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Brownfields Program Quality Assurance Project Plan
City of Salem
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Former FlynnTan Manufacturing Company Site
70-92 Boston Street
and
61 Ward Street Site
Salem,Massachusetts
g
April 2004
T Prepared By:
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TRC Environmental Corporation
h Boott Mill's South.
Foot of John Street
Lowell, MA 01852
(978)970-5600
'A_Y.
TRC
Customer-Focused Solutions
TRC Reference Number: 28367-0010-00000
April 29, 2004
Mr. Alan Peterson
US EPA Region 1
11 Technology Drive
North Chelmsford, MA 01863-2431
Subject: Brownfields Program Quality Assurance Project Plan (Revision 0)
Former F1ynnTan Site, 70-92 Boston Street and
61 Ward Street Site
Salem, Massachusetts
Dear Alan:
On behalf of the City of Salem, TRC Environmental Corporation is pleased to submit this Quality
Assurance Project Plan for the above-referenced properties for your review and approval.
If you have any questions, please contact either of the undersigned at 978-970-5600.
Sincerely,
Amy'Stattel Paul Arnold
Project Engineer Project Manager
Enclosure
cc: Kate Gormly, City of Salem
Joonu Andrews, EPA
TRC Project File
Boott Mills South, Foot of John Street • Lowell, Massachusetts 01852
Telephone 978-970-5600 • Fax 978-453-1995
Brownfields Program Quality Assurance Project Plan
City of Salem
Former F1ynnTan Manufacturing Company Site
70-92 Boston Street
and
61 Ward Street Site
Salem, Massachusetts
April 2004
Prepared By:
TRC Environmental Corporation
Boott Mills South
Foot of John Street
Lowell, MA 01852
(978) 970-5600
TABLE OF CONTENTS
1.0 APPENDIX A......................................................... ..... 1
1.1 Title and Approval Page................................................................................................ 1
2.0 APPENDIX B .....................................................................................................................2
2.1 Project Organization and Responsibility.......................................................................2
3.0 APPENDIX C......................................................................................................................4
3.1 Problem Definition............................................. ......4
4.0 APPENDIX D.....................................................................................................................6
4.1 Project Description........................................................................................................6
4.2 Project Timeline.......................................................................................................... 17
5.0 APPENDIX E.............................................................................................................._..... 18
5.1 Sampling Design......................................................................................................... 18
5.2 Equipment Decontamination Procedures.................................................................... 19
6.0 APPENDIX F....................................................................................................................21
6.1 Sampling and Analytical Methods Requirements.......................................................21
6.2 Method and SOP References.......................................................................................26
7.0 APPENDIX G...................................................................................................................27
7.1 Preventative Maintenance—Field Equipment ............................................................27
8.0 APPENDIX H...................................................................................................................29
8.1 Calibration and Corrective Action—Field Equipment................................................29
9.0 APPENDIX I.....................................................................................................................30
9.1 Preventative Maintenance—Laboratory Equipment....................................................30
10.0 APPENDIX J.................................................:...................................................................31
10.1 Calibration and Corrective Action—Laboratory Equipment......................................31
11.0 APPENDIX K...................................................................................................................34
11.1 Sample Handling and Custody Requirements.............................................................34
11.1.1 Field Sampling Operations........................
11.1.2 Sample Identification............................................................................................37
11.2 Laboratory Operations.................................................................................................39
12.0 APPENDIX L....................................................................................................................40
12.1 Analytical Precision, Accuracy and Sensitivity..........................................................40
13.0 APPENDIX M...................................................................................................................49
13.1 Field Quality Control Requirements...........................................................................49
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14.0 APPENDIX N...................................................................................................................50
14.1 Data Management and Documentation.......................................................................50
14.1.1 Field Log Book Records........................................................................................50
14.1.2 Laboratory Data Package Deliverables .................................................................50
15.0 APPENDIX O...................................................................................................................51
15.1 Assessment and Response Actions .............................................................................51
16.0 APPENDIX P....................................................................................................................53
16.1 Project Reports............................................................................................................53
17.0 APPENDIX Q...................................................................................................................54
17.1 Data Evaluation...........................................................................................................54
18.0 APPENDIX R...................................................................................................................55
18.1 Data Usability..............................................................................................................55
FIGURES
Figure D-1 Site Plan—Former F1ynnTan Manufacturing Company Site..................................7
Figure D-2 Site Plan—61 Ward Street Site............................................................................. 13
Figure K-1 Sample Label and Chain-of-Custody Seal ............................................................35
Figure K-2 Chain-of-Custody Record......................................................................................36
TABLES
Table F-1 Sampling and QA Summary Former FlynnTan Manufacturing Company Site-
Salem, MA............................................................................................................21
Table F-2 Sampling and QA Summary 61 Ward Street Site- Salem, MA...........................24
ATTACHMENTS
Attachment A TRC Standard Operating Procedures
Attachment B Laboratory Quality Assurance Manual
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City of Salem Brownfields QAPP Revision Number:0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 1 of 56
1.0 APPENDIX A
1.1 Title and Approval Page
City of Salem Quality Assurance Project Plan
Document Title
Amy Stattel
TRC Environmental Corporation
Prepared by
04/26/04
Day/Month/Year
Boott Mills South, Foot of John Street Lowell MA 01852
Phone: (978) 970-5600
Project Manager:
Signature
Paul Arnold
Printed Name/Date
Project QA Officer:
Si t/ore
Elizabeth Denly
Printed Name/Date
U.S. EPA Project Manager Approval:
Signature
Joonu Andrews
Printed Name/Date
[2004-123
City of Salem Brownfields QA-PP Revision Number: 0
Former F1ynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 2 of 56
2.0 APPENDIX B
2.1 Project Organization and Responsibility
The following chart presents the organizational structure for this project.
EPA Project Coordinator: Joonu Andrews has been assigned to oversee the project for the U.S.
Environmental Protection Agency(EPA). Ms. Andrews will determine whether activities
proposed by the City of Salem are within the scope of the City's Grant Agreement with the EPA.
City of Salem Project Manager: Kate Gormly will direct all aspects of the project for the City
of Salem. Ms. Gormly will coordinate all contractor activities and provide managerial support
during the field investigation, and is ultimately responsible for successful project completion.
Ms. Gormly will seek any necessary approvals for all activities under this project from the EPA
Project Coordinator.
TRC Project Manager: TRC Environmental Corporation(TRC)will be conducting the Site
assessment activities of this project. The TRC Project Manager,Paul Arnold, will provide
overall direction to the field investigation team including both the sampling crew and drillers.
TRC Quality Assurance Officer. TRC's Quality Assurance(QA) officer, Elizabeth Denly, will
be the QA Officer responsible for this project. The QA Officer reports independently to a TRC
Vice President, and hence, has full authority to act independently from the technical line
management structure. She will monitor compliance of the project with this plan, and perform
any necessary performance or system audits. TRC's QA Officer will initiate and monitor any
necessary formal corrective actions. She will assist in preparing QA/Quality Control (QC)
project summaries for the final report, including analysis of precision, accuracy and completeness
of data collected.
Field Staff A Field QC Coordinator will be selected for this project to be in charge of the field
investigation. This individual will also serve as the Field Team Leader. The Field QC
Coordinator will work with the field crew to prepare for field activities and conduct
investigations. The Field QC Coordinator will be on Site to: 1) ensure that required QC
procedures are followed for sample collection and drilling; 2) initiate informal and/or formal
corrective actions, as necessary; and 3)maintain and report QC records (i.e., chain—of—custody).
This individual reports to the TRC Project Manager.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 3 of 56
EPA
Joonu Andrews
Project Coordinator
City of Salem
Kate Gormly
Project Manager
TRC
Dale Weiss, P.G.
Brownfields Program Manager
TRC
Paul Arnold
Project Manager
Elizabeth Denly
TRC Quality Assurance Officer
Phase I Staff Phase II Staff
Environmental Site Assessments Subsurface Investigation
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City of Salem Brownfields QAPP Revision Number:0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 4 of 56
3.0 APPENDIX C
3.1 Problem Definition
Former FlynnTan Manufacturing Company Site: The Former FlynnTan site(the"site"),
located at 70-92 Boston Street, is currently owned by the City of Salem(the City). The site is
approximately 1.9 acres in size and is bordered to the south by Boston Street and to the north by
Goodhue Street. The site currently contains four separate, vacant buildings, three of which are
enclosed by a perimeter fence with a locking gate, and the fourth is securely locked. Available
records indicate the site was historically occupied by commercial and manufacturing operations
from prior to 1900 until approximately 1999. Flynn and Sons operated a leather tannery on site
from approximately 1922 until approximately 1988. Based on an interview with Thomas St.
Pierre of the City of Salem Public Property Department, small commercial operations took place
on site until 1999, including a small metals recyclingbusiness.
Site buildings include the main factory building, a storage building, and a garage/storage shed.
The main entrance to the site is located on Boston Street. Parking areas and secondary entrances
are located to the northwest, southeast and the northeast ends of the site. To the east of the
parking area located northwest of the main building is the location of a former site building. This
area was filled in after the building was demolished, sometime after the FlynnTan factory closed
in the 1990s.
The area surrounding the site is comprised primarily of commercial and residential properties.
The North River, an inlet to Salem Harbor, is located approximately %mile northeast of the site.
A feeder canal to the North River runs east to west approximately 500 feet north of the site.
Salem's downtown center is located approximately 3/4 miles east of the site. Because of its prime
location, the City of Salem plans to redevelop the FlynnTan site with new buildings consisting of
mixed-use residential and retail spaces that will serve as part of a revitalized corridor
representing the "entrance"to the City.
Based on the extensive history of industrial uses including leather products manufacturing on
site, assessment of subsurface conditions at this site is warranted.
61 Ward Street Site: The 61 Ward Street site(the"site") is approximately 965 square feet in
size and is situated in a mixed residential/commercial area. The site is developed with a one-
story, vacant brick building and a small paved area. The site is bordered to the north by Peabody
Street and bordered to the south by Ward Street. A substation is located approximately 300 feet
northwest of the site, adjacent to a municipal parking lot, on the north side of Peabody Street. A
small parking lot borders the site to the west. Further west are multiple-family residential
buildings. Several commercial properties are located south of the site along Ward Street.
Directly east of the site, across the intersection of Peabody, Ward, and Congress Streets,is
Shetland Corporate Park. Salem center is located approximately %4 mile northwest of the site.
C2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 5 of 56
The site was historically used for a number of commercial purposes since the late 1800s. Earliest
available information indicates a photo shop occupied the site in 1890. The building currently
occupying the site was constructed around 1920. From approximately 1937 to 1983, the site was
used for several different automotive service stations. Historical street directories for Salem
indicate site uses included gas stations until 1960, a taxi garage from 1960 to 1968, and an
automobile repair garage until approximately 1983. Tax assessor's records indicate that
Frederick D. Small took ownership of the site in 1986 and renovated the existing building for
office use.
During an August 2001 site reconnaissance, TRC observed assorted paints,maintenance supplies
and household cleaners in the storage area within the site building. A surface depression was
noted in the asphalt-paved area adjoining the west side of the building. A hydraulic lift is
believed to have been located in the former automotive repair area. A grassy area on the east side
of the building was reportedly the location of the former fuel pumping area. Based on available
information from City of Salem and Fire Department, there are no records of registered
underground storage tanks (USTs) or the removal of USTs for the site. However, due to historic,
automotive service activities,USTs are considered likely to be present at the site.
The City of Salem anticipates the 61 Ward Street site will redeveloped for uses related to a
planned urban riverfront parkway to be constructed on the adjacent properties located to the
north, along Peabody Street.
Due to the previous industrial uses of this site, including automobile repair and maintenance
activities, assessment of subsurface conditions at this site is warranted.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 6 of 56
4.0 APPENDIX D
4.1 Project Description
The City of Salem is currently implementing a Brownfields Demonstration Pilot Program for
EPA. Portions of this program include environmental sampling of various media at selected sites
that have been identified, and may include assessment of some sites that have not yet been
identified. This Quality Assurance Project Plan (QAPP),which is required as part of the City's
Grant Agreement with EPA, documents proposed sampling and monitoring activities to be
implemented during the Brownfields Program. The plan describes the QA/QC procedures to be
employed to ensure the integrity, validity, and usability of the analytical results to be provided in
support of this project.
This document was prepared in accordance with the following EPA documents:
• Quality Assurance Guidance for Conducting Brownfields Site Assessments (EPA-540-R-
98-038), dated September 1998; and
• QA/R-5, EPA Requirements for Quality Assurance Project Plans (EPA—240/B-01/003),
dated March 2001.
This plan defines sampling strategies, methods, and locations, analytical methods, data handling
and tracking procedures, and specific QC procedures and QA mechanisms that will be used for
this Brownfields Program. The purpose of the QAPP is to establish procedures to ascertain the
precision, accuracy and representativeness, and objectives for the collected data.
Former FlynnTan Manufacturing Company Site:
The former FlynnTan Manufacturing Company was involved in the softening, cutting and dyeing
of leather. Potential contaminant source areas related to previous industrial use of the site
include numerous sumps and trenches, a concrete underground vault, three or more USTs,
stained surface soils, former chemical vats, and unspecified fill material, as discussed below.
Figure D-1 shows the features and layout of the site.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 8 of 56
During operation of the tannery, various chemicals and hazardous materials were used and stored
on site in association with these processes. Former areas and structures in which hazardous
materials were used and stored included leather-processing vats, dipping tanks, tumblers, settling
tanks, storage tanks, drums and floor trenches. Two on-site USTs (one 20,000-gallon fuel oil
UST and one 9,800-gallon UST with contents not reported) are recorded in Fire Department
records for the site. Although the Fire Department records did not indicate the location of these
USTs, based on existing surficial features (e.g. the presence of fill and vent pipes, broken
pavement, etc.) it appears three USTs are located within the parking area northwest of the main
building, and additional USTs may be located near the loading dock of the main building and
east of the storage building.
In September through November 1998, EPA conducted a Removal Action at the site to address
hazardous materials that were abandoned at the site and were considered a threat of a release.
EPA's removal action included the removal of hazardous materials located in drums and
aboveground storage tanks in the buildings, as well as the removal of liquids and sludges present
in several recessed drainage trenches and pits located below the floors of the buildings. Wastes
removed during the EPA Removal Action were disposed off site. The on-site USTs were not
addressed as part of the 1998 EPA Removal Action.
During an August 2001 site reconnaissance, TRC observed wood, glass, and metal debris on site
including a large pile of light ballasts. TRC observed approximately 20 empty drums located in
several areas around the site. An underground structure, referred to in EPA Removal Program
documents as a"sealed concrete vault", is located northwest of the main building. The contents
and/or former use of this vault structure are unknown. TRC also observed stained soils in two
locations at the site. A storm water catch basin, as well as numerous raceways and sumps, are
located on site. A former transformer pad is located on the north side of the storage building.
Potential source areas for this site are summarized in the table below and are indicated on Figure
D-1.
L.2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 9 of 56
Former FlynnTan Manufacturing Company Site
No. Potential Source Area Location/Description Contaminants of Concern
1 Previous on-site Tannery and leather VOCs, VPH,EPH,
industrial uses manufacturing operations on SVOCs, PCBs,Metals,
site 1922-1988. Metals shop cyanide, Cr+6
and mixed commercial uses
1988-1999.
2 Filled areas Former site building area. VPH, EPH, SVOCs, PCBs,
Metals
3 USTs Northern portion of site, VOCs, VPH,EPH,
loading dock on south side of SVOCs, Metals, cyanide,
main building, and east of Cr+6
storage building annex.
Contents, conditions of tanks,
etc. need further evaluation.
4 Subsurface Vault Northwest portion of site, west VOCs, VPH,EPH,
of paved parking area. SVOCs, Metals, cyanide,
Cr+6
5 Stormwater Catch Basin South of storage building. VOCs, VPH, EPH,
SVOCs, PCBs, Metals,
cyanide, Cr+6
6 Trenches, raceways, and Throughout floors of storage VOCs, VPH, EPH,
sumps building and main building. SVOCs, Metals, cyanide,
Cr+6
7 Former transformer pad Northeast side of storage PCBs
building.
8 Drums Empty drums located in VOCs, VPH, EPH,
several areas around the site; SVOCs, PCBs, Metals,
potential for past leaking of cyanide, Cr+6
wastes or chemicals.
9 Stained soils Pile in northern storage VOCs, VPH, EPH,
building and surface soils west SVOCs, PCBs, Metals,
of single car garage. cyanide, Cr+6
10 Site Ground Water Impacts due to potential VOCs, VPH,EPH,
discharges from below-ground SVOCs, PCBs, Metals,
structures, including USTs, cyanide
sumps and drainage conduits.
VOCs-Volatile Organic Compounds; VPH—Volatile Petroleum Hydrocarbons;
EPH—Extractable Petroleum Hydrocarbons; SVOCs—Semivolatile Organic Compounds;
PCBs—Polychlorinated biphenyls;and Cr+6—Hexavalent chromium
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 10 of 56
The following activities are planned as part of the Site investigation.
EPA File Review
A file review will be performed at the EPA Region 1 Office in Boston, Massachusetts to update
information regarding the regulatory history of the Site and to review EPA records regarding sump
and raceway contents pumped in 1998.
Geophysical Survey
A geophysical survey will be conducted at the site to evaluate the presence of potential USTs,
subsurface drainage structures, vault(s) and potential buried debris from the former site building
demolished in approximately 1988. The results of the geophysical work will be used to identify
some of the target locations that warrant subsurface investigation under the tasks described
below.
Hazardous Materials Survey
The site buildings shall be inspected for the presence of hazardous materials and/or wastes. A
complete inventory of the hazardous and potentially hazardous materials (including,but not
limited to, flammable liquids, mercury switches, PCB-containing ballasts or transformers,
suspect lead paint, and suspect asbestos) will be compiled to evaluate the need for further testing.
Soil Borings and Monitoring Well Program
Based on information gathered during previous EPA inspections at the site, as well as data
collected during the initial stages of this assessment, a total of ten soil borings will be advanced
at the site, and seven of the soil borings will be completed as monitoring wells. Soil and ground
water samples will be collected at these locations, as described below, in order to assess the
nature and extent of subsurface contamination. Based on local topography, ground water at the
site is expected to flow in a northeasterly direction.
Soil borings/monitoring wells will be advanced in the following locations:
(1) Near the northeast edge of the former on-site building, close to Goodhue Street.
Boring to be completed as a monitoring well;
(2), (3), (4) Near each UST/potential UST area: (a)near loading dock on south side of main
building and (b) east of storage building annex and (c) in northern portion of site,
north of former site building. Three borings to be completed as monitoring wells;
(5), (6) Near sump area in main building and one near sump area in storage building. Two
borings to be completed as monitoring wells;
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 11 of 56
(7), (8) Near areas of stained soil, northeast of the main building, and northwest of storage
building annex. Two soil borings to be installed;
(9) Near the northwest end of the main tannery building, downgradient from elevator.
Boring to be completed as a monitoring well; and
(10) Near a former equipment area in the southeast portion of the storage building annex.
Soil boring to be installed.
Soil samples will be obtained continuously at two-foot intervals up to a depth of ten feet,and
every five feet thereafter until groundwater or refusal is encountered, during the advancement of
borings and/or monitoring wells. Soil samples will be screened continuously in the field for
VOCs using the jar headspace method. Immediately upon collecting the sample, TRC will pass a
photoionization detector(PID) or equivalent over the surface of the sample and note any organic
vapor readings above background. If VOC and/or VPH analysis is required, samples from each
depth interval should be immediately and carefully placed (in a manner to minimize
volatilization) in preserved vials upon collection, and then immediately placed on ice. Soil
recovered from each depth interval will be placed into stainless steel bowls using stainless steel
spoons (all equipment to be decontaminated properly prior to use).
Soil recovered from each depth interval will be placed into stainless steel bowls using stainless
steel spoons (all equipment to be decontaminated properly prior to use).
Next, soils for headspace screening will be transferred for each depth interval into glass jars
(>_8oz.) and capped with foil followed by a screw-on lid. Then, samples will be containerized
from remaining soils for each depth interval for other potential soil analyses, and immediately
placed on ice. After at least 30 minutes, soil headspace readings will be obtained by removing
the sample caps from each jar and inserting a PID or equivalent through the foil to measure the
organic vapor concentration in the headspace. All soil headspace readings will be recorded.
Based on field observations (e.g., visual and/or olfactory evidence of contamination) and jar
headspace screening results, TRC will select the specified number of soil sample(s) from each
boring and/or monitoring well to be submitted to an off-site laboratory for analysis.
Unless otherwise noted, one soil sample from each of the ten proposed soil borings and/or
monitoring wells will be submitted to a Massachusetts-certified laboratory for VOCs, VPH,
EPH, Metals, pH and oxidation-reduction potential (ORP) analyses. The soil samples collected
from borings in the vicinity of the former on-site building,potential USTs, and subsurface
drainage structures (described under items 1 through 6, above)will also be analyzed for SVOCs
and total cyanide. The soil samples collected from borings in the vicinity of the freight elevator
and the observed stained soil areas (described under items 7 through 9, above)will also be
analyzed for PCBs. If elevated chromium concentrations are detected in soil samples (i.e., above
MCP reportable concentrations) and if the pH and ORP analyses reveal the presence of an
oxidizing environment, then these samples will subsequently be analyzed for hexavalent
chromium.
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Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 12 of 56
Ground water samples collected in each of the seven monitoring wells installed at the site will be
submitted to a Massachusetts-certified laboratory for VOCs, VPH, EPH, Metals and Cyanide
analyses. In addition,the ground water samples collected from the two monitoring wells installed in
the vicinity of the subsurface drainage structures and the freight elevator(described above under
items 5,6 and 9)will be submitted for SVOC analysis. The ground water sample collected from the
monitoring well near the freight elevator will be also analyzed for PCBs.
Ground Water Elevation Survey and SPH Measurements
Following the installation and development of the monitoring wells,the wells will be surveyed to an
arbitrary site datum, depth to ground water readings will be recorded, and the wells will be gauged
for the presence of separate phase hydrocarbons(SPH). The survey information,in conjunction with
the depth to ground water readings, will be used to evaluate shallow ground water flow across the
Site.
Phase II Report
A Phase II report will be prepared which will include a summary of the work conducted,site history,
and site testing results based on TRC's proposed work. Further information concerning the Phase H
report is provided in Section 16 (Appendix P).
61 Ward Street Site:
The existing site building was constructed around 1920. Prior to 1920, site uses reportedly
included residential uses, and use as a photo shop for an unreported period of time around 1890.
From approximately 1937 to 1983, the site was used as an automotive garage, and occupied by
gasoline service stations until 1960, a taxi garage from 1960 to 1968, and an automobile repair
garage until approximately 1983. In approximately 1986, the site was remodeled into a
maintenance office and storage space related to the adjacent apartment buildings along Ward
Street. Soon thereafter, the site was vacated and has reportedly remained vacant since.
The on-site building, during its previous use as an automotive garage,was described by
neighboring business occupants as including a hydraulic lift in the main entrance area facing
eastward. The currently existing grassy area, located east of the main entrance,was the location
of the former fuel pumping area. Based on available information from City of Salem Fire
Department, there are no records of registered USTs or the removal of USTs from the site.
However, due to historic, automotive service activities, USTs are considered to be present at the
site. During a recent site visit on March 23, 2004,TRC observed a potential petroleum-storage
fill cap in the sidewalk along Ward Street (along the southern site boundary).
Potential source areas for this site are summarized below and are indicated on Figure D-2.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 13 of 56
Figure D-2 Site Plan—61 Ward Street Site
12004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 14 of 56
61 Ward Street Site
No. Potential Source Area Location/Description Contaminants of Concern
1 Former on-site gasoline Site occupied by gas stations and VOCs, VPH, EPH, Metals
service station and auto repair garage 1937-1983.
vehicle maintenance
area
2 USTs, former fill Potential USTs located on site. VPH, EPH, Metals
pumps, and associated Contents , conditions of tanks etc.
piping need further evaluation. Former
fill pumps located in eastern
(grassy) portion of site.
3 Filled areas Areas where USTs may have been VPH, EPH, Metals
removed from the site (i.e.,
depression on west side of
building).
4 Hydraulic lifts Records indicate hydraulic lift(s) VOCs, VPH, EPH, Metals,
may have been located in former and PCBs
on-site garage.
6 Household hazardous Throughout site building(last use VOCs, VPH, EPH, Metals
wastes was a maintenance office for
surrounding properties).
8 Former photo shop Historical records indicate photo Metals
shop occupied site around 1890 for
an unreported period of time.
9 Site Ground Water Potential impacts from historic VPH, EPH, Metals
USTs, gasoline filling activities,
and vehicle maintenance.
VOCs-Volatile Organic Compounds; VPH—Volatile Petroleum Hydrocarbons;
EPH—Extractable Petroleum Hydrocarbons;and PCBs—Polychlorinated biphenyls.
The following activities are planned as part of the Site investigation.
Geophysical Survey
A geophysical survey will be conducted at the site to evaluate the presence of potential USTs and
piping in the eastern portion of the site, as well as in the location of the former auto repair garage
to evaluate the presence of buried hydraulic lifts. The results of the geophysical work will be
used to identify target locations that warrant subsurface investigation under the tasks described
below.
L2004-123
SITE LEGEND
SITE BOUNDARY
PARKING AREA BOUNDARY
RESIDENTIAL ♦ '� %�/�� � <— X FENCE
VACANT 5
FENCE %/ / BUILDING SUBSURFACE STRUCTURES
APPRO�T -
`✓� C��AT�CS�:O�UR�EI MONITORING WELL (ORIGIN UNKNOWN)
BING; ; INSTALLED PRIOR TO 1990
�>-�-(DEMd�IISIJE j APPROXIMATE LOCATION of
♦!j<,� F C�f1 LINE 1 Q9aS��`\ OBSERVED STAINED SOIL PROPOSED MONITORING WELL
./ PROPOSED SOIL BORING
tiC REL9
STO"",,\ ENTR/WCE PROPOSED GEOPHYSICAL SURVEY AREA
BEING,
iCt ,�n�ON CATCH BASIN
�.,• OBSFRkED_ � �� - --MONITORING WELL
'_STAI ll NED-SOIL-;� /i y/� APPROXIMATE LOCATION OF
OBSERVED STAINED SOIL
� C�P 1EI��� SINGLE CAR GARAGE
MAC` �P 14
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BUII.
SECONDARY NJI ,, -
�O ENTRANCE t,9, `�✓
FREIGHT
Q ELEVATOR / t;' STORAGE \ C
J/ BUILDING
MAIN \ ' 0VAC
ANNE ANT
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FORMER
WASHTANK ��.,� ir, \\ 7
SECONDARY ENTRANCE \,; FJ NT PIPE ` 00
LOADING DOCK ASPHALT\,♦
\ COVERED \ A
\ PARKING `
\ AREA \ ♦ o ��
\ VACANT LOT c�
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DUNKIN
DONUTS
NI
FORMER FLYNNTAN SITE
70-92 BOSTON STREET 0 30 60
o SALEM, MASSACHUSETTS
z APPROXIMATE SCALE IN FEET SITE PLAN
9oott MIIIs South
o< ��� Fool of John Street
Lowell. Maaaaehuastta 01852
n (976) 970-5600 FIGURE
DRAWN BY:JEL D-1
DATE:04/05/04
CHECKED BY:ALS
�x
\X
MASS ELECTRIC
X \X \t SUBSTATION N >
E m
x \t ' ` Lu
\X S 7
\X O\X
APPROX. 6-IN. �t (—
DEPRESSION IN ASPHALT
ASPHALT-PAVED
FgBOOY �x \ _
AREA STR�FT
SITE
APT. MAIN ENTRANCE
BLDNG.
PARKING
LOT I� GRASSY AREA
(FORMER LOCATION
I I —STORY OF FILL PUMPS)
I BRICK
PARKING AREA
STORAGE ROOM
ENTRANCE SIDEWALK
WARD STREET EXISTING OFFICE BUILDING
(FORMER GARAGE)
POTENTIAL UST FILLCAP
IN SIDEWALK
COMMERCIAL
/CWFLOW (INFERRED)
w
61 WARD STREET
o LEGEND SALEM, MASSACHUSETTS
a
SITE BOUNDARY SITE SKETCH
w _
PROPOSED BORING/MONITORING TRC —t,," _
,e, p,°.i
•°h—ft. 01652
WELL LOCATION `—U,Mo. FIGURE
^ (975)970-5600
D-2
m DRAWN BY:MAN DATE 9/17/01
r
QiECKED BY:AMB
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 16 of 56
Hazardous Materials Survey
The site building shall be inspected for the presence of hazardous materials and/or wastes. An
inventory of hazardous materials (including, but not limited to, flammable liquids, mercury
switches, PCB-containing ballasts or transformers, suspect lead paint, and suspect asbestos) will
be compiled to evaluate the need for further testing.
Soil Borings and Monitoring Well Program
Based on observations and historic information gathered during the initial stages of this
assessment, three soil borings will be advanced at the Site and completed as monitoring wells.
Based on local topography, ground water at the site is expected to flow in a northerly direction.
Soil and ground water samples will be collected in each of the boring/monitoring well locations
in order to assess the nature and extent of subsurface contamination.
Soil borings/monitoring wells will be advanced in the following locations:
(1) near the northwest corner of the site, in a location interpreted to be downgradient from the
surface depression in the asphalt-paved area on the site;
(2) north of the site building, near Peabody Street, in a location interpreted to be
downgradient from the former automobile service area and potential hydraulic lift(s); and
(3) in the northeast portion of the site, in a location interpreted to be downgradient from the
former gasoline fill pumps.
Soil samples will be obtained continuously at two-foot intervals up to a depth of ten feet,and
every five feet thereafter until groundwater or refusal is encountered, during the advancement of
borings and/or monitoring wells. Soil samples will be screened continuously in the field for
VOCs using the jar headspace method. Immediately upon collecting the sample TRC will pass a
photoionization detector(PID) or equivalent over the surface of the sample and note any organic
vapor readings above background. If VOC and/or VPH analysis is required, samples from each
depth interval should be immediately and carefully placed(in a manner to minimize
volatilization) in preserved vials upon collection, and then immediately placed on ice. Soil
recovered from each depth interval will be placed into stainless steel bowls using stainless steel
spoons (all equipment to be decontaminated properly prior to use).
Next, soils for headspace screening will be transferred for each depth interval into glass jars
(>_8oz.) and capped with foil followed by a screw-on lid. Then, samples will be containerized
from remaining soils for each depth interval for other potential soil analyses, and immediately
placed on ice. After at least 30 minutes, soil headspace readings will be obtained by removing
the sample caps from each jar and inserting a PID or equivalent through the foil to measure the
organic vapor concentration in the headspace. All soil headspace readings,will be recorded.
Based on field observations (e.g., visual and/or olfactory evidence of contamination) and jar
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 17 of 56
headspace screening results, TRC will select the specified number of soil sample(s) from each
boring and/or monitoring well to be submitted to an off-site laboratory for analysis.
One soil sample from each boring will be selected for submittal to a Massachusetts-certified
laboratory for analysis of VPH, EPH, and metals. In each boring, one sample may also be
selected based on field observations and headspace readings and submitted for VOC analysis.
The soil sample collected in the boring located downgradient from the former vehicle
maintenance area (north of the site building) will also be submitted for PCB analysis.
Ground water samples will be collected from each of the three monitoring wells and submitted to
a Massachusetts-certified laboratory for VPH, EPH and metals analyses.
Ground Water Elevation Survey and SPH Measurements
Following the installation and development of the monitoring wells, the wells will be surveyed to
an arbitrary site datum, depth to ground water readings will be recorded, and wells will be
gauged for the presence of SPH. The survey information, in conjunction with the depth to ground
water readings, will be used to evaluate shallow ground water flow across the Site.
Phase II Report
A Phase II report will be prepared which will include a summary of the work conducted,site history,
and site testing results based on TRC's proposed work. Further information concerning the Phase H
report is provided in Section 16 (Appendix P).
4.2 Project Timeline
Activities (List Products) Project Start Project End
Final QAPP Submission 03/08/04 04/28/04
EPA Approval 05/10/04
Site Testing 05/13/04 06/15/04
Phase 11 Report 106/01/04 08/16/04
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 18 of 56
5.0 APPENDIX E
5.1 Sampling Design
Field work will be performed in accordance with TRC's Standard Operating Procedures(SOPs),
which are attached to this document. TRC will enlist the services of a qualified drilling
subcontractor to advance soil borings and install ground water monitoring wells as set forth in
Appendix D, the Project Description. Each boring and/or well will be advanced using either the
hollow-stem auger technique or a GeoProbe. TRC will be responsible for the collection of soil
samples for field screening and laboratory analysis during boring and well placement activities.
GeoProbe sampling will be performed in accordance with the MADEP Standard References for
Monitoring Wells, Supplement for Small Diameter Driven Wells.
Soil samples will be collected continuously at two-foot intervals to a depth of ten feet. Below ten
feet, samples will be collected at a minimum of five-foot intervals. Samples will be screened
using a PID, or equivalent, and any odors or visual indication of contamination will be noted.
Equipment will be decontaminated between soil borings to reduce the possibility of cross-
contamination.
Based on jar headspace screening observations, one soil sample from each of the borings will be
selected for laboratory analysis. If no indications of possible contamination are observed, one
soil sample will be collected immediately above the ground water interface and submitted for
analysis. Soil samples from the borings will be submitted to a Massachusetts-certified laboratory
for analysis.
Ground water monitoring wells will be constructed of two-inch diameter Schedule 40 PVC. The
pipe sections will be threaded screw type, eliminating the need for solvent-based glue. Each well
will have a 10-foot, 10-slot (0.010-inch machine slotted) screen section placed so as to extend
above and below the upper surface of the water table. A sand pack will be placed around the
screen extending to a level approximately one foot above the top of the screen. A bentonite seal
approximately two feet thick will be placed above the sand pack in order to seal off the screened
portion of the well from the overlying strata. The remainder of the well annulus will be filled
with a cement/bentonite grout to ground surface. A locking steel protective cover will be
installed over the top of the wells and the cap will be flush with the ground surface for any wells
located in paved areas.
After installation, each well will be developed by removing at least three well volumes by
purging with a submersible or peristaltic pump. Headspace measurement of VOCs will be made
on purged ground water using the field screening equipment. If the headspace VOC reading
exceeds 10 parts per million(ppm), the purge water will be drummed or containerized until the
ground water sample test results are obtained to evaluate disposal options. If the headspace VOC
readings are less than 10 ppm, the water will be discharged onsite.
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 19 of 56
Monitoring wells will be allowed to stabilize for a period of at least seven days prior to sampling.
At this time the water level in the wells will be surveyed in an attempt to confirm the direction of
ground water flow at the sites.
Following the well installation and development process, TRC will collect ground water samples
from each monitoring well to determine whether Site use has impacted ground water conditions
at the Site. Samples will be obtained using low-flow sampling techniques. TRC will submit the
ground water samples to a laboratory for chemical analysis. Prior to ground water sample
collection, TRC will also measure water levels to assist in data interpretation. TRC will measure
well casing elevations and prepare a Site sketch with taped distance measurements for use in
drafting an approximated ground water contour plan.
All soil and ground water samples from the Site will be placed on ice, kept cool (4°C±2'Q and
will be delivered to an off-site laboratory following proper chain-of-custody procedures. A trip
blank and field duplicate samples will also be collected to provide quality assurance/quality
control data.
5.2 Equipment Decontamination Procedures
All major decontamination of downhole and excavation equipment will be conducted at a
designated decontamination area(s). When appropriate, drill rigs will be steam cleaned and
drilling equipment will be decontaminated prior to moving. Drilling equipment used for multiple
boreholes will be decontaminated by steam cleaning prior to beginning each boring. (Split-
spoons should be made of stainless steel, but carbon steel is acceptable if it is rust-free.)
Minor decontamination such as cleaning of sampling equipment will be performed at each
sampling site. Smaller sampling equipment such as split spoons, stainless steel or Teflon
spatulas and stainless steel mixing pans will be decontaminated using the following procedures:
• Wash and scrub with low-phosphate detergent in tap water;
• Rinse with deionized water;
• Rinse with nitric acid (10%nitric acid for stainless steel equipment and 1%nitric acid on
all other equipment);
• Rinse with pesticide-grade methanol;
• If oily, rinse with pesticide-grade hexane;
• Air dry- on clean polyethylene sheeting;
• Rinse with deionized water;
• Air dry- on clean polyethylene sheeting;
• Wrap in aluminum foil, shiny side out for transport; and
• Clean equipment may rest on-but never be wrapped in - clean polyethylene sheeting.
Soils (excess sample volume, auger cuttings, etc.)will be returned to their place of origin(either
placed inside of the boreholes or dispersed near the borehole location). The PID and visual
observations will be used to determine if residuals require further handling and disposal
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 20 of 56
(e.g., off-site disposal as RCRA wastes). Residuals screened for disposal as a hazardous material
will be properly disposed of by the City of Salem.
L2004-123
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2003
61 Ward Street
Salem,MA Page 26 of 55
6.2 Method and SOP References
Analytical Method Reference: Project Analytical Standard Operating
Procedures(SOPS):
Ia. 40 CFR 136.3e Required containers,preservative techniques, lb. See the Lab QA Manual
and holding times (Attachment A).
2a. Wagner,R.E.,Kotas,W.A.,Hotaling,I.C.,Hynes,T.C.,Daly,J. 2b. Same as above
and McTague,M.F.(eds.). Guide to Environmental Analytical
Methods,5`h ed. Genium Publishing Corporation,Amsterdam,
NY. 2003. Reference for SW-846 information on method
validation,calibration guidelines,and QC checks.
3a. USEPA.Total and Amenable Cyanide:Distillation. SW846 _ 3b. Same as above
Method 901013,Revision 2. December 1996.
4a. USEPA. Volatile Organic Compounds by Gas 4b. Same as above
Chromatography/Mass Spectrometry. SW846 Method 826013,
Revision 2. December 1996.
5a_ USEPA. Closed-System Purge-and-Trap and Extraction for 5b. Same as above
Volatile Organics in Soil and Waste Samples. SW846 Method
5035A,Draft Revision 1. July 2002.
6a. USEPA. Inductively Coupled Plasma-Atomic Emission 6b. Same as above
Spectrometry. SW846 Method 601013,Revision 2. December
1996.
7a. USEPA. Mercury in Solid or Semisolid Waste(Manual Cold- 7b. Same as above
Vapor Technique). SW846 Method 7471A,Revision 1.
September 1994.
8a. USEPA. Mercury in Liquid Waste(Manual Cold-Vapor 8b. Same as above
Technique). SW846 Method 7470A,Revision 1. September
1994.
9a. MADEP. Method for the Determination of Extractable 9b. Same as above
Petroleum Hydrocarbons(EPH). January 1998.
10a. MADEP. Method for the Determination of Volatile Petroleum 10b. Same as above
Hydrocarbons(VPH). January 1998.
1 la. USEPA. Polychlorinated Biphenyls(PCB)by Gas 1 lb. Same as above
Chromatography. SW846 Method 8082,Revision 0. December
1996.
12a. USEPA.Titrimetric and Manual Spectrophotometric 12b. Same as above
Determinative Methods for Cyanide. SW846 Method 9014,
Revision 0. December 1996.
13a. USEPA. Chromium Hexavalent(Colorimetric).SW846 Method 13b. Same as above
7196A,Revision 1.July 1992.
14a. USEPA. Semivolatile Organic Compounds by Gas 14b. Same as above
Chromatography/Mass Spectrometry. SW846 Method 8270C,
Revision 3. December 1996.
15a. USEPA. Alkaline Digestion for Hexavalent Chromium. SW846 15b. Same as above
Method 3060A,Revision 1. December 1996.
16a. USEPA. Soil and Waste pH. SW846 Method 9045C,Revision 16b. Same as above
3. January 1995.
17a. ASTM. Standard Practice for Oxidation-Reduction Potential of 17b. Same as above
Water. ASTM D1498-00.
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2003
61 Ward Street
Salem,MA Page 27 of 55
7.0 APPENDIX G
7.1 Preventative Maintenance—Field Equipment
Instruments and equipment used to gather, generate, or measure environmental data will be
calibrated with sufficient frequency and in such a manner that accuracy and reproducibility of
results are consistent with the manufacturer's specifications. The calibration and internal
standards shall meet all criteria specified in the referenced analytical method.
For all analyses for which EPA or DEP approved methods exist, the laboratory will employ such
methods and follow the calibration procedures and frequencies specified.
Calibration of field instruments and equipment will be performed as specified by the
manufacturer or more frequently as conditions dictate. The minimum calibration of field
instrumentation is once at the beginning of each day, and as necessary. Calibration standards
used as reference standards will be traceable to the National Institute of Standards and
Technology(MIST), when existent.
Records of calibration, repair, or replacement will be filed and maintained by the designated
laboratory personnel performing quality control activities. Calibration records of assigned
laboratories will be filed and maintained at the laboratory location where the work is performed
and subject to QA audit.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2003
61 Ward Street
Salem,MA Page 28 of 55
Instrument Activity Frequency SOP Ref.
PID' Field Sample Screening Daily Per Headspace Field Screening
Procedure,TRC SOP 016.
Water level meter Clean meter and visually Daily prior to use Per Water Level and Product
inspect for defective parts Measurement SOP,TRC SOP
012
Turbidimeter Visually inspect for defective Daily prior to use Per Calibration of Field
parts Instruments for Water Quality
Parameters SOP,TRC SOP 024
Water quality (See below) (See below) (See below).
instrument(YSI or
equivalent multi-
parameter meter)
pH Probe Clean/visually inspect probe Prior to initial use,and Per Calibration of Field
when unstable Instruments for Water Quality
readings occur Parameters SOP,TRC SOP 024
DO Probe Clean/visually inspect probe, Prior to initial use,and (Same as above)
change KCI,and change if bubbles appear
Teflon®membrane below membrane,if
unstable readings are
given,or if dried
electrolyte visible on
membrane or o-ring.
Specific Clear opening to probe Prior to initial use (Same as above)
Conductance
Electrode
Thermistor-Temp. Visually inspect probe Daily before use (Same as above)
Sensor
ORP Electrode Visually inspect probe Daily before use (Same as above)
1 -PID—Photoionization detector.
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Former FlynnTan Manufacturing Company and Revision Date: April 27,2003
61 Ward Street
Salem,MA Page 29 of 55
8.0 APPENDIX H
8.1 Calibration and Corrective Action—Field Equipment
Instrument Activity Frequency Acceptance CorrectiveSOP Ref.
Criteria Action
PID Check Beginning ± 10%of true value Re-calibrate using Per TRC SOP for
calibration on and end of manufacturer's Headspace Field
site with span day instructions and re- Screening
gas(e.g., check with span gas; Procedure.
isobutylene) replace if faulty.
Water level TRC to Prior to use ±0.1,feet Re-calibrate using Per TRC SOP for
meter perform manufacturer's Water Level and
independent instructions and re- Product
check of check;replace if Measurement.
accuracy faulty.
Turbidimeter Check Daily ±5% Re-calibrate using Per TRC SOP for
calibration before use manufacturer's Calibration of
using standard instructions and re- Field Instruments
turbidity check;replace if for Water Quality
solutions faulty. Parameters.
YSI or Check Daily Temperature— Re-calibrate using Per TRC SOP for
equivalent accuracy using before use ±0.15°C of NIST manufacturer's Calibration of
water quality standard certified thermometer instructions and re- Field Instruments
probe solutions check;replace if for Water Quality
D.O.-+_0.2 mg/L for faulty. Parameters.
0.0
pH—stable readings
±0.1 pH units within
3 minutes
specific conductance-
+ 1 umho/cm of
standard
ORP-+1 mV of
standard JI
NA—Not applicable.
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City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2003
61 Ward Street
Salem,MA Page 30 of 55
9.0 APPENDIX I
9.1 Preventative Maintenance—Laboratory Equipment
Instrument Activity Frequency SOP Ref.*
GC/MS Maintain per manufacturer's Per manufacturer's 4a, 14a
instructions instructions
ICP-AES Maintain per manufacturer's Per manufacturer's 6a
instructions instructions
GC/ECD Maintain per manufacturer's Per manufacturer's I la
instructions instructions
CVAA Maintain per manufacturer's Per manufacturer's 7a,8a
instructions instructions
GC/FID Maintain per manufacturer's Per manufacturer's 9a, 10a
instructions instructions
GC/PID Maintain per manufacturer's Per manufacturer's 10a
instructions instructions
Spectrophotometer Maintain per manufacturer's Per manufacturer's 3a, 12a, 13a, 15a
instructions instructions
pH Meter Maintain per manufacturer's Per manufacturer's 16a
instructions instructions
ORP Meter Maintain per manufacturer's Per manufacturer's 17a
instructions instructions
*Reference Number from Appendix F,Method and SOP Reference Table.
L2004-123
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City of Salem Brownfields QAPP Revision Number: 0
Former F1ynniran Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 34 of 55
11.0 APPENDIX K
11.1 Sample Handling and Custody Requirements
The purpose of chain-of-custody procedures is to document the identity of the sample and its
handling from its first existence as a sample until analysis and data reduction are completed.
Custody records trace a sample from its collection through all transfers of custody until it is
transferred to the analytical laboratory. Internal laboratory records then document the custody of
the sample through its final disposition.
All materials such as field and laboratory notebooks and logbooks, field and laboratory data
records, correspondence, reports, chain-of-custody records and instrument printouts will be
clearly labeled with the project number and become a permanent part of the project file.
II.1.1 Field Sampling Operations
Preprinted sample identification labels will be used to ensure that the required information is
entered in the field. Each collected sample shall have a completely filled-in sample label
securely attached. In addition, the sample identification number will be marked on the container
with a permanent marker so that the sample can be properly identified even if the label is
separated from the sample.
Figure K-I shows the general sample label and custody seal that will be used to identify and seal
samples in the field. Figure K-2 shows a general use chain-of-custody record. This two-part
form will be used to document sample transfer in the field, from sampling personnel to the
analytical laboratory.
The Field Team Leader will coordinate the packing and shipment of all samples.
TRC intends to ship all samples via a courier service or an overnight delivery service within 24
hours of collection.
L2004-123
City of Salem Brownfields QAPP Revision Number: 0
Former FlynnTan Manufacturing Company and Revision Date: April 27,2004
61 Ward Street
Salem,MA Page 35 of 55
Sample Label
GL[EM/SOURCE 11 GRAB
OTHER
SrfENAME p47E
SAMPLE# 77ME
ANALYSIS PMMVA nVE,
COLL BY
Custody Seal
CUSTODY:WAIL
DI
Figure K-1 Sample Label and Chain-of-Custody Seal
L2004-123