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SOUTH MASON STREET (002)�uifi /1%9SoN �7�iT C4ie//S> 9 Soot basoll) NWfn'S `JNI1StlH ��e10 15% I4CJ® rON OEM Odn Permit # GHL-15-172 Date of Print 7/14/2015 Permit Issued 7/14/2015 Permit Expires 12/31/2019 Permit Fee $0.00 Late Fee $0.00 6) Kimberley Driscoll Mayor City Of Salem, Massachusetts Board of Health 120 Washington Street, 4th Floor, Salem, MA 01970 TEL. (978) 741-1800 FAX. (978) 745-0343 Iramdin@salem.com GENERAL HEALTH PERMIT Granted To: Address: License For: 167 Main Street Site Assessment Larry Ramdin, MPH, REHS, CHO Health Agent Derosa Environmental Consulting Rowley MA Location of Establishment: 9 SOUTH MASON STREET Restrictions: Notes: Montering Well Permit This permit or license is granted in conformity with the statues and ordinances relating thereto, and expires on 12/31/2019 , unless sooner revoked or suspended. ®EROSA Environmental CONSULTING, INC. Tyler C. Ferrick Environmental Scientist 167 Main Street, PO Box 716, Rowley MA 01969 derosaenvironmental.com • Cell: (978) 500-9053 . Licensed Site Professional (Lit. No. 3452) . i'9ZardOus Waste Treatment . *Emim.mental Sita Assessment (ASTM) . Wetland Restoration 8 Permitting . Wildlife Pond Design -Management . Landscape Restoration r Renewable Energy Permitting . Green Building (LEER AP) Technical Review Expert Testimony Tyler C. Ferrick Environmental Scientist o (978) 948-7717 c (978) 500-9053 f (978) 948-7718 ferrick.derosa®gmail.com KIMBERLI3Y DRISCOLL MAYOR CITY OF SALEM, MASSACHUSETTS BOARD OF HEAL F1 120 WASHINGTON STREET, 4." FLOOR T'EL. (978) 741-1800 FAx (978) 745-0343 Iramditi@salem.com salem.com uffi PublicHeatth Prevent Promote. Protect. LARRY RAMDIN, RS/REHS, (A 10, CP -FS HEAL: PI-[ AGPINT Well Construction Permit Application Fee: $180. Check payable to the City of Salem (no cash. No charge for monitoring wells) n, MA. 01970 Tel. Type of well: t or' Well use: SamP�ino Well Contractor: jkp\ask v'AmekI Covsvk, Pum ontractor: Address: i67 MrNN SiCeeij KoA-_Yr' M Address: Phone: 978 -JC -7717 Phone: Reg. #: Have abutters been notified? (y)�O How? In the space provided below (or on back) show the location of the proposed well in relation to existing or proposed above or below ground structures. A description of visible prior and current land use within (200) feet of the proposed well location, which represent a potential source of contamination. 5oij D�`°qq5 �vlll Ge, candtic��d o\I�.1 sal tell be sa\,+�led, Grotti�d�✓ti�e(' be, �.d�Ance� C'411MAWN4ef w,ll o�is� �e sum�l�dt A W" \ be prov'I f io HIie UeNi}t1 DgP\r4mt6) t,oea, ons -Kcber'\(\�5'WCi�S l %, 4 {�j wk ir �W� -4t. There is no fee for monitoring wells but a permit is required for installation. B.O.H. use only Check #: Check date: Permit #: Well const permit appl. UPDATED 5/23/11 Oct 30 01 02:53p Joanne Scott Salem HCH 970 740 9705 CITY OF SALEM, MASSACHU'SLOTS �� BOARD OF HEALTH • • 120 WAGHINCTON STREET, 4TH FLOOR SALEM, MA 01970 TEL. 978=74 1.1900 n � FAX DT745 0343 - STAN LEY USOVICZ, JK, JOANNE SCOTT; ; MPH, R5, GHQ MAYOR HEALTH AGENT _ i,UV 9 2001 CITY OF SALEM HEALTH DEPT. WELL CONSTRUCT10 RERMIT Location 9 South Mason Street Owner Bay State Adhesives Address 9 South Mason Street This permit is granted in conformity with the statutes and ordinances relating to well permits. Well construction permits are non -transferable. This permit shall be on site at all times that work is taking place. Permit shall• expire one (1) year from the date of issuance unless revoked from cause. This permit does not constitute a Water Supply Certificate. Permit # Date issued (monitoring wells) 5-01 10/30/01 �f ;6a/lth=ge/ p.2 Massachusetts Department of Environmental Management 105152 -I- Office of Water Resources 4YPE OR PRINT ONLY Well Completion Repot 1WELLLQCAtIO GP.S (OPTIONi\L'') LATITUDE:ManON6ITUE Address at Well Location: �C)Tt{ 1 (AfJlw)ST Property Owner: T' , t (ESI i Subdivision Name: Mailing Address: " City/Town: `'�t tom( City/Town: �E C_I n streebaddress Assessors Map Assessors_L tk,� NOTE: Assessors Map and Lot # mandatory if no available Board of Health permit obtained: Yes �tAeeluir2cT1�— Permit Number - 01 D jsss e'd '� D 2.�VYORK'i?EREORMED � 3?PROPQS�DUSE;;"*�, „, * New Well ❑ Abandon ❑ Domestic ❑ Irrigation Cable '�❑jAuger f ❑ Deepen ❑ Recondition E Monitoring ❑ Municipal Air Hammer K Direct Push ❑ Re lace ❑ Other El ❑ Industrial ❑ Other Mud;f3o`[a ❑ Other— ,. Ir Unconsolidated Consolidated 6"SITEtSKE7CH,".(usey nam d �;m+-cy —Msjl ,.`-' H Q Permeability o m ry d E2 �R > 4.� cwvq From ft O TO ft O � Hi h g Low (J N C7 m Other Rock Type g 3 �rw %� YSTATE ' i�N�IvtS i ' t S'O:li1.4 ;r 4 MA T * C -m ( I 7:WELV'C0NSTRQCTI0N . ', 8 BASING Total Depth Drilled :From (ft) :To (ft) Casing Type; and Material Size O.D. (in) Well Seal Type Q ' ° fol,)1TE— Date Drilling Complete I -2 -OI 9 SCREEN. From (ft) To (ft) Slot Size „ Screen Type and Material Screen Diameter -010 66114G, PVC A 'r 10'FILTER.PACK/4GROt3T,l'ABANDONMENTGMATERIAL ,"f 4W1W9tjMVW, 11FACDfT[ONACrWELL=iNF.ORMATIONLV Y Developed? ❑Yes ❑ No From (ft) To (ft) Material Description Purpose Fracture Enhancement? ❑ Yes ❑ No Method Disinfected? El Yes EJNo 12- � �r-:� "f` A' a( ACA� eL 160 �. `� Cjl� S 12 WELL TESTiDATA`(PRODUCTLONLWELIS), "" �� E . , 13fSTATIC:WATERLEVEC,(ALVV14LS)g ti .. Yield ' Time Pumped Drawdown to Time Recovery to Depth Below Date Method (GPM(hrs'& min) (Ft. BGS) (hrs & min) (Ft. BGS) Dat Measured Ground Surface (FT) 14 PERMANENTzP,UMR (IF AV)11,L'"ABLE] t 3 a " 15. NAME ADDRESS OF IRUMP.INSTALLATION COMPANY Pump Description Horsepower Pump Intake Depth _ >b (ft) Nom net Pump Capacity (gpm) 16COMMEN#S 17WELLrDR1LtER'S`STATEMENT` This well was drilled and/or abandoned under my supervision, according to applicable rules and regulations, and this report is complete and correct to the best of my knowledge. Driller: Y % ' ` d Supervising Driller_ Signature: t 1019Registration 81 9I 7 IrU Firm: Date: 11 r 01 Rig Permit #: NOTE We[[FCompletion Reports must be filed, by the registered well driller -within 30 days of well.completion. 'ankon ne Ui:AI TN rnDV Cot 30 01 02:53p U STANLEY USOVICZ, JR. MAYOT Location Owner Address Joanne Soott Salem HCH 978 740 9705 CITY OF SALEM, MASSACHUSETTS BOARD OF HEALTH 120 WASHINCTON S'rRVET, 4TH FLOOR SALQM, MA 01970 TEL, 978=74 I -1800 (�(� � FAX 97T 745 0343 D FUS �{ JOANNE SCOTT; MPH, R5, CHO u HEALTH AGENT NUV 9 •2001 CITY OF SALEM HEALTH DEPT. WELL CONSTRUCTION PERMIT 9 South Mason Street Bay State Adhesives 9 South Mason Street This permit is granted in conformity with the statutes and ordinances relating to well permits. Well construction permits are non -transferable. This permit shall be on site at all times that work is taking place. Permit shall - expire one (1) year from the date of issuance unless revoked from cause. This permit does not constitute a Water Supply Certificate. Permit # Date issued (monitoring wells) 5-01 10/30/01 %Gd-� ealth Agent p.2 Massachusetts Department of Environmental Management 105152 Office of Water Resources TYPE OR PRINT ONLY Well Completion Report 1. WELL LOCATION 4,wj GPS (OPTIONAL) vA 'h: -'LATITUDE S m ar -. -="� : _ -' s LONGITUDES ""'` • - k - ` b r Address at Well Location: G :IYJTI-f MA�-40&) Property Owner:, PAY T' -r G At(E� I4�(S Subdivision Name: Mailing Address: t t lel !J wT CityfTown: �`l J �( City/Town: ��1t-kms 1 Assessors Map Assessorsl.ot-&NOTE: Assessors Map and Lot # mandatory if no st et address available Board of Health permit obtained: Yes .Not t a� o-� p equre��C� Permit Number �- ( D4*1" sued' f� t O 2. WORK PERFORMED v 3 PROPOSED USE I- - 4 DRILLING METHODS s' `- kj New Well ❑ Abandon ❑ Domestic ❑ Irrigation ❑ Cable`❑'Auger ❑ Deepen ❑ Recondition ®, Monitoring ❑ Municipal ❑ Air Hammer ,KJ' Direct Push ❑ Replace ❑Other El E:1 Other EJMud'Rota .❑ Other 5r WELVLOG '- - Q Q 2i Permeability High a Low 7J Unconsolidated o N N a g -je. m Other Consolidated Rock Type 6. SITE SKETCH (use Per'manem landmarks With -distances); s J 31r, w cel From (ft) To (ft) X r4 2 X 06AYSrt�� F(i)Nwe 5 2 ( 6 t CIW 7 I I 7. WELL CONSTRUCTION.' &CASING�s: Total Depth Drilled i From (ft) To (ft) Casing Type and Material Size O.D. (in) Well Seal Type Date Drilling Complete Q < ° I OAJ i �-2-i{{1ss ..:,�._''=gym.. 9. SCREEN= 2 ` _ r a- & a.s... v aR w— fi®_ .'..,;. �M � ".ci. £ s...-$'$ ' a.x`=3€"3 +°� .r�p=V From (ft) To (ft) Slot Size Screen Type and Material Screen Diameter o(o 1 6Q.fAo PVC 10. FILTER PACK/GROUT/ABANDONMENT MATERIAL „;jv? " As aass$` :mss 11 ADDITIONAL WELL'INFORMATION ' rr Developed? ❑ Yes ❑ No From (ft) To (ft) Material Description Qw Purpose Fracture Enhancement? ❑ Yes ❑ No Method Disinfected? ❑ Yes ❑ No 70) fAa#m a' �r `j 1 Imo(_ 12. WELL,TEST,DATA (PRODUCTION WELLS)b. r (a .n " T r *.mss v 13 STATIC, WATER LEVEL'(ALL` WELLS) Yield I dime Pumped Drawdown to Time Recovery to Depth Below Date Method (GPM) (hrs'& min) (Ft. BGS) (hrs & min) (Ft. BGS) Dat Measured Ground Surface (FT) E o 14. PERMANENT PUMP (IF AVAILABLE) ,„L 3f. -,!k_31 �. .' ,s v. � 15.NAME/ADDRESSOF,PUMP INSTALLATIONCOMPANYt„ Pump Descriptions ~� Horsepower Pump Intake Depth _ ° (ft) ` Nominal Pump Capacity (gpm) 16: COMMENTST L ``°' 17'WELL DRILLER'S STATEMENT" This well was drilled and/or abandoned under my supervision, according to applicable rules and regulations, and this report is complete and correct to the best of my knowledge. Driller: y Supervising Driller Signature: 1 Registration#:J SI �I 7i 1�1 , 0 1 IQ 1, 311 Firm: z Date:I r Rig Permit #: NOTE: Well Completion Reports must be filed by the registered well driller within 30 days of well completion. BOARD OF HEALTH COPY rpa ICEIVED �, tvoY 9 ,?.001 HEEALTH DEPT CITY OF SALEM, MASSACHUSETTS BOARD OF HEALTH 3 e 120 WASHINGTON STREET, 4TH FLOOR SALEM, MA 01970 TEL. 978-741-1800 FAX 978-745-0343 STANLEY USOVICZ, JR. ,JOANNE SCOTT; MPH, RS, CHO MAYOR HEALTH AGENT WELL CONSTRUCTION PERMIT Location 9 South Mason Street Owner Bay State Adhesives Address 9 South Mason Street .This permit is granted in conformity with the statutes and ordinances relating to well permits: Well construction permits are non -transferable. This permit shall be onsite at all times that work is taking place. Permit shall expire one (1) year from the date of issuance unless revoked from cause. This permit does not constitute a Water Supply Certificate. Permit # Date issued (monitoring wells) 5-01 10/30/01 6flealth Agent I Oct -29-01 02:43p Joanne Scott Salem.HOH 978 740 9705 1 p.2 JOANNE SCOTT, MPI I, RS, CHO HFAI TH AGENI Date: to 3b a t CITY OF SALEM BOARD OF HEALTH Salem, Massachusetts 01970 120 Washington Street 4"' floor Tel: (978) 741-isoo Fax: (978)745 0343 Well Construction Permit Application Fee: $40. Check payable to the City of Salem (no cash) n, MA. 01970 Tel. Type of well*. Well use: Well Contractor: t.esscrl Pump Contractor. Address: L4(. pr;Sfi ect I��r�u� N�q Address: Phone: qj8'-.-1T -L3c ' Phone: Reg. #: $43M Have abutters been notified? (y) How? _ ------------------------------------------------------------------------------------------------------- in the space provided below (or on back) show the location of the proposed well in relation to existing or proposed above or below ground structures. A description of visible prior and current land use within (200) feet of the proposed well location, which represent a potential source of contamination. q ".%-P\4 ln5'�\A To vl0. 'M<S -1ir�c . J \� �CO�t�a< �EW �"Tv\ 2 Coe os CTETWgD OCT .3 0 '1001 CITY OF SALEM HEALTH DEPT. �.-------------------- ---- ------ -- B.O.H, use only. Check #: '�' 3 V'0 Checkdate: lej3o/o, Permit#: 5 —oj • E WEB ENGINEERING ASSOCIATES, INC. 106 LONGWATER DRIVE. SUITE 1 NORWELL, MASSACHUSETTS 02061 617-878-7766 • FAX 617-878-8001 1-800-273-7289 BY FAX AND CERTIFIED MAIL Mr. Tom DiPersio MADEP/NERD Site Assessment Branch Ten Commerce Way Woburn, MA 01801 Dear Mr. DiPersio: January 13, 1994 FEE, 1994 CITY, OF. SALEM! 1HEAiyA DEPT.; RE: Interim Report Regarding Monitoring Well Sampling (August 1993) Bay State Adhesive Corporation j M4500% Q°= Salem, Massachusetts MADEP File No.: 3-3959 Web File No.: 92-E-011 As we discussed in our September 1993 telephone conversation, based on August 31, 1993 analytical data collected from the six (6) existing groundwater monitoring wells at the site, the need for a soil and groundwater treatment system appears to be not necessary at this time. Accordingly, these six (6) monitoring wells will be sampled quarterly for the next 12 month period to verify that these low levels persist at the site and to demonstrate that this sampling round was, not an anomaly. Groundwater from each monitoring well will be collected and analyzed for USEPA Method 8240 series compounds including acetone and MEK. Analytical testing will be conducted by Groundwater Analytical, Inc., a Massachusetts Certified Laboratory, located in Bass River, Massachusetts. On August 12, 1993 samples were collected and analyzed by Groundwater Analytical, Inc.. These results reported a significant decrease in the organic compound concentrations initially reported in our July 1992 analytical data. Testing data from subsequent sampling periods (December 1993, March 1994, July 1994, and December 1994) will be summarized and forwarded to you under separate cover. Should contaminant levels remain below applicable standards, Web Engineering will submit a Response Penofeum, Chemical Operations Engineering - Tank Alnnagement . Remedianon Sistems - Ha_ardoua. Solid 11'nsre Srslem.s - Site /rsresagunans - Regu6uort Compliance Action outcome Statement (RAOS) as provided under the newly • revised MCP. Should you have any questions or comments regarding this matter, please call me. MJD/mjd A:\BAYSTATE\JULY93.SAM cc: Mr. Michael DeGregorio, Bay State Adhesive Corporation Mr. Mark Casey, MADEP/NERD -Mr-,—Stephe M T hnson-, Salem Board of Health Mr. Frank Wright, ESQ, Wright & Moehrke • E Cl 11 VOLATILE of MONITOR TABLE 1 ORGANIC CONCENTRATIONS WELLS (AUGUST 31, 1993) MW -1 MW -2 MW -3 MW -4 MW -5 MW -6 ACETONE BRL BRL BRL BRL BRI, BRL 2-BUTANONE (MEK) BRL BRL BRL BRL BRL BRL BENZENE BRL BRL 38 BRL 3 7 CHLOROETHANE BRL BRL BRL BRL BRL BRL 1,1-DICHLOROPROPENE BRL BRL BRL BRL BRL BRL ETHYLBENZENE BRL BRL 32 BRL BRL 3 TOLUENE BRL BRL 71 47,000 BRL BRL 1,1,1 -TRICHLOROETHANE BRL BRL BRL BRL SRL BRL TOTAL XYLENE BRL BRL 118 BRL BRL 40 1,3,5-TRIMETHYLBENZENE BRL BRL 6 BRL BRL BRL 1,2,4-TRIMETHYLBENZENE BRL BRL 8 BRL BRL 4 1,1-DICHLOROETHANE BRL BRL BRL BRL 4 BRL 11 0 • • I ALTAR ANALY September 16, 1993 Groundwater Analytical, Inc. 228 Main Sten Buzzwas Bay. MA 02532 Talephone (508) 759.4441 FAX (508) 759.4475 Mr. Michael DeRosa WEB Engineering Associates, Inc. 106 Longwater Drive Norwell, MA 02061 Dear Mike: Enclosed are the Volatile Organic Analyses performed for the Bay State Adhesives project, number 92E011, sampled on 08-31-93. This project was processed for Standard Two Week turnaround. A brief description of the Quality Assurance/Quality Control procedures employed by Groundwater Analytical, and a statement of our state • certifications are contained within the report. This letter authorizes the release of the analytical results and should be considered a part of this report. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, 38440 Jonathan R. Sanford Vice President JRS cac Enclosures GROUNDWATER EPA METHOD 8260 Volatile Organics (GC/NS) Field ID: NW #1Lab Project: Bay State Adhesives/92E011 ID: 5888-01 Batch ID: VM2-0488-W Client: WEB Engineering 40ML VOA Vial/NaHSO4 Coot Sampled: 08-31-93 Cont/Prsv: Matrix: Aqueous Analyzed: 9-01-93 PARAMETER CONCENTRATTION REPORTING(LIIMIT Dichlorodifluoromethane BRL 10 10 Chloromethane BRL BRL 10 Vinyl Chloride BRL 10 Bromomethane BRL 10 Chloroethane Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL BRL 5 Methylene Chloride trans-12-Dichloroethene BRL 5 1,14Gl oroethane 5 cis-1,2-Dichloroethene 5 5 2,2-Dichloropropane BRL L 5 BRL 5 Bromochloromethane BRL 5 Chloroform • 1,1,1 -Trichloroethane BRL Carbon Tetrachloride 5 5BRL 1,1-Dichloropropene BRL 5 Benzene 1, 2-Dichloroethane BRL 5 Trichloroethene BRL 5 1,2-Dichloropropane BRL 5 Dibromomethane 5 cis-1,3-Dichloropropene 5 Bromodichloromethane BRL BRL Toluene trans-113-Dichloropropene BRL RL 5 -Trichloroethane 1,1,2 5 1,2-Dibromoethane (EDB) 5 Tetrachloroethene BRL BRL 5 1,3-Dichloropropane BRL 5 Dibromochloromethane BRL 5 Chlorobenzene 1,1,1,2 -Tetrachloroethane BRL 5 Ethylbenzene BRLBRL 5 ml Xylene BRL 5 o -Xylene BRL 5 Styrene Isopropylbenzene BRL 5 Bromobenzene 5 5 L 5 1,1,2,2 5 Bromoform -Tetrachloroethane BRL L 5 5 1,2,3-Trichloropropane BRL BRL 5 n-Propylbenzene (Continued) Page 1 of 2 GRDLJNDWATER ANALYTICAL volatile organiccs(GC/NS) Field ID: HW #1 Project: Bay State Adhesives/92E011 Lab ID: Batch ID: 5888-01 VN2-0488-W Client: WEB Engineering Analyzed: 09-13-93 PARAMETER CONCENTRATTI`N REPORTING(LIIMIT 2-Chlorotoluene BRL 5 5 1,3 5-Trimethylbenzene 4-C�lorotoluene BRL 5 tert-Butylbenzene BRL 5 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene BRL 5 4-Isopropyltoluene BRL 5 1,4 -Dichlorobenzene BRL 5 1,2 -Dichlorobenzene BRL n-Butylbenzene 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 5 1,2,4-Trichlorobenzene BRL 5 Hex achlorobutadiene BRL 5 Naphthalene 1,2,3-Trichlorobenzene BRL 5 50 Acetone * • BRL BRL 50 2-Butanone * QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 49 97 % 99 % 86 - 118 % 88 - 110 % Toluene -dB 50 4-Bromofluorobenzene 50 5o 51 102 % 86 - 115 % BRL - Below Reporting Limit. * Non -target compound. Method Reference: Method for Evaluating 10 Compounds by Gas Chromatography/Maas Spectranetry: Capillary Column Technique. Solid Vaste, US EPA SV -846, Third Edition (Revised 1990)• Page 2 of 2 • GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (BC/MS) Field ID: NN #2 Project: Bay State Adhesives/92E011 Lab ID: Batch ID: 5888-02 VM2-0488-V Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/WaHSO4 Cool Sampled: 08-31-93 09-01-93 9 01-93 Matrix: Aqueous Analyzed: PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 10 10 Chloromethane BRL BRL 10 Vinyl Chloride BRL 10 Bromomethane BRL 10 Chloroethane Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL 5 5 Methylene Chloride BRL BRL 5 trans-1,2-Dichloroethene 5 1,1-Dichloroethane BRL 5 2,2-Dichloropropane BRL BRL cis-1,2-Dichloroethene 5 Bromochloromethane BRL 5 Chloroform 1,1,1 -Trichloroethane BRL BRL 5 Carbon Tetrachloride BRL BRL 5 5 1,1-Dichloropropene 5 Benzene 1,2-Dichloroethane BRL BRLBSL Trichloroethene BRL 5 5 1,2-Dichloropropane BRL Oibromomethane cis-1,3-Dichloropropene 5 Bromodichloromethane BRL 5 BRL Toluene trans-1,3-Dichloropropene 1,1,2 BRL 5 -Trichloroethane BRL 5 1,2-Dibromoethane (EDB) 5 Tetrachloroethene BRL BRL 5 113-Dichloropropane BRL 5 Dibromochloromethane BRL 5 Chlorobenzene 1,1,1,2 -Tetrachloroethane BRL 5 Ethylbenzene BRLBRL 5 m+ -xylene BRL o -Xylene BRL 5 Styrene BRL Isopropylbenzene 5 Bromobenzene BRL BRL 5 Bromoform 1,1,2.2 -Tetrachloroethane BRL 5 1,2,3-Trichloropropane BRL BRL 5 n-Propylbenzene • (Continued) Page 1 of 2 6MLINGMTER ANALYTICAL volatile organics ATHOD 8260 Field ID: MW M2 Project: Bay State Adhesives/92E011 Client: WEB Engineering PARAMETER 2-Chlorotoluene 1,3 5-Trimethylbenzene 4-M orotoluene tert-Butylbenzene 1,2,4-Trimethylbenzens sec-Butylbenzene 1,3 -Dichlorobenzene 4-Isopro%ltoluene 1,4 -Dichlorobenzene 1,2 -Dichlorobenzene n-Butylbenzene 1,2-Dibromo-3-chloropr 1,2,4-Trichlorobenzene Hexachlorobutadiene Naphthalene • 1,2,3-Trichlorobenzene Acetone 2-Butanone QC SURROGATE COMPOUND Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene (DBCP) CONCENTRATION (ug/L) BRL BRL BRL BRL BRL BRL BRL BRL BR BRL BRL BRL BRL BRL BRL BRL Lab I0: 5888-02 Batch ID: VM2-0488-W Analyzed: 09-13-93 REPORTING LIMIT (ug/L) 5 5 5 5 5 5 5 5 5 5 5 5 5 5 50 50 SPIKED MEASURED RECOVERY QC LIMITS 5o 51 101 % 86 - 118 % 50 50 99 % 88 - 110 % 50 50 100 % 86 - 115 % BRL - Below Reporting Limit. * Non -target compound. Method Reference: Method 2st 60 - Volatile Evaluating Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Solid Waste, US EPA SW -646, Third Edition (Revised 1990). Page 2 of 2 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW M3 Project: Bay State Adhesives/92E011 Lab ID: 5888-03 Batch ID: VM2-0488-W Client: WE Engineering Sampled: 08-31-93 tont/Prsv: 4OmL VOA Vial/NaHSO4 Cool Received: 09-01-93 Analyzed: 09-13-93 Matrix: Aqueous PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 10 Chloromethane BRL 10 10 Vinyl Chloride BRL BRL 10 Bromomethane Chloroethane BRL 10 Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL 5 5 Methylene Chloride BRL 5 trans-1,2-Dichloroethene BRL 1,1-Dichloroethane BRL 5 2,2-Dichloropropane BRL 5 cis-1,2-Dichloroethene BRL 5 5 Bromochloromethane BRL Chloroform BRL 5 5 • 1,1 1 -Trichloroethane BRL BRL 5 Caron Tetrachloride 5 1,1-Dichloropropene BRL Benzene 38 5 5 1,2-Dichloroethane BRL Trichloroethene BRL 5 1,2-Dichloropropane BRL 5 Dibromomethane BRL 5 Bromodichloromethane BRL 5 cis-1,3-Dichloropropene BRL 5 Toluene trans-1,3-Dichloropropene 71 BRL 5 5 1,1,2 -Trichloroethane BRL 5 (EDB) BRL1,2-Dibromoethane Tetrachloroethene BRL 5 5 1 3-Dichloropropane Dibromochloromethane BRL BRL 5 Chlorobenzene BRL 5 5 1,1,1,2 -Tetrachloroethane BRL Ethylbenzene 32 5 5 m+ -Xylene o -Xylene 110 B Styrene Isopropylbenzene BRL L 5 5 Bromobenzene BRL BRL 5 5 Bromoform 1,1,2,2 -Tetrachloroethane BRL 5 1,2,3-Trichloropropane BRL 5 n-Propylbenzene BRL (Continued) Page 1 of 2 0 • GROUNDWATER ANALYTICAL Field ID: MW 93 Project: Bay State Adhesives/92E011 Client: WEB Engineering EPA METHOD 826U Volatile Organics (GC/MS) Lab ID: 5888-03 Batch ID: VN2-0488-W Analyzed: 09-13-93 PARAMETER CONCENTRATION (ug/L) 2-Chlorotoluene BRL 1,3 5-Trimethylbenzene 440 orotoluene 6 BRL Cert-Butylbenzene BRL 1,2,4-Trimethylbenzene 8BRL sec-Butylbenzene BRL 1,3 -Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,4 -Dichlorobenzene 1,2 -Dichlorobenzene BRL n-Butylbenzene 1,2-Dibromo-3-chloropropane (DBCP) BRL BRL 1,2,4-Trichlorobenzene BRL Nexachlorobutadiene RL Naphthalene BRL 1,2,3-Trichlorobenzene BRL Acetone * BRL RL 2-Butanone QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY Dibromofluoromethane 50 48 97 % Toluene -d8 50 49 97 % 4-Bromofluorobenzene 50 49 98 % REPORTING LIMIT (ug/L) 5 5 5 5 5 5 5 5 5 5 6 505 50 QC LIMITS 86 - 118 % 88 - 110 % 86 - 115 % BRL = Below Reporting Limit. " Non -target compound. Method Reference: Method 6260 - Volatile Organic . Compounds by Gas Chromatography/Mass Spectro,:etryu Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 9990). Page 2 of 2 • GROUNOWATER ANALYTICAL EPA METHOD 6260 Volatile Organics (GC/MS) Field ID: MW N4 Lab ID: 5888-04 Project: Bay State Adhesives/92E011 Batch ID: VM2-0488-W Client: WEB Engineering Sampled: 08-31-93 Cont/Prsv: 40mL VOA Vial/HaHSO4 Cool Received: 09-01-93 Matrix: Aqueous Analyzed: 09-13-93 -PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 5,000 Chloromethane BRL Vinyl Chloride BRL 5,000 Bromomethane BRL 5,000 Chloroethane BRL 5,000 Trichlorofluoromethane BRL 5,000 1,1-Dichloroethene BRL 2,500 Methylene Chloride BRL 2,500 trans-1,2-Dichloroethene BRL 2,500 1,1-Dichloroethane BRL 2,500 2 2-Dichloroppropane crs-1,2-_r %roethene BRL BRL 2,500 2,500 Bromochloomethane BRL 2,500 • Chloroform 1,1,1 -Trichloroethane BRL BRL 2,500 2,500 Carbon Tetrachloride BRL 2,500 1,1-Dichloropropene BRL 2,500 Benzene 'BRL 2,500 1,2-Oichloroethane BRL 2,500 Trichloroethene BRL 2,500 1 2-Dichloropropane BRL 2,500 Dibromomethane BRL 2,500 Bromodichloromethane BRL 2,500 cis-1,3-Dichloropropene BRL 21500 Toluene 47,000 2,500 trans-1,3-Dichloropropene BRL 2,50D 1,1,2 -Trichloroethane BRL 2,500 1,2-Dibromoethane (EDB) BRL 2,500 Tetrachloroethene BRL 2,500 1,3-Dichloropropane BRL 2,500 Dibromochloromethane BRL 2,500 Chlorobenzene 1,1,1,2,Tetrachloroethane BRL BRL 2,500 2,500 Ethylbenzene BRL 2,500 m+ -Xylene BRL 2,500 o -Xylene BRL BRL 2,500 2,500 Styrene Isopropylbenzene BRL 2,500 Bromobenzene BRL BRL 2,500 2,500 Bromoform 1,1,2,2 -Tetrachloroethane BRL 2,500 1,2,3-Trichloropropane BRL 2,500 500 n-Propylbenzene • (Continued) Page 1 of 2 -2E -E4 i_:-3 Pi+i ;G_:)rjNn7iATEF. .ANALYTICAL WEB 4475.;F 9,_� . GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW 64 Project: Bay State Adhesives/92E011 Lab ID: Batch ID: 5888-04 W Client: WEB Engineering Analyzed: 09213493 PARAMETER CONCENTRATION REPORTING (LIMIT 2-Chlorotoluene BRL 2,500 21500 2 Soo 1,3,5-Trimethylbenzene BRL 4-Chtorotoluene tert-Butylbenzene BRL 2,500 1,2,4-Trimethylbenzene BRL BRL 2,500 2,50D sec-Butylbenzene 1,3 -Dichlorobenzene BRL 2,500 4-Isopropyltoluene BRL BRL 2,500 2,500 1,4 -Dichlorobenzene 1,2 -Dichlorobenzene BRL 2,500 n-Butylbenzene BRL 2+500 1,2-Dibromo-3-chloropropane (DBCP) BRL 20500 1,2,4-Trichlorobenzene BRL 2,500 Hexachlorobutadiene BRL 2,500 Naphthalene 1,2,3-Trichlorobenzene BRL BRL 2,500 •500 Acetone * BRL BRL 25,000 25,000 2-Butanone QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 49 98 % 86 - 118 % Toluene -dB 50 49 91 % 88 - 110 % 4-Bromofluorobenzene 50 49 98 % 86 - 115 % Elevated reporting limit due to required sample dilution. BRL - Below Reporting Limit. * Non -target • compound. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Colunm Technique, Test Methods for Evaluating Solid Waste, US EPA SV -846, Third Edition (Revised 1990). Page 2 of 2 • GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW i5 Lab ID: 5888-05 Project: Bay State Adhesives/92EO11 Batch ID: VMZ-0488-W Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Sampled: 08-31-93 Received: 09-01-93 Matrix: Aqueous Analyzed: 09-13-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 10 Chloromethane BRL 10 Vinyl Chloride BRL BRL 10 10 Bromomethane Chloroethane BRL 10 Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL 5 Methylene Chloride BRL 5 trans-1,2-Dichloroethene BRL 5 1,1-Dichloroethane 4 2,2-Dichloropropane BRL 5 5 tis-1,2-Dichloroethene BRL Bromochloromethane BRL 5 • Chloroform 1,1,1 -Trichloroethane BRL BRL 5 5 Carbon Tetrachloride BRL 5 1,1-Dichloropropene BRL 5 Benzene 3 1,2-Dichloroethane BRL 5 Trichloroethene BRL 5 112-Dichloropropane BRL 5 Dibromomethane BRL 5 Bromodichloromethane BRL 5 cis-1,3-Dichloropropene BRL 5 Toluene trans-1,3-Dichloropropene BRL BRL 5 5 1,1,2 -Trichloroethane BRL 5 1,2-Dibromoethane (EDB) BRL 5 Tatrachloroethene BRL 5 1,3-Dichloropropane Dibromochloromethane BRL BRL 5 5 Chlorobenzene 1,1,1 2rTetrachlorcethane BRL BRL 5 5 Ethylbenzene BRL 5 w -Xylene o -Xylene BRL Styrene Isopropylbenzene BRL 5 Bromobenzene 5 5 Bromoform 1,1,2,2 -Tetrachloroethane BRL BRL 5 1,2,3-Trichloropropane BRL 5 5 n-Propylbenzene BRL • (Continued) Page 1 of 2 1-46-35 _ ?M , 3nr'JP: JIAIE2. ANALI-!C;,- VER z-.-::[1_.'15 d 0 GROLNVOWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (6C/NS) Field ID: MW N5 Lab ID• 5888-05 Project: Bay State Adhesives/92EO11 Batch 10: Client: WEB Engineering Analyzed: 091393-W PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 1,3 5-Trimethylbenzene BRL 5 5 4-C�llorotoluene tert-Butylbenzene BRL 5 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL BRL 5 1,3 -Dichlorobenzene 4-Isopro%ltoluene BRL BRL 1,4 5 -Dichlorobenzene 5 1,2 -Dichlorobenzene BRL 5 n-Butylbenzene BRL 5 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 1,2,4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL 5 Naphthalene BRL BRL 5 1,2,3-Trichlorobenzene 50 • Acetone * BRL BRL 50 2-Butanone * QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 51 102 % 86 - 118 % Toluene -d8 50 50 101 % 88 - 110 % 4-Bromofluorobenzene 50 50 100 % 86 - 115 % 1 = Analyte detected below the reporting limit. Analyte result is an estimate- BRL Below Reporting Limit. * Non -target compound. Method Reference: Method 826D - Volatile Organic Compounds by Gas Chromatography/Masa Spectrometry: Capillary Column Technique, Teat Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: NV #6 Lab ID: 5888-06 Project: Bay State Adhesives/92E0ll Batch ID: VM2-04884 Client: VEB Engineering Sampled: 08-31-93 09-01-93 Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Received: Matrix: Aqueous Analyzed: 09-13-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 10 Chloromethane BRL 10 Vinyl Chloride BRL 10 Bromomethane BRL 10 Chloroethane BRL 10 Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL 5 Methylene Chloride BRL 5 trans -1 2-Dichloroethene BRL BRL 5 5 1,1-Dir.Ailoroethane 2,2-Dichloropropane BRL 5 cis-1,2-Dichloroethene BRL 5 Bromochloromethane BRL 5 Chloroform BRL 5 1,1 1 -Trichloroethane BRL 5 Car;on Tetrachloride BRL 5 1,1-Dichloropropene BRL 5 Benzene 7 5 1,2-Dichloroethane BRL 5 Trichloroethene BRL 5 1,2-Dichloropropane BRL 5 Dibromomethane BRL 5 Bromodichloromethane BRL 5 cis-1,3-Dichloropropene BRL 5 Toluene BRL 5 trans-1,3-Dichloropropene BRL 5 1,1,2 -Trichloroethane BRL 5 1,2-Dibromoethane (EDB) BRL 5 Tetrachloroethene BRL 5 1,3-Dichloropropane BRL 5 Dibromochloromethane BRL 5 Chlorobenzene BRL 5 1,1,1 2.Tetrachlorcethane Ethylenzene BRL 3 5 j m+pp-Xylene 40 BRL 5 0-J�ylene Styrene BRL 5 Isopropylbenzene BRL 5 Bromobenzene BRL 5 Bromoform BRL 5 1,1,2,2 -Tetrachloroethane BRL 5 1,2,3-Trichloropropane BRL 5 n-Propylbenzene BRL 5 (Continued) Page 1 of 2 __.b3 eM p GROUNDWATER ANALYTICAL EPA METHOD 8260 volatile Organics (GC/MS) Field ID: MW Y6 Project: Bay State Adhesives/92E011 Lab ID: Batch ID: 5888-06 VM2-0488-V Client: VEB Engineering Analyzed: 09-13-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 5 1,3,5-Trimethylbenzene BRL 5 4-Chlorotoluene BRL 5 tert-Butylbenzene 4 j 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene 4 -Isopropyl tol uene BRL 5 1,4 -Dichlorobenzene BRL n-Butyylbenzene 1,2 -Dichlorobenzene 5 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 5 1,2.4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL Naphthalene 1,2,3-Trichlorobenzene BRL 5 Acetone * is BRL BRL 50 50 2-Butanone QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 51 51 102 % 101 % 86 - 118 % 88 - 110 % Toluene -d8 50 4-Bromofluorobenzene 50 51 101 % 86 - 115 % J . Analyte detected below the reporting limit. Analyte result is an estieete. BRL - Below Reporting Limit. * Non -target canpound. Method Reference: Method 8260 - WelaLlle Organic Compounds by Gas Chromatography/Mese Spectrometry: Capillary Cal" Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 N I NAtYTICAAt� rr PM)ect Name: ��,} tiAN 4rMt AVk4vIA �� PiDNumber. N SemWer Name• . 1Im(AAa, J - PAA 2211 Main St'eet CHAIN -OF -CUSTODY ItrEA LI Boa=rds Bay. MA 02532 (506 Telephone ) 758-4441 AND WORK ORDER FAX (608) 7694475 Yyypp � ��,.y�p�p,'� TURNAROUND ,w 1`��"e gfANDARD p0 Husinsea Days) s keas: ❑ PROORIIY (5 bignem Do") C $ ao0 I(NP fgrv��C O RUSH (RAN- g� t 13°118 Zip: INw• •9+� nr'101r'�°n 60 — ��A n�tu Please FAX ❑YES NO C NA 4l W t P ( FA)( Number. RAW//� n t j 618 710Y BILLING . INMUCRONS: Use sepmale line for own corawner (accept duplicates)• Purcaase Order No: MWh Contalnet(s) Pleaeroratlon Faeces l, I I U IDENTIflt: Vm 6 JIlSAMPLE ` q s _ 3 (I 3 d IFWMAKS // SPECIAL INS RUCRONS kp7q j4 aid DUPLICATES / T� -- ",yc ::rqjtw % MorM �brorY I�ro eM BA meaoea maws p eism epeclM nm• a ` � lose arms d areprieli eamPw Exn !,^-�y�� ....�t��yyyy � W ��F1'.r�l (" , M&MSD wwumoadupkaw amw■a sn addmonal sample w4.nt . `I(o �t'l�'�I U YESL M � °dap=$ em BAI 6iM4nMto,) "pgU��n� W 1v lN' W o ND. Pwass dp a7. wimp a PMax el0pl Reu°p°b�4Me mMe&ndMySeiDr tam.( sMamle pra ' =1(114T n'110 LAUBUOMMTM OM 0.0 um Orm ANALYSIS REOUEST a 0 a aria C11111N-0F•CUSWDY RECORD '� ,� 1 ; / l/3R l N! 8314 SMpph*&u ie NwMm: 9 0 is WEB ENGINEERING ASSOCIATES, INC. 106 LONGWATER DRIVE, SUITE 4 NORWELL, MASSACHUSETTS 02061 617-878-7766 • FAX 617-878-8004 1-800-273-7289 BY FAX AND CERTIFIED MAIL Mr. Tom DiPersio MADEP/NERD Site Assessment Branch Ten Commerce Way Woburn, MA 01801 Dear Mr. DiPersio: 13, 1994 FEB 1 <: 1994 CITY OF SALEM HEALTH DEPT. RE: Analytical Testing Results (December 1993) j,,,,"$,—Bay State Adhesive Corporation 'Ia�onY Salem, Massachusetts MADEP File No.: 3-3959 Web File No.: 92-E-011 As mentioned in the August, 1993 Interim Report, the existing six (6) monitoring wells at Bay State Adhesive Corporation will be sampled quarterly. On December 8, 1993 samples were collected and analyzed for volatile organic compounds (vocs) by USEPA Method 8240 including MEK and acetone by Ground Water Analytical, Inc. These results follow in Table 1. These data continue to report values below MCP Method 1 standards for GW -2 groundwater categories. Should you have any questions or comments regarding this matter, please call me. Very truly yours, Web Engineering Ass ciates, Inc. John C. Gaudet, r. Assistant Engineer Petroleum, Chemical Operations Engineering - Tank Management - Remediation Systems - Hazardous. Solid Waste Systems - Site Imestigations - Regulatory Compliance • JCG\j cg B:\BAYSTATE\DEC93.SAM cc: Mr. Michael DeGregorio, Bay State Adhesive Corporation Mr. Mark Casey, MADEP/NERD .-M�-.-- St—spho^ M '^h*&on Salem, Board of Health Mr. Frank Wright, ESQ, Wright & Moehrke • 0 0 TABLE 1 VOLATILE ORGANIC CONCENTRATIONS of MONITOR WELLS (December 8, 1993) MW -1 MW -2 MW -3 MW -4 MW -5 MW -6 ACETONE BRL BRL BRL BRL BRL - BRL 2-BUTANONE (MEK) BRL BRL BRL BRL BRL BRL BENZENE BRL. 4 7 BRL 10 3 CHLOROETHANE BRL BRL BRL BRL BRL BRL 1,1-DICHLOROPROPENE BRL BRL BRL BRL BRL BRL ETHYLBENZENE BRL 3 BRL BRL BRL 3 TOLUENE 13 24 40 20,000 6 22 1,1,1 -TRICHLOROETHANE BRL BRL BRL BRL BRL BRL TOTAL XYLENE 11 16 19 BRL BRL 16 1,3,5-TRIMETHYLBENZENE BRL BRL 4 BRL SRL BRL 1,2,4-TRIMETHYLBENZENE BRL BRL 6 BRL BRL BRL 0 0 ANALYTIC 0 • • GROUNDWATER Groundwater Analytical, Inc. 228 Main Street 4 w Buzzards Bay, MA 02532 ANALYTICAL Telephone (508) 759-4441 FAX (508) 759-4475 December 23, 1993 Mr. Michael DeRosa WEB Engineering Associates, Inc. 106 Longwater Drive Norwell, MA 02061 Dear Mike: Enclosed are the Volatile Organic Analyses performed for the Bay State Adhesys project, number 92E011, sampled on 12-08-93. This project was processed for Standard Two Week turnaround. A brief description of the Quality Assurance/Quality Control procedures employed by Groundwater Analytical, and a statement of our state certifications are contained within the report. This letter authorizes the release of the analytical results and should be considered a part of this report. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, Z 1r07ik. Jonathan R. Sanford Vice President JRS/cac Enclosures 0 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) (Continued) Page 1 of 2 Field ID: MW #1 Lab ID: 6604-01 Project: Bay State Adhesys/92EO11 Batch ID: VM2-0571-W Client: WEB Engineering Sampled: 12-08-93 Cont/Prsv: 40mL VOA Vial/NaHSO4 C001 Received: 12-09-93 Matrix: Aqueous Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) Dichlorodifluoromethane BRL 10 Chloromethane BRL 10 Vinyl Chloride BRL 10 Bromomethane BRL 10 Chloroethane BRL 10 Trichlorofluoromethane BRL 10 1,1-Dichloroethene BRL 5 Methylene Chloride BRL 5 trans-1,2-Dichloroethene BRL 5 1,1-Dichloroethane BRL 5 2,2-Dichloropropane BRL 5 cis-1,2-Dichloroethene BRL 5 Bromochloromethane Chloroform BRL BRL 5 5 1,1,1 -Trichloroethane BRL 5 Carbon Tetrachloride BRL 5 1,1-Dichloropropene BRL 5 Benzene BRL 5 1,2-Dichloroethane BRL 5 Trichloroethene BRL 5 1,2-Dichloropropane BRL 5 Dibromomethane BRL 5 Bromodichloromethane BRL 5 cis-1,3-Dichloropropene BRL 5 Toluene 13 5 trans-1,3-Dichloropropene BRL 5 1,1,2 -Trichloroethane BRL 5 1,2-Dibromoethane (EDB) BRL 5 Tetrachloroethene BRL 5 1,3-Dichloropropane BRL 5 Dibromochloromethane BRL 5 Chlorobenzene BRL 5 1,1,1,2 -Tetrachloroethane BRL 5 Ethylbenzene BRL 5 m+p-Xylene 8 5 o -Xylene 3 j 5 Styrene BRL 5 Isopropylbenzene BRL 5 Bromobenzene BRL 5 Bromoform BRL 5 1,1,2,2 -Tetrachloroethane BRL 5 1,2,3-Trichloropropane BRL 5 n-Propylbenzene BRL 5 (Continued) Page 1 of 2 GROUNDWATER • ANALYTICAL Volatile OrEPA ganics (GC/MS) Field ID: MW #1 Lab ID: 6604-01 Project: Bay State Adhesys/92E011 Batch ID: VM2-0571-W Client: WEB Engineering Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 1,3,5-Trimethylbenzene BRL 5 4-Chlorotoluene BRL 5 tert-Butylbenzene BRL 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene BRL 5 4-Isopro%ltoluene BRL 5 1,4 -Dichlorobenzene BRL 5 1,2 -Dichlorobenzene BRL 5 n-Butylbenzene BRL 5 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 1,2,4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL 5 Naphthalene BRL 5 1,2,3-Trichlorobenzene BRL 5 Acetone * BRL 50 2-Butanone * BRL 50 QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 50 100 % 86 - 118 % Toluene -d8 50 53 105 % 88 - 110 % 4-Bromofluorobenzene 50 50 100 % 86 - 115 % j = Analyte detected below the reporting limit. Analyte result is an estimate. BRL = Below Reporting Limit. * Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 9 • 0 GROUNDWATER ANALYTICAL Field ID: MW #2 Project: Bay State Adhesys/92E011 Client: WEB Engineering Cant/Prsv: 40mL VOA Vial/NaHSO4 Cool Matrix: Aqueous PARAMETER Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 212-Dichloropropane cis-1,2-Dichloroethene Bromochloromethane Chloroform 1,1,1 -Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,2-Dibromoethane (EDB) Tetrachloroethene 1,3-Dichloropropane Dibromochloromethane Chlorobenzene 1,1,1,2 -Tetrachloroethane Ethylbenzene m+p-Xylene o -Xylene Styrene Isopropylbenzene Bromobenzene Bromoform 1,1,2,2 -Tetrachloroethane 1,2,3-Trichloropropane n-Propylbenzene CONCENTRATION (ug/L) 24 3 11 5 EPA METHOD 8250 Volatile Organics (GC/MS) BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-02 Batch ID: VM2-0571-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-16-93 REPORTING LIMIT (ug/L) 10 10 10 10 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 (Continued) Page 1 of 2 GROUNDWATER ANALYTICAL EPA OD 8260 Volatile Organics (GC/MS) Field ID: MW #2 Lab ID: 6604-02 Project: Bay State Adhesys/92E011 Batch ID: VM2-0571-W Client: WEB Engineering Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 1,3,5-Trimethylbenzene BRL 5 4-Chlorotoluene BRL 5 tert-Butylbenzene BRL 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene BRL 5 4-Isopro%ltoluene BRL 5 1,4 -Dichlorobenzene BRL 5 1,2 -Dichlorobenzene BRL 5 n-Butylbenzene BRL 5 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 1,2,4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL 5 Naphthalene BRL 5 1,2,3-Trichlorobenzene BRL 5 • Acetone * BRL 50 2-Butanone * BRL 50 QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 52 103 % 86 - 118 % Toluene -d8 50 54 109 % 88 - 110 % 4-Bromofluorobenzene 50 51 101 % 86 - 115 % j = Analyte detected below the reporting limit. Analyte result is an estimate. BRL = Below Reporting Limit. x Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 0 C� • GROUNDWATER ANALYTICAL Field ID: MW #3 Project: Bay State Adhesys/92E011 Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Matrix: Aqueous PARAMETER Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 2,2-DichloroPropane cis-1,2-Dich%roethene Bromochloromethane Chloroform 1,1,1 -Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,2-Dibromoethane (EDB) Tetrachloroethene 1,3-Dichloropropane Dibromochloromethane Chlorobenzene 1,1,1,2 -Tetrachloroethane Ethylbenzene m+p-Xylene o -Xylene Styrene Isopropylbenzene Bromobenzene Bromoform 1,1,2,2 -Tetrachloroethane 1,2,3-Trichloropropane n-Propylbenzene CONCENTRATION (ug/L) 40 19 EPA METHOD 8260 Volatile Organics (GC/MS) BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-03 Batch ID: VM2-0571-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-16-93 REPORTING LIMIT (ug/L) 10 10 10 10 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 (Continued) Page 1 of 2 0 0 GROUNDWATER ANALYTICAL Field ID: MW #3 Project: Bay State Adhesys/92E011 Client: WEB Engineering PARAMETER 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene tert-Butylbenzene 1,2,4-Trimethylbenzene sec-Butylbenzene 1,3 -Dichlorobenzene 4-Isopro%ltoluene 1,4 -Dichlorobenzene 1,2 -Dichlorobenzene n-Butylbenzene 1,2-Dibromo-3-chloropropane (DBCP) 1,2,4-Trichlorobenzene Hexachlorobutadiene Naphthalene 1,2,3-Trichlorobenzene Acetone * 2-Butanone QC SURROGATE COMPOUND Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene EPA METHOD 8260 Volatile Organics (GC/MS) Lab ID: 6604-03 Batch ID: VM2-0571-W Analyzed: 12-16-93 CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) BRL 5 4 j 5 BRL 5 BRL 5 6 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 5 BRL 50 BRL 50 SPIKED MEASURED RECOVERY QC LIMITS 50 51 103 % 86 - 118 50 54 108 % 88 - 110 50 50 100 % 86 - 115 j = Analyte detected below the reporting limit. Analyte result is an estimate. BRL = Below Reporting Limit. - Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 GROUNDWATER ANALYTICAL Field ID: MW #4 Project: Bay State Adhesys/92E011 Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Matrix: Aqueous PARAMETER CONCENTRATION (ug/L) 20,000 EPA METHOD 8260 Volatile Organics (GC/MS) BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-04 Batch ID: VM2-0572-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-17-93 REPORTING LIMIT (ug/L) 1,000 1,000 1,000 1,000 1,000 1,000 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 (Continued) Page 1 of 2 Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 2,2-Dichloroppropane cis-1,2-Dich%roethene Bromochloromethane Chloroform 1,1,1 -Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,2-Dibromoethane (EDB) Tetrachloroethene 1,3-Dichloropropane Dibromochloromethane Chlorobenzene 1,1,1,2 -Tetrachloroethane Ethylbenzene m+p-Xylene o -Xylene Styrene Isopropylbenzene Bromobenzene Bromoform 1,1,2,2 -Tetrachloroethane . 1,2,3-Trichloropropane n-Propylbenzene CONCENTRATION (ug/L) 20,000 EPA METHOD 8260 Volatile Organics (GC/MS) BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-04 Batch ID: VM2-0572-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-17-93 REPORTING LIMIT (ug/L) 1,000 1,000 1,000 1,000 1,000 1,000 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 500 (Continued) Page 1 of 2 0 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW #4 Lab ID: 6604-04 Project: Bay State Adhesys/92EO11 Batch ID: VM2-0571-W Client: WEB Engineering Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 500 1,3,5-Trimethylbenzene BRL 500 4-Chlorotoluene BRL 500 tert-Butylbenzene BRL 500 1,2,4-Trimethylbenzene BRL 500 sec-Butylbenzene BRL 500 1,3 -Dichlorobenzene BRL 500 4-Isopropyltoluene BRL 500 1,4 -Dichlorobenzene BRL 500 1,2 -Dichlorobenzene BRL 500 n-Butylbenzene BRL 500 1,2-Dibromo-3-chloropropane (DBCP) BRL 500 1,2,4-Trichlorobenzene BRL 500 Hexachlorobutadiene BRL 500 Naphthalene BRL 500 1,2,3-Trichlorobenzene BRL 500 Acetone * BRL 5,000 2-Butanone * BRL 5,000 QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 48 95 % 86 - 118 Toluene -d8 50 49 97 % 88 - 110 4-Bromofluorobenzene 50 45 89 % 86 - 115 Elevated reporting limit due to required sample dilution. BRL = Below Reporting Limit. * Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 • 0 GROUNDWATER ANALYTICAL Field ID: MW #5 Project: Bay State Adhesys/92E011 Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Matrix: Aqueous PARAMETER Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 2,2-Dichloropropane cis-1,2-Dichloroethene Bromochloromethane Chloroform 1,1,1 -Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,2-Dibromoethane (EDB) Tetrachloroethene 1,3-Dichloropropane Dibromochloromethane Chlorobenzene 1,1,1,2 -Tetrachloroethane Ethylbenzene m+p-Xylene o -Xylene Styrene Isopropylbenzene Bromobenzene Bromoform 1,1,2,2 -Tetrachloroethane 1,2,3-Trichloropropane n-Propylbenzene EPA METHOD 8260 Volatile Organics (GC/MS) CONCENTRATION (ug/L) 10 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-05 Batch ID: V142 -0571-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-16-93 REPORTING LIMIT (ug/L) 10 10 10 10 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 (Continued) Page 1 of 2 • BRL = Below Reporting Limit. " Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW #5 Lab ID: 6604-05 Project: Bay State Adhesys/92E011 Batch ID: VM2-0571-W Client: WEB Engineering Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 1,3,5-Trimethylbenzene BRL 5 4-Chlorotoluene BRL 5 tert-Butylbenzene BRL 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene BRL 5 4-Isopropyltoluene 1,4 -Dichlorobenzene BRL BRL 5 5 1,2 -Dichlorobenzene BRL 5 n-Butylbenzene BRL 5 1,2-Dibromo-3-chloropropane (DBCP) BRL 5 1,2,4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL 5 Naphthalene BRL 5 • 1,2,3-Trichlorobenzene Acetone * BRL BRL 5 50 2-Butanone * BRL 50 QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 50 100 % 86 - 118 Toluene -d8 50 54 109 % 88 - 110 4-Bromofluorobenzene 50 51 101 % 86 - 115 • BRL = Below Reporting Limit. " Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 0 GROUNDWATER ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW #6 Project: Bay State Adhesys/92EO11 Client: WEB Engineering Cont/Prsv: 40mL VOA Vial/NaHSO4 Cool Matrix: Aqueous PARAMETER Dichlorodifluoromethane Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene Chloride trans-1,2-Dichloroethene 1,1-Dichloroethane 2,2-Dichloropropane cis-1,2-Dichloroethene Bromochloromethane Chloroform 1,1,1 -Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,2-Dibromoethane (EDB) Tetrachloroethene 1,3-Dichloropropane Dibromochloromethane Chlorobenzene 1,1,1,2 -Tetrachloroethane Ethylbenzene m+p-Xylene o -Xylene Styrene Isopropylbenzene Bromobenzene Bromoform 1,1,2,2 -Tetrachloroethane 1,2,3-Trichloropropane n-Propylbenzene CONCENTRATION (ug/L) 22 3 11 5 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Lab ID: 6604-06 Batch ID: VM2-0571-W Sampled: 12-08-93 Received: 12-09-93 Analyzed: 12-16-93 REPORTING LIMIT (ug/L) 10 10 10 10 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 (Continued) Page 1 of 2 GROUNDWATER . ANALYTICAL EPA METHOD 8260 Volatile Organics (GC/MS) Field ID: MW #6 Lab ID: 6604-06 Project: Bay State Adhesys/92EO11 Batch ID: VM2-0571-W Client: WEB Engineering Analyzed: 12-16-93 PARAMETER CONCENTRATION REPORTING LIMIT (ug/L) (ug/L) 2-Chlorotoluene BRL 5 1,3,5-Trimethylbenzene BRL 5 4-Chlorotoluene BRL 5 tert-Butylbenzene BRL 5 1,2,4-Trimethylbenzene BRL 5 sec-Butylbenzene BRL 5 1,3 -Dichlorobenzene BRL 5 4-Isopro%ltoluene BRL 5 1,4 -Dichlorobenzene BRL 5 1,2 -Dichlorobenzene BRL 5 n-Butylbenzene BRL 5 1,2-Dibromo-3-chloropropane (OBCP) BRL 5 1,2,4-Trichlorobenzene BRL 5 Hexachlorobutadiene BRL 5 Naphthalene BRL 5 1,2,3-Trichlorobenzene BRL 5 Acetone * BRL 50 2-Butanone * BRL 50 QC SURROGATE COMPOUND SPIKED MEASURED RECOVERY QC LIMITS Dibromofluoromethane 50 51 102 % 86 - 118 % Toluene -d8 50 54 108 % 88 - 110 % 4-Bromofluorobenzene 50 52 104 % 86 - 115 % j = Analyte detected below the reporting limit. Analyte result is an estimate. BRL = Below Reporting Limit. * Non -target analytes. Method Reference: Method 8260 - Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry: Capillary Column Technique, Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1990). Page 2 of 2 S N V SAMPLE e 5 j .IDENTIFICATION < < - rs a 3 z o � �(a.�•�, �.ru ►� 1 PM =I 2I §XI +I U LABORATORY NUMBER m t i (Lob Use Only) a ° V U 228 Main Street CHAIN -W CUSTODY RECORD GROUNDWATER Buzzards Bay, MA 02532 AND WORK ORDER any regulatory Programa and EPA ethods require Project apxifie meNIs ouPlicatea ANALYTICAL Telephone (508) 759-4441 FAX (508) 759-4475 Date aivolellke PeWHerbRM TURNAROUND Project Name: M. 2k �LhL` �I Firm: w� OJ610 �l`lS, rA STANDARD (10 Business Days) v0 € Project Number: `w Address: /1 p 11'' 0VLJ\j'ii '�1�' ❑ PRIORITY (5 Business Days) RUSH (RAN- _ 00 (y v✓/ ( (p� t7K/�W� ❑ (Rush re Im Hush Fuaarorbaaen Number) w ° Sampler Name: City / State I zip: N�wya?, M4 0��I please FAX ❑ YES VLNO ° ° FAX Number: YES. Meese perform a PmJW apxlncRelin MSDor sample dupilcate above❑ Project Manager. Telephone: wi ^^ ! 1 BILLING `3 N w o ❑ o° NO. Please do rmt perform a prWectral specific MS. MSD or semDle Met od of Shipment: No: ❑ EXPress I ❑ Expr INSTRUCfIONS:Use seperele line for t d each container (except duplicates). Purchase Order 0 (JPS ❑ Hand Metrix Contalner(s) Preservation Flaered 'z o _ .. S N V SAMPLE e 5 j .IDENTIFICATION < < - rs a 3 z o � �(a.�•�, �.ru ►� 1 PM =I 2I §XI +I U LABORATORY NUMBER m t i (Lob Use Only) a ° V U 0 CHAIN -OF -CUSTODY RECORD SPECIAL IJIONSSPIKES rnwc.....��,...._ _. _ _ and DUPLICATES a 6251 771 any regulatory Programa and EPA ethods require Project apxifie meNIs ouPlicatea _ ANALYSIS REQUEST Date aivolellke PeWHerbRM andbr wrix spike(MS). matAX011kedupliceto r§lit. ,,.A M(Ui./(q q �r tp'V(�MSO)eMsample vY1wP'eEecP duplicate ehouE be Reli wishedendsampleduplicaterequires De Time ReceNed bY: 013 YES. Meese perform a PmJW apxlncRelin MSDor sample dupilcate above❑ �,n❑ ate borato❑ Time R elved by ryMS, Cooler Serial Number.requested ❑ o° NO. Please do rmt perform a prWectral specific MS. 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(JPS ❑ Hand 13 GROUNDWATER ,9 ANALYTICAL go QUALITY ASSURANCE QA/QC Program Statement Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA SW -846, Third Edition (Revised 1992). Quality Control protocols include Standard Operating Procedures (SOPS) developed for each analytical method. SOPS are derived from US EPA methodologies and other established references. Equipment and facility maintenance conform to Good Laboratory Practices(GLPs). Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one calibration standard, one method blank, one laboratory control sample, and one matrix spike and one sample duplicate for each sample batch. All samples, standards, blanks, laboratory control samples and matrix spikes are spiked with internal standards and surrogate compounds. GC/MS systems are tuned to BFB ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one calibration standard, one method blank, one laboratory control sample, one matrix spike and one sample duplicate for each sample batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples which are analyzed together with the same method sequence and the same lots of reagents and with the same manipulations common to each sample within the same continuum of time within a 24 hour period. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliqot of sodium sulfate. Method Blanks are taken through all the appropriate steps of an analytical method. Sample data reported is not corrected for blank contamination. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target compounds representative of the method analytes. Accuracy is defined as the degree of agreement of a measured value with the true or expected value. Percent Recoveries for the Laboratory Control Sample are calculated to assess accuracy. Surrogate Compounds are used to assess the effectiveness of the method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to organic analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound.