Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) - %jR M Cyanide 75-125 24.1760 100-00 24.2 Z_ oo!�' f t 1 I I i II i j Comments: FORM V (Part 1) - IN SW846 0126 U.S. EPA - CLP 5A EPA SAMPLE NO SPIKE SAMPLE RECOVERY MFI-6 Lab Name: Mitkem Corporation Contract: 28367-0050- Lab Code: MITKEM Case No, SAS No. : SDG No. : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED % Solids for Sample: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Antimony 75-125 453.9091 20.0000 U 455.50 99.7 P Arsenic 75-125 461.3849 20.0000 U 455.50 101.3 P Barium 75-125 8715.4382 200.0000 U 9100.00 95.8 P Beryllium 75-125 219.6424 5.0000 U 227.00 96.8 P Cadmium 75-125 212.8834 5.0000 U 227.00 93.8 P. Chromium 75-125 870.6539 20.0000 U 910.00 95.7 P Lead 75-125 431.1052 10.0000 U 455.00 94.7 P Nickel 75-125 2193.3999 50.0000 U 2270.00 96.6 P Selenium 75-125 435.1203 30.0000 U 455.00 95.6 P Silver 75-125 1176.6854 30.0000 U 1130.00 104.1 P. Thallium 75-125 387.4990 20.0000 U 455.00 85.2 P Vanadium 75-125 2208.8549 50.0000 U 2270.00 97.3 P Zinc 75-125 2175.3672 50.0000 U 2270.00 95.8 P Mercury 75-125 4.8231 0.3100 U 4.55 106.0 CV Comments: FORM V (Part 1) - IN SW846 1 I - U.S. EPA - CLP 5B EPA SAMPLE NO POST DIGEST- SPIKE SAMPLE RECOVERY MW-6 Lab Name: Mitkem Corporation Contract: 28367-0050- Lab Code: MITKEM Case No_ SAS No. : SDG No_ : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED i Concentration Units: ug/L i - I Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Cyanide 50.42 9.10 U 40.0 126.0 CA i i Comments- i J FORM V (Part 2) - IN SW846 U_S_ EPA - CT.P 6 EPA SAMPLE NO DUPLICATES -- -.... MW-6 Lab Name: Mi-tkem Corporation Contract: 28367-0050- Lab Code: MITKEM Case No. SAS No.: SDG No. : MC1600 Matrix (soil/water) : WATER Level (low/med) : MED % Solids For Sample: 0.0 % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Anaiyte Limit Sample (S) C Duplicate {D) C HRPDQ M Antimony 20.0 20.0000 U 20.0000 UP Arsenic 20.0 20.0000 U 20.0000 UP Barium 200.0 200.0000 U 200.0000 Up Beryllium 5.0 5.0000 U 5.0000 U P .Cadmium 5.0 5.0000 U 5.0000 U P ,Chromium 20.0 20.0000 U 20.0000 U P Lead 10.0 10.0000 U 10.0000 U P Nickel 50.0 50.0000 U 50.0000 U P Selenium 30.0 30.0000 U 30.0000 U P Silver- 30.0 30.0000 Li 30.0000 U p Thallium 20.0 20.0000 U 20.0000 U P Vanadium 50.0 50.0000 U 50.0000 U P Zinc 50.0 50.0000 U 50.0000 U P Mercury 0.3 0.3100 U 0.2800 U Cv Cyanide 28.8 2$.0066 U 24-94" U CA.01 10 FORM VI - 1N SW846 01,2 4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY VBLK6W Lab Name: MITKEM CORPORATION Contract: i - Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 i Lab File ID: V6D5093 Lab Sample ID: MB-16366 Date Analyzed: 01/04/05 Time Analyzed: 1048 i GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (YIN) N Instrument ID: V6 i THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED O1 VGWLCS LCS-16366 V6D5094 1119 02 V6WLCSD LCSD-16366 V6D5095 1146 03 V6WLFB LFB-16366 V6D5096 1226 04 MW-5 C1600-01A V6D5099 1350 05 MW-6 C1600-02A V6D5100 1417 06 MW-X C1600-03A V6D5101 1444 07 MW-3 C1600-04A V6D5104 1605 08 MW-2 C1600-05A V6D5105 1631 09 10 1 11 12 13 14 15 16 17 - - 18 19 20 21 ---- 22 -- 23 - - 24 25 - — - - 26 - - — 27 -- -- - 28 -329 0 - - - -- I —COMMENTS: : page 1 of 1 , FORM IV VOA OLM03 .0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6W Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5093 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 2 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-'69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 1 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomet e- 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether 5 U 75-34-3---------1,1-Dichloroethane 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropene 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1, 1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethene 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropene 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 u 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3---------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6W Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : 'MC1600 Matrix: (soil/water) WATER Lab Sample .ID: MB-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5093 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5--------=1, 1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4--------Tetrachloroethene 5 U 591-78-6----=---2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane _ 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Ethylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7-------Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1, 1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6---------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene _ 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene _ 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1, 2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03.0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6W Lab Name: MITKE24 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16366 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5093 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/04/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume.: (uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03:0 1 4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY VBLK6X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID: V6D5133 Lab Sample ID: MB-16380 Date Analyzed: 01/05/05 Time Analyzed: 1044 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (YIN) N Instrument ID: V6 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED ------------ -------------- -------------- ---------- ------------ -------------- -------------- ---------- 01 VGXLCS LCS-16380 V6D5134 1111 02 V6XLCSD LCSD-16380 V6D5135 1137 03 V6XLFB LFB-16380 V6D5136 1204 04 MW-2DL C1600-05ADL V6D5139 1359 05 MW-6MS C1600702AMS V6D5143 1557 06 MW-6MSD C1600-02AMSD V6D5144 1637 07 MW-3DL C1600-04ADL V6D5145 1703 08 09 10 - - 11 12 13 14 15 16 17 18 19 20 21 22 23 24 _ 25 - 26 - -- 27 28 - -- - 29 - -- - - 30 COMMENTS: i page 1 of 1 FORM IV VOA OLM03:0 I lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. :_ MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5133 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: JUL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 75-71-8---------Dichlorodifluoromethane 5 U 74-87-3---------Chloromethane 5 U 75-01-4---------Vinyl Chloride 5 U 74-83-9---------Bromomethane 5 U 75-00-3---------Chloroethane 5 U 75-69-4---------Trichlorofluoromethane 5 U 75-35-4---------1,1-Dichloroethene 5 U 67-64-1---------Acetone 5 U 74-88-4---------Iodomethaiie 5 U 75-15-0---------Carbon Disulfide 5 U 75-09-2---------Methylene Chloride 5 U 156-60-5--------trans-1,2-Dichloroethene 5 U 1634-04-4-------Methyl tert-butyl ether -5 U 75-34-3----------1, 1-Dichloroethene 5 U 108-05-4--------Vinyl acetate 5 U 78-93-3---------2-Butanone 5 U 156-59-2--------cis-1,2-Dichloroethene 5 U 590-20-7--------2,2-Dichloropropane 5 U 74-97-5---------Bromochloromethane 5 U 67-66-3---------Chloroform 5 U 109-99-9--------Tetrahydrofuran 5 U 71-55-6---------1,1,1-Trichloroethane 5 U 563-58-6--------1,1-Dichloropropene 5 U 56-23-5---------Carbon Tetrachloride 5 U 107-06-2--------1,2-Dichloroethane 5 U 71-43-2---------Benzene 5 U 79-01-6---------Trichloroethene 5 U 78-87-5---------1,2-Dichloropropane 5 U 74-95-3---------Dibromomethane 5 U 75-27-4---------Bromodichloromethane 5 U 10061-01-5------cis-1,3-Dichloropropene 5 U 108-10-1--------4-Methyl-2-pentanone 5 U 108-88-3--------Toluene 5 U 10061-02-6------trans-1,3-Dichloropropene 5 U FORM I VOA OLM03 :0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. :- SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5133 Level: (low/med) LOW Date Received: o Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: . _(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 79-00-5---------1, 1,2-Trichloroethane 5 U 142-28-9--------1,3-Dichloropropane 5 U 127-18-4-------=Tetrachloroethene 5 U 591-78-6--------2-Hexanone 5 U 124-48-1--------Dibromochloromethane 5 U 106-93-4--------1,2-Dibromoethane 5 U 108-90-7--------Chlorobenzene 5 U 630-20-6--------1,1,1,2-Tetrachloroethane 5 U 100-41-4--------Euhylbenzene 5 U ----------------m,p-Xylene 5 U 95-47-6---------o-Xylene 5 U 1330-20-7---.----Xylene (Total) 5 U 100-42-5--------Styrene 5 U 75-25-2---------Bromoform 5 U 98-82-8---------Isopropylbenzene 5 U 79-34-5---------1,1,2,2-Tetrachloroethane 5 U 108-86-1--------Bromobenzene 5 U 96-18-4---------1,2,3-Trichloropropane 5 U 103-65-1--------n-Propylbenzene 5 U 95-49-8---------2-Chlorotoluene 5 U 108-67-8--------1,3,5-Trimethylbenzene 5 U 106-43-4--------4-Chlorotoluene 5 U 98-06-6---------tert-Butylbenzene 5 U 95-63-6--7-------1,2,4-Trimethylbenzene 5 U 135-98-8--------sec-Butylbenzene 5 U 99-87-6---------4-Isopropyltoluene 5 U 541-73-1--------1,3-Dichlorobenzene 5 U 106-46-7--------1,4-Dichlorobenzene 5 U 104-51-8--------n-Butylbenzene 5 U 95-50-1---------1,2-Dichlorobenzene 5 U 96-12-8---------1,2-Dibromo-3-chloropropane_ 5 U 120-82-1--------1,2,4-Trichlorobenzene 5 U 87-68-3---------Hexachlorobutadiene 5 U 91-20-3---------Naphthalene 5 U FORM I VOA OLM03:0 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLK6X Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16380 Sample wt/vol: 5.000 (g/mL) ML Lab File ID: V6D5133 Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 01/05/05 GC Column: DB-624 ID: 0.25 (mm) Dilution Factor: 1.0 Soil Extract Volume: (uL) Soil Aliquot Volume: -(uL) CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 87-61-6---------1,2,3-Trichlorobenzene 5 U 60-29-7---------Ether 5 U 108-20-3--------Diisopropyl Ether 5 U 637-92-3--------Ethyl tert-butyl ether 5 U 994-05-8--------tert-Amyl methyl ether 5 U 123-91-1--------1,4-Dioxane 100 U FORM I VOA OLM03.0 -4B EPA SAMPLE NO. SEMIVOLATILE METHOD BLANK SUMMARY SBLK2Q Lab Name: MITKE4 CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID: S2E3101 Lab Sample ID: MB-16345 Instrument ID: S2 Date Extracted: 01/03/05 Matrix: (soil/water) WATER Date Analyzed: 01/05/05 Level• (low/med) LAW Time Analyzed: 1954 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED ------------ -------------- - -- --------- ---------- 01 S2QLCS LCS-16345 S2E3100 01/05/05 02 MW-5 C1600-01D S2E3107 01/05/05 03 MW-6 C1600-02D S2E3108 01/05/05 04 MW-6MS C1600-02DMS S2E3109 01/05/05 05 MW-6MSD C1600-02DMSD S2E3110 01/06/05 06 MW-X C1600-03D S2E3111 01/06/05 07 08 09 10 11 12 13 14 15 16 _ 17 18 19 20 21 22 23 24 25 26 27 28 29 30 COMMENTS: : page 1 of 1 FORM IV SV OLM03.0 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SBLK2Q Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3101 Level: (low/med) LOW Date Received: Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000(uL) Date Analyzed: O1/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 108-95-2--------Phenol _ 10 U 111-44-4--------bis (2-Chloroethyl) Ether 10 U 95-57-8---------2-Chlorophenol 10 U 541-73-1--------1,3-Dichlorobenzene 10 U 106-46-7--------1,4-Dichlorobenzene 10 U 95-50-1---------1,2-Dichlorobenzene 10 U 95-48-7---------2-Methylphenol 10 U 108=60-1--------2,2 '-oxybis (1-Chloropropane) 10 U 106-44-5--------4-Methylphenol 10 U 621-64-7--------N-Nitroso-di-n-propylamine_ 10 U 67-72-1---------Hexachloroethane 10 U 98-95-3---------Nitrobenzene 10 U 78-59-1---------Isophorone 10 U 88-75-5---------2-Nitrophenol 10 U 105-67-9--------2,4-Dimethylphenol 10 U 120-83-2--------2,4-Dichlorophenol 10 U 120-82-1--------1,2,4-Trichlorobenzene 10 U 91-20-3---------Naphthalene 10 U 106-47-8--------4-Chloroaniline 10 U 111-91-1--------bis(2-Chloroethoxy methane_ 10 U 87-68-3---------Hexachlorobutadiene 10 U 59-50-7-------- 4-Chloro-3-Methylphenol 10 U 91-57-6---------2-Methylnaphthalene 10 U 77-47-4---------Hexachlorocyclopentadiene 10 U 88-06-2---------2,4,6-Trichlorophenol 10 U 95-95-4---------2,4,5-Trichlorophenol 20 U 91-58-7---------2-Chloronaphthalene 10 U 88-74-4---------2-Nitroaniline 20 U 131-11-3--------Dimethylphthalate 10 U 208-96-8--------Acenaphthylene 10 U 606-20-2--------2,6-Dinitrotoluene 10 U 99-09-2---------3-Nitroaniline 20 U 83-32-9---------Acenaphthene 10 U FORM I SV-1 OLM03:0 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SBLK2Q Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEMM Case No. : SAS No. : SDG No. : MC1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16345 Sample wt/vol: 1000 (g/mL) ML Lab File ID: S2E3101 Level: (low/med) LOW Date Received: o Moisture: decanted: (Y/N) Date Extracted:01/03/05 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 01/05/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 _.. GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 51-28-5---------2,4-Dinitrophenol_ 20 U 100-02-7--------4-Nitrophenol 20 U 132-64-9--------Dibenzofuran 10 U 121-14-2--------2,4-Dinitrotoluene 10 U 84-66-2---------Diethylphthalate 10 U 7005-72-3-------4-Chlorophenyl-phenylether 10 U 86-73-7---------Fluorene 10 U 100-01-6--------4-Nitroaniline 20 U 534-52-1--------4,6-Dinitro-2-methylphenol_ 20 U 86-30-6---------N-Nitrosodiphenylamine (1)_ 10 U 101-55-3--------4-Bromophenyl-phenylether 10 U 118-74-1--------Hexachlorobenzene 10 U 87-86-5---------Pentachlorophenol 20 U 85-01-8---------Phenanthrene 10 U 120-12-7--------Anthracene 10 U 86-74-8---------Carbazole _ 10 U 84-74-2---------Di-n-butylphthalate_ 10 U 206-44-0--------Fluoranthene__ 10 U 129-00-0--------Pyrene 10 U 85-68-7---------Butylbenzylphthalate 10 U 91-94-1---------3,3' -Dichlorobenzidine 10 ,U 56-55-3---------Benzo(a)anthracene 10 'U 218-01-9--------Chrysene 10 U 117-81-7--------bis(2-Ethylhexyl)phthalate_ 10 U 117-84-0--------Di-n-octylphthalate 10 U 205-99-2--------Benzo(b) fluoranthene 10 U 207-08-9--------Benzo(k)fluoranthene 10 U 50-32-8---------Benzo(a)pyrene _ 10 U 193-39-5--------Indeno(1,2,3-cd per_ 10 U 53-70-3---------Dibenzo(a,h)anthracene 10 U. 191-24-2--------Benzo(g,h, i)perylene 10 U (15 - Cannot be separated from Diphenylamine FORM I SV-2 OLM03.0 FORM 4 CLIENT SAMPLE NO. PCB METHOD BLANK SUMMRY PBLK2P Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No_ : SDG No. : C1600 Lab Sample ID: MB-16376 Lab File ID: E2E3239F Matrix (soil/water) WATER Extraction: (SepF/Cant/Sonc) SEPF Sulfur Cleanup (YIN) Y Date Extracted: 01/05/05 Date Analyzed (1) : 01/11/05 Date Analyzed (2) : 01/11/05 Time Analyzed (1) : 0145 Time Analyzed (2) : 0145 Instrument ID (1) : E2 Instrument ID (2) : E2 GC Column (1) : RTXCLPPEST ID: 0.53 (mm) GC Column (2) : RTXCLPPEST 2 ID: 0.53'(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD: LAB DATE DATE SAMPLE NO. SAMPLE ID ANALYZED 1 ANALYZED 2 ------------ -------------- ---------- ---------- ------------ -------------- ---------- ---------- 01 P2PLCS LCS-16376 01/11/05 01/11/05 02 P2PLCSD LCSD-16376 01/11/05 01/11/05 03 MW-6 C1600-02D 01/11./05 01/11/05 04 05 06 07 08 09 10 11 w 12 13 14 15 16 17 18 19 20 21 22 23 24 25 - - - 26 COMMENTS: page 1 of 1 FORM IV PCB FORM 1 CLIENT SAMPLE NO_ . PCB ORGANICS ANALYSIS DATA SHEET PBLK2P Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : C1600 Matrix: (soil/water) WATER Lab Sample ID: MB-16376 Sample wt/vol: 1000 (g/ml) ML Lab File ID. E2E3239F i Moisture: decanted: (Y/N) Date Received: Extraction: (SepF/font/Sons) SEPF Date Extracted:01/05/05 Concentrated Extract Volume: 2000(uL) Date Analyzed: 01/11/05 Injection Volume: 1.0(uL) Dilution Factor: 1.0 GPC Cleanup: '(Y/N) N pH: Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q 12674-11-2------Aroclor-1016 _ _ 0.20 U 11104-28-2------Aroclor-1221 0.20 U 11141-16-5------Aroclor-1232 0.20 U 53469-21-9------Aroclor=1242 0.20 U 12672-29-6------Aroclor-1248 0.20 U 11097-69-1------Aroclor-1254 0.20 U 11096-82-5------Aroclor-1260 0.20 U FORM I PCB U.S_ EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No_ : SDG No. : MC1600 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C- 1 C 2 C 3 C Blank C M Mercury 0.0 U 0.0 U 0.0 U 1 0.2 B 0.047 U CV FORM III - IN SW846 i U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Mercury 1 0.1 B CV I FORM III - IN SW846 U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Preparation Blank Matrix (coil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 U 9.1 U 9.1 U 9.1 U 9.100 U CA FORM III - IN SW846 a U.S. EPA - CLP 3 BLANKS i Lab Name: Mitkem Corporation Contract: 28367-0050=0000 Lab Code: MITKEM Case No. SAS No. : SDG No_ : MC160.0 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Cyanide 9.1 u CA t i FORM III - IN SW846 I 1 U.S. EPA - CLP 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No.. : SDG No. . MC1600 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Antimony 11.9 B 5.7 B 2.9 B 3.3 B 1.200 U P Arsenic 1.7 B 1.6 U 1.6 U 1.6 U 1.600 U P Barium 15.2 B 9.2 B 5.9 B 7.3 B 2.100 U P Beryllium 0.2 B 0.5 B 0.1 U 0.1 U 0.150 U P Cadmium 0.1 B 0.1 U -0.2 B -0.1 B 0.100 U P Chromium 1.1 B 0.6 B 0.4 U 0.5 B 0.380 U P Lead 1.2 B -1.4 B -0.5 B -0.6 B 0.651 B P Nickel 3.7 B 2.2 B 1.6 B 1.9 B 1.276 B P Selenium 2.3 B 1.0 U 1.0 U 1.0 U 0.980 U P Silver 6.8 B 2.5 B 2.1 B 2.0 B 0.910 U P Thallium 3.7 B 2.9 B 3.9 B 8.1 B -4.184 B P Vanadium 1.9 B 2.1 B 1.1 B 1.2 B 0.470 U P Zinc 4.5 B 4.8 B 2.3 U 2.3 U 16.797 B P FORM III - IN SW846 'r U.S. EPA - CLP I 3 BLANKS Lab Name: Mitkem Corporation Contract: 28367-0050-0000 Lab Code: MITKEM Case No. SAS No. : SDG No. : MC1600 Preparation Blank Matrix (soil/water) : Preparation Blank Concentration Units (ug/L or mg/kg) : Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Antimony 3.0 B P Arsenic 1.6 U p Barium 8.0 B P Beryllium 0.1 U P Cadmium -0.2 B P. Chromium 0.6 B P Lead 0.5 U P Nickel 2.0 B P Selenium 1.0 U p Silver 1.9 B P Thallium 5.0 B P Vanadium 1.4 B P Zinc 2.3 U p FORM III - IN SW846 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : V6D5091 Date Analyzed: 01/04/05 Instrument ID: V6 Time Analyzed: 0946 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (YIN) N IS1 IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT # ------------ ---------- ------- ---------- ------- ---------- ------- ------------ ---------- ------- ---------- ------- ---------- ------- 12 HOUR STD 1254041 5.69 979194 9.31 595531 12.28 UPPER LIMIT 2508082 6.19 1958388 9.81 1191062 12.78 LOWER LIMIT 627021 5.19 489597 8.81 297766 11.78 ------------ ---------- ------- ---------- ------- ---------- ------- ------------ ---------- ------- ---------- ------- ---------- ------- EPA SAMPLE NO. ------------ ---------- ------- ---------- ------- ---------- ------- ------------ ---------- ------- ---------- ------- ---------- ------- 01 VBLKGW 1082800 5.69 838062 9.31 459355 12.28 02 V6WLCS 1122075 5.69 867157 9.30 533632 12.28 03 V6WLCSD 1098175 5.70 870698 9.31 531242 12.28 04 V6WLFB 1139168 5.69 880198 9.31 493146 12.28 05 MW-5 1085406 5.69 835585 9.31 463660 12.28 06 MW-6 1111915 5.69 842493 9.31 467074 12.28 07 MW-X 1060318 5.70 822849 9.31 449003 12.28 08 MW-3 1191821 5.69 918968 9.30 574487 12.28 09 MW-2 1380904 5.70 1063946 9.31 595842 12.28 10 11 12 13 14 15 16 17 18 19 20 21 22 IS1 = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 IS3 (DCB). = 1,4-Dichlorobenzene-d4 AREA UPPER LIMIT = +1000 of internal standard area AREA LOWER LIMIT = - 5006 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03.0 8A VOLATILE INTERIM, STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : V6D5131 Date Analyzed: 01/05/05 Instrument ID: V6 Time Analyzed: 0943 GC Column: DB-624 ID: 0.25 (mm) Heated Purge: (YIN) N IS1 IS2 CBZ IS3 DCB AREA # RT # AREA # RT # AREA # RT # ------------ ---------- ------- ---------- ------- ---------- ------- 12 HOUR STD 1277052 5.69 925287 9.31 542187 12.28 UPPER LIMIT 2554104 6.19 1850574 9.81 1084374 12.78 DOWER LIMIT 638526 5.19 462644 8.81 271094 11.78 ------------ ---------- ------- ---------- ------- ---------- ------- ------------ ---------- ------- ---------- ------- ---------- ------- EPA SAMPLE NO. ------------ ---------- ------- ---------- ------- ---------- ------- ------------ ---------- ------- ---------- ------- ---------- ------- 01 VBLK6X 11.86587 5.69 821619 9.31 391099 12.28 02 V6XLCS 1282813 5.69 913049 9.31 543721 12.28 03 V6XLCSD 1276723 5.69 910202 9.31 524488 12.28 04 V6XLFB 1230971 5.69 857081 9.31 423470 12.28 05 MW-2DL 1212495 5.69 851652 9.31 460303 12.28 06 MW-6MS 1356002 5.69 961182 9.31 555419 12.28 07 MW-6MSD 1396537 5.69 978535 9.31 562504 12.28 08 MW-3DL 1376067 5.69 949794 9.31 506083 12.28 09 10 11 _ 12 13 14 15 16 17 18 19 20 21 22 IS1 = Fluorobenzene IS2 (CBZ) = Chlorobenzene-d5 IS3 (DCB) = 1,4-Dichlorobenzene-d4 AREA UPPER LIMIT = +1000-o of internal standard area AREA LOWER LIMIT = - 500 of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM03:0 8B SEMIVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : S2E3096 Date Analyzed: 01/05/05 Instrument ID: S2 Time Analyzed: 1648 IS1 DCB IS2 NPT IS3 ANT AREA # RT # AREA # RT # AREA # RT # ------------ ---------- ------- ---- 12 HOUR STD 296671 6.39 1152334 8.33 628299 11.14 UPPER LIMIT 593342 6.89 2304668 8.83 1256598 11.64 LOWER LIMIT 148336 5.89 576167 7.83 314150 10.64 EPA SAMPLE NO. ------------ ---------- ------- --- 01 S2QLCS 284576 6.38 1089611 8.33 607066 11.14 02 SBLK2Q 286951 6.38 1112165 8.32 620030 11.14 03 MW-5 292953 6.39 1111524 8.32 613208 11.14 04 MW-6 293093 6.38 1103577 8.33 608562 11.13 05 MW-61MS 305097 6.39 1164650 8.33 650294 11.14 06 MW-61MSD 293230 6.38 111520.0 8.33 616463 11.14 07 MW-X 265165 6.38 1010076 8.33 565724 11.13 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 IS1 (DCB) = 1,4-Dichlorobenzene-d4 IS2 (NPT) = Naphthalene-d8 IS3 (ANT) = Acenaphthene-d10 AREA UPPER LIMIT = +1000-. of internal standard area AREA LOWER LIMIT = - 500-. of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT ## Column used to flag internal standard area values with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII SV-1 OLM03.0 8C SEMIVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: MITKEM CORPORATION Contract: Lab Code: MITKEM Case No. : SAS No. : SDG No. : MC1600 Lab File ID (Standard) : S2E3096 Date Analyzed: 01/05/05 Instrument ID: S2 Time Analyzed: 1648 IS4 PHN IS5 CRY IS6 PRY AREA # RT # AREA # RT # AREA #. RT ## ------------ ---------- --- -- 12 HOUR STD 1114180 13.54 936462 17.03 763720 18.66 UPPER LIMIT 2228360 . 14.04 1872924 17.53 1527440 19.16 LOWER LIMIT 557090 13.04 . 468231 16.53 381860 18.16 EPA SAMPLE NO. O1 S2QLCS 1052731 13.53 861869 17.02 757179 18.66 02 S8LK2Q 1089198 13.54 944709 17.01 779784 18.66 03 MW-5 1056015 13.54 926658 17.02 748006 18.67 04 MW-6 1036880 13.53 892655 17.02 724690 18.66 05 MW-6MS 1108799 13.54 924647 17.03 769831 18.66 06 MW-6MSD 1058390 13.55 876722 17.03 744718 18.67 07 MW-X 984375 13.53 859066 17.02 701059 18.66 08 09 10 11 12 - 13 14 15 16 17 18 19 20 21 22 IS4 (PHN) = Phenanthrene-d10 IS5 (CRY) = Chrysene-dl2 IS6 (PRY) = Perylene-d12 AREA UPPER LIMIT = +1000i of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT # Column used to .flag internal standard area values with an asterisk. * Values outside of QC limits. f page 1 of 1 FORM VIII SV-2 O1,M03:0 l